CN105177818A - Manufacturing method of milk fiber containing woolen fabric - Google Patents
Manufacturing method of milk fiber containing woolen fabric Download PDFInfo
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- CN105177818A CN105177818A CN201510685868.4A CN201510685868A CN105177818A CN 105177818 A CN105177818 A CN 105177818A CN 201510685868 A CN201510685868 A CN 201510685868A CN 105177818 A CN105177818 A CN 105177818A
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- fabric
- wool
- yarn
- milk fibre
- fibre
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- 239000004744 fabric Substances 0.000 title claims abstract description 117
- 239000000835 fiber Substances 0.000 title claims abstract description 101
- 235000013336 milk Nutrition 0.000 title claims abstract description 86
- 210000004080 milk Anatomy 0.000 title claims abstract description 86
- 239000008267 milk Substances 0.000 title claims abstract description 86
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 48
- 210000002268 wool Anatomy 0.000 claims abstract description 113
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 36
- 238000009987 spinning Methods 0.000 claims abstract description 33
- 238000005406 washing Methods 0.000 claims abstract description 13
- 238000002156 mixing Methods 0.000 claims abstract description 12
- 241001122767 Theaceae Species 0.000 claims description 54
- 239000000463 material Substances 0.000 claims description 44
- 238000000034 method Methods 0.000 claims description 43
- 239000002023 wood Substances 0.000 claims description 38
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 29
- 238000004043 dyeing Methods 0.000 claims description 25
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 23
- 239000007864 aqueous solution Substances 0.000 claims description 23
- 238000001035 drying Methods 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 19
- 238000002360 preparation method Methods 0.000 claims description 17
- 206010004542 Bezoar Diseases 0.000 claims description 15
- 238000009835 boiling Methods 0.000 claims description 15
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 13
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 12
- 229910052742 iron Inorganic materials 0.000 claims description 12
- 238000004140 cleaning Methods 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 11
- 241001463139 Vitta Species 0.000 claims description 10
- 238000010025 steaming Methods 0.000 claims description 10
- 238000010792 warming Methods 0.000 claims description 10
- 125000003118 aryl group Chemical group 0.000 claims description 6
- 239000000796 flavoring agent Substances 0.000 claims description 6
- 235000019634 flavors Nutrition 0.000 claims description 6
- 230000008569 process Effects 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 238000003980 solgel method Methods 0.000 claims description 6
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims description 5
- 235000011613 Pinus brutia Nutrition 0.000 claims description 5
- 241000018646 Pinus brutia Species 0.000 claims description 5
- 238000013019 agitation Methods 0.000 claims description 5
- 238000010276 construction Methods 0.000 claims description 5
- 239000000986 disperse dye Substances 0.000 claims description 5
- 239000000428 dust Substances 0.000 claims description 5
- 239000000975 dye Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 239000000985 reactive dye Substances 0.000 claims description 5
- 238000004804 winding Methods 0.000 claims description 5
- 230000036541 health Effects 0.000 abstract description 5
- 238000012545 processing Methods 0.000 abstract description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 abstract 1
- 230000005540 biological transmission Effects 0.000 abstract 1
- 239000003063 flame retardant Substances 0.000 abstract 1
- 238000002834 transmittance Methods 0.000 abstract 1
- 238000012986 modification Methods 0.000 description 6
- 230000004048 modification Effects 0.000 description 6
- 239000004753 textile Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 235000018102 proteins Nutrition 0.000 description 4
- 108090000623 proteins and genes Proteins 0.000 description 4
- 102000004169 proteins and genes Human genes 0.000 description 4
- 206010013786 Dry skin Diseases 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 210000004209 hair Anatomy 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
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- 239000002904 solvent Substances 0.000 description 3
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- 102000004190 Enzymes Human genes 0.000 description 2
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- 239000011858 nanopowder Substances 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 102000014171 Milk Proteins Human genes 0.000 description 1
- 108010011756 Milk Proteins Proteins 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000001046 anti-mould Effects 0.000 description 1
- 239000002546 antimould Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
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- 229910052799 carbon Inorganic materials 0.000 description 1
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- 235000021239 milk protein Nutrition 0.000 description 1
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- 230000037303 wrinkles Effects 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
Abstract
The invention relates to a manufacturing method of milk fiber containing woolen fabric. The fabric comprises non-shrinkable wool and milk fiber, wherein the specification of the non-shrinkable wool is that the fineness ranges from 70 <S> to 80 <S> and the length ranges from 60 mm to 70 mm, and the specification of the milk fiber is 4-5 dtexX (65-70) mm; the mass percentage ratio of the non-shrinkable wool to the milk fiber is (30%-60%): (70%-40%). The manufacturing method comprises steps as follows: non-shrinkable wool balls are dyed for preparing colored wool tops, milk yarn is dyed and spun to form fine yarn through sliver blending, the fine yarn is subjected to back spinning, worsted yarn is obtained and is prepared to form woolen fabric with a manufacturing process, then the fabric is subjected to padding fabric processing twice, and the milk fiber containing woolen fabric is prepared. According to the fabric and the manufacturing method thereof, the transmittance and the breathability can be effectively improved, the amount of water vapor transmission can be effectively increased, and the fabric has a good natural bacteriostasis function, is mildewproof, mothproof, durable and washable and is high in strength and easy to store; the washed fabric is easy to dry, can keep permanent performance, fastness to rubbing and color fastness to washing and has good antistatic property, flame retardant property, breathability and health care efficacy.
Description
Technical field
The present invention relates to weaving face fabric production art field, be specifically related to a kind of manufacture method containing milk fibre wool spinning fabric.
Background technology
Wool fibre is the deformations of the skin of sheep, and warmth retention property is splendid, is used for the clothes of autumn and winter season, but very easily damages by worms, and the time of dress has been grown and easily grown various germ.Weaving wool fibre is main is sheep's wool, so-called wool, or claims wool fibre, or is called for short hair.Wool is natural protein fibre, and main component makes the protein of angle protein form, and angle protein content accounts for 97%, and inorganic matter accounts for 1 ~ 3%, and the essential element of wool angle protein is C, O, N, H, S.
Because wool surface has scale layer, in washing process, easily produce shrinkage, shape is unstable, have much the treatable research of wool fibre, be divested by physics, chemical method or weaken the scale layer of wool fibre mostly, thus improve the shortcoming of its shrinkage; But adopt Chemical Physics method inevitably to use various physics and chemistry reagent, it not only can residue in wool fibre, also pollute the environment, produce a large amount of industrial wastewaters, such as, in prior art conventional chloridizing and permanganimetric method (as CN201010269379).Along with the development of biological zymetology, the defect utilizing zymetology technology to change wool fibre is problem more popular in recent years.Chinese patent CN200810059502 and CN201010127072, all employs enzyme preparation, but in said method, many places employ chemical reagent equally, easily causes environmental pollution, and can partly residue in wool fibre, works the mischief to human body.
How utilizing merely enzyme preparation to process wool fibre, and reach the object of wrinkle resistant environmental protection, is prior art technical problem anxious to be resolved.
Current in addition, adopt colloidal sol to carry out functionalization to textiles in the prior art to arrange and mainly realized by following approach: first prepare Nano sol by sol-gel process, then its gelation is made, then by gel drying with remove the inside organic principle, under the high temperature of 300 ~ 800 DEG C, ultra-fine nano-powder is made in roasting again, and the functional modification finally nano-powder being applied to textiles arranges.
Wool spinning fabric is the important fabric with making high-grade business shirt, and wool spinning fabric good hand touch is comfortable and easy to wear, dark liking by consumers in general.But carry out health care arrangement to it at present, thus meet people and have to it function energy sexual demand had containing milk fibre, need further research and development.
Summary of the invention
The object of the invention is to overcome defect of the prior art, design one effectively can improve transmitance, vapor transfer rate and air penetrability, there is good soft feel, fastness to rubbing, color fastness to washing, and there is good antistatic behaviour, fire resistance and gas permeability, also have the manufacture method of health-care effect containing milk fibre wool spinning fabric.
For achieving the above object, the technical solution adopted in the present invention is:
Containing a manufacture method for milk fibre wool spinning fabric, described fabric comprises: specification is fineness 70
s~ 80
s, length is the non-shrinkable wool of 60 ~ 70mm; Specification is the milk fibre of 4 ~ 5dtexX (65 ~ 70) mm; The mass percent of non-shrinkable wool and milk fibre two components is 30 ~ 60%:70 ~ 40%; By non-shrinkable wool hair ball dyeing make coloured wool top, milk yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing milk fibre wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce milk fibre strip: by milk fibre dyeing yarn, obtain milk fibre vitta;
S3, rove spin: wool yarn and milk fibre vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 75 ~ 90 DEG C, 80 ~ 120 minutes time; The speed of a motor vehicle of described high speed doubling is 500 ~ 700 ms/min, and the double twisting speed of a motor vehicle is 5000 ~ 8000 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and blended by milk fibre;
S6, first time dip fabric: the worsted fabric of wool fibre and blended by milk fibre two is soaked two and rolls in coloured Nano silica sol, and pressure is 0.5 ~ 2.5kg/cm
2, pick-up is 75 ~ 85%, preliminary drying under the temperature conditions of 70 ~ 90 DEG C, then under the temperature conditions of 120 ~ 180 DEG C, bake 3 ~ 5 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 1 ~ 3kg/cm
2, pick-up is 60 ~ 80%, preliminary drying under the temperature conditions of 60 ~ 80 DEG C, then under the temperature conditions of 100 ~ 160 DEG C, bake 2 ~ 3 minutes; Through washing, after naturally drying, obtain containing milk fibre wool spinning fabric.
Preferred technical scheme is, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described milk fibre dyeing yarn adopts DISPERSE DYES.
Preferred technical scheme also has, and the number of described worsted yarn is 90 ~ 120/2.
Preferred technical scheme also has, and the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
Preferred technical scheme also has, and described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 2 ~ 11:1, water: ethyl silicate 40 is 5 ~ 20:0.5, FeCl
36H2O: ethyl silicate 40 is 0.6 ~ 0.8:0.6, is prepared from.
Preferred technical scheme also has further, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, 50 ~ 70 DEG C are warming up to again after dropwising, stir 2.5 ~ 3 hours, namely obtain a kind of coloured Nano silica sol.
Preferred technical scheme also has, and the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 3 ~ 4 hours with the temperature of 90 DEG C ~ 100 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 3 ~ 4 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 60% ~ 80%:40% ~ 20% proportioning and both obtains the wooden aqueous solution of scented tea.
Preferred technical scheme also has, and first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, and microwave frequency is 130MHz ~ 280MHz, and microwave treatment time is 6 ~ 8min.
Advantage of the present invention and beneficial effect are: the described manufacture method containing milk fibre wool spinning fabric can make up the deficiency of wool fibre, and developing can at the health care wool worsted fabric being applicable to take each season.Breakthrough wool worsted fabric is taken limitation in season by the present invention, expands the scope of application of wool worsted fabric, also can meet the demand of the high-grade woolen of consumer.Innovated by raw material simultaneously, by milk fibre and fleece fibre blended spinning, hand over also, interweave, give flexibility, skin-friendly that fabric is lasting.Owing to having natural bacteriostatic function, anti-mould and anti-moth, intensity is high, endurable washable, easily preserves, ventilative, wet guilding is good, refreshing body; Warmth retention property is close to cashmere, and warmth retention property is good, and the ABRASION RESISTANCE of milk suede, anti-pilling, coloring, brute force are all better than cashmere; Owing to containing amino acid in milk protein, skin can not repel this fabric, quite the same with one deck skin of people, and has maintenance action to skin; Easily dry after washing, still can keep the permanent performance of product after washing, thus overcome the shortcoming of current wool bacteriostasis property difference, what expand wool takes scope, improve the added value of wool product, be conducive to the development of wool textile industry, meet modern textiles trend.
In addition owing to selecting ethyl silicate 40 to be the sol solutions of precursor power containing iron ion, sol solutions is coloured, nontoxic, and sol particles is uniformly dispersed and stablizes; Adopt and roll the method for sorting curing this applicable textiles, only need carry out the heat treatment of 100 ~ 160 DEG C to fabric, can be formed at fabric face and adsorb firmly gel film.Fabric after arrangement not only has the color compared with high color fastness, have also obtained excellent antistatic behaviour, anti-flammability and gas permeability simultaneously.
After have employed scented tea wood again mixed liquor dipping, make the weaving woollen internal penetration aromatic odor of tea material and timber, effectively can remove the pollutants such as formaldehyde in air, clean air, make fabric have cleaning efficacy; Fabric itself can give out unique tea wood mixing natural flavor, can calm the nerves salubrious, have health care effectiveness, and fragrance is prolonged does not fall apart.
The present invention not only solves the potential pollution problem of existing hair side material, more effectively improve effect and the quality of existing hair side material, also solve a large amount of tea rim charge simultaneously, wood boundary material leave unused, the problem such as production waste and environmental pollution that processing procedure is brought, be environmental protection, health care, comfortableness the technical scheme of depositing.
Detailed description of the invention
Below in conjunction with embodiment, the specific embodiment of the present invention is further described.Following examples only for technical scheme of the present invention is clearly described, and can not limit the scope of the invention with this.
Embodiment 1
The present invention is a kind of manufacture method containing milk fibre wool spinning fabric, and described fabric comprises: specification is fineness 70
s, length is the non-shrinkable wool of 60mm; Specification is the milk fibre of 4dtexX65mm; The mass percent of non-shrinkable wool and milk fibre two components is 30%:70%; By non-shrinkable wool hair ball dyeing make coloured wool top, milk yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing milk fibre wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce milk fibre strip: by milk fibre dyeing yarn, obtain milk fibre vitta;
S3, rove spin: wool yarn and milk fibre vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 75 DEG C, 80 minutes time; The speed of a motor vehicle of described high speed doubling is 500 ms/min, and the double twisting speed of a motor vehicle is 5000 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and blended by milk fibre;
S6, first time dip fabric: the worsted fabric of wool fibre and blended by milk fibre two is soaked two and rolls in coloured Nano silica sol, and pressure is 1.5kg/cm
2, pick-up is 75%, preliminary drying under the temperature conditions of 70 DEG C, then under the temperature conditions of 120 DEG C, bake 3 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 1kg/cm
2, pick-up is 60%, preliminary drying under the temperature conditions of 60 DEG C, then under the temperature conditions of 100 DEG C, bake 2 minutes; Through washing, after naturally drying, obtain containing milk fibre wool spinning fabric.
The preferred embodiment of the invention is, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described milk fibre dyeing yarn adopts DISPERSE DYES.
The preferred embodiment of the invention also has, and the number of described worsted yarn is 90/2.
The preferred embodiment of the invention also has, and the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
The preferred embodiment of the invention also has, and described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 2:1, water: ethyl silicate 40 is 5:0.5, FeCl
36H2O: ethyl silicate 40 is 0.6:0.6, is prepared from.
Further preferred embodiment of the present invention also has, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, 50 DEG C are warming up to again after dropwising, stir 2.5 hours, namely obtain a kind of coloured Nano silica sol.
41.7gTEOS, 27.6gEtOH and appropriate HCl are joined in 500ml tri-mouthfuls of round-bottomed flasks successively, regulates pH to be 2 ~ 3.Stir under the rotating speed of 100 revs/min, mix the iron ion aqueous solution (5.42gFeCl36H2O+7.2gH2O) while stirring, and at 50 DEG C, continue stirring 2.5 hours.Namely transparent, coloured and uniform nanometer coloured silicasol system is obtained.Wool spinning fabric first time two leaching two in nanometer coloured silicasol is rolled, pressure 1kg/cm
2, pick-up 80%.Then 60 DEG C of preliminary dryings in convection oven, bake 3 minutes after washings, naturally dry at 130 DEG C.
First there is poly-condensation and hydrolysis in ethyl silicate 40, generate sol particles in alcohol solvent; Mix iron ion, form the coloured Nano silica sol of tool.Be adsorbed onto fully on fabric by this colloidal sol by the mode of padding, in follow-up heating process, colloidal sol changes xerogel into and at the surface filming of fabric, and this film can firmly cover at web surface, to realize arranging the functional modification of fabric.
The preferred embodiment of the invention also has, and the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 3 hours with the temperature of 90 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 3 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 60%:40% proportioning and both obtains the wooden aqueous solution of scented tea.
The preferred technical scheme of the present invention also has, and first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, and microwave frequency is 130MHz, and microwave treatment time is 6min.
Embodiment 2
The present invention is a kind of manufacture method containing milk fibre wool spinning fabric, and described fabric comprises: specification is fineness 75
s, length is the non-shrinkable wool of 65mm; Specification is the milk fibre of 4dtexX65mm; The mass percent of non-shrinkable wool and milk fibre two components is 45%:55%; By non-shrinkable wool hair ball dyeing make coloured wool top, milk yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing milk fibre wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce milk fibre strip: by milk fibre dyeing yarn, obtain milk fibre vitta;
S3, rove spin: wool yarn and milk fibre vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 80 DEG C, 100 minutes time; The speed of a motor vehicle of described high speed doubling is 600 ms/min, and the double twisting speed of a motor vehicle is 6500 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and blended by milk fibre;
S6, first time dip fabric: the worsted fabric of wool fibre and blended by milk fibre two is soaked two and rolls in coloured Nano silica sol, and pressure is 0.5kg/cm
2, pick-up is 85%, preliminary drying under the temperature conditions of 90 DEG C, then under the temperature conditions of 180 DEG C, bake 5 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 2kg/cm
2, pick-up is 70%, preliminary drying under the temperature conditions of 70 DEG C, then under the temperature conditions of 130 DEG C, bake 2 minutes; Through washing, after naturally drying, obtain containing milk fibre wool spinning fabric.
The preferred embodiment of the invention is, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described milk fibre dyeing yarn adopts DISPERSE DYES.
The preferred embodiment of the invention also has, and the number of described worsted yarn is 100/2.
The preferred embodiment of the invention also has, and the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
The preferred embodiment of the invention also has, and described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 2:1, water: ethyl silicate 40 is 5:0.5, FeCl
36H2O: ethyl silicate 40 is 0.6:0.6, is prepared from.
Further preferred embodiment of the present invention also has, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, 60 DEG C are warming up to again after dropwising, stir 2.5 hours, namely obtain a kind of coloured Nano silica sol.
41.7gTEOS, 73.6gEtOH and appropriate HCl are joined in 500ml tri-mouthfuls of round-bottomed flasks successively, regulates pH to be 2 ~ 3.Stir under the rotating speed of 250 revs/min, mix the iron ion aqueous solution (5.42gFeCl36H2O+36.0gH2O) while stirring, and at 70 DEG C, continue stirring 2 hours.Namely transparent, coloured and uniform nanometer coloured silicasol system is obtained.Wool spinning fabric two leachings two in nanometer coloured silicasol are rolled, pressure 2kg/cm
2, pick-up 70%, then 60 DEG C of preliminary dryings in convection oven, bake 2 minutes after washings, naturally dry at 150 DEG C.
First there is poly-condensation and hydrolysis in ethyl silicate 40, generate sol particles in alcohol solvent; Mix iron ion, form the coloured Nano silica sol of tool.Be adsorbed onto fully on fabric by this colloidal sol by the mode of padding, in follow-up heating process, colloidal sol changes xerogel into and at the surface filming of fabric, and this film can firmly cover at web surface, to realize arranging the functional modification of fabric.
The preferred embodiment of the invention also has, and the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 3.5 hours with the temperature of 95 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 3 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 70%:30% proportioning and both obtains the wooden aqueous solution of scented tea.
The preferred technical scheme of the present invention also has, and first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, and microwave frequency is 200MHz, and microwave treatment time is 7min.
Embodiment 3
The present invention is a kind of manufacture method containing milk fibre wool spinning fabric, and described fabric comprises: specification is fineness 80
s, length is the non-shrinkable wool of 70mm; Specification is the milk fibre of 4dtexX70mm; The mass percent of non-shrinkable wool and milk fibre two components is 60%:40%; By non-shrinkable wool hair ball dyeing make coloured wool top, milk yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing milk fibre wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce milk fibre strip: by milk fibre dyeing yarn, obtain milk fibre vitta;
S3, rove spin: wool yarn and milk fibre vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 90 DEG C, 120 minutes time; The speed of a motor vehicle of described high speed doubling is 700 ms/min, and the double twisting speed of a motor vehicle is 8000 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and blended by milk fibre;
S6, first time dip fabric: the worsted fabric of wool fibre and blended by milk fibre two is soaked two and rolls in coloured Nano silica sol, and pressure is 2.5kg/cm
2, pick-up is 80%, preliminary drying under the temperature conditions of 80 DEG C, then under the temperature conditions of 150 DEG C, bake 4 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 3kg/cm
2, pick-up is 80%, preliminary drying under the temperature conditions of 80 DEG C, then under the temperature conditions of 160 DEG C, bake 3 minutes; Through washing, after naturally drying, obtain containing milk fibre wool spinning fabric.
The preferred embodiment of the invention is, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described milk fibre dyeing yarn adopts DISPERSE DYES.
The preferred embodiment of the invention also has, and the number of described worsted yarn is 120/2.
The preferred embodiment of the invention also has, and the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
The preferred embodiment of the invention also has, and described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 11:1, water: ethyl silicate 40 is 20:0.5, FeCl
36H2O: ethyl silicate 40 is 0.8:0.6, is prepared from.
Further preferred embodiment of the present invention also has, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, 70 DEG C are warming up to again after dropwising, stir 3 hours, namely obtain a kind of coloured Nano silica sol.
41.7gTEOS, 119.6gEtOH and appropriate HCl are joined in 500ml tri-mouthfuls of round-bottomed flasks successively, regulates pH to be 2 ~ 3.Stir under the rotating speed of 500 revs/min, mix the iron ion aqueous solution (5.42gFeCl36H2O+57.6gH2O) while stirring, and at 70 DEG C, continue stirring 2 hours.Namely transparent, coloured and uniform nanometer coloured silicasol system is obtained.Wool spinning fabric two leachings two in the nanometer coloured silicasol prepared are rolled, pressure 3kg/cm
2, pick-up 90%.Then 70 DEG C of preliminary dryings in convection oven, bake 2 minutes after washings, naturally dry at 150 DEG C.
First there is poly-condensation and hydrolysis in ethyl silicate 40, generate sol particles in alcohol solvent; Mix iron ion, form the coloured Nano silica sol of tool.Be adsorbed onto fully on fabric by this colloidal sol by the mode of padding, in follow-up heating process, colloidal sol changes xerogel into and at the surface filming of fabric, and this film can firmly cover at web surface, to realize arranging the functional modification of fabric.
The preferred embodiment of the invention also has, and the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 4 hours with the temperature of 100 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 4 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 80%:20% proportioning and both obtains the wooden aqueous solution of scented tea.
The preferred technical scheme of the present invention also has, and first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, and microwave frequency is 280MHz, and microwave treatment time is 8min.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (8)
1., containing a manufacture method for milk fibre wool spinning fabric, it is characterized in that, described fabric comprises: specification is fineness 70
s~ 80
s, length is the non-shrinkable wool of 60 ~ 70mm; Specification is the milk fibre of 4 ~ 5dtexX (65 ~ 70) mm; The mass percent of non-shrinkable wool and milk fibre two components is 30 ~ 60%:70 ~ 40%; By non-shrinkable wool hair ball dyeing make coloured wool top, milk yarn is dyeed, adopt strip mixing be spun into spun yarn, then through after spin to obtain spun yarn, manufacture containing milk fibre wool spinning fabric by manufacturing technique; The concrete steps of described manufacture method comprise:
S1, by non-shrinkable wool hair ball bar dye recombing: by pine group, dyeing, combing, obtain wool yarn;
S2, produce milk fibre strip: by milk fibre dyeing yarn, obtain milk fibre vitta;
S3, rove spin: wool yarn and milk fibre vitta adopt wool top to mix and be spun into rove;
S4, after spin: through rove, spun yarn, automatic winding, yarn steaming, high speed doubling, double twisting, obtain spun yarn; Described yarn steaming temperature is 75 ~ 90 DEG C, 80 ~ 120 minutes time; The speed of a motor vehicle of described high speed doubling is 500 ~ 700 ms/min, and the double twisting speed of a motor vehicle is 5000 ~ 8000 revs/min;
S5, by fabric manufacturing process and finishing technique, make the worsted fabric of wool fibre and blended by milk fibre;
S6, first time dip fabric: the worsted fabric of wool fibre and blended by milk fibre two is soaked two and rolls in coloured Nano silica sol, and pressure is 0.5 ~ 2.5kg/cm
2, pick-up is 75 ~ 85%, preliminary drying under the temperature conditions of 70 ~ 90 DEG C, then under the temperature conditions of 120 ~ 180 DEG C, bake 3 ~ 5 minutes;
S7, second time dip fabric: dip the fabric after oven dry by through first time, then put into the scented tea wood aqueous solution two and soak and two to roll, and pressure is 1 ~ 3kg/cm
2, pick-up is 60 ~ 80%, preliminary drying under the temperature conditions of 60 ~ 80 DEG C, then under the temperature conditions of 100 ~ 160 DEG C, bake 2 ~ 3 minutes; Through washing, after naturally drying, obtain containing milk fibre wool spinning fabric.
2. the manufacture method containing milk fibre wool spinning fabric as claimed in claim 1, is characterized in that, described in state the dyeing of non-shrinkable wool hair ball and adopt REACTIVE DYES, described milk fibre dyeing yarn adopts DISPERSE DYES.
3. the manufacture method containing milk fibre wool spinning fabric as claimed in claim 1, it is characterized in that, the number of described worsted yarn is 90 ~ 120/2.
4. the manufacture method containing milk fibre wool spinning fabric as claimed in claim 1, is characterized in that, the fabric construction of described fabric to adopt on plain weave, two once twill or cassimere twill.
5. the manufacture method containing milk fibre wool spinning fabric as claimed in claim 1, it is characterized in that, described coloured Nano silica sol is in molar ratio, ethanol: ethyl silicate 40 is 2 ~ 11:1, water: ethyl silicate 40 is 5 ~ 20:0.5, FeCl
36H2O: ethyl silicate 40 is 0.6 ~ 0.8:0.6, is prepared from.
6. the manufacture method containing milk fibre wool spinning fabric as claimed in claim 5, it is characterized in that, described coloured Nano silica sol adopts sol-gel process preparation, step comprises: by even to ethyl silicate 40, ethanol and mixed in hydrochloric acid, slowly drip the iron ion aqueous solution under agitation, be warming up to 50 ~ 70 DEG C again after dropwising, stir 2.5 ~ 3 hours, namely obtain a kind of coloured Nano silica sol.
7. the manufacture method containing milk fibre wool spinning fabric as claimed in claim 1, is characterized in that, the making of the described scented tea wood aqueous solution comprises:
The preparation of scented tea material water, producer in Tea Production process is savored tealeaves to select the tea rim charges such as rear remaining tea head, tea stalk, tea dust, Lao Ye and mix after preliminary cleaning, boil 3 ~ 4 hours with the temperature of 90 DEG C ~ 100 DEG C, then obtain scented tea material water by filtering, distilling;
The preparation of incense wood material water, by the incense wood material for preparing through preliminary cleaning, digesting apparatus boiling is put into after draining, first with 60 DEG C of temperature boilings 3 hours, be warming up to 120 DEG C and continue boiling about 3 ~ 4 hours, until wooden aromatic flavour and do not have the smell of burning, period repeatedly can stir the dissolving that short raw material promote incense wood material, is then filtered, distills and obtain incense wood material water;
Mixing, mixes scented tea material water and incense wood material water by weight 60% ~ 80%:40% ~ 20% proportioning and both obtains the wooden aqueous solution of scented tea.
8. the manufacture method containing milk fibre wool spinning fabric as claimed in claim 1, it is characterized in that, first time of described S6 step dips second time that fabric and S7 walk and dips in fabric process and need respectively to carry out microwave treatment, microwave frequency is 130MHz ~ 280MHz, and microwave treatment time is 6 ~ 8min.
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Application publication date: 20151223 |