CN105088401A - Chinese herbal medicine anti-bacterial health care composite down fiber textile material - Google Patents
Chinese herbal medicine anti-bacterial health care composite down fiber textile material Download PDFInfo
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- CN105088401A CN105088401A CN201510461942.4A CN201510461942A CN105088401A CN 105088401 A CN105088401 A CN 105088401A CN 201510461942 A CN201510461942 A CN 201510461942A CN 105088401 A CN105088401 A CN 105088401A
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- 239000000835 fiber Substances 0.000 title claims abstract description 30
- 239000002131 composite material Substances 0.000 title claims abstract description 28
- 239000000463 material Substances 0.000 title claims abstract description 27
- 239000004753 textile Substances 0.000 title claims abstract description 20
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 17
- 230000036541 health Effects 0.000 title claims abstract description 14
- 241000411851 herbal medicine Species 0.000 title abstract 4
- 210000003746 feather Anatomy 0.000 claims abstract description 37
- -1 polypropylene Polymers 0.000 claims abstract description 17
- 239000004743 Polypropylene Substances 0.000 claims abstract description 13
- 229920001155 polypropylene Polymers 0.000 claims abstract description 13
- 238000009987 spinning Methods 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 230000001954 sterilising effect Effects 0.000 claims abstract description 9
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000006087 Silane Coupling Agent Substances 0.000 claims abstract description 7
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims abstract description 7
- 239000004810 polytetrafluoroethylene Substances 0.000 claims abstract description 7
- 244000144977 poultry Species 0.000 claims abstract description 7
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 4
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 4
- 241001330002 Bambuseae Species 0.000 claims abstract description 4
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 4
- 239000011425 bamboo Substances 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 9
- 238000001035 drying Methods 0.000 claims description 9
- 239000005543 nano-size silicon particle Substances 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 7
- 102000011782 Keratins Human genes 0.000 claims description 6
- 108010076876 Keratins Proteins 0.000 claims description 6
- 239000004594 Masterbatch (MB) Substances 0.000 claims description 6
- 229960000583 acetic acid Drugs 0.000 claims description 6
- 238000004090 dissolution Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 241000594394 Hedyotis Species 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 238000002485 combustion reaction Methods 0.000 claims description 3
- 238000005520 cutting process Methods 0.000 claims description 3
- 238000004332 deodorization Methods 0.000 claims description 3
- 238000001125 extrusion Methods 0.000 claims description 3
- 239000012362 glacial acetic acid Substances 0.000 claims description 3
- 230000007935 neutral effect Effects 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- 230000002269 spontaneous effect Effects 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000000967 suction filtration Methods 0.000 claims description 3
- 239000004744 fabric Substances 0.000 abstract description 5
- 229920001661 Chitosan Polymers 0.000 abstract description 4
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 3
- 241000732800 Cymbidium Species 0.000 abstract 1
- 241000305491 Gastrodia elata Species 0.000 abstract 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- 230000003115 biocidal effect Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000003519 biomedical and dental material Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000012779 reinforcing material Substances 0.000 description 1
- 238000009958 sewing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
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Abstract
The invention discloses a Chinese herbal medicine anti-bacterial health care composite down fiber textile material. The Chinese herbal medicine anti-bacterial health care composite down fiber textile material is characterized by being prepared from, by weight, 40-60 parts of poultry feathers, 14-17 parts of down feathers, 1-3 parts of silane coupling agents KH550, 1-2 parts of nano-silica, 1-2 parts of nano-silver, 14-20 parts of chitosan, 30-50 parts of polypropylene, 2-3 parts of bamboo fiber, 1-2 parts of polytetrafluoroethylene, 4-5 parts of gastrodia elata, 3-4 parts of cymbidium candidum and an appropriate amount of water. Due to the added Chinese herbal medicines, the sterilization and health care functions of composite down fibers are greatly enhanced, the anti-bacterial effect is obvious, the duration time is long, and the anti-bacterial property cannot be lowered after the composite down fibers are washed with water; the prepared composite down fiber textile material has the better spinning property, can be separately spun or spun by cooperating with other fabrics and is high in practicability and worthy of popularization.
Description
Technical field
The present invention relates to textile material technical field, be specifically related to a kind of Chinese herbal antibacterial health care composite eiderdown fiber textile material and preparation method thereof.
Background technology
In textile industry, only have Isotactic polypropylene can be used to produce textile fabric, this is because Isotactic polypropylene fiber has higher degree of crystallinity and the degree of orientation, regularity is better.Therefore Isotactic polypropylene fiber is widely used as sewing thread, bandage, textile bags and bio-medical material.But because Isotactic polypropylene fiber lacks dyeability, limit its application in textile garment field.Eider down is a kind of natural protein fibre material, except a small amount of for making warming packing material in clothes and bedding and in the composite as except reinforcing material, major part just simple processing process is used as feed or adopts the methods such as fermentation to degrade, and causes a large amount of wastes.When fiber made separately by eider down, fragility is large, tensile strength is low, is not suitable for making coat, is only suitable for being filled in inside clothes obtaining very strong warmth retention property, because eider down content in feather is very few, usually only account for 20 ~ 25%, use cost is too high, feather fiber is not utilized very well, very unfortunately.The present invention utilizes discarded feather to be degraded into keratin solution, then with the chitosan solution blend spinning of modification, compatibility is good, recycling Isotactic polypropylene fills feather fiber, reduce the consumption of feather, gain in weight, and improve the performance of the aspects such as the intensity of fiber, modulus, heat resistance, chemical resistance and anti-corrosive properties, develop novel weaving face fabric, facilitate society and expanding economy.
Summary of the invention
The object of this invention is to provide a kind of Chinese herbal antibacterial health care composite eiderdown fiber textile material and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the invention is to be realized by following technological means:
A kind of Chinese herbal antibacterial health care composite eiderdown fiber textile material, it is characterized in that, be made up of the raw material of following weight portion: poultry feather 40-60, eider down 14-17, Silane coupling agent KH550 1-3, nano silicon 1-2, Nano Silver 1-2, shitosan 14-20, polypropylene 30-50, bamboo fibre 2-3, polytetrafluoroethylene (PTFE) 1-2, rhizoma Gastrodiae 4-5, ribbed hedyotis herb 3-4, water are appropriate;
A kind of Chinese herbal antibacterial health care composite eiderdown fiber textile material of the present invention, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization under 100-200 ° of C in high-pressure sterilizing pot is added to eider down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol and soaks 4-6 hour, then be neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) Silane coupling agent KH550 appropriate isopropyl alcohol dissolving is placed in reaction vessel, add nano silicon, Nano Silver again, stirring and refluxing 1-3h under 70-90 ° of C, cooling, for subsequent use after suction filtration, washing, drying, again shitosan glacial acetic acid solution is dissolved and make the chitosan-acetic acid solution that content is 3%, then with after NaOH alkalization 2-3h, add above-mentioned mixture for subsequent use, 2-3h is reacted under 40-60 ° of C, cooling, filters, washs, for subsequent use after drying;
(3) material prepared by step (1) and step (2) is used equivalent dissolution with solvents respectively, makes keratin content in feather within the scope of 8-13%, then be mixed and made into composite spinning stoste, carry out after spinning short cut for subsequent use;
(4) polypropylene and all the other remaining material mixing are added to main feeding trough in double screw extruder, the short collodion silk of cutting step (3) obtained again adds at natural exhaust outlet, blending extrusion temperature section is 195 ° of C, 190 ° of C, 190 ° of C, 185 ° of C, 180 ° of C, 165 ° of C, 110 ° of C, obtain composite master batch, composite master batch is carried out spinning.
Advantage of the present invention is: the present invention utilizes discarded feather to carry out dehydration taste removal deodorizing degreasing, the keratin solution of suitable solubility is made by dissolution with solvents, and utilize nano silicon and Nano Silver modification of chitosan, shitosan is had excellent antibacterial, sterilization, the performance that antibacterial and uvioresistant etc. are excellent, the fabric that the present invention utilizes chitosan solution and keratin solution co-blended spinning to obtain has good hygroscopicity, antibiotic property, the features such as biodegradability, and the ABRASION RESISTANCE of material is enhanced again by adding polypropylene, tensile strength, the characteristic of the aspects such as weight, decrease the consumption of feather fiber, add the novelty teabag of feather, the Chinese medicine added enhances the sterilization of composite eiderdown fiber and the function of health care greatly, and antibacterial effect is obvious, duration is long, washing can not reduce antibiotic property, composite eiderdown textile material prepared by the present invention has preferably can textile, other fabrics can separately or be coordinated to weave together, practicality is high, be worthy to be popularized.
Detailed description of the invention
A kind of Chinese herbal antibacterial health care composite eiderdown fiber textile material, it is characterized in that, be made up of the raw material of following weight portion (kilogram): poultry feather 60, eider down 16, Silane coupling agent KH550 3, nano silicon 1 Nano Silver 1, shitosan 18, polypropylene 43, bamboo fibre 3, polytetrafluoroethylene (PTFE) 2, rhizoma Gastrodiae 4, ribbed hedyotis herb 3, water are appropriate;
A kind of Chinese herbal antibacterial health care composite eiderdown fiber textile material of the present invention, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization under 150 ° of C in high-pressure sterilizing pot is added to eider down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol to soak 6 hours, then is neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) Silane coupling agent KH550 appropriate isopropyl alcohol dissolving is placed in reaction vessel, add nano silicon, Nano Silver again, stirring and refluxing 3h under 80 ° of C, cooling, for subsequent use after suction filtration, washing, drying, again shitosan glacial acetic acid solution is dissolved and make the chitosan-acetic acid solution that content is 3%, then with after NaOH alkalization 3h, add above-mentioned mixture for subsequent use, 2h is reacted under 50 ° of C, cooling, filters, washs, for subsequent use after drying;
(3) material prepared by step (1) and step (2) is used equivalent dissolution with solvents respectively, makes keratin content in feather in 11% scope, then be mixed and made into composite spinning stoste, carry out after spinning short cut for subsequent use;
(4) polypropylene and all the other remaining material mixing are added to main feeding trough in double screw extruder, the short collodion silk of cutting step (3) obtained again adds at natural exhaust outlet, blending extrusion temperature section is 195 ° of C, 190 ° of C, 190 ° of C, 185 ° of C, 180 ° of C, 165 ° of C, 110 ° of C, obtain composite master batch, composite master batch is carried out spinning.
The eider down composite fibre performance indications parameter using the present invention to prepare is as follows:
Hydroscopicity (%): 13.2;
Regain (%): 5.7;
Extensibility (%): 30.6;
Tensile break strength (N): 6.7.
Claims (2)
1. a Chinese herbal antibacterial health care composite eiderdown fiber textile material, it is characterized in that, be made up of the raw material of following weight portion: poultry feather 40-60, eider down 14-17, Silane coupling agent KH550 1-3, nano silicon 1-2, Nano Silver 1-2, shitosan 14-20, polypropylene 30-50, bamboo fibre 2-3, polytetrafluoroethylene (PTFE) 1-2, rhizoma Gastrodiae 4-5, ribbed hedyotis herb 3-4, water are appropriate.
2. a kind of Chinese herbal antibacterial health care composite eiderdown fiber textile material according to claim 1, is characterized in that, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization under 100-200 ° of C in high-pressure sterilizing pot is added to eider down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol and soaks 4-6 hour, then be neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) Silane coupling agent KH550 appropriate isopropyl alcohol dissolving is placed in reaction vessel, add nano silicon, Nano Silver again, stirring and refluxing 1-3h under 70-90 ° of C, cooling, for subsequent use after suction filtration, washing, drying, again shitosan glacial acetic acid solution is dissolved and make the chitosan-acetic acid solution that content is 3%, then with after NaOH alkalization 2-3h, add above-mentioned mixture for subsequent use, 2-3h is reacted under 40-60 ° of C, cooling, filters, washs, for subsequent use after drying;
(3) material prepared by step (1) and step (2) is used equivalent dissolution with solvents respectively, makes keratin content in feather within the scope of 8-13%, then be mixed and made into composite spinning stoste, carry out after spinning short cut for subsequent use;
(4) polypropylene and all the other remaining material mixing are added to main feeding trough in double screw extruder, the short collodion silk of cutting step (3) obtained again adds at natural exhaust outlet, blending extrusion temperature section is 195 ° of C, 190 ° of C, 190 ° of C, 185 ° of C, 180 ° of C, 165 ° of C, 110 ° of C, obtain composite master batch, composite master batch is carried out spinning.
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CN201510461942.4A CN105088401A (en) | 2015-07-31 | 2015-07-31 | Chinese herbal medicine anti-bacterial health care composite down fiber textile material |
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CN201510461942.4A CN105088401A (en) | 2015-07-31 | 2015-07-31 | Chinese herbal medicine anti-bacterial health care composite down fiber textile material |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105951211A (en) * | 2016-05-23 | 2016-09-21 | 安徽孔雀公主工艺品有限公司 | Antibacterial self-cleaned artificial wig fiber containing peacock feather |
CN106637591A (en) * | 2016-08-31 | 2017-05-10 | 浙江兆新织造有限公司 | Antibacterial skin-smoothing lining with natural faint scent |
CN113789589A (en) * | 2021-10-08 | 2021-12-14 | 晋江市滨浪制衣织造有限公司 | Antibacterial protective knitted fabric and preparation process thereof |
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Publication number | Priority date | Publication date | Assignee | Title |
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JPH02277886A (en) * | 1989-04-17 | 1990-11-14 | Shigesaburo Mizushima | Method for processing synthetic fiber and vegetable fiber with fibroin protein |
CN1435516A (en) * | 2002-12-12 | 2003-08-13 | 内蒙古鄂尔多斯羊绒集团有限责任公司 | Technique for processing regenerated keratin functional fibre |
CN102085023A (en) * | 2010-06-02 | 2011-06-08 | 成钢 | Nanometer Chinese medicine element anion far infrared electromagnetic wave pollution preventing and blood pressure reducing health care coat |
CN103572403A (en) * | 2012-08-07 | 2014-02-12 | 香港理工大学 | Polypeptide and chemical fiber composite fiber and preparation method thereof |
CN104195664A (en) * | 2014-08-30 | 2014-12-10 | 安徽一隆羽绒有限公司 | Down feather composite fiber modified by polypropylene fiber and preparation method of down feather composite fiber |
CN104195665A (en) * | 2014-08-30 | 2014-12-10 | 安徽一隆羽绒有限公司 | Down feather composite fiber compounded by waste down feather fiber and acrylic staple fiber and preparation method of down feather composite fiber |
-
2015
- 2015-07-31 CN CN201510461942.4A patent/CN105088401A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH02277886A (en) * | 1989-04-17 | 1990-11-14 | Shigesaburo Mizushima | Method for processing synthetic fiber and vegetable fiber with fibroin protein |
CN1435516A (en) * | 2002-12-12 | 2003-08-13 | 内蒙古鄂尔多斯羊绒集团有限责任公司 | Technique for processing regenerated keratin functional fibre |
CN102085023A (en) * | 2010-06-02 | 2011-06-08 | 成钢 | Nanometer Chinese medicine element anion far infrared electromagnetic wave pollution preventing and blood pressure reducing health care coat |
CN103572403A (en) * | 2012-08-07 | 2014-02-12 | 香港理工大学 | Polypeptide and chemical fiber composite fiber and preparation method thereof |
CN104195664A (en) * | 2014-08-30 | 2014-12-10 | 安徽一隆羽绒有限公司 | Down feather composite fiber modified by polypropylene fiber and preparation method of down feather composite fiber |
CN104195665A (en) * | 2014-08-30 | 2014-12-10 | 安徽一隆羽绒有限公司 | Down feather composite fiber compounded by waste down feather fiber and acrylic staple fiber and preparation method of down feather composite fiber |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105951211A (en) * | 2016-05-23 | 2016-09-21 | 安徽孔雀公主工艺品有限公司 | Antibacterial self-cleaned artificial wig fiber containing peacock feather |
CN106637591A (en) * | 2016-08-31 | 2017-05-10 | 浙江兆新织造有限公司 | Antibacterial skin-smoothing lining with natural faint scent |
CN113789589A (en) * | 2021-10-08 | 2021-12-14 | 晋江市滨浪制衣织造有限公司 | Antibacterial protective knitted fabric and preparation process thereof |
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Application publication date: 20151125 |