CN105147532A - Amino acid facial cleanser and preparation method thereof - Google Patents
Amino acid facial cleanser and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the technical field of cosmetics and particularly relates to amino acid facial cleanser and a preparation method thereof. The amino acid facial cleanser comprises sodium lauroyl glutamate, sodium taurine laurate, sodium cocoyl glycinate, sorbitol, glycerin, sodium chloride, glycol distearate, cetearyl alcohol, sodium lactate, plant extracts, PEG(polyethylene glycol)-150 distearate, acrylate copolymers, EDTA (ethylene diamine tetraacetic acid) disodium, a preservative, essence and water. The amino acid facial cleanser is mild, skin-friendly, safe, non-irritating and capable of deeply cleaning skin, also can replenish water and whiten skin and can be used for a long time.
Description
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of amino acid cleansing breast and preparation method thereof.
Background technology
In the past, ultraviolet radiation is the largest source injuring our skin, and present environmental pollution is the second key factor of skin problem, and it can cause the drying of skin, stimulation, allergy, brings various skin situation.As 1. physical attack (dust, haze, sandstorm, PM2.5, radiation etc.): PM2.5 diameter is less than pore and enters skin, skin hydropenia, sensitivity, fat secretion are unbalance, aging, the problem that also can make blackhead, corse sweat pore.2. chemical attack (second hand smoking, vehicle exhaust, industrial pollution, waste gas etc.): except causing free radical increase, also can promote collagen disintegrate, reduce fine circulation, causes skin lax, dry, obscure.3. tired: skin resistance declines, and is the most easily subject to external invasion and attack, cause allergy, dimness, lax dry skin.4. pressure: dry lax, tarnishes, colour of skin wan shape, thus accelerates skin aging, hinders skin vigorous and graceful.Protection skin is very urgent, the skin nursing work that clean skin has become every day very important.
At present facial milk cleanser on the market mainly contains following several types: 1. soap base facial milk cleanser: dirt-removing power and degrease ability strong, but with after obviously can feel skin hydropenia and tight, easily damage skin; 2. surfactant facial milk cleanser: gentleer, do not stimulate, but still have tight and hydropenia phenomenon with rear, dirt-removing power is more weak, rinse have residual; 3. emulsibility facial milk cleanser: with after there is no the senses of discomfort such as tight, hydropenia, but dirt-removing power and degrease ability the poorest, cleaning capacity is the poorest; 4. amino acid cleansing breast: aminoacid itself is in faintly acid; just in time suit the Acidity of Aikalinity of skin, can not impact the acid-base value of skin, very little to the zest of skin; skin-friendly is also good especially; cleaning strength is moderate, uses rear noresidue, avoids the injury of residuals to skin natural containment; frothing capacity is fabulous; foam, as " cushion ", can form tension force between palm and skin, avoids friction injury skin.
Chinese patent application CN104337734A discloses a kind of reparation cleansing milk, and it comprises glycerol 5 ~ 10%, hydroxyethyl-cellulose 0.1 ~ 1%, sodium lauroyl glutamate 20 ~ 30%, sodium cocoyl glycinate 5 ~ 7%, Agrimonia eupatoria extract 0.1 ~ 1%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0.1 ~ 0.3%, antiseptic 0 ~ 0.3%, hyaluronate sodium 0.01 ~ 0.1%, essence 0 ~ 0.3%, hydroxylated lecithin 0.1 ~ 1%, avenabeta glucosan 0.1 ~ 1%, potassium hydroxide 0.1 ~ 1% and water.It contains potassium hydroxide, uses rear skin easily to produce tight sense and hydropenia phenomenon, unsuitable life-time service.
Chinese patent application CN104758223A discloses a kind of hydrolyzed silkworm silk facial milk cleanser, and it comprises myristic acid, glycerol, Sorbitol, stearic acid, Palmic acid, lauric acid, butanediol, amino acid surfactant, glycol distearate, potassium hydroxide, glyceryl monostearate, ceteareth-25, skin conditioning agent, hydrolyzed silkworm silk, polyquaternary ammonium salt conditioner, polyethylene glycols and water.The various complexity of this facial milk cleanser composition, composition is high, is also containing potassium hydroxide simultaneously, easily causes the tight hydropenia of skin, unsuitable life-time service.
In sum, be necessary to research and develop a kind of cleaning effect good, gentle non-stimulated, and cost is low, can life-time service amino acid cleansing breast.
Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of amino acid cleansing breast, its gentle pro-skin, safe and non-stimulating, deep layer cleaning skin, the whitening of moisturizing simultaneously, can life-time service.
The present invention is by following technical solution to realize above-mentioned purpose:
An amino acid cleansing breast, comprises the raw material of following weight percent meter: sodium lauroyl glutamate 20 ~ 30%, lauric acid sodium taurocholate 3 ~ 6%, sodium cocoyl glycinate 3 ~ 8%, Sorbitol 9 ~ 11%, glycerol 3 ~ 8%, sodium chloride 3 ~ 5%, glycol distearate 1 ~ 6%, cetearyl alcohol 1 ~ 4%, sodium lactate 4 ~ 8%, plant extract 0.4 ~ 4%, PEG-150 distearate 0.1 ~ 0.6%, acrylic acid esters co-polymer 0.2 ~ 0.6%, EDETATE SODIUM 0.05 ~ 0.15%, antiseptic 0.06 ~ 0.18%, essence 0.005 ~ 0.05% and water 20 ~ 40%.
As the preferred embodiment of the present invention, described amino acid cleansing breast is made up of the raw material of following weight percent meter: sodium lauroyl glutamate 25%, lauric acid sodium taurocholate 5%, sodium cocoyl glycinate 5%, Sorbitol 10%, glycerol 5%, sodium chloride 4%, glycol distearate 3%, cetearyl alcohol 2%, sodium lactate 5%, plant extract 2.5%, PEG-150 distearate 0.3%, acrylic acid esters co-polymer 0.5%, EDETATE SODIUM 0.1%, antiseptic 0.15%, essence 0.01% and water 32.44%.
Further, described plant extract by Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and Flos Spatholirionis longifolii form.
Further, described Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and the weight ratio of Flos Spatholirionis longifolii be (0.2 ~ 1): (0.2 ~ 1): (0.2 ~ 1): (0.2 ~ 1).
Further, described Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and the weight ratio of Flos Spatholirionis longifolii be 0.5:0.5:0.6:0.6.
Further, described antiseptic is made up of methyl hydroxybenzoate and Methylisothiazolinone, and the weight ratio of described methyl hydroxybenzoate and Methylisothiazolinone is 4:1.
Sodium lauroyl glutamate, lauric acid sodium taurocholate and sodium cocoyl glycinate three seed amino acid class surfactant are contained in amino acid cleansing Ruzhong of the present invention, three's character is gentle, soft to skin, do not cause allergy, also there is excellent wettability, foaming characteristic, water solublity, anti-water hardness tolerance and antibiotic property, its faintly acid same with skin makes skin feel comfortable, soft and moist simultaneously, the all low stimulation of what is more important three, low toxicity, have good biodegradability properties; And three works in coordination with, reach the effect of gentle non-stimulated, safe and effective cleaning skin.
Flos Rosae Rugosae extract of the present invention can effectively remove body ages cutin, cleans dirt and unnecessary sebum, keeps the cuticular water balance of skin, makes the bright and clean water profit of skin, and skin is releived soft and smooth, high resilience.Described leaf of Herb Gynostemmae Pentaphylli extract can improve the function of the aquaporin in Skin Cell, promotes to produce aquaporin, imports moisture to cell interior, brings skin water profit from cell interior.Described youth, algae was the active component extracted from the badderlocks Brown algae of French Brittany Asia, and it is rich in elastin laminin, can promote the quick new life of skin corium Collagen material, strengthened the elasticity of epidermis and degree of compacting.Described Flos Spatholirionis longifolii is from having the active component extracted the deep-sea plant coralline algae of " seabed Nidus collocaliae " good name, it has potent moisture pick-up properties, can hydrone in strong seizure skin surface air, and form water conservation thin film, reduce water loss, promote the hyaluronic synthesis of epidermis deep layer.
Described Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, youth algae and Flos Spatholirionis longifolii work in coordination with sodium lauroyl glutamate, lauric acid sodium taurocholate and sodium cocoyl glycinate, timely replenishing water and preserving moisture while clean skin, supply skin desired nutritional, the bright skin of whitening, skin is got well state, coordinate Sorbitol again, glycerol, sodium chloride, glycol distearate, cetearyl alcohol, sodium lactate, PEG-150 distearate, acrylic acid esters co-polymer, the basic materials such as EDETATE SODIUM obtain amino acid cleansing of the present invention breast, each component is worked in coordination with, make stable system safety, gentle non-stimulated, bubble abundant, easy flushing, noresidue, can life-time service.
Present invention also offers the preparation method of above-mentioned amino acid cleansing breast, specifically comprise the following steps:
S1. in water, add sodium chloride and EDETATE SODIUM, be stirred to and dissolve completely, then add glycerol, Sorbitol, be stirred to stock dispersion even;
S2. then add lauric acid sodium taurocholate, sodium lauroyl glutamate and sodium cocoyl glycinate, be stirred to stock dispersion even, then be placed in 90 ~ 96 DEG C of water-baths, start and be stirred to raw material and dissolve completely, control mixing speed is 100 ~ 120rpm;
S3. then add PEG-150 distearate, cetearyl alcohol and glycol distearate again, continue to be stirred to raw material and dissolve completely, after adding sodium lactate, stop heating;
S4. reduce mixing speed to 75 ~ 85rpm, treat that system temperature is down to 55 ~ 65 DEG C, add acrylic acid esters co-polymer;
S5. treat that system is cooled to 40 ~ 50 DEG C, add plant extract, antiseptic and essence, under 55 ~ 65rpm, be stirred to system retrogradation, get final product discharging, obtain amino acid cleansing breast.
Therefore, compared with prior art, advantage of the present invention is:
(1) amino acid cleansing of the present invention breast is containing lauric acid sodium taurocholate, sodium lauroyl glutamate and sodium cocoyl glycinate three seed amino acid class cleansing; the excess oil of the safe and effective clean skin surface of energy and pore depths and dust dirt; natural faintly acid is close with skin PH; skin-friendly is good; cause any burden and injury to tender skin; keep skin moisture, the sebum film that face skin is natural can not be destroyed.
(2) amino acid cleansing of the present invention breast adds Flos Spatholirionis longifolii, leaf of Herb Gynostemmae Pentaphylli extract, and instantaneous-locking also stores moisture, wakes cell of being sunk into sleep up, promotes skin microcirculation, supplies the nutrition needed for skin, makes skin reply being full of profit to have vigor; Add youth algae and Flos Rosae Rugosae extract, the tender jade-like stone of same seasonal skin water effectively removing body ages cutin be white, compact penetrating.
(3) the gentle pro-skin of amino acid cleansing of the present invention breast, easily rinse, heavy metal free, without foaming agent, without stearic acid etc., 100% employing aminoacid cleaning gene and plant extract, non-stimulated to skin; Can deep layer cleaning, replenishing water and preserving moisture, the bright skin of whitening, amino acid cleansing dairy milk starting material cost of the present invention is low simultaneously, and preparation method is simple, and process stabilizing, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, amino acid cleansing breast of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
The information such as the producer of the Ruzhong of amino acid cleansing described in embodiment of the present invention part material and article No. are as follows:
embodiment 1, amino acid cleansing of the present invention breast and preparation thereof
formula:be made up of the raw material of following weight percent meter: sodium lauroyl glutamate 25%, lauric acid sodium taurocholate 5%, sodium cocoyl glycinate 5%, Sorbitol 10%, glycerol 5%, sodium chloride 4%, glycol distearate 3%, cetearyl alcohol 2%, sodium lactate 5%, plant extract 2.5%, PEG-150 distearate 0.3%, acrylic acid esters co-polymer 0.5%, EDETATE SODIUM 0.1%, antiseptic 0.15%, essence 0.01% and water 32.44%.
Described plant extract by Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and Flos Spatholirionis longifolii form according to weight ratio 0.5:0.5:0.6:0.6.Described antiseptic is made up of according to weight ratio 4:1 methyl hydroxybenzoate and Methylisothiazolinone.
preparation method:s1. in water, add sodium chloride and EDETATE SODIUM, be stirred to and dissolve completely, then add glycerol, Sorbitol, be stirred to stock dispersion even;
S2. then add lauric acid sodium taurocholate, sodium lauroyl glutamate and sodium cocoyl glycinate, be stirred to stock dispersion even, then be placed in 95 DEG C of water-baths, start and be stirred to raw material and dissolve completely, control mixing speed is 120rpm;
S3. then add PEG-150 distearate, cetearyl alcohol and glycol distearate again, continue to be stirred to raw material and dissolve completely, after adding sodium lactate, stop heating;
S4. reduce mixing speed to 80rpm, treat that system temperature is down to 60 DEG C, add acrylic acid esters co-polymer;
S5. treat that system is cooled to 45 DEG C, add plant extract, antiseptic and essence, be stirred to system retrogradation at 60 rpm, get final product discharging, obtain amino acid cleansing breast.
embodiment 2, amino acid cleansing of the present invention breast and preparation thereof
formula:be made up of the raw material of following weight percent meter: sodium lauroyl glutamate 20%, lauric acid sodium taurocholate 6%, cocos nucifera oil acyl glycine 8%, Sorbitol 9%, glycerol 8%, sodium chloride 3%, glycol distearate 6%, cetearyl alcohol 1%, sodium lactate 4%, plant extract 1%, PEG-150 distearate 0.6%, acrylic acid esters co-polymer 0.2%, EDETATE SODIUM 0.05%, antiseptic 0.18%, essence 0.05% and water 32.92%.
Described plant extract by Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and Flos Spatholirionis longifolii form according to weight ratio 0.2:0.2:1:1.Described antiseptic is made up of according to weight ratio 4:1 methyl hydroxybenzoate and Methylisothiazolinone.
preparation method:s1. in water, add sodium chloride and EDETATE SODIUM, be stirred to and dissolve completely, then add glycerol, Sorbitol, be stirred to stock dispersion even;
S2. then add lauric acid sodium taurocholate, sodium lauroyl glutamate and sodium cocoyl glycinate, be stirred to stock dispersion even, then be placed in 90 DEG C of water-baths, start and be stirred to raw material and dissolve completely, control mixing speed is 120rpm;
S3. then add PEG-150 distearate, cetearyl alcohol and glycol distearate again, continue to be stirred to raw material and dissolve completely, after adding sodium lactate, stop heating;
S4. reduce mixing speed to 75rpm, treat that system temperature is down to 55 DEG C, add acrylic acid esters co-polymer;
S5. treat that system is cooled to 40 DEG C, add plant extract, antiseptic and essence, under 55rpm, be stirred to system retrogradation, get final product discharging, obtain amino acid cleansing breast.
embodiment 3, amino acid cleansing of the present invention breast and preparation thereof
formula:be made up of the raw material of following weight percent meter: sodium lauroyl glutamate 30%, lauric acid sodium taurocholate 3%, sodium cocoyl glycinate 3%, Sorbitol 11%, glycerol 3%, sodium chloride 5%, glycol distearate 1%, cetearyl alcohol 4%, sodium lactate 8%, plant extract 4%, PEG-150 distearate 0.1%, acrylic acid esters co-polymer 0.6%, EDETATE SODIUM 0.15%, antiseptic 0.06%, essence 0.01% and water 27.08%.
Described plant extract by Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and Flos Spatholirionis longifolii form according to weight ratio 1:1:0.2:0.2.Described antiseptic is made up of according to weight ratio 4:1 methyl hydroxybenzoate and Methylisothiazolinone.
preparation method:s1. in water, add sodium chloride and EDETATE SODIUM, be stirred to and dissolve completely, then add glycerol, Sorbitol, be stirred to stock dispersion even;
S2. then add lauric acid sodium taurocholate, sodium lauroyl glutamate and sodium cocoyl glycinate, be stirred to stock dispersion even, then be placed in 96 DEG C of water-baths, start and be stirred to raw material and dissolve completely, control mixing speed is 100rpm;
S3. then add PEG-150 distearate, cetearyl alcohol and glycol distearate again, continue to be stirred to raw material and dissolve completely, after adding sodium lactate, stop heating;
S4. reduce mixing speed to 85rpm, treat that system temperature is down to 65 DEG C, add acrylic acid esters co-polymer;
S5. treat that system is cooled to 50 DEG C, add plant extract, antiseptic and essence, under 65rpm, be stirred to system retrogradation, get final product discharging, obtain amino acid cleansing breast.
Do testing performance index to the amino acid cleansing breast of embodiment 1 ~ 3, its test result is as follows:
1, outward appearance: white mastic;
2, pH value: 5.5 ~ 7.0;
3, viscosity: 5 ~ 100,000;
4, heat-resistant stability investigates (45 DEG C × 24h): qualified;
5, cold-resistant study on the stability (-15 DEG C × 24h): qualified.
comparative example 1,
formula:be made up of the raw material of following weight percent meter: sodium lauroyl glutamate 25%, lauric acid sodium taurocholate 6%, sodium cocoyl glycinate 6.5%, Sorbitol 10%, glycerol 5%, sodium chloride 4%, glycol distearate 3%, cetearyl alcohol 2%, sodium lactate 5%, PEG-150 distearate 0.3%, acrylic acid esters co-polymer 0.5%, EDETATE SODIUM 0.1%, antiseptic 0.15%, essence 0.01% and water 32.44%.
Described antiseptic is made up of according to weight ratio 4:1 methyl hydroxybenzoate and Methylisothiazolinone.
Preparation method is with reference to embodiment 1.
comparative example 2,
formula:be made up of the raw material of following weight percent meter: sodium lauroyl glutamate 30%, Sorbitol 10%, glycerol 5%, sodium chloride 4%, glycol distearate 3%, cetearyl alcohol 2%, sodium lactate 5%, plant extract 2.5%, PEG-150 distearate 0.3%, acrylic acid esters co-polymer 0.5%, EDETATE SODIUM 0.1%, antiseptic 0.15%, essence 0.01% and water 32.44%.
Described plant extract by Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and Flos Spatholirionis longifolii form according to weight ratio 0.5:0.5:0.6:0.6.Described antiseptic is made up of according to weight ratio 4:1 methyl hydroxybenzoate and Methylisothiazolinone.
Preparation method is with reference to embodiment 1.
comparative example 3,
formula:be made up of the raw material of following weight percent meter: sodium lauroyl glutamate 25%, lauric acid sodium taurocholate 5%, sodium cocoyl glycinate 5%, Sorbitol 10%, glycerol 5%, sodium chloride 4%, glycol distearate 3%, cetearyl alcohol 2%, sodium lactate 5%, plant extract 2.5%, PEG-150 distearate 0.3%, acrylic acid esters co-polymer 0.5%, EDETATE SODIUM 0.1%, antiseptic 0.15%, essence 0.01% and water 32.44%.
Described plant extract is made up of according to weight ratio 1:1 Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract.Described antiseptic is made up of according to weight ratio 4:1 methyl hydroxybenzoate and Methylisothiazolinone.
Preparation method is with reference to embodiment 1.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: the amino acid cleansing breast that embodiment 1 ~ 3, comparative example 1 ~ 3 prepare
Tested crowd's number: 60 people, women
Age: between 20 ~ 50 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: 6 groups, often organize 10 people, 28 ± 2 years old mean age.
Two, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.020g ~ 0.025g drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Three, experimental result: human skin patch result shows: each group experimenter is by the patch test of the amino acid cleansing breast of embodiment 1 ~ 3, comparative example 1 ~ 3, dermoreaction is observed at 0.5,6,12,24,48 hour, wherein there is skin adverse reaction in 0 example, the amino acid cleansing breast use safety described in explanation.
test example two, product effect assessment
part I:
One, trial target: the amino acid cleansing breast that embodiment 1 ~ 3, comparative example 1 ~ 3 prepare
Two, tested crowd
Sex number: female, 60 people
Age: between 20 ~ 40 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 6 groups, often organize 10 people.
Three, method of testing: experimenter uses Fes Kai Er SK-III skin moisture detector to test the moisture of forehead, left face, right face and chin skin respectively after using clean water face, and get arithmetic mean of instantaneous value, experimenter re-uses the moistening face of warm water, then the clean face of above-mentioned amino acid cleansing milk surum is used, by clean water, again by the skin moisture content of skin moisture tester test forehead, left face, right face and the same position of chin, and get arithmetic mean of instantaneous value, re-use skin moisture tester after 24 hours and test one time.Often organize 10 experimenters and tested result is got arithmetic mean of instantaneous value, test result is as following table 1:
Table 1 skin moisture content table with test results
From upper table 1, after using clean of the embodiment of the present invention 1 ~ 3 amino acid cleansing breast, moisture of skin can not only be kept not run off, also can replenishing water and preserving moisture in time, skin beauty water is moistened, wherein with the moistening effect of embodiment 1 amino acid cleansing breast the best.Comparative example 1 is not containing plant extract, and it can keep moisture of skin not run off substantially; Comparative example 2 only contains a kind of amino acids cleansing of sodium lauroyl glutamate, its moisturizing poor effect; Comparative example 3 is only containing Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, and its moisturizing effect, not as good as embodiment 1 ~ 3, illustrates that plant extract of the present invention is worked in coordination with, and plays unexpected replenishing water and preserving moisture effect.
part II:
One, trial target: embodiment 1 ~ 3, prepared by comparative example 1 ~ 3 amino acid cleansing breast
Two, tested crowd
Sex number: female, 120 people
Age: between 20 ~ 50 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 6 groups, often organize 20 people.
Three, method of testing: use example 1 ~ 3, the clean face of amino acid cleansing milk surum prepared by comparative example 1 ~ 3 respectively, observe and experience result of use.Using method: experimenter directly uses tested products, every day is sooner or later each to be used once, face is drenched with clear water, extrude appropriate facial milk cleanser in the centre of the palm before using, and adds a small amount of clear water and has rubbed and enrich foam, rinse well in a moment at face message with clear water.Adhere to use one month, at least check weekly once to understand with or without whole body and local untoward reaction, and itemized record result.
Testing evaluation result is as follows:
(one month) on probation feedback conclusive table of table 2 embodiment 1 amino acid cleansing breast
(one month) on probation feedback conclusive table of table 3 embodiment 2 amino acid cleansing breast
(one month) on probation feedback conclusive table of table 4 embodiment 3 amino acid cleansing breast
(one month) on probation feedback conclusive table of table 5 comparative example 1 facial milk cleanser
(one month) on probation feedback conclusive table of table 6 comparative example 2 facial milk cleanser
(one month) on probation feedback conclusive table of table 7 comparative example 3 facial milk cleanser
(1) from upper table 2 ~ 4, the amino acid cleansing breast of embodiment 1 ~ 3 almost obtains the accreditation of all experimenters, illustrate that amino acid cleansing of the present invention breast gentleness does not stimulate, foaming is enriched, is easily rinsed, and the excess oil of effectively clean skin surface and pore depths and dust dirt, use the salubrious non-greasy of rear face, without tight sense, skin moisture can be kept, can not destroy the sebum film that face skin is natural, skin water is moistened smooth, flexible, moisturizing is lasting.In embodiment 1 ~ 3, the degree of recognition of embodiment 1 is the highest, and therefore embodiment 1 is most preferred embodiment.
(2) from upper table 5 ~ 7, the result of use of comparative example 1 ~ 3 facial milk cleanser is all not as embodiment 1 ~ 3, illustrate that amino acid cleansing of the present invention breast formula is not obtained by the simple combination of each component, then further illustrate between each component of formula of the present invention and there is synergism.
There is not people to occur allergic phenomena in whole experimenter simultaneously, all do not occur the situations such as skin pruritus, twinge, redness yet.Therefore, the gentle safety of amino acid cleansing breast of the present invention, can life-time service.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (7)
1. an amino acid cleansing breast; it is characterized in that, comprise the raw material of following weight percent meter: sodium lauroyl glutamate 20 ~ 30%, lauric acid sodium taurocholate 3 ~ 6%, sodium cocoyl glycinate 3 ~ 8%, Sorbitol 9 ~ 11%, glycerol 3 ~ 8%, sodium chloride 3 ~ 5%, glycol distearate 1 ~ 6%, cetearyl alcohol 1 ~ 4%, sodium lactate 4 ~ 8%, plant extract 0.4 ~ 4%, PEG-150 distearate 0.1 ~ 0.6%, acrylic acid esters co-polymer 0.2 ~ 0.6%, EDETATE SODIUM 0.05 ~ 0.15%, antiseptic 0.06 ~ 0.18%, essence 0.005 ~ 0.05% and water 20 ~ 40%.
2. amino acid cleansing breast as claimed in claim 1; it is characterized in that, be made up of the raw material of following weight percent meter: sodium lauroyl glutamate 25%, lauric acid sodium taurocholate 5%, sodium cocoyl glycinate 5%, Sorbitol 10%, glycerol 5%, sodium chloride 4%, glycol distearate 3%, cetearyl alcohol 2%, sodium lactate 5%, plant extract 2.5%, PEG-150 distearate 0.3%, acrylic acid esters co-polymer 0.5%, EDETATE SODIUM 0.1%, antiseptic 0.15%, essence 0.01% and water 32.44%.
3. amino acid cleansing breast as claimed in claim 1 or 2, is characterized in that, described plant extract by Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and Flos Spatholirionis longifolii form.
4. amino acid cleansing breast as claimed in claim 3, is characterized in that, described Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and the weight ratio of Flos Spatholirionis longifolii be (0.2 ~ 1): (0.2 ~ 1): (0.2 ~ 1): (0.2 ~ 1).
5. amino acid cleansing breast as claimed in claim 4, is characterized in that, described Flos Rosae Rugosae extract, leaf of Herb Gynostemmae Pentaphylli extract, the youth algae and the weight ratio of Flos Spatholirionis longifolii be 0.5:0.5:0.6:0.6.
6. amino acid cleansing breast as claimed in claim 1 or 2, it is characterized in that, described antiseptic is made up of methyl hydroxybenzoate and Methylisothiazolinone, and the weight ratio of described methyl hydroxybenzoate and Methylisothiazolinone is 4:1.
7. prepare as arbitrary in claim 1 ~ 6 as described in the method for amino acid cleansing breast, it is characterized in that, comprise the following steps:
S1. in water, add sodium chloride and EDETATE SODIUM, be stirred to and dissolve completely, then add glycerol, Sorbitol, be stirred to stock dispersion even;
S2. then add lauric acid sodium taurocholate, sodium lauroyl glutamate and sodium cocoyl glycinate, be stirred to stock dispersion even, then be placed in 90 ~ 96 DEG C of water-baths, start and be stirred to raw material and dissolve completely, control mixing speed is 100 ~ 120rpm;
S3. then add PEG-150 distearate, cetearyl alcohol and glycol distearate again, continue to be stirred to raw material and dissolve completely, after adding sodium lactate, stop heating;
S4. reduce mixing speed to 75 ~ 85rpm, treat that system temperature is down to 55 ~ 65 DEG C, add acrylic acid esters co-polymer;
S5. treat that system is cooled to 40 ~ 50 DEG C, add plant extract, antiseptic and essence, under 55 ~ 65rpm, be stirred to system retrogradation, get final product discharging, obtain amino acid cleansing breast.
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Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106236690A (en) * | 2016-08-31 | 2016-12-21 | 福建省梦娇兰日用化学品有限公司 | A kind of amino acid cleansing cream containing various plants composition |
| CN106701375A (en) * | 2016-12-28 | 2017-05-24 | 广东国方医药科技有限公司 | Amino acid facial soap containing Dendrobium officinale and preparation method thereof |
| CN106726873A (en) * | 2016-11-21 | 2017-05-31 | 西安博和医疗科技有限公司 | Amino acid clean water and preparation method thereof |
| CN107049859A (en) * | 2017-04-16 | 2017-08-18 | 广东科玮生物技术股份有限公司 | A kind of gently moist mildy wash and preparation method thereof |
| CN107349121A (en) * | 2017-07-19 | 2017-11-17 | 广州众乐生物科技有限公司 | A kind of amino acid mildy wash that sebum film ability is protected by Balancing and preparation method thereof |
| CN107582460A (en) * | 2017-10-13 | 2018-01-16 | 李丹丹 | A kind of amino acid cleansing breast and preparation method thereof |
| CN107693403A (en) * | 2017-11-02 | 2018-02-16 | 青海喜玛拉雅健康产业发展有限公司 | A kind of face cleaning emulsion and preparation method thereof |
| CN107714500A (en) * | 2017-11-30 | 2018-02-23 | 苏州龙腾万里化工科技有限公司 | Multiple-effect skin cleaning and nursing agent |
| CN108096048A (en) * | 2018-01-20 | 2018-06-01 | 广州康芙莱生物科技有限公司 | A kind of pure amino acid mildy wash with reproducibility and preparation method thereof and application method |
| CN108524389A (en) * | 2018-05-18 | 2018-09-14 | 广东盛美化妆品有限公司 | A kind of whitening cleansing milk of the root extract containing Aplotaxis auriculata and preparation method thereof |
| CN108938442A (en) * | 2018-08-09 | 2018-12-07 | 上海美兰化妆品有限公司 | Amino acid cleansing cream and preparation method |
| CN109833268A (en) * | 2017-11-27 | 2019-06-04 | 重庆戴贺李生物科技有限公司 | A kind of black fruit fructus lycii amino acid cleansing cream and preparation method thereof |
| CN110151578A (en) * | 2019-07-05 | 2019-08-23 | 广东天源生物科技有限公司 | A kind of clean face cream of amino acid skin-active and preparation method thereof of mild cleaning moisturizing |
| CN110339111A (en) * | 2019-07-19 | 2019-10-18 | 伊犁弥玥泉生物科技有限公司 | A kind of cleaning compositions of the hot spring containing mineral |
| CN110339150A (en) * | 2019-08-15 | 2019-10-18 | 广东芭薇生物科技股份有限公司 | A kind of amino acid cleansing cream and preparation method thereof |
| CN110638671A (en) * | 2019-08-30 | 2020-01-03 | 美肌化妆品有限公司 | Cubilose amino acid facial cleanser and preparation method thereof |
| CN110742819A (en) * | 2019-12-10 | 2020-02-04 | 广州瑞誉化工科技有限公司 | Amino acid facial cleansing honey |
| CN110812288A (en) * | 2018-08-10 | 2020-02-21 | 重庆戴贺李生物科技有限公司 | Soothing and moisturizing cosmetic composition and amino acid facial cleanser |
| CN111658578A (en) * | 2020-07-29 | 2020-09-15 | 雷菁 | Oil-control acne-removing facial cleanser and production method thereof |
| CN111671702A (en) * | 2020-06-22 | 2020-09-18 | 山东花物堂生物科技有限公司 | Cleaning amino acid cleaning product and preparation method thereof |
| CN111803407A (en) * | 2020-07-28 | 2020-10-23 | 广州葆妍生物科技有限公司 | Facial cleanser containing parasitic algae and plant amino acids |
| CN113786360A (en) * | 2021-09-23 | 2021-12-14 | 广州欧米亚生物科技有限公司 | Red mud amino acid facial cleanser and preparation method thereof |
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Cited By (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106236690A (en) * | 2016-08-31 | 2016-12-21 | 福建省梦娇兰日用化学品有限公司 | A kind of amino acid cleansing cream containing various plants composition |
| CN106726873A (en) * | 2016-11-21 | 2017-05-31 | 西安博和医疗科技有限公司 | Amino acid clean water and preparation method thereof |
| CN106701375A (en) * | 2016-12-28 | 2017-05-24 | 广东国方医药科技有限公司 | Amino acid facial soap containing Dendrobium officinale and preparation method thereof |
| CN107049859A (en) * | 2017-04-16 | 2017-08-18 | 广东科玮生物技术股份有限公司 | A kind of gently moist mildy wash and preparation method thereof |
| CN107349121A (en) * | 2017-07-19 | 2017-11-17 | 广州众乐生物科技有限公司 | A kind of amino acid mildy wash that sebum film ability is protected by Balancing and preparation method thereof |
| CN107582460A (en) * | 2017-10-13 | 2018-01-16 | 李丹丹 | A kind of amino acid cleansing breast and preparation method thereof |
| CN107693403A (en) * | 2017-11-02 | 2018-02-16 | 青海喜玛拉雅健康产业发展有限公司 | A kind of face cleaning emulsion and preparation method thereof |
| CN109833268A (en) * | 2017-11-27 | 2019-06-04 | 重庆戴贺李生物科技有限公司 | A kind of black fruit fructus lycii amino acid cleansing cream and preparation method thereof |
| CN107714500A (en) * | 2017-11-30 | 2018-02-23 | 苏州龙腾万里化工科技有限公司 | Multiple-effect skin cleaning and nursing agent |
| CN108096048A (en) * | 2018-01-20 | 2018-06-01 | 广州康芙莱生物科技有限公司 | A kind of pure amino acid mildy wash with reproducibility and preparation method thereof and application method |
| CN108524389A (en) * | 2018-05-18 | 2018-09-14 | 广东盛美化妆品有限公司 | A kind of whitening cleansing milk of the root extract containing Aplotaxis auriculata and preparation method thereof |
| CN108938442A (en) * | 2018-08-09 | 2018-12-07 | 上海美兰化妆品有限公司 | Amino acid cleansing cream and preparation method |
| CN110812288A (en) * | 2018-08-10 | 2020-02-21 | 重庆戴贺李生物科技有限公司 | Soothing and moisturizing cosmetic composition and amino acid facial cleanser |
| CN110151578A (en) * | 2019-07-05 | 2019-08-23 | 广东天源生物科技有限公司 | A kind of clean face cream of amino acid skin-active and preparation method thereof of mild cleaning moisturizing |
| CN110339111A (en) * | 2019-07-19 | 2019-10-18 | 伊犁弥玥泉生物科技有限公司 | A kind of cleaning compositions of the hot spring containing mineral |
| CN110339150A (en) * | 2019-08-15 | 2019-10-18 | 广东芭薇生物科技股份有限公司 | A kind of amino acid cleansing cream and preparation method thereof |
| CN110339150B (en) * | 2019-08-15 | 2021-11-02 | 广东芭薇生物科技股份有限公司 | Amino acid facial cleanser and preparation method thereof |
| CN110638671A (en) * | 2019-08-30 | 2020-01-03 | 美肌化妆品有限公司 | Cubilose amino acid facial cleanser and preparation method thereof |
| CN110742819A (en) * | 2019-12-10 | 2020-02-04 | 广州瑞誉化工科技有限公司 | Amino acid facial cleansing honey |
| CN111671702A (en) * | 2020-06-22 | 2020-09-18 | 山东花物堂生物科技有限公司 | Cleaning amino acid cleaning product and preparation method thereof |
| CN111803407A (en) * | 2020-07-28 | 2020-10-23 | 广州葆妍生物科技有限公司 | Facial cleanser containing parasitic algae and plant amino acids |
| CN111658578A (en) * | 2020-07-29 | 2020-09-15 | 雷菁 | Oil-control acne-removing facial cleanser and production method thereof |
| CN113786360A (en) * | 2021-09-23 | 2021-12-14 | 广州欧米亚生物科技有限公司 | Red mud amino acid facial cleanser and preparation method thereof |
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