CN105267097B - Dandruff control shampoo containing and preparation method thereof - Google Patents
Dandruff control shampoo containing and preparation method thereof Download PDFInfo
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- CN105267097B CN105267097B CN201510794191.8A CN201510794191A CN105267097B CN 105267097 B CN105267097 B CN 105267097B CN 201510794191 A CN201510794191 A CN 201510794191A CN 105267097 B CN105267097 B CN 105267097B
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- 239000002453 shampoo Substances 0.000 title claims abstract description 80
- 238000002360 preparation method Methods 0.000 title claims abstract description 35
- 229940075285 dandruff control Drugs 0.000 title abstract 4
- 239000000284 extract Substances 0.000 claims abstract description 179
- 208000001840 Dandruff Diseases 0.000 claims abstract description 54
- 239000011159 matrix material Substances 0.000 claims abstract description 42
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims abstract description 41
- 235000003140 Panax quinquefolius Nutrition 0.000 claims abstract description 41
- 235000008434 ginseng Nutrition 0.000 claims abstract description 41
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 41
- 241000334160 Isatis Species 0.000 claims abstract description 40
- 241000411851 herbal medicine Species 0.000 claims abstract description 38
- 235000005979 Citrus limon Nutrition 0.000 claims abstract description 32
- 244000131522 Citrus pyriformis Species 0.000 claims abstract description 32
- 229940069521 aloe extract Drugs 0.000 claims abstract description 21
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- 238000002156 mixing Methods 0.000 claims abstract description 20
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 13
- 239000003755 preservative agent Substances 0.000 claims abstract description 13
- 230000002335 preservative effect Effects 0.000 claims abstract description 13
- 241001289529 Fallopia multiflora Species 0.000 claims description 45
- 241000208340 Araliaceae Species 0.000 claims description 40
- 239000000843 powder Substances 0.000 claims description 40
- 240000001549 Ipomoea eriocarpa Species 0.000 claims description 38
- 235000005146 Ipomoea eriocarpa Nutrition 0.000 claims description 38
- 238000001035 drying Methods 0.000 claims description 35
- 239000000706 filtrate Substances 0.000 claims description 30
- 229940072113 onion extract Drugs 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 22
- 238000003756 stirring Methods 0.000 claims description 22
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 21
- 241000234282 Allium Species 0.000 claims description 20
- 235000002732 Allium cepa var. cepa Nutrition 0.000 claims description 20
- 240000000249 Morus alba Species 0.000 claims description 19
- 238000001914 filtration Methods 0.000 claims description 15
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- 239000010231 banlangen Substances 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 14
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 claims description 12
- 244000060011 Cocos nucifera Species 0.000 claims description 12
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 12
- 229920002907 Guar gum Polymers 0.000 claims description 12
- 150000001408 amides Chemical class 0.000 claims description 12
- 229960002154 guar gum Drugs 0.000 claims description 12
- 235000010417 guar gum Nutrition 0.000 claims description 12
- 239000000665 guar gum Substances 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 238000005520 cutting process Methods 0.000 claims description 10
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 10
- 238000002791 soaking Methods 0.000 claims description 10
- 238000000605 extraction Methods 0.000 claims description 6
- 238000007605 air drying Methods 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 5
- 239000003205 fragrance Substances 0.000 claims description 5
- 235000020710 ginseng extract Nutrition 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000002137 ultrasound extraction Methods 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 4
- 210000004761 scalp Anatomy 0.000 abstract description 25
- 230000017531 blood circulation Effects 0.000 abstract description 6
- 241000894006 Bacteria Species 0.000 abstract description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 abstract 2
- 244000303965 Cyamopsis psoralioides Species 0.000 abstract 1
- 241000218231 Moraceae Species 0.000 abstract 1
- QZXSMBBFBXPQHI-UHFFFAOYSA-N N-(dodecanoyl)ethanolamine Chemical compound CCCCCCCCCCCC(=O)NCCO QZXSMBBFBXPQHI-UHFFFAOYSA-N 0.000 abstract 1
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- 208000003251 Pruritus Diseases 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 235000013343 vitamin Nutrition 0.000 description 3
- 239000011782 vitamin Substances 0.000 description 3
- 229940088594 vitamin Drugs 0.000 description 3
- 229930003231 vitamin Natural products 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
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- 230000002378 acidificating effect Effects 0.000 description 2
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- 239000003795 chemical substances by application Substances 0.000 description 2
- OWEGWHBOCFMBLP-UHFFFAOYSA-N 1-(4-chlorophenoxy)-1-(1H-imidazol-1-yl)-3,3-dimethylbutan-2-one Chemical compound C1=CN=CN1C(C(=O)C(C)(C)C)OC1=CC=C(Cl)C=C1 OWEGWHBOCFMBLP-UHFFFAOYSA-N 0.000 description 1
- 201000004384 Alopecia Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 231100000360 alopecia Toxicity 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
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- 229960003344 climbazole Drugs 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000002124 endocrine Effects 0.000 description 1
- 230000003779 hair growth Effects 0.000 description 1
- 230000003646 hair health Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
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- 230000007774 longterm Effects 0.000 description 1
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- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
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- 235000016709 nutrition Nutrition 0.000 description 1
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- 230000004936 stimulating effect Effects 0.000 description 1
- 229940043810 zinc pyrithione Drugs 0.000 description 1
- PICXIOQBANWBIZ-UHFFFAOYSA-N zinc;1-oxidopyridine-2-thione Chemical compound [Zn+2].[O-]N1C=CC=CC1=S.[O-]N1C=CC=CC1=S PICXIOQBANWBIZ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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- Public Health (AREA)
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- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a kind of dandruff control shampoo containing, including：Chinese herbal medicine extract, shampoo matrix, essence and preservative；Chinese herbal medicine extract after the Chinese medical extract mixing of following parts by weight by being made：20~30 parts of Cacumen Platycladi extract, 10~15 parts of mint extract, black 2~10 parts of 10~20 parts of extract of leading a cow, 12~18 parts of isatis root extract, 8~15 parts of aloe extract, 10~18 parts of green-tea extract, 6~12 parts of Bulbus Allii Cepae extract, 6~12 parts of lemon extract, 5~8 parts of mulberries extract, the fleece-flower root and ginseng combined extracting thing；Shampoo matrix is made up of the component of following portions by weight：40~50 parts of dodecyl sodium sulfate, 40~60 parts of water, 5~10 parts of coconut monoethanolamide, 2~4 parts of guar hydroxypropyltrimonium ammonium chloride；Present invention also offers a kind of preparation method of dandruff control shampoo containing, the dandruff control shampoo containing prepared by the present invention can effectively remove dandruff, promote the blood circulation of scalp, dispel the grease of scalp, and the growth of scalp bacterium can be suppressed, pass through the fat secretion for the balance scalp that kept the skin wet to scalp.
Description
Technical Field
The invention relates to the technical field of cosmetics. More specifically, the invention relates to an anti-dandruff shampoo and a preparation method thereof.
Background
With the increasing pace of life and the increasing working pressure, more and more people are worried about scurf, and the scurf problem becomes the second biggest hair health problem which is only secondary to alopecia and troubles consumers. According to professional survey reports, about 67% of people have the problem of dandruff trouble, namely 2/3 people have the problem of dandruff passing, and in addition, nearly 95% of the interviewees have recurrence, and the proportion of patients with dandruff recurrence within 5 days is as high as 90%.
In the prior art, chemical dandruff removers such as zinc pyrithione, climbazole, and the like are used to remove dandruff.
In the process of implementing the invention, the inventor finds that the prior art has at least the following problems: the anti-dandruff shampoo in the prior art is effective when being used at first, and has no obvious effect even if the effect is weakened after a long time, because the chemical anti-dandruff agent only stays on the surface of scalp for cleaning, and can not completely eradicate dandruff, but rather chemical components remain on the scalp, thereby further stimulating and damaging the scalp. Therefore, the long-term use of the chemical anti-dandruff agent does not fundamentally solve the balance of three major scalp problems of hair oil, pruritus and much dandruff.
In the prior art, although the traditional Chinese medicine anti-dandruff shampoo is also available, the functions are single, and the effects of sterilization, oil control and water replenishing are not obvious.
Disclosure of Invention
The invention aims at the problems, and an object of the invention is to provide an anti-dandruff shampoo which integrates anti-dandruff, sterilization, oil control, water replenishing and moistening, can regulate the blood circulation of scalp, can relieve scalp pressure to a certain extent, and is particularly suitable for people with dandruff caused by high working pressure and endocrine.
The invention also aims to provide a preparation method of the anti-dandruff shampoo, the preparation method is simple and easy for industrial production, the extraction method of various traditional Chinese medicine extracts in the anti-dandruff shampoo is simple and reasonable, and the production cost is greatly reduced.
Therefore, the anti-dandruff shampoo provided by the invention comprises 12-17 parts of Chinese herbal medicine extract, 83-88 parts of shampoo matrix, 0.01-0.05 part of essence and 0.05-0.1 part of preservative;
the Chinese herbal medicine extract is prepared by mixing the following Chinese herbal medicine extracts in parts by weight: 20-30 parts of cacumen biotae extract, 10-15 parts of mint extract, 10-20 parts of black morning glory extract, 12-18 parts of radix isatidis extract, 8-15 parts of aloe extract, 10-18 parts of green tea extract, 6-12 parts of onion extract, 6-12 parts of lemon extract, 5-8 parts of mulberry extract and 2-10 parts of polygonum multiflorum and ginseng combined extract;
the shampoo matrix comprises the following components in parts by weight: 40-50 parts of sodium dodecyl sulfate, 40-60 parts of water, 5-10 parts of coconut amide and 2-4 parts of guar gum hydroxypropyl trimethyl ammonium chloride.
Preferably, the anti-dandruff shampoo comprises 14 parts of Chinese herbal medicine extract, 86 parts of shampoo matrix, 0.02 part of essence and 0.08 part of preservative;
the Chinese herbal medicine extract is prepared by mixing the following Chinese herbal medicine extracts in parts by weight: 26 parts of cacumen biotae extract, 14 parts of mint extract, 15 parts of black morning glory extract, 13 parts of isatis root extract, 10 parts of aloe extract, 12 parts of green tea extract, 8 parts of onion extract, 8 parts of lemon extract, 6 parts of mulberry extract and 5 parts of polygonum multiflorum and ginseng combined extract;
the shampoo matrix comprises the following components in parts by weight: 47 parts of sodium dodecyl sulfate, 45 parts of water, 7 parts of coconut amide and 3 parts of guar gum hydroxypropyl trimethyl ammonium chloride.
The preparation method of the anti-dandruff shampoo comprises the following steps:
step one, under the stirring of room temperature and the rotation speed of 500-800 r/min, mixing 40-50 parts of sodium dodecyl sulfate, 40-60 parts of water, 5-10 parts of coconut amide and 2-4 parts of guar gum hydroxypropyl trimethyl ammonium chloride, and uniformly stirring to obtain a shampoo matrix;
adding 6-12 parts of lemon extract into the shampoo matrix, adjusting the pH value to 5.0-6.0 by using citric acid, then sequentially adding 20-30 parts of cacumen biotae extract, 10-15 parts of mint extract, 10-20 parts of black morning glory extract, 12-18 parts of radix isatidis extract, 8-15 parts of aloe extract, 10-18 parts of green tea extract, 6-12 parts of onion extract, 5-8 parts of mulberry extract, 2-10 parts of polygonum multiflorum and ginseng combined extract, and uniformly mixing under stirring at the rotating speed of 800-1000 r/min to obtain a Chinese herbal medicine and fragrance matrix mixture;
respectively adding 0.01-0.05 part of essence and 0.05-0.1 part of preservative into the mixture of the Chinese herbal medicine and the shampoo matrix, uniformly stirring and bottling to obtain the anti-dandruff shampoo;
wherein,
the preparation method of the black morning glory extract comprises the following specific steps: baking the black morning glory at 65-75 ℃, crushing to 20 meshes, adding water which is 3-5 times of the weight of the black morning glory powder, soaking at 60 ℃ for 15-20 hours, filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.2 g/mL to obtain the black morning glory extract;
the preparation method of the isatis root extract comprises the following specific steps: the method comprises the following steps of cleaning the radix isatidis with water, cutting the cleaned radix isatidis into small sections with the length of 1-2 cm, and placing the small sections into a low-temperature vacuum drying oven to be subjected to low-temperature vacuum drying treatment, wherein the low-temperature vacuum drying treatment is divided into three stages, the drying temperature of the first stage is 60-75 ℃, and the drying time is 20-30 min; the drying temperature of the second stage is 80-95 ℃, and the drying time is 10-20 min; the drying temperature of the third stage is 40-60 ℃, and the drying time is 10-15 min; crushing the dried isatis root, adding water which is 6-8 times of the weight of the isatis root powder, performing ultrasonic extraction with the power of 90-110W for 15-25 min, filtering to obtain filtrate, and concentrating the filtrate to 0.15-0.25 g/mL to obtain the isatis root extract.
Preferably, the preparation method of the lemon extract comprises the following steps:
cutting fresh lemon into slices with the thickness of 0.5-1.0 cm, drying the slices and crushing the slices into powder, putting the powder into 80% ethanol for extraction, and concentrating an extracting solution to 0.15-0.25 g/mL to obtain the lemon extract.
Preferably, the preparation method of the onion extract comprises the following steps:
dicing fresh onions, putting the diced fresh onions into a juicer for juicing to obtain onion juice, and concentrating the onion juice to 0.3-0.4 g/mL to obtain an onion extract.
Preferably, the preparation method of the mixed extract of polygonum multiflorum and ginseng comprises the following steps:
air-drying the cleaned polygonum multiflorum and ginseng to ensure that the water content is 6-8%, respectively crushing the polygonum multiflorum and the ginseng to 40 meshes, wherein the weight ratio of the polygonum multiflorum powder to the ginseng powder is 2:1, adding water which is 10-12 times of the total weight of the polygonum multiflorum powder and the ginseng powder, soaking for 30min, heating and extracting, keeping slight boiling for 2.0-2.5 h, then filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.3 g/mL to obtain polygonum multiflorum and ginseng extracts.
Preferably, wherein the cacumen biotae extract, the mint extract and the green tea extract are prepared according to the same method as the isatis root extract.
Preferably, the aloe extract and the mulberry extract are prepared according to the same method as the onion extract.
Preferably, in the second step, the preparation method of the mixture of Chinese herbal medicine and aromatherapy matrix is as follows:
adding 9 parts of lemon extract into the shampoo matrix, adjusting the pH value to 5.5 by using citric acid, then sequentially adding 28 parts of cacumen biotae extract, 14 parts of mint extract, 13 parts of black morning glory extract, 15 parts of isatis root extract, 10 parts of aloe extract, 12 parts of green tea extract, 10 parts of onion extract, 7 parts of mulberry extract, 5 parts of polygonum multiflorum and ginseng combined extract, and uniformly mixing at the stirring speed of 900r/min to obtain a Chinese herbal medicine and fragrance matrix mixture.
The invention at least comprises the following beneficial effects:
1. the anti-dandruff shampoo provided by the invention can solve various problems of dandruff, greasiness, dryness, hair split, pruritus and the like, and Chinese herbal medicine extracts in the anti-dandruff shampoo can permeate into scalp, promote blood circulation of the scalp, inhibit fungi and bacteria of the scalp, effectively remove dandruff, promote absorption of nutrient components and water of the scalp, and keep the scalp fresh and the hair smooth for a long time.
2. The anti-dandruff shampoo provided by the invention contains the lemon extract, is rich in abundant vitamins, moistens scalp, and has fragrant and pleasant fragrance, so that the use content of chemical essence is greatly reduced.
3. The anti-dandruff shampoo provided by the invention is acidic shampoo, and the acidic shampoo is more suitable for the scalp surrounding environment.
4. The black morning glory extract in the anti-dandruff shampoo provided by the invention has the function of promoting blood circulation to the scalp, the isatis root extract has a good sterilization function, and the proportion of the black morning glory extract and the isatis root extract can fully play the functions of the black morning glory extract and the isatis root extract.
The traditional Chinese medicine extract has the following effects:
cacumen biotae extract: has effects in cooling blood, stopping bleeding, promoting hair growth, and blackening hair;
and (3) mint extract: sterilization is carried out, thus being beneficial to refreshing the scalp;
black morning glory extract: promoting blood circulation, and promoting blood circulation of scalp;
isatis root extract, onion extract: antibacterial and antiviral effects, and can inhibit fungi and bacteria in scalp;
aloe extract: moisturizing, anti-inflammatory and balancing the oil and fat of the scalp;
green tea extract: antioxidant, antibacterial and detoxicating effects;
lemon extract: rich vitamins are contained, vitamins are supplemented for the scalp, and the faint scent of the hair is kept;
combined extracts of polygonum multiflorum and ginseng: providing sufficient nutrition to the scalp.
Detailed Description
The present invention is further described in detail with reference to specific examples, so that those skilled in the art can implement the invention with reference to the description.
< example 1>
The anti-dandruff shampoo provided by the invention comprises: 12 parts of Chinese herbal medicine extract, 88 parts of shampoo matrix, 0.01 part of essence and 0.05 part of preservative;
the Chinese herbal medicine extract is prepared by mixing the following Chinese herbal medicine extracts in parts by weight: 20 parts of cacumen biotae extract, 15 parts of mint extract, 10 parts of black morning glory extract, 18 parts of isatis root extract, 8 parts of aloe extract, 18 parts of green tea extract, 6 parts of onion extract, 12 parts of lemon extract, 5 parts of mulberry extract and 2 parts of polygonum multiflorum and ginseng combined extract;
the shampoo matrix comprises the following components in parts by weight: 40 parts of sodium dodecyl sulfate, 60 parts of water, 10 parts of coconut amide and 2 parts of guar gum hydroxypropyl trimethyl ammonium chloride.
< example 2>
The anti-dandruff shampoo provided by the invention comprises: 17 parts of Chinese herbal medicine extract, 83 parts of shampoo matrix, 0.05 part of essence and 0.1 part of preservative;
the Chinese herbal medicine extract is prepared by mixing the following Chinese herbal medicine extracts in parts by weight: 30 parts of cacumen biotae extract, 10 parts of mint extract, 20 parts of black morning glory extract, 12 parts of isatis root extract, 8 parts of aloe extract, 18 parts of green tea extract, 6 parts of onion extract, 12 parts of lemon extract, 5 parts of mulberry extract and 5 parts of polygonum multiflorum and ginseng combined extract;
the shampoo matrix comprises the following components in parts by weight: 50 parts of sodium dodecyl sulfate, 40 parts of water, 10 parts of coconut amide and 2 parts of guar gum hydroxypropyl trimethyl ammonium chloride.
< example 3>
The anti-dandruff shampoo provided by the invention comprises 14 parts of Chinese herbal medicine extract, 86 parts of shampoo matrix, 0.02 part of essence and 0.08 part of preservative;
the Chinese herbal medicine extract is prepared by mixing the following Chinese herbal medicine extracts in parts by weight: 26 parts of cacumen biotae extract, 14 parts of mint extract, 15 parts of black morning glory extract, 13 parts of isatis root extract, 10 parts of aloe extract, 12 parts of green tea extract, 8 parts of onion extract, 8 parts of lemon extract, 6 parts of mulberry extract and 5 parts of polygonum multiflorum and ginseng combined extract;
the shampoo matrix comprises the following components in parts by weight: 47 parts of sodium dodecyl sulfate, 45 parts of water, 7 parts of coconut amide and 3 parts of guar gum hydroxypropyl trimethyl ammonium chloride.
< example 4>
The preparation method of the anti-dandruff shampoo comprises the following steps:
step one, mixing 47 parts of sodium dodecyl sulfate, 45 parts of water, 7 parts of coconut amide and 3 parts of guar gum hydroxypropyl trimethyl ammonium chloride under stirring at room temperature and a rotation speed of 500-800 r/min, and uniformly stirring to obtain a shampoo matrix;
adding 9 parts of lemon extract into the shampoo matrix, adjusting the pH value to 5.5 by using citric acid, then sequentially adding 28 parts of cacumen biotae extract, 14 parts of mint extract, 13 parts of black morning glory extract, 15 parts of isatis root extract, 10 parts of aloe extract, 12 parts of green tea extract, 10 parts of onion extract, 7 parts of mulberry extract and 5 parts of polygonum multiflorum and ginseng combined extract, and uniformly mixing under stirring at the rotating speed of 900r/min to obtain a Chinese herbal medicine and shampoo matrix mixture;
respectively adding 0.02 part of essence and 0.05 part of preservative into the mixture of the Chinese herbal medicine and the shampoo matrix, uniformly stirring and bottling to obtain the anti-dandruff shampoo;
wherein,
the preparation method of the black morning glory extract comprises the following specific steps: baking the black morning glory at 70 ℃, crushing to 20 meshes, then adding water with the weight being 4 times of that of the black morning glory powder, soaking for 18 hours at 60 ℃, filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.2 g/mL to obtain the black morning glory extract;
the preparation method of the isatis root extract comprises the following specific steps: washing radix isatidis with water, cutting the washed radix isatidis into small sections with the length of 1-2 cm, and placing the small sections into a low-temperature vacuum drying oven for low-temperature vacuum drying treatment, wherein the low-temperature vacuum drying treatment is divided into three stages, the drying temperature of the first stage is 68 ℃, and the drying time is 25 min; the drying temperature of the second stage is 90 ℃, and the drying time is 10 min; the drying temperature of the third stage is 50 ℃, and the drying time is 15 min; crushing the dried isatis root, adding water 7 times the weight of the isatis root powder, performing ultrasonic extraction with the power of 100W for 18min, filtering to obtain filtrate, and concentrating the filtrate to 0.15-0.25 g/mL to obtain the isatis root extract.
The preparation method of the lemon extract comprises the following steps: cutting fresh lemon into slices with the thickness of 0.5-1.0 cm, drying the slices and crushing the slices into powder, putting the powder into 80% ethanol for extraction, and concentrating an extracting solution to 0.15-0.25 g/mL to obtain the lemon extract.
The preparation method of the onion extract comprises the following steps: dicing fresh onions, putting the diced fresh onions into a juicer for juicing to obtain onion juice, and concentrating the onion juice to 0.3-0.4 g/mL to obtain an onion extract.
The preparation method of the mixed extract of the polygonum multiflorum and the ginseng comprises the following steps: air-drying the cleaned polygonum multiflorum and ginseng to ensure that the water content is 6-8%, respectively crushing the polygonum multiflorum and the ginseng to 40 meshes, wherein the weight ratio of the polygonum multiflorum powder to the ginseng powder is 2:1, adding water which is 10-12 times of the total weight of the polygonum multiflorum powder and the ginseng powder, soaking for 30min, heating and extracting, keeping slight boiling for 2.0-2.5 h, then filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.3 g/mL to obtain polygonum multiflorum and ginseng extracts.
The cacumen biotae extract, the mint extract and the green tea extract are all prepared according to the same method as the isatis root extract; the aloe extract and the mulberry extract are both prepared according to the same method as the onion extract.
< example 5>
The invention provides a preparation method of anti-dandruff shampoo, which comprises the following steps:
step one, under the stirring of room temperature and the rotation speed of 500-800 r/min, mixing 40 parts of sodium dodecyl sulfate, 60 parts of water, 5 parts of coconut amide and 4 parts of guar gum hydroxypropyl trimethyl ammonium chloride, and uniformly stirring to obtain a shampoo matrix;
adding 12 parts of lemon extract into the shampoo matrix, adjusting the pH value to 5.0 by using citric acid, then sequentially adding 20 parts of cacumen biotae extract, 15 parts of mint extract, 10 parts of black morning glory extract, 8 parts of isatis root extract, 8 parts of aloe extract, 18 parts of green tea extract, 6 parts of onion extract, 8 parts of mulberry extract and 2 parts of polygonum multiflorum and ginseng combined extract, and uniformly mixing under stirring at the rotating speed of 800-1000 r/min to obtain a Chinese herbal medicine and shampoo matrix mixture;
respectively adding 0.01 part of essence and 0.05 part of preservative into the mixture of the Chinese herbal medicine and the shampoo matrix, uniformly stirring and bottling to obtain the anti-dandruff shampoo;
wherein,
the preparation method of the black morning glory extract comprises the following specific steps: baking the black morning glory at 65 ℃, crushing to 20 meshes, then adding water with the weight being 3 times of that of the black morning glory powder, soaking for 20 hours at 60 ℃, filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.2 g/mL to obtain the black morning glory extract;
the preparation method of the isatis root extract comprises the following specific steps: washing radix isatidis with water, cutting the washed radix isatidis into small sections with the length of 1-2 cm, and placing the small sections into a low-temperature vacuum drying oven for low-temperature vacuum drying treatment, wherein the low-temperature vacuum drying treatment is divided into three stages, the drying temperature of the first stage is 75 ℃, and the drying time is 20 min; the second stage drying temperature is 95 deg.C, and drying time is 10 min; the drying temperature of the third stage is 40 ℃, and the drying time is 15 min; crushing the dried isatis root, adding water which is 6 times of the weight of the isatis root powder, performing ultrasonic extraction with the power of 90-110W for 15-25 min, filtering to obtain filtrate, and concentrating the filtrate to 0.15-0.25 g/mL to obtain the isatis root extract.
The preparation method of the lemon extract comprises the following steps: cutting fresh lemon into slices with the thickness of 0.5-1.0 cm, drying the slices and crushing the slices into powder, putting the powder into 80% ethanol for extraction, and concentrating an extracting solution to 0.15-0.25 g/mL to obtain the lemon extract.
The preparation method of the onion extract comprises the following steps: dicing fresh onions, putting the diced fresh onions into a juicer for juicing to obtain onion juice, and concentrating the onion juice to 0.3-0.4 g/mL to obtain an onion extract.
The preparation method of the mixed extract of the polygonum multiflorum and the ginseng comprises the following steps: air-drying the cleaned polygonum multiflorum and ginseng to ensure that the water content is 6-8%, respectively crushing the polygonum multiflorum and the ginseng to 40 meshes, wherein the weight ratio of the polygonum multiflorum powder to the ginseng powder is 2:1, adding water which is 10-12 times of the total weight of the polygonum multiflorum powder and the ginseng powder, soaking for 30min, heating and extracting, keeping slight boiling for 2.0-2.5 h, then filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.3 g/mL to obtain polygonum multiflorum and ginseng extracts.
The cacumen biotae extract, the mint extract and the green tea extract are all prepared according to the same method as the isatis root extract.
The aloe extract and the mulberry extract are both prepared according to the same method as the onion extract.
< example 6>
The preparation method of the anti-dandruff shampoo provided by the invention comprises the following steps:
step one, mixing 50 parts of sodium dodecyl sulfate, 40 parts of water, 10 parts of coconut amide and 2 parts of guar gum hydroxypropyl trimethyl ammonium chloride under stirring at room temperature and the rotation speed of 500-800 r/min, and uniformly stirring to obtain a shampoo matrix;
adding 6 parts of lemon extract into the shampoo matrix, adjusting the pH value to 6.0 by using citric acid, then sequentially adding 30 parts of cacumen biotae extract, 10 parts of mint extract, 20 parts of black morning glory extract, 12 parts of isatis root extract, 8 parts of aloe extract, 18 parts of green tea extract, 6 parts of onion extract, 8 parts of mulberry extract and 2 parts of polygonum multiflorum and ginseng combined extract, and uniformly mixing under stirring at the rotating speed of 800-1000 r/min to obtain a Chinese herbal medicine and shampoo matrix mixture;
respectively adding 0.05 part of essence and 0.1 part of preservative into the mixture of the Chinese herbal medicine and the shampoo matrix, uniformly stirring and bottling to obtain the anti-dandruff shampoo;
wherein,
the preparation method of the black morning glory extract comprises the following specific steps: baking the black morning glory at 75 ℃, crushing to 20 meshes, then adding water which is 5 times of the weight of the black morning glory powder, soaking for 20 hours at 60 ℃, filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.2 g/mL to obtain the black morning glory extract;
the preparation method of the isatis root extract comprises the following specific steps: washing radix isatidis with water, cutting the washed radix isatidis into small sections with the length of 1-2 cm, and placing the small sections into a low-temperature vacuum drying oven for low-temperature vacuum drying treatment, wherein the low-temperature vacuum drying treatment is divided into three stages, the drying temperature of the first stage is 60 ℃, and the drying time is 30 min; the second stage drying temperature is 80 deg.C, and drying time is 20 min; the drying temperature of the third stage is 60 ℃, and the drying time is 10 min; crushing the dried isatis root, adding water which is 6-8 times of the weight of the isatis root powder, performing ultrasonic extraction with the power of 90W for 25min, filtering to obtain filtrate, and concentrating the filtrate to 0.15-0.25 g/mL to obtain the isatis root extract.
The preparation method of the lemon extract comprises the following steps: cutting fresh lemon into slices with the thickness of 0.5-1.0 cm, drying the slices and crushing the slices into powder, putting the powder into 80% ethanol for extraction, and concentrating an extracting solution to 0.15-0.25 g/mL to obtain the lemon extract.
The preparation method of the onion extract comprises the following steps: dicing fresh onions, putting the diced fresh onions into a juicer for juicing to obtain onion juice, and concentrating the onion juice to 0.3-0.4 g/mL to obtain an onion extract.
The preparation method of the mixed extract of the polygonum multiflorum and the ginseng comprises the following steps: air-drying the cleaned polygonum multiflorum and ginseng to ensure that the water content is 6-8%, respectively crushing the polygonum multiflorum and the ginseng to 40 meshes, wherein the weight ratio of the polygonum multiflorum powder to the ginseng powder is 2:1, adding water which is 10-12 times of the total weight of the polygonum multiflorum powder and the ginseng powder, soaking for 30min, heating and extracting, keeping slight boiling for 2.0-2.5 h, then filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.3 g/mL to obtain polygonum multiflorum and ginseng extracts.
The cacumen biotae extract, the mint extract and the green tea extract are all prepared according to the same method as the isatis root extract. The aloe extract and the mulberry extract are both prepared according to the same method as the onion extract.
After the anti-dandruff shampoo provided by the invention is used for cleaning hair for 7-10 days continuously, the hair is smooth and soft, no dandruff can be seen by naked eyes, the itching phenomenon completely disappears, and the hair can be kept fresh and clean for a long time.
While embodiments of the invention have been disclosed above, it is not intended to be limited to the uses set forth in the specification and examples. It can be applied to all kinds of fields suitable for the present invention. Additional modifications will readily occur to those skilled in the art. The invention is therefore not to be limited to the specific details described herein, without departing from the general concept as defined by the appended claims and their equivalents.
Claims (8)
1. A preparation method of anti-dandruff shampoo, which is characterized in that,
the anti-dandruff shampoo comprises 12-17 parts of Chinese herbal medicine extract, 83-88 parts of shampoo matrix, 0.01-0.05 part of essence and 0.05-0.1 part of preservative;
the Chinese herbal medicine extract is prepared by mixing the following Chinese herbal medicine extracts in parts by weight: 20-30 parts of cacumen biotae extract, 10-15 parts of mint extract, 10-20 parts of black morning glory extract, 12-18 parts of radix isatidis extract, 8-15 parts of aloe extract, 10-18 parts of green tea extract, 6-12 parts of onion extract, 6-12 parts of lemon extract, 5-8 parts of mulberry extract and 2-10 parts of polygonum multiflorum and ginseng combined extract;
the shampoo matrix comprises the following components in parts by weight: 40-50 parts of sodium dodecyl sulfate, 40-60 parts of water, 5-10 parts of coconut amide and 2-4 parts of guar gum hydroxypropyl trimethyl ammonium chloride;
the preparation method comprises the following steps:
step one, under the stirring of room temperature and the rotation speed of 500-800 r/min, mixing 40-50 parts of sodium dodecyl sulfate, 40-60 parts of water, 5-10 parts of coconut amide and 2-4 parts of guar gum hydroxypropyl trimethyl ammonium chloride, and uniformly stirring to obtain a shampoo matrix;
adding 6-12 parts of lemon extract into the shampoo matrix, adjusting the pH value to 5.0-6.0 by using citric acid, then sequentially adding 20-30 parts of cacumen biotae extract, 10-15 parts of mint extract, 10-20 parts of black morning glory extract, 12-18 parts of radix isatidis extract, 8-15 parts of aloe extract, 10-18 parts of green tea extract, 6-12 parts of onion extract, 5-8 parts of mulberry extract, 2-10 parts of polygonum multiflorum and ginseng combined extract, and uniformly mixing under stirring at the rotating speed of 800-1000 r/min to obtain a Chinese herbal medicine and fragrance matrix mixture;
respectively adding 0.01-0.05 part of essence and 0.05-0.1 part of preservative into the mixture of the Chinese herbal medicine and the shampoo matrix, uniformly stirring and bottling to obtain the anti-dandruff shampoo;
wherein,
the preparation method of the black morning glory extract comprises the following specific steps: baking the black morning glory at 65-75 ℃, crushing to 20 meshes, adding water which is 3-5 times of the weight of the black morning glory powder, soaking at 60 ℃ for 15-20 hours, filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.2 g/mL to obtain the black morning glory extract;
the preparation method of the isatis root extract comprises the following specific steps: the method comprises the following steps of cleaning the radix isatidis with water, cutting the cleaned radix isatidis into small sections with the length of 1-2 cm, and placing the small sections into a low-temperature vacuum drying oven to be subjected to low-temperature vacuum drying treatment, wherein the low-temperature vacuum drying treatment is divided into three stages, the drying temperature of the first stage is 60-75 ℃, and the drying time is 20-30 min; the drying temperature of the second stage is 80-95 ℃, and the drying time is 10-20 min; the drying temperature of the third stage is 40-60 ℃, and the drying time is 10-15 min; crushing the dried isatis root, adding water which is 6-8 times of the weight of the isatis root powder, performing ultrasonic extraction with the power of 90-110W for 15-25 min, filtering to obtain filtrate, and concentrating the filtrate to 0.15-0.25 g/mL to obtain the isatis root extract.
2. The method for preparing the anti-dandruff shampoo as claimed in claim 1, wherein the anti-dandruff shampoo comprises 14 parts of Chinese herbal medicine extract, 86 parts of shampoo matrix, 0.02 part of essence and 0.08 part of preservative;
the Chinese herbal medicine extract is prepared by mixing the following Chinese herbal medicine extracts in parts by weight: 26 parts of cacumen biotae extract, 14 parts of mint extract, 15 parts of black morning glory extract, 13 parts of isatis root extract, 10 parts of aloe extract, 12 parts of green tea extract, 8 parts of onion extract, 8 parts of lemon extract, 6 parts of mulberry extract and 5 parts of polygonum multiflorum and ginseng combined extract;
the shampoo matrix comprises the following components in parts by weight: 47 parts of sodium dodecyl sulfate, 45 parts of water, 7 parts of coconut amide and 3 parts of guar gum hydroxypropyl trimethyl ammonium chloride.
3. The method for preparing the anti-dandruff shampoo as claimed in claim 1, wherein the method for preparing the lemon extract comprises:
cutting fresh lemon into slices with the thickness of 0.5-1.0 cm, drying the slices and crushing the slices into powder, putting the powder into 80% ethanol for extraction, and concentrating an extracting solution to 0.15-0.25 g/mL to obtain the lemon extract.
4. The method for preparing the anti-dandruff shampoo as claimed in claim 1, wherein the method for preparing the onion extract comprises:
dicing fresh onions, putting the diced fresh onions into a juicer for juicing to obtain onion juice, and concentrating the onion juice to 0.3-0.4 g/mL to obtain an onion extract.
5. The method for preparing the anti-dandruff shampoo as claimed in claim 1, wherein the method for preparing the mixed extract of polygonum multiflorum and ginseng comprises the following steps:
air-drying the cleaned polygonum multiflorum and ginseng to ensure that the water content is 6-8%, respectively crushing the polygonum multiflorum and the ginseng to 40 meshes, wherein the weight ratio of the polygonum multiflorum powder to the ginseng powder is 2:1, adding water which is 10-12 times of the total weight of the polygonum multiflorum powder and the ginseng powder, soaking for 30min, heating and extracting, keeping slight boiling for 2.0-2.5 h, then filtering to obtain filtrate, and concentrating the filtrate to 0.1-0.3 g/mL to obtain polygonum multiflorum and ginseng extracts.
6. The method for preparing an anti-dandruff shampoo as claimed in claim 1, wherein the cacumen biotae extract, the mint extract and the green tea extract are prepared in the same manner as the isatis root extract.
7. The method for preparing an anti-dandruff shampoo according to claim 4, wherein the aloe extract and the mulberry extract are prepared in the same manner as the onion extract.
8. The method for preparing the anti-dandruff shampoo as claimed in claim 1, wherein in the second step, the method for preparing the mixture of the Chinese herbal medicine and the shampoo matrix comprises the following specific steps:
adding 9 parts of lemon extract into the shampoo matrix, adjusting the pH value to 5.5 by using citric acid, then sequentially adding 28 parts of cacumen biotae extract, 14 parts of mint extract, 13 parts of black morning glory extract, 15 parts of isatis root extract, 10 parts of aloe extract, 12 parts of green tea extract, 10 parts of onion extract, 7 parts of mulberry extract, 5 parts of polygonum multiflorum and ginseng combined extract, and uniformly mixing at the stirring speed of 900r/min to obtain a Chinese herbal medicine and fragrance matrix mixture.
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| CN105853277A (en) * | 2016-04-27 | 2016-08-17 | 深圳市好青丝生物科技有限公司 | Plant shampoo with hair washing and scurf removing effects and preparation method thereof |
| CN107375131B (en) * | 2017-07-17 | 2020-06-16 | 武汉爱民制药股份有限公司 | Dandruff-removing and hair-nourishing plant shampoo containing aescin |
| CN107648139A (en) * | 2017-10-18 | 2018-02-02 | 桂林大创科技有限公司 | A kind of dandruff control shampoo containing traditional Chinese medicines and preparation method thereof |
| CN108578311A (en) * | 2018-04-03 | 2018-09-28 | 苏州高新区鼎正精密机电有限公司 | A kind of aloe liquid shampoo and preparation method thereof |
| CN111671694A (en) * | 2020-07-20 | 2020-09-18 | 西安幸福未来化妆品有限公司 | Pure natural animal and plant extract hair conditioner and preparation method thereof |
| CN113116779A (en) * | 2021-04-19 | 2021-07-16 | 西安蓝风生物科技有限公司 | Special plant anti-dandruff shampoo for women and preparation method thereof |
| CN113081925A (en) * | 2021-04-26 | 2021-07-09 | 西安蓝风生物科技有限公司 | Special plant anti-dandruff shampoo for men and preparation method |
| CN114469801B (en) * | 2022-01-19 | 2023-06-06 | 南京上元堂沉香生物科技有限公司 | Agilawood shampoo for regulating scalp microecological balance and preparation method thereof |
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