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CN104630009B - Liver-protecting white spirit of resisting alcoholic hepatic injury and preparation method thereof - Google Patents

Liver-protecting white spirit of resisting alcoholic hepatic injury and preparation method thereof Download PDF

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Publication number
CN104630009B
CN104630009B CN201510086520.3A CN201510086520A CN104630009B CN 104630009 B CN104630009 B CN 104630009B CN 201510086520 A CN201510086520 A CN 201510086520A CN 104630009 B CN104630009 B CN 104630009B
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liver
hepatic injury
white spirit
alcoholic hepatic
wine
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CN104630009A (en
Inventor
张光雄
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Neu (Shanghai) Food Technology Co., Ltd.
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Wine Pocket (shanghai) Klc Holdings Ltd
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    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00—Preparation of other alcoholic beverages
    • C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/488—Pueraria (kudzu)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/732—Chaenomeles, e.g. flowering quince
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/734—Crataegus (hawthorn)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
    • A61K36/815—Lycium (desert-thorn)

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
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  • Mycology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Medical Informatics (AREA)
  • Medicinal Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Biochemistry (AREA)
  • General Engineering & Computer Science (AREA)
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  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Genetics & Genomics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The present invention relates to liver-protecting white spirit of a kind of resisting alcoholic hepatic injury and preparation method thereof, the liver-protecting white spirit of described resisting alcoholic hepatic injury comprises following weight parts raw material composition: white wine 400-800 part, root of kudzu vine 20-40 part, hawthorn 20-40 part, pawpaw 20-40 part, fruit of Chinese wolfberry 20-40 part. The liver-protecting white spirit of resisting alcoholic hepatic injury of the present invention, can bring into play to greatest extent the comprehensive function of various medicinal materials, wine body is soft, sweet tasty and refreshing, all fragrant harmonies, taste is refreshing clean, there is the effect of resisting alcoholic hepatic injury, remarkable to reducing the effect of hepatic injury, after especially having used additive, solve the problem of white wine poor stability.

Description

Liver-protecting white spirit of resisting alcoholic hepatic injury and preparation method thereof
Technical field
The present invention relates to the manufacture field of white wine, be specifically related to a kind of liver-protecting white spirit of resisting alcoholic hepatic injuryAnd preparation method thereof.
Background technology
White wine is taking Cereals as primary raw material, taking Daqu, little song or wheat bran and distiller's yeast etc. as saccharifying ferment,Through boiling, saccharification, fermentation, distillation and the Spirit of making. Claim again liquor, white spirit, aquavit etc.Vinosity colourless (or micro-Huang) is transparent, and fragrant odour is pure, and entrance is sweet refreshing clean, and alcohol content is higher,Through store aging after, there is the compound fragrant taking ester class as main body.
White wine has another name called liquor, white spirit, is Chinese conventional beverage wine, welcome by Chinese. According to " thisGrass detailed outline " record: " liquor Fei Gufa is also, original in the time of unit, and its method enters rice steamer by heavy wine and grain and (refers to steamPot), steam and make on gas, hold to drip with device and reveal. " can draw thus, the production of China's white wine is existing very longHistory.
White wine is the distinctive a kind of Spirit of China. The wine degree of white wine is generally more than 41 degree, how 55More than degree, be generally no more than 65 degree. Low powered posterior chamber white wine refers to and adopted degree of falling technique, and wine degree generally exists38 degree, even reach the white wine of spending 20 more, are called for short low wine. The degree of falling of wine is generally to adopt at female wineIn add highly purified distilled water to realize.
So-called " wine is got over Chen Yuexiang ", refers to white wine more than 38 degree more. These white wine only need to indicate lifeProduce the date, do not need to indicate the shelf-life. But for low powered posterior chamber white wine, be not but " more Chen Yuexiang ".Research discovery, the total acid in white wine is deposited in process and is all risen at shelf life, 30 ° of width that wine risesSpend largerly, 20%～28%, the 38 ° of wine that rise every year on average rise 13%～22% every year on average. ?In storage process, the main cause that acid increases is: a, white wine occur hydrolysis phenomenon, ester depositing in processAfter hydrolysis, generate corresponding acid and ethanol. The volatility coefficient of b, acid is little, not volatile in storage process.And total ester in white wine is deposited in process at shelf life and all declined, the amplitude that 30 ° of wine declines is larger,7%～13%, the 38 ° of wine that decline every year on average decline 5%～9% every year on average. For low wine,Due to CH3CH2OH concentration is lower, H2O concentration is higher, the speed of forward hydrolysis, thereby hydrolysisTo cause total ester to deposit at shelf life the main cause declining in process.
Health-care spirit or medicinal liquor, be generally taking white wine as base wine, but added in order to possess health-care efficacyThe traditional Chinese medicine ingredients of some medicine-food two-purposes, in order to ensure the drug effect of traditional Chinese medicine ingredients, and facilitates specific crowdQuote, the medicinal liquor with health-care efficacy on market, is all 35 degree or the lower low powered posterior chamber of the number of degrees conventionallyWhite wine. Therefore, health-care spirit generally has the less stable of low powered posterior chamber white wine, between storage period, and acid amountDegradation shortcoming under rising, ester amount.
Summary of the invention
One of technical problem to be solved by this invention be to provide a kind of resisting alcoholic hepatic injury to protect liver whiteWine.
Two of technical problem to be solved by this invention is to provide the liver-protecting white spirit of above-mentioned resisting alcoholic hepatic injuryPreparation method.
The scheme solving this technical problem is:
A liver-protecting white spirit for resisting alcoholic hepatic injury, comprises following weight parts raw material composition: white wine400-800 part, root of kudzu vine 20-40 part, hawthorn 20-40 part, pawpaw 20-40 part, fruit of Chinese wolfberry 20-40 part.
Preferably,
Described white wine is the white wine of wine degree 25-38 degree.
Described white wine be delicate fragrance type or aromatic Chinese spirit.
The liver-protecting white spirit of described resisting alcoholic hepatic injury can also comprise the additive of 1-9 weight portion.
Further preferred, described additive, comprises the component of following weight parts: 3-hydroxyl-2-ethyl-4-Pyrones 10-30 part, xylitol 20-40 part, carragheen 10-20 part.
The present invention also provides the preparation method of the liver-protecting white spirit of described resisting alcoholic hepatic injury, under it comprisesState step:
(1) take each raw material by proportioning, by pawpaw, the root of kudzu vine, hawthorn and the fruit of Chinese wolfberry are put into white wine and are soaked;
(2) adsorb with active carbon for liquor, filter.
Preferably,
The described soak time of step (1) is 15-30 days.
Soaking conditions is to soak under normal temperature (25 ± 5 DEG C) air-proof condition.
In step (2) afterwards, can add additive by proportioning, make and preferably contain the anti-of additiveThe liver-protecting white spirit of alcoholic liver injury.
In the present invention,
Pawpaw, Chinese medicine name. For the dry almost ripe fruit of rosaceous plant chaenomeles lagenaria. Summer, Qiu ErjiWhen fruit is greenish-yellow, gather, put in boiling water and scald to crust canescence, double vertical profile, dries. Function: have relaxing muscles and tendonsActive, and effect of stomach dampness elimination. Compendium of Material Medica: the main cholera of pawpaw is told profit convulsion, beriberi, allThe spleen-stomach diseases, non-hepatic disorder also. Though the main muscle of liver, convulsion is attacked due to the impairment of the spleen by heresy damp and hot, cold-dampness,Therefore myospasm must arise from sufficient calf, it is bright that calf and penis all belong to sun. Pawpaw is controlled convulsion, non-beneficial muscle also, reason spleen and cutting downAlso, native disease gold declines and wood is contained liver, therefore with the dissipation of sour Wen Yishou taste, and walk muscle with flat liver heresy by means of it,Be in soil, to rush down wood to help gold also. Flat native must the order and Jin Shouyin of wood. " Plain Questions " cloud: sour flavor being apt to act on the tendon, muscleSick without many food acid. The Meng numerous cloud: eat pawpaw more and damage tooth and bone. The bright of clear felling liver tested, and pawpaw is started with, footLunar, be taste medicine, non-liver medicine, benefit can be levied.
The root of kudzu vine, Chinese medicine name. For the dry root of legume pueraria lobata, practise and claim elegant jessamine. Autumn, two seasons of winter excavate,Take advantage of fresh-cut and become sheet or fritter; Dry. Sweet, pungent, cool. Have relieving muscles to expel heat, promoting eruption, promotes the production of body fluid to quench thirst,Rise the merit of positive antidiarrheal. Be usually used in illness that has not attacked the vital organs of the human body heating, stiff nape and back, measles without adequate eruption, pyreticosis is thirsty, and the deficiency of Yin disappearsYearningly, the heat dysentery of purging heat, splenasthenic diarrhea. " book on Chinese herbal medicine converges and says ": " root of kudzu vine, fresh breeze is cold, and clean table is evil, expelling pathogenic factors from muscles and skinHeat, only polydipsia. Rush down the medicine of stomach fire also. Taste and see the medicine of delivering loose heresy, its product are also many, as Chinese ephedra is pulled out the sunBattalion's point trembling with fear, the wind that cassia twig Xie Taiyangwei divides, the loose sun of windproof, purple perilla is in the chill of table, Jehol Ligusticum Rhizome, QiangThe loose sun alive, in the cold-dampness of table, all claim to disperse medicine also, and dispersing of the root of kudzu vine also enters the sun, also dispersing wind and cold,Different again, if non-numb, osmanthus, Soviet Union, anti-, pungent fragrant temperature is dry, disperse and the mistake that damages middle gas also; Non-If Jehol Ligusticum Rhizome, notopterygium root, disperse and have consumption ying blood anxiety also. "
Hawthorn, Chinese medicine name. For the dry mature fruit of rosaceous plant large-fruited Chinese hawthorn or hawthorn. Autumn fruitWhen ripe, gather, section, dry. " Records of Tradition Chinese and Western Medicine in Combination ": hawthorn, if help it with sweet medicine, changesHemostasis and do not hinder new blood, opens strongly fragrant gas and does not hinder healthy tendency, and the outstanding peace of its property also.
The fruit of Chinese wolfberry is traditional rare traditional Chinese medicine, is again a kind of tonic food. In 63 of Ministry of Public Health's announcementPlant in the list of medicine-food two-purpose, rank first. As traditional Chinese medicine, the flat taste of the fruit of Chinese wolfberry is sweet, has tasteEffect of filling liver kidney, benefiting shrewd head, moistening lung. By chemical composition analysis, the fruit of the fruit of Chinese wolfberry detectsContain abundant natural Beta-carotene, vitamin C, fruit of Chinese wolfberry proteoglycan, betaine, linoleic acid withAnd the nutritional labeling such as iron, phosphorus, calcium, there is qi-restoratives to calm the nerves, improving eyesight is dispeled the wind, nourshing kidney moistening lung and to protect liver anti-swollenThe effects such as knurl. The fruit of Chinese wolfberry contains the healthy eye such as abundant carrotene, multivitamin and calcium, ironEssential nutriment, therefore there is the merit of improving eyesight, is commonly called as " bright eye ". Ancient Chinese medicine doctor treatment deficiency of liver-blood,What deficiency of kidney-YIN caused looks thing duskization and yctalopia, usually uses the fruit of Chinese wolfberry. And the fruit of Chinese wolfberry is from the Book of SongsIn time, rises " to combine in luxuriant Qi ", and just for medicine, the history of existing more than 3000 just has Shanxi court from ancient times so farThe alone fruit of Chinese wolfberry of Ge Hong is smash juice and is dripped order, the story for the treatment of ophthalmology illness. The name of the fruit of Chinese wolfberry is first appeared in " the legendary god of farmingBook on Chinese herbal medicine warp ", be listed as top grade, very popular over the past thousands of years.
3-hydroxyl-2-ethyl-pyrokomane, No. CAS: 4940-11-8. China GB2760-86 is defined asAllowing the food and the spices that use, is a kind of fragrance synergist, is a kind of safety non-toxic, has flavouring, increasingSweet, to protect the effects such as perfume (or spice) and covering smell food additives.
Xylitol, No. CAS: 87-99-0.
Carragheen, No. CAS: 11114-20-8. Carragheen is that one (is mainly various Qi from marine red algaUnicorn dish) in the polysaccharide that extracts, its chemical constitution is D-galactolipin and 3,6-dehydration-D-galactose residue instituteComposition linear polysaccharide compound, on residue with ester formula sulfate group.
The liver-protecting white spirit of resisting alcoholic hepatic injury of the present invention, can bring into play various medicinal materials to greatest extentComprehensive function, wine body is soft, sweet tasty and refreshing, all fragrant harmonies, taste is refreshing clean, has resisting alcoholic liver and damagesThe effect of wound, remarkable to reducing the effect of hepatic injury, after especially having used additive, solve lowThe problem of number of degrees white wine poor stability. In prior art, white wine does not normally add additive, stillDue to medicinal liquor or the health-care spirit number of degrees lower, along with the time, part acidic can occur, acid number rise, ester amountDecline, the xylitol in additive can react with acid, and react with it and generate the ester with fragranced,Carragheen is as a kind of dispersant, and the liver-protecting white spirit of antagonism alcoholic liver injury has played stable effect,3-hydroxyl-2-ethyl-pyrokomane can be removed the peculiar smell of the Chinese medicine in health-care spirit. Unexpectedly, researchFind: in the time using 3-hydroxyl-2-ethyl-pyrokomane, xylitol and carragheen, for slowing down guarantor simultaneouslyIn strong white wine, the effect of Synergistic has been played in the decline of ester amount. Resisting alcoholic hepatic injury of the present inventionLiver-protecting white spirit preparation method simple, easily preservation.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
Get 600 kilograms of 35 degree white wine, put into 30 kilograms of pawpaws, 30 kilograms of the roots of kudzu vine, 30 kilograms of hawthorn,30 kilograms of the fruits of Chinese wolfberry, sealing, soak at room temperature 30 days, with active carbon for liquor SB-204 removal peculiar smell and muddyTurbid, filter, obtain the liver-protecting white spirit of the resisting alcoholic hepatic injury of embodiment 1.
Show through acute toxicity testing result, acute toxicity is extremely low, safe; Pharmacodynamic experiment resultShow to there is the effect of resisting alcoholic hepatic injury, from pathological section and Antioxidant index, to reducingThe effect of hepatic injury is remarkable.
The liver-protecting white spirit of resisting alcoholic hepatic injury of the present invention, can bring into play various medicinal materials to greatest extentComprehensive function, wine body is soft, sweet tasty and refreshing, all fragrant harmonies, taste is refreshing clean, has resisting alcoholic liver and damagesThe effect of wound, remarkable to reducing the effect of hepatic injury.
Embodiment 2-5
Additive formulations according to embodiment 2-5 in table 2 takes each raw material, mixes, and makes interpolationAgent. Take 3 grams of additives join resisting alcoholic hepatic injury that 720 grams of embodiment 1 make to protect liver whiteIn wine, be uniformly mixed, make the liver-protecting white spirit of the resisting alcoholic hepatic injury of embodiment 2-5.
Table 1: additive formulations table (unit: kilogram)
3-hydroxyl-2-ethyl-pyrokomane Xylitol Carragheen
Embodiment 2 20 30 15
Embodiment 3 / 30 35
Embodiment 4 20 45 /
Embodiment 5 20 / 45
Test case
Detect lucifuge normal temperature sealed type storage after 20 months, main ester class in the health-care spirit of embodiment 1-5The content of compound, test result is in table 2.
Table 2: embodiment 1-5 health-care spirit ester type compound is containing scale (unit: g/L)
Ethyl acetate Ethyl lactate Ethyl butyrate Ethyl hexanoate
Just prepared embodiment 1 0.6020 0.7885 0.0185 0.0232
Embodiment 1 after 20 months 0.3788 0.4211 0.0084 0.0126
Embodiment 2 after 20 months 0.4652 0.5921 0.0155 0.0186
Embodiment 3 after 20 months 0.4173 0.4956 0.0122 0.0142
Embodiment 4 after 20 months 0.4384 0.5102 0.0133 0.0145
Embodiment 5 after 20 months 0.4091 0.4825 0.0124 0.0137
From experimental result, store after 20 months, the resisting alcoholic hepatic injury of embodiment 1-5 protect liverIn white wine, several main ester type compound content has maintained higher level, kept good fragranced andMouthfeel, after especially embodiment 2-4 has used additive, ester class content is higher.
More particularly, embodiment 2 has used xylitol, carragheen, 3-hydroxyl-2-ethyl-pyrokomane threePerson is composite, adopts respectively in xylitol, carragheen and 3-hydroxyl-2-ethyl-pyrokomane compared with embodiment 3-5Any two kinds composite, lucifuge normal temperature sealed type storage after 20 months ester type compound content maintain compared with Gao ShuiFlat, three's Synergistic, effect is more obvious.

Claims (4)

1. a liver-protecting white spirit for resisting alcoholic hepatic injury, is characterized in that, under comprisingState weight portion raw material composition: white wine 400-800 part, root of kudzu vine 20-40 part, hawthorn 20-40 part,Pawpaw 20-40 part, fruit of Chinese wolfberry 20-40 part, additive 1-9 part;
Described additive, comprises the component of following weight parts: 3-hydroxyl-2-ethyl-4-Pyrones 10-30 part, xylitol 20-40 part, carragheen 10-20 part.
2. the liver-protecting white spirit of resisting alcoholic hepatic injury as claimed in claim 1, its feature existsIn: the wine degree of the liver-protecting white spirit of described resisting alcoholic hepatic injury is 25-38 degree.
3. the liver-protecting white spirit of resisting alcoholic hepatic injury as claimed in claim 1, its feature existsIn: the liver-protecting white spirit of described resisting alcoholic hepatic injury is delicate fragrance type or aromatic Chinese spirit.
Claim 1 ?the liver-protecting white spirit of the resisting alcoholic hepatic injury described in any one in 3Preparation method, is characterized in that, comprises the steps:
(1) take each raw material by proportioning, by pawpaw, the root of kudzu vine, hawthorn and the fruit of Chinese wolfberry are put into whiteIn wine, soak;
(2) adsorb with active carbon for liquor, filter;
(3) add additive.
CN201510086520.3A 2015-02-23 2015-02-23 Liver-protecting white spirit of resisting alcoholic hepatic injury and preparation method thereof Expired - Fee Related CN104630009B (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109306308A (en) * 2017-07-27 2019-02-05 甄青松 A kind of odor type health white wine
CN109136025A (en) * 2018-07-11 2019-01-04 山西三十七度酒业有限公司 A kind of composite fragrant assembled alcoholic drinks and its preparation method

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5558087A (en) * 1978-10-23 1980-04-30 Sumie Hihara Low calorie apricot liquor
CN1153818A (en) * 1996-10-23 1997-07-09 宁夏农林科学院农副产品贮藏加工研究所 Fresh lycium chinense with stalk wine and its brewage process
CN101874857A (en) * 2010-05-28 2010-11-03 劲牌有限公司 Liver-protecting white spirit for resisting alcoholic liver injury and production process thereof
CN102660445A (en) * 2012-06-06 2012-09-12 重庆修贤商贸有限公司 Functional low-damage healthcare wine
CN103103097A (en) * 2013-01-16 2013-05-15 丽水市林业科学研究院 Rhizoma polygonati kidney tonifying wine and preparation method thereof
CN103666982A (en) * 2012-09-08 2014-03-26 哈尔滨艾克尔食品科技有限公司 Pineapple jelly wine

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5558087A (en) * 1978-10-23 1980-04-30 Sumie Hihara Low calorie apricot liquor
CN1153818A (en) * 1996-10-23 1997-07-09 宁夏农林科学院农副产品贮藏加工研究所 Fresh lycium chinense with stalk wine and its brewage process
CN101874857A (en) * 2010-05-28 2010-11-03 劲牌有限公司 Liver-protecting white spirit for resisting alcoholic liver injury and production process thereof
CN102660445A (en) * 2012-06-06 2012-09-12 重庆修贤商贸有限公司 Functional low-damage healthcare wine
CN103666982A (en) * 2012-09-08 2014-03-26 哈尔滨艾克尔食品科技有限公司 Pineapple jelly wine
CN103103097A (en) * 2013-01-16 2013-05-15 丽水市林业科学研究院 Rhizoma polygonati kidney tonifying wine and preparation method thereof

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