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CN104529582A - Method and product for producing high-fertilizer-efficiency organic fertilizer by utilizing monosodium waste liquid - Google Patents

Method and product for producing high-fertilizer-efficiency organic fertilizer by utilizing monosodium waste liquid Download PDF

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Publication number
CN104529582A
CN104529582A CN201510004149.1A CN201510004149A CN104529582A CN 104529582 A CN104529582 A CN 104529582A CN 201510004149 A CN201510004149 A CN 201510004149A CN 104529582 A CN104529582 A CN 104529582A
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China
Prior art keywords
fertilizer
waste liquid
fermentation
monosodium glutamate
glutamate waste
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Pending
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CN201510004149.1A
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Chinese (zh)
Inventor
陈志峰
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Zhengda Ogden (fujian) Ecological Agriculture Development Co Ltd
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Zhengda Ogden (fujian) Ecological Agriculture Development Co Ltd
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Priority to CN201510004149.1A priority Critical patent/CN104529582A/en
Publication of CN104529582A publication Critical patent/CN104529582A/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Fertilizers (AREA)

Abstract

The invention discloses a method for producing a high-fertilizer-efficiency organic fertilizer by utilizing monosodium waste liquid. The method comprises the step of material mixing, wherein the monosodium waste liquid, rice husk bran and chicken muck ash are mixed and stacked into a material to be fermented according to the proportion of (7-3): (2-4): (1-2); the step of fermentation, the step of screening and crushing and the step of product packaging. According to the method, the chicken muck ash with a low water content and a large PH value is selected as an auxiliary material to be mixed with the monosodium waste liquid with a high water content and a small PH value, the water and the PH value of the monosodium waste liquid can be rapidly adjusted, energy consumed by evaporation and water drying is saved, and therefore production cost is reduced. The total nutrient content of N, P and K in the organic fertilizer prepared through the method reaches above 13%, the use effect of the organic fertilizer is equivalent to the use effect of an organic and chemical fertilizer when the organic fertilizer is used for production of organic agricultural products, and the yield-increasing effect is obvious.

Description

A kind of utilize monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer method and product
Technical field
The present invention relates to fertilizer preparation technology field, particularly relate to a kind of utilize monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer method and product.
Background technology
Monosodium glutamate waste liquid is mainly derived from fermented gournet powder liquid and extracts the L-glutamic acid stage.According to statistics, produce 1 ton of monosodium glutamate and will discharge high-concentration waste water about 20 tons.And monosodium glutamate waste liquid to have COD high, BOD is high, and thalline content is high, and sulfate radical content is high, the feature that ammonia-nitrogen content is high and pH value is low " five high low ", once entering river, produces severe contamination to water body, destruction ecotope, and is that one of resource is wasted greatly.The utilization of monosodium glutamate waste liquid comprises extraction yeastex, produces fodder yeast, fertilizer etc.; At present, domestic to the direct spray pelleting process of the many employings of producing fertilizer with gourmet powder waste liquor, there is evaporation in its production process and dry water consumption mass energy, the defect that cost is high; Simultaneously the monosodium glutamate waste liquid fertilizer organic content of producing through direct spray granulating is low, cannot reach national fertilizer standard.
Summary of the invention
One of the object of the invention is to provide a kind of method utilizing monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer.
The technical scheme realizing the object of the invention one is: a kind of method utilizing monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer, it comprises batch mixing, fermentation, screening pulverizing and finished product packing step, and described batch mixing step is: by monosodium glutamate waste liquid, husk chaff and chicken manure ash in (7 ~ 3): (2 ~ 4): (1 ~ 2) ratio mixes, is stacked to fermentation materials.
In order to better technique effect, the method that the present invention utilizes monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer can also do following improvement:
1, described fermenting process is divided into one time fermentation and Secondary Fermentation; Be down to less than 50 DEG C when fermentation materials temperature no longer to raise, when test in laboratory moisture is down to 40% ~ 45%, one time fermentation terminates; When fermentation materials moisture is down to less than 30%, temperature is close to normal temperature and no longer go up, and during without acid smell, Secondary Fermentation terminates; The bacillus acidocldarius of spray concentration 200,000,000/more than ml before described one time fermentation, the yeast of spray concentration 200,000,000/more than ml in Secondary Fermentation process.One time fermentation stage windrow temperature is high, oxygen requirement large, and select high temperature resistant, aerobic bacillus acidocldarius to be zymophyte, Secondary Fermentation stage temperature of charge is low, and oxygen requirement is less, selects middle psychrophile yeast to be zymophyte; Adding bacterium by rationally arranging stepwise fermentation segmentation, improve the quality of material fermentation speed and fertilizer.
2, described bacillus acidocldarius and yeast consumption are 0.5 ‰ of fermentation materials weight; Improve fermenting speed but production cost is unlikely too large again, if will improve production cost higher than 0.5 ‰ of fermentation materials weight.
3, in described batch mixing step, the optimum proportioning of monosodium glutamate waste liquid, husk chaff and chicken manure ash is (6 ~ 5): (3 ~ 4): (1 ~ 2), by this mix proportion scheme fermenting mixture material moisture 50% ~ 55%, pH value 6-7, C/N is than 18 ~ 22, the good dissolved oxygen amount of material permeability is high, be comparatively suitable for fermentation, can fermentation time be shortened, save production cost.
4, after described batch mixing step, fragmentation is carried out to mixture, make raw meal particle size be less than below 10mm, moisture distribution is even.Diminished by broken material granularity, moisture distribution is even, be beneficial to fermentation, shortening fermentation period.
5, in the fertilizer that obtains of screening pulverising step, directly add chicken manure ash and the oxalic acid of different ratios, regulate N, P, K ratio in fertilizer and pH value to produce various speciality fertilizers on commercial crops.
Two of object of the present invention is to provide a kind of low cost high fertilizer efficiency organic fertilizer, and it is obtained by the preparation method of goal of the invention one.
Beneficial effect of the present invention is as follows:
1, the present invention select water content is low, pH value is higher chicken manure ash for auxiliary material and the monosodium glutamate waste liquid that water content is high, pH value is lower mixed, moisture in quick adjustment monosodium glutamate waste liquid and pH value, save the energy consumption of evaporation and oven dry moisture, reduce production cost, simultaneously, pH regulator can accelerate material fermentation to neutral left and right.
2, use containing organic higher husk chaff in preparation technology is fermentation auxiliary material simultaneously, organic content in effective raising target fertilizer, overcome the fertilizer organic content that Gourmet Powder Factory's tankage tail washings produces through direct spray granulating low, the defect of national fertilizer standard can not be reached.
2, chicken manure ash P, K content is high, by adding certain proportion chicken manure ash and oxalic acid in fertilizer finished product in proportion, conveniently can produce the special fertilizer of different N, P, K content, meet different planting soil, different crops and different growth and development stage thereof the different demands to fertilizer, produce various fertilizer special for organic, achieve the target of balance fertilizing.Organic fertilizer product N, P, K ratio overcoming domestic production is fixed, and is difficult to the shortcoming that demand adjusts or Setup Cost is high according to Different Crop.
3, fertilizer N, P, K total nutrient content of producing of preparation method of the present invention is up to more than 13%, and use on organic farm products is produced, be equivalent to the result of use of organic and inorganic fertilizer, effect of increasing production is obvious.
The compound organic and inorganic fertilizer that a small amount of inorganic fertilizer carrys out production low cost is added in the fertilizer that 4, preparation method of the present invention can also be utilized to produce.
Embodiment
Below in conjunction with preferred embodiment, the present invention is described further.
Embodiment 1:
Utilize monosodium glutamate waste liquid to produce a method for high fertilizer efficiency fertilizer, it comprises the following steps:
1) batch mixing: by monosodium glutamate waste liquid, husk chaff and chicken manure ash mix in the ratio of 5:4:1, stacking, after batch mixing, fragmentation is carried out to mixture, make raw meal particle size be less than below 10mm, moisture distribution is even, spray bacillus acidocldarius in mixture weight ratio 0.5 ‰ ratio simultaneously;
2) ferment: be divided into one time fermentation and Secondary Fermentation; Be down to less than 50 DEG C when temperature of charge no longer to raise, when test in laboratory moisture is down to about 45%, one time fermentation terminates; When mixture moisture is down to less than 30%, temperature is close to normal temperature and no longer go up, and terminates without Secondary Fermentation during acid smell;
3) material particle diameter being greater than 6mm by sifting machine returns fermentation, and the material after sub-sieve is through pulverizing obtained fertilizer finished product;
4) test in laboratory Ministry of Agriculture NY525 ~ 2012 fertilizer standard indices up to standard after can packing and selling.As not up to standard in PH by adding unslaked lime or oxalic acid adjustment.
Embodiment 2:
Adopt the preparation method identical with embodiment 1, difference is that by monosodium glutamate waste liquid, husk chaff and chicken manure ash proportioning be 6:3:1.
Embodiment 3
Organic tea fertilizer special for organic is prepared:
1) special fertilizer formula is determined: understand to local bureau of agriculture and collect organic tea fertilization compositions based on earth measurement situation.Through understanding the plantation of local organic tea to the requirement of formula fertilizer be: organic >=45%, pH value 6 ~ 7, N, P, K optimum proportioning=2:(0.5 ~ 0.8): (0.7 ~ 1).
2) produce high nutrient organic fertilizer by case study on implementation one compound method step, as female fertile, recording female fertile N content is 9.4%, P 2o 5content is 1.79%, K 2o content is 1.98%.
3) productive target fertilizer, i.e. organic tea fertilizer special for organic.
3.1) amount that production organic tea fertilizer special for organic need add chicken manure ash in female fertilizer is calculated.
3.2) lab scale.Get 1 ton and female fertile add 0.2 ton of chicken manure ash, bar buttress is banked up, and after throwing continuously turn over three times with the throwing machine that turns over, laboratory sampling data detection is moisture content 20%; N content 8.1%; P 2o 5content 2.53%; K 2o content is 3.20%; Organic content 46%; PH7.8.Except above data are higher compared with pH value requires with tealeaves special fertilizer, other data fit requirements.
3.3) oxalic acid adjusted to ph is added to 6-7.
3.4) by said ratio scheme and Mixing Method production Special organic fertilizer for tea 30 tons.Indices is detected by Ministry of Agriculture's NY525 ~ 2012 fertilizer standard detecting method in laboratory.
4) field test.
5) produce in batches.
Supplementary material of the present invention selects chicken manure ash to be chicken manure burning electricity generation factory of Sheng Nong group tankage; Husk chaff is paddy processing enterprise tankage; High density tail washings after extracting glutamic acid is Gourmet Powder Factory's tankage.These supplementary material costs are low, stable to be easy to get.
The properties data of the fertilizer obtained with embodiment 1-3 are as shown in table 1:
As seen from the above table, the fertilizer property indices adopting formula of the present invention and preparation method to obtain all is better than organic fertilizer industry standard (NY525-2012), fertilizer N, P, K total nutrient content is up to more than 13%, use on organic farm products is produced, be equivalent to the result of use of organic and inorganic fertilizer, effect of increasing production is obvious.
Monosodium glutamate waste liquid of the present invention, husk chaff and chicken manure ash consumption is not limited to ratio described in embodiment, according to (7 ~ 3): (2 ~ 4): the proportioning of (1 ~ 2) all can produce national standard fertilizer, required supplementary material content can be added according to the requirement of fertilizer finished product in actual production, and utilize oxalic acid to adjust finished product pH value.But test shows that monosodium glutamate waste liquid, husk chaff and chicken manure ash proportioning is in (6 ~ 5): (3 ~ 4): time (1 ~ 2), fermentation time is shorter and production cost is lower.
Fermentation mode of the present invention is not limited to Secondary Fermentation, and traditional fermentation mode also can.But be aided with suitable fermented bacterium in Secondary Fermentation, the quality of material fermentation speed and fertilizer can be significantly improved, reduce production cost.
In addition, because chicken manure ash P, K content is high, according to reality fertilising needs, by directly adding chicken manure ash and oxalic acid in proportion in fertilizer finished product, conveniently can produce the special fertilizer of different N, P, K content, meet different planting soil, different crops and different growth and development stage thereof the different demands to fertilizer, produce various fertilizer special for organic, achieve the target of balance fertilizing.
The fertilizer utilizing technique of the present invention to prepare also can according to the nutrient uptake feature of different cash crop and different growth and development stage thereof, nutrient and pH value is adjusted by adding a small amount of inorganic fertilizer, production low cost high density compound organic and inorganic fertilizer and various Special Fertilizers for Various Crops, significantly reduce the production cost of compound organic and inorganic fertilizer.
The foregoing is only embodiments of the invention; not thereby the scope of the claims of the present invention is limited; every utilize description of the present invention to do equivalent structure or equivalent flow process conversion; or be directly or indirectly used in other relevant technical fields, be all in like manner included in scope of patent protection of the present invention.

Claims (7)

1. the method utilizing monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer, it comprises batch mixing, fermentation, screening pulverizing and finished product packing step, it is characterized in that, described batch mixing step is: by monosodium glutamate waste liquid, husk chaff and chicken manure ash in (7 ~ 3): (2 ~ 4): (1 ~ 2) ratio mixes, is stacked to fermentation materials.
2. the method utilizing monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer according to claim 1, it is characterized in that, in described batch mixing step, the proportioning of monosodium glutamate waste liquid, husk chaff and chicken manure ash is (6 ~ 5): (3 ~ 4): (1-2).
3. the method utilizing monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer according to claim 1, is characterized in that, carry out fragmentation, make raw meal particle size be less than below 10mm, moisture distribution is even after described batch mixing step to mixture.
4. the method utilizing monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer according to claim 1, it is characterized in that, described fermenting process is divided into one time fermentation and Secondary Fermentation; Be down to less than 50 DEG C when fermentation materials temperature no longer to raise, when test in laboratory moisture is down to 40% ~ 45%, one time fermentation terminates; When fermentation materials moisture is down to less than 30%, temperature is close to normal temperature and no longer go up, and during without acid smell, Secondary Fermentation terminates; The bacillus acidocldarius of spray concentration 200,000,000/more than ml before described one time fermentation, the yeast of spray concentration 200,000,000/more than ml in Secondary Fermentation process.
5. the method utilizing monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer according to claim 2, it is characterized in that, described bacillus acidocldarius and yeast consumption are 0.5 ‰ of fermentation materials weight.
6. the method utilizing monosodium glutamate waste liquid to produce high fertilizer efficiency fertilizer according to claim 1, it is characterized in that, in the fertilizer that screening pulverising step obtains, directly add chicken manure ash and the oxalic acid of different ratios, regulate N, P, K ratio in fertilizer and pH value to produce various speciality fertilizers on commercial crops.
7. a low cost high fertilizer efficiency organic fertilizer, its according to claim 1-6 any one utilize monosodium glutamate waste liquid produce high fertilizer efficiency fertilizer method obtain.
CN201510004149.1A 2015-01-06 2015-01-06 Method and product for producing high-fertilizer-efficiency organic fertilizer by utilizing monosodium waste liquid Pending CN104529582A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105585386A (en) * 2016-03-23 2016-05-18 山东绿亨生物工程有限公司 Amino acid biological organic water-soluble fertilizer and preparing method thereof
CN106565340A (en) * 2016-11-08 2017-04-19 福建省星源农牧科技股份有限公司 Cultivation material for improving agaricus bisporus yield and amino acid content and cultivating method of cultivation material
CN108658671A (en) * 2018-06-28 2018-10-16 靖西市秀美边城农业科技有限公司 A kind of preparation method being retained long-acting fructus crataegi pinnatifidae tree dedicated fertilizer
CN108911835A (en) * 2018-06-28 2018-11-30 靖西市秀美边城农业科技有限公司 A method of compound fertilizer is prepared using monosodium glutamate waste liquid
CN109970495A (en) * 2017-12-28 2019-07-05 许传高 A kind of technique preparing organic fertilizer using amino acid fermentation tail washings
CN109988042A (en) * 2019-04-08 2019-07-09 齐鲁工业大学 A kind of method that utilizes monosodium glutamate waste liquid to manufacture organic fertilizer

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CN102992827A (en) * 2012-12-14 2013-03-27 山东新超农业科技有限公司 Active organic bacterial fertilizer and preparation method thereof

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105585386A (en) * 2016-03-23 2016-05-18 山东绿亨生物工程有限公司 Amino acid biological organic water-soluble fertilizer and preparing method thereof
CN106565340A (en) * 2016-11-08 2017-04-19 福建省星源农牧科技股份有限公司 Cultivation material for improving agaricus bisporus yield and amino acid content and cultivating method of cultivation material
CN109970495A (en) * 2017-12-28 2019-07-05 许传高 A kind of technique preparing organic fertilizer using amino acid fermentation tail washings
CN108658671A (en) * 2018-06-28 2018-10-16 靖西市秀美边城农业科技有限公司 A kind of preparation method being retained long-acting fructus crataegi pinnatifidae tree dedicated fertilizer
CN108911835A (en) * 2018-06-28 2018-11-30 靖西市秀美边城农业科技有限公司 A method of compound fertilizer is prepared using monosodium glutamate waste liquid
CN109988042A (en) * 2019-04-08 2019-07-09 齐鲁工业大学 A kind of method that utilizes monosodium glutamate waste liquid to manufacture organic fertilizer

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