CN104860748A - Agent for controlling oil-use peony pests and diseases, and preparation method thereof - Google Patents
Agent for controlling oil-use peony pests and diseases, and preparation method thereof Download PDFInfo
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- CN104860748A CN104860748A CN201510178344.6A CN201510178344A CN104860748A CN 104860748 A CN104860748 A CN 104860748A CN 201510178344 A CN201510178344 A CN 201510178344A CN 104860748 A CN104860748 A CN 104860748A
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- Prior art keywords
- agent
- oil
- sodium
- pest
- medicament
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- 241000607479 Yersinia pestis Species 0.000 title claims abstract description 25
- 201000010099 disease Diseases 0.000 title claims abstract description 24
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 241000736199 Paeonia Species 0.000 title abstract 6
- 235000006484 Paeonia officinalis Nutrition 0.000 title abstract 6
- 239000003814 drug Substances 0.000 claims abstract description 23
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 14
- 239000006185 dispersion Substances 0.000 claims abstract description 3
- 239000000080 wetting agent Substances 0.000 claims abstract description 3
- 235000003889 Paeonia suffruticosa Nutrition 0.000 claims description 30
- 240000005001 Paeonia suffruticosa Species 0.000 claims description 23
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- -1 polyoxyethylene groups Polymers 0.000 claims description 12
- 244000147058 Derris elliptica Species 0.000 claims description 8
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 125000000217 alkyl group Chemical group 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 238000005469 granulation Methods 0.000 claims description 5
- 230000003179 granulation Effects 0.000 claims description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 239000003002 pH adjusting agent Substances 0.000 claims description 3
- 239000004151 Calcium iodate Substances 0.000 claims description 2
- RZXLPPRPEOUENN-UHFFFAOYSA-N Chlorfenson Chemical compound C1=CC(Cl)=CC=C1OS(=O)(=O)C1=CC=C(Cl)C=C1 RZXLPPRPEOUENN-UHFFFAOYSA-N 0.000 claims description 2
- 108010010803 Gelatin Proteins 0.000 claims description 2
- FQYUMYWMJTYZTK-UHFFFAOYSA-N Phenyl glycidyl ether Chemical compound C1OC1COC1=CC=CC=C1 FQYUMYWMJTYZTK-UHFFFAOYSA-N 0.000 claims description 2
- 239000004698 Polyethylene Substances 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 2
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 2
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 125000005233 alkylalcohol group Chemical group 0.000 claims description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
- 150000001408 amides Chemical class 0.000 claims description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 2
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 2
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 2
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 2
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 claims description 2
- 150000004056 anthraquinones Chemical class 0.000 claims description 2
- 229960000892 attapulgite Drugs 0.000 claims description 2
- 229920001400 block copolymer Polymers 0.000 claims description 2
- 229910021538 borax Inorganic materials 0.000 claims description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- UHWJJLGTKIWIJO-UHFFFAOYSA-L calcium iodate Chemical compound [Ca+2].[O-]I(=O)=O.[O-]I(=O)=O UHWJJLGTKIWIJO-UHFFFAOYSA-L 0.000 claims description 2
- 235000019390 calcium iodate Nutrition 0.000 claims description 2
- 239000007859 condensation product Substances 0.000 claims description 2
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims description 2
- 229910000397 disodium phosphate Inorganic materials 0.000 claims description 2
- 235000019800 disodium phosphate Nutrition 0.000 claims description 2
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 2
- 239000000945 filler Substances 0.000 claims description 2
- 229920000159 gelatin Polymers 0.000 claims description 2
- 239000008273 gelatin Substances 0.000 claims description 2
- 235000019322 gelatine Nutrition 0.000 claims description 2
- 235000011852 gelatine desserts Nutrition 0.000 claims description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 2
- 125000006353 oxyethylene group Chemical group 0.000 claims description 2
- 229910052625 palygorskite Inorganic materials 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 2
- 229920002503 polyoxyethylene-polyoxypropylene Polymers 0.000 claims description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 2
- 229940096992 potassium oleate Drugs 0.000 claims description 2
- MLICVSDCCDDWMD-KVVVOXFISA-M potassium;(z)-octadec-9-enoate Chemical compound [K+].CCCCCCCC\C=C/CCCCCCCC([O-])=O MLICVSDCCDDWMD-KVVVOXFISA-M 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000004405 propyl p-hydroxybenzoate Substances 0.000 claims description 2
- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 claims description 2
- 229960003415 propylparaben Drugs 0.000 claims description 2
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 2
- 239000004299 sodium benzoate Substances 0.000 claims description 2
- 235000010234 sodium benzoate Nutrition 0.000 claims description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
- 235000017550 sodium carbonate Nutrition 0.000 claims description 2
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 2
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 2
- 239000008109 sodium starch glycolate Substances 0.000 claims description 2
- 229940079832 sodium starch glycolate Drugs 0.000 claims description 2
- 229920003109 sodium starch glycolate Polymers 0.000 claims description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 2
- 235000011152 sodium sulphate Nutrition 0.000 claims description 2
- 239000004328 sodium tetraborate Substances 0.000 claims description 2
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 2
- 229940032147 starch Drugs 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- 150000003871 sulfonates Chemical class 0.000 claims description 2
- 229940104261 taurate Drugs 0.000 claims description 2
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 claims description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 abstract description 4
- 239000004202 carbamide Substances 0.000 abstract description 4
- 235000015097 nutrients Nutrition 0.000 abstract description 3
- 238000004806 packaging method and process Methods 0.000 abstract description 3
- 239000005925 Pymetrozine Substances 0.000 abstract description 2
- 239000012752 auxiliary agent Substances 0.000 abstract description 2
- 239000000428 dust Substances 0.000 abstract description 2
- QHMTXANCGGJZRX-WUXMJOGZSA-N pymetrozine Chemical compound C1C(C)=NNC(=O)N1\N=C\C1=CC=CN=C1 QHMTXANCGGJZRX-WUXMJOGZSA-N 0.000 abstract description 2
- 230000001276 controlling effect Effects 0.000 abstract 2
- 229940079593 drug Drugs 0.000 abstract 2
- 230000001105 regulatory effect Effects 0.000 abstract 2
- 239000000725 suspension Substances 0.000 abstract 2
- 231100000674 Phytotoxicity Toxicity 0.000 abstract 1
- 239000011230 binding agent Substances 0.000 abstract 1
- 239000002270 dispersing agent Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000003381 stabilizer Substances 0.000 abstract 1
- 241000531392 Helicobasidium mompa Species 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 2
- 230000000857 drug effect Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 241000130993 Scarabaeus <genus> Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 238000005338 heat storage Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 231100000820 toxicity test Toxicity 0.000 description 1
- 239000004563 wettable powder Substances 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses an agent used for controlling oil-use peony pests and diseases, and a preparation method thereof. The agent is composed of the components of, by weight, 20-70% of pymetrozine, 5-20% of urea, 1-10% of a wetting agent, 5-30% of a dispersing agent, 2-15% of a disintegrating agent, 0.5-10% of a binding agent, 0.1-8% of a stabilizing agent, and balance of a filling material. The pH value of the agent is regulated to 5-7 with a pH regulating agent. The agent provided by the invention has a good controlling effect against oil-use peony common pests and diseases, and has no phytotoxicity to oil-use peony. With the added urea, drug effective component utilization rate and drug efficiency are improved, and nutrient elements are provided for oil-use peony during application, such that oil-use peony growth is promoted. Auxiliary agents with different components are added, such that the agent has the advantages of good dispersion, high suspension rate, effective component indefinite suspension, good fluidity, and high disintegration speed. Therefore, the utilization rate of effective components is improved, and dose is reduced. The agent has the advantages of good thermal storage stability, easy packaging, convenient storage and transportation, convenient application, low dust, and low environment pollution.
Description
Technical field
The present invention relates to oil tree peony techniques of pest control field, particularly relating to a kind of medicament for preventing and treating oil tree peony disease and pest and preparation method thereof.
Background technology
Oil is the one of national flower tree peony with tree peony, it is the plant that traditional oil tree has again pharmaceutical use, also be the high green tree species of ornamental value, strong adaptability, drought-resistant barren, not only be adapted at hilly country but also be adapted at the growth of plains region, the north of the Changjiang River, Anhui, be implement soil synergy, afforest rural area, improve the fine tree species of ecological condition.Oil when planting with tree peony, needs to carry out wholely, applies fertilizer, PCO.Oil has leaf spot, purple root rot (Helicobasidium mompa) and stem rot by the disease that tree peony is common, and common insect pest has subterranean pest-insect, scarabs etc.Also be not specifically designed to the medicament of control oil tree peony disease and pest at present.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, there is provided low, the easy packaging of a kind of use cost, storing conveniently, to medicament for preventing and treating oil tree peony disease and pest of the healthy fanout free region of people and environmentally safe and preparation method thereof, a kind of environment-friendly highly efficient, broad spectrum pesticide, add urea, not only improve utilization ratio and the drug effect rate of effective ingredient, and for oil to have additional nutrients element with tree peony when using, promote the oil growth of tree peony.
The present invention adopts following technical scheme to achieve these goals:
For preventing and treating the medicament of oil with tree peony disease and pest, be made up of the component of following weight content:
Described wetting agent is selected from one or more in alkyl alcohol polyoxyethylene groups ether sodium sulfate, alkylphenol-polyethenoxy base ether formaldehyde condensation products vitriol, alkyl sodium sulfonate, dialkyl succinylsuccinate sulfonate, fatty alcohol ethylene oxide adduct sulfonate, alkyl amide taurate, Sodium dodecylbenzene sulfonate, octylphenol polyethylene oxyethylene group ether sulfate.
Described dispersion agent is selected from xylogen calcium iodate, alkyl naphthalene formaldehyde condensate sulfonates, sodium lauryl sulphate, potassium oleate, alkyl polyoxyethylene ether sulfonate, cocoyl sodium sulfonate, polyoxyethylene polyoxypropylene base ether block copolymers, pull open in powder, poly-second carboxylic esters sodium salt one or more.
Described disintegrating agent is selected from one or more in ammonium sulfate, sodium carbonate, sodium bicarbonate, sodium starch glycolate.
Described caking agent is for being selected from one or more in gelatin, polyvinyl alcohol, ethylene glycol, Xylo-Mucine, starch.
Described stablizer be selected from Sodium phosphate dibasic, hexanodioic acid, borax, phenyl glycidyl ether, Sodium Benzoate, oleum lini, anthraquinone, citric acid, one or more in propylparaben.
Described filler is selected from one or more in kaolin, light calcium carbonate, diatomite, attapulgite.
Described pH adjusting agent is selected from one or more in sodium hydroxide, ammoniacal liquor, acetic acid, phosphoric acid.
The described preparation method for preventing and treating the oil medicament of tree peony disease and pest: comprise following preparation process: first described component mixed, carry out micronizing with micronizer mill, then through oscillating granulator granulation, cryodrying at 50-100 DEG C.
Compared with the prior art, beneficial effect of the present invention is as follows:
(1) medicament of the present invention is to oil common disease leaf spot, purple root rot (Helicobasidium mompa) and the stem rot of tree peony, common insect pest has the effect of well control, to oil with tree peony without poisoning, add urea, not only improve utilization ratio and the drug effect rate of effective ingredient, and for oil to have additional nutrients element with tree peony when using, promote the oil growth of tree peony.
(2) add the auxiliary agent of heterogeneity in medicament of the present invention, have good dispersiveness, suspensibility is high, and working substance suspends indefinitely, good fluidity, and disintegration rate is fast, improves the rate of utilization of effective constituent, reduces dosage; Medicament heat storage stability is good, and easily conveniently, easy to use, dust is few, and environmental pollution is little for packaging, storing.
Embodiment
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1:
20%, for preventing and treating the medicament of oil with tree peony disease and pest, is made up of the component of following weight content:
Preparation: first described component is mixed, carry out micronizing with micronizer mill, then through oscillating granulator granulation, cryodrying at 70 DEG C.
Embodiment 2:
30%, for preventing and treating the medicament of oil with tree peony disease and pest, is made up of the component of following weight content:
Preparation: first described component is mixed, carry out micronizing with micronizer mill, then through oscillating granulator granulation, cryodrying at 100 DEG C.
Embodiment 3:
50%, for preventing and treating the medicament of oil with tree peony disease and pest, is made up of the component of following weight content:
Preparation: first described component is mixed, carry out micronizing with micronizer mill, then through oscillating granulator granulation, cryodrying at 80 DEG C.
Test example:
1, embodiment 1, embodiment 2, embodiment 3 and 25% pymetrozine wettable powder toxicity test results contrast:
Test site: Hefei
Test unit: Medical University Of Anhui
2, the control oil test-results of tree peony disease and pest
Claims (9)
1., for preventing and treating the medicament of oil with tree peony disease and pest, it is characterized in that: be made up of the component of following weight content:
PH adjusting agent adjust ph is 5-7.
2. according to claim 1 for preventing and treating the medicament of oil with tree peony disease and pest, it is characterized in that: described wetting agent is selected from one or more in alkyl alcohol polyoxyethylene groups ether sodium sulfate, alkylphenol-polyethenoxy base ether formaldehyde condensation products vitriol, alkyl sodium sulfonate, dialkyl succinylsuccinate sulfonate, fatty alcohol ethylene oxide adduct sulfonate, alkyl amide taurate, Sodium dodecylbenzene sulfonate, octylphenol polyethylene oxyethylene group ether sulfate.
3. the medicament for preventing and treating oil tree peony disease and pest according to claim 1, is characterized in that: described dispersion agent is selected from xylogen calcium iodate, alkyl naphthalene formaldehyde condensate sulfonates, sodium lauryl sulphate, potassium oleate, alkyl polyoxyethylene ether sulfonate, cocoyl sodium sulfonate, polyoxyethylene polyoxypropylene base ether block copolymers, pull open in powder, poly-second carboxylic esters sodium salt one or more.
4. according to claim 1 for preventing and treating the medicament of oil with tree peony disease and pest, it is characterized in that: described disintegrating agent is selected from one or more in ammonium sulfate, sodium carbonate, sodium bicarbonate, sodium starch glycolate.
5. according to claim 1 for preventing and treating the medicament of oil with tree peony disease and pest, it is characterized in that: described caking agent is for being selected from one or more in gelatin, polyvinyl alcohol, ethylene glycol, Xylo-Mucine, starch.
6. the medicament for preventing and treating oil tree peony disease and pest according to claim 1, is characterized in that: described stablizer be selected from Sodium phosphate dibasic, hexanodioic acid, borax, phenyl glycidyl ether, Sodium Benzoate, oleum lini, anthraquinone, citric acid, one or more in propylparaben.
7. according to claim 1 for preventing and treating the medicament of oil with tree peony disease and pest, it is characterized in that: described filler is selected from one or more in kaolin, light calcium carbonate, diatomite, attapulgite.
8. according to claim 1 for preventing and treating the medicament of oil with tree peony disease and pest, it is characterized in that: described pH adjusting agent is selected from one or more in sodium hydroxide, ammoniacal liquor, acetic acid, phosphoric acid.
9. the preparation method for preventing and treating the oil medicament of tree peony disease and pest as claimed in claim 1: it is characterized in that: comprise following preparation process: first described component is mixed; micronizing is carried out with micronizer mill; then through oscillating granulator granulation; cryodrying at 50-100 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510178344.6A CN104860748A (en) | 2015-04-15 | 2015-04-15 | Agent for controlling oil-use peony pests and diseases, and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510178344.6A CN104860748A (en) | 2015-04-15 | 2015-04-15 | Agent for controlling oil-use peony pests and diseases, and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104860748A true CN104860748A (en) | 2015-08-26 |
Family
ID=53906989
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510178344.6A Pending CN104860748A (en) | 2015-04-15 | 2015-04-15 | Agent for controlling oil-use peony pests and diseases, and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104860748A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109089670A (en) * | 2018-08-28 | 2018-12-28 | 华亭县正元生态农业发展有限公司 | Stems of dragon fruits maize ear rot control method in a kind of Internet of Things greenhouse |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070149401A1 (en) * | 2005-12-22 | 2007-06-28 | Syngenta Crop Protection, Inc. | Methods and composition for growth engineering and disease control |
| CN101880205A (en) * | 2010-06-29 | 2010-11-10 | 江苏克胜集团股份有限公司 | Paichongding water dispersible granule and preparation method thereof |
| CN101948350A (en) * | 2010-08-19 | 2011-01-19 | 北京农学院 | Composite fertilizer and preparation method thereof |
| CN102643133A (en) * | 2012-03-26 | 2012-08-22 | 张仕耀 | Formula mixing fertilizer with multiple pesticides and preparation method thereof |
| CN103288557A (en) * | 2013-05-29 | 2013-09-11 | 张仕耀 | Mixture of secondary element fertilizer and pesticide |
-
2015
- 2015-04-15 CN CN201510178344.6A patent/CN104860748A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070149401A1 (en) * | 2005-12-22 | 2007-06-28 | Syngenta Crop Protection, Inc. | Methods and composition for growth engineering and disease control |
| CN101880205A (en) * | 2010-06-29 | 2010-11-10 | 江苏克胜集团股份有限公司 | Paichongding water dispersible granule and preparation method thereof |
| CN101948350A (en) * | 2010-08-19 | 2011-01-19 | 北京农学院 | Composite fertilizer and preparation method thereof |
| CN102643133A (en) * | 2012-03-26 | 2012-08-22 | 张仕耀 | Formula mixing fertilizer with multiple pesticides and preparation method thereof |
| CN103288557A (en) * | 2013-05-29 | 2013-09-11 | 张仕耀 | Mixture of secondary element fertilizer and pesticide |
Non-Patent Citations (1)
| Title |
|---|
| 徐汉虹: "《花卉病虫害防治首选农药手册》", 31 October 2001, 广东科技出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109089670A (en) * | 2018-08-28 | 2018-12-28 | 华亭县正元生态农业发展有限公司 | Stems of dragon fruits maize ear rot control method in a kind of Internet of Things greenhouse |
| CN109089670B (en) * | 2018-08-28 | 2020-07-14 | 华亭县正元生态农业发展有限公司 | Method for preventing and treating stem rot of pitaya in greenhouse of Internet of things |
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Application publication date: 20150826 |