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CN104405377B - Method and device for accurately simulating core under-pressure placing displacement in laboratories - Google Patents

Method and device for accurately simulating core under-pressure placing displacement in laboratories Download PDF

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CN104405377B
CN104405377B CN201410718929.8A CN201410718929A CN104405377B CN 104405377 B CN104405377 B CN 104405377B CN 201410718929 A CN201410718929 A CN 201410718929A CN 104405377 B CN104405377 B CN 104405377B
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displacement
core
valve
porosity
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CN104405377A (en
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张继成
位建成
陈新宇
匡力
郑灵芸
张军
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Northeast Petroleum University
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    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B49/00Testing the nature of borehole walls; Formation testing; Methods or apparatus for obtaining samples of soil or well fluids, specially adapted to earth drilling or wells
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/16Enhanced recovery methods for obtaining hydrocarbons

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Abstract

一种用于实验室内精确模拟岩心带压放置驱替的方法及其装置。主要为了解决目前在实验室内模拟岩心驱替时岩心在变形过程中的孔隙度易发生变化导致所获得的数据不准确的问题。该方法概括为:通过经验公式计算得出驱替时所需的合理驱替压力,根据孔隙度变化公式来计算保持孔隙度所需的环压和驱替压力,以保持岩心孔隙度不变,并保持岩心驱替过程中环压随驱替压力的变化而变化,使得其压差不变。设计了一个装置具有可调节温度的电加热岩心夹持器,在岩心夹持器出口端加回压阀,保持夹持器内始终有一定的压力,根据经验公式求得合理驱替压力,然后通过环压系统保持夹持器环压与驱替压力的压差不变,确保岩心在变形过程中的孔隙度不变。

A method and device for accurately simulating rock core displacement under pressure in a laboratory. The main purpose is to solve the problem that the porosity of the core is easy to change during the deformation process when simulating the core displacement in the laboratory, which leads to the inaccurate data obtained. The method is summarized as follows: Calculate the reasonable displacement pressure required for displacement through empirical formulas, calculate the ring pressure and displacement pressure required to maintain porosity according to the porosity change formula, so as to keep the core porosity unchanged, And keep the ring pressure changing with the displacement pressure during the core displacement process, so that the pressure difference remains unchanged. A device with an adjustable temperature electric heating core holder is designed, and a back pressure valve is added at the outlet end of the core holder to keep a certain pressure in the holder. According to the empirical formula, a reasonable displacement pressure is obtained, and then The pressure difference between the ring pressure of the holder and the displacement pressure is kept constant through the ring pressure system to ensure that the porosity of the core remains unchanged during the deformation process.

Description

用于实验室内精确模拟岩心带压放置驱替的方法及装置Method and device for accurately simulating rock core displacement under pressure in the laboratory

技术领域technical field

本发明涉及一种用于实验室内岩心带压放置驱替的方法及其装置,具体涉及一种在油田开发生产中对地层岩心进行更精确模拟实验的方法及装置。The invention relates to a method and a device for placing and displacing rock cores under pressure in a laboratory, in particular to a method and a device for performing more accurate simulation experiments on formation cores in oil field development and production.

背景技术Background technique

在油藏开发工程中,对岩心进行测试驱替实验一般都在实验室内进行。但是经过长时间的实际应用后,发现现有的测试驱替方法存在以下问题:目前实验室内常用的测试驱替方法只是对待测试岩心的一端加压注水和饱和油,加温放置后,然后直接进行测试实验。由此导致:1、在待测试岩心加温放置的过程中没有加压;2、仅对待测试岩心一端加高压可能造成岩心孔隙结构被破坏或者压裂;3、目前实验室内使用的恒温箱不能实现高温,因此也就难以模拟地层温度。以上三方面因素使得目前室内实验所获得的对岩心测试驱替实验的数据误差较大。In reservoir development engineering, testing and displacement experiments on cores are generally carried out in laboratories. However, after a long period of practical application, it was found that the existing test flooding method has the following problems: the test flooding method commonly used in the laboratory is only to inject water and saturated oil under pressure at one end of the test core, heat it and place it, and then Go straight to the test experiment. As a result: 1. There is no pressurization during the heating and placement of the core to be tested; 2. Only applying high pressure to one end of the core to be tested may cause the core pore structure to be damaged or fractured; 3. The constant temperature box currently used in the laboratory High temperature cannot be realized, so it is difficult to simulate formation temperature. The above three factors lead to large errors in the data of the core test and displacement experiments obtained in the laboratory experiments.

发明内容Contents of the invention

为了解决背景技术中所提到的技术问题,本发明提供一种实验室内模拟岩心带压放置驱替的方法及其装置。利用该方法和装置可以在驱替过程中岩心孔隙度保持不变,从而确保所获得的数据真实可靠。In order to solve the technical problems mentioned in the background technology, the present invention provides a method and a device for simulating rock core displacement under pressure in a laboratory. By using the method and device, the porosity of the rock core can be kept constant during the flooding process, thereby ensuring the authenticity and reliability of the obtained data.

本发明的技术方案是:该种用于实验室内精确模拟岩心带压放置驱替的装置,由第一恒压恒速泵、第二恒压恒速泵、第一活塞容器、第二活塞容器、流量计量器、电加热岩心夹持器、带有压力显示表的第一压力传感器和第二压力传感器、回压阀以及量筒组成。The technical solution of the present invention is: the device for accurately simulating the displacement of rock cores under pressure in the laboratory consists of a first constant pressure and constant speed pump, a second constant pressure and constant speed pump, a first piston container, a second piston The container is composed of a flow meter, an electric heating core holder, a first pressure sensor and a second pressure sensor with a pressure display gauge, a back pressure valve and a measuring cylinder.

其中,所述回压阀具有阀座和回压容器腔、进液口、出液口、活塞、弹簧以及弹簧调整旋钮,进液口和出液口位于回压容器腔内的液流通道两端,弹簧推动活塞沿回压容器腔的内腔向上运动,弹簧调整旋钮用于调整弹簧的弹性力。Wherein, the back pressure valve has a valve seat, a back pressure container chamber, a liquid inlet, a liquid outlet, a piston, a spring, and a spring adjustment knob, and the liquid inlet and the liquid outlet are located on two sides of the liquid flow channel in the back pressure container chamber. At the end, the spring pushes the piston to move upward along the inner cavity of the back pressure container cavity, and the spring adjustment knob is used to adjust the elastic force of the spring.

电加热岩心夹持器具有可封闭岩心的内腔,所述内腔外套有耐高温高压的胶套,所述内腔的两端通过带有密封塞的螺纹连接端封闭,并分别引出与所述内腔相连通的夹持器液流输入管和夹持器液流输出管;在所述两个螺纹连接端之间固定有密封的环形圆筒外壁和环形圆筒内壁;环形圆筒内壁与胶套之间形成第一环套空间,环形圆筒外壁与环形圆筒内壁之间形成第二环套空间,在第二环套空间内置有电加热器,电加热器的调温装置位于环形圆筒外壁之外;经密封处理后贯穿环形圆筒外壁和环形圆筒内壁,固定有一根环压导入管,环压导入管的开口位于第一环套空间内。The electric heating core holder has an inner cavity that can close the core, and the inner cavity is covered with a rubber sleeve resistant to high temperature and high pressure. The clamper liquid flow input pipe and the clamper liquid flow output pipe that are connected to the inner cavity; the outer wall of the annular cylinder and the inner wall of the annular cylinder that are sealed are fixed between the two threaded connection ends; the inner wall of the annular cylinder The first ring space is formed between the rubber sleeve and the second ring space is formed between the outer wall of the annular cylinder and the inner wall of the annular cylinder. An electric heater is built in the second ring space, and the temperature adjustment device of the electric heater is located at Outside the outer wall of the annular cylinder; through the outer wall of the annular cylinder and the inner wall of the annular cylinder after sealing treatment, a ring pressure introduction pipe is fixed, and the opening of the ring pressure introduction pipe is located in the space of the first ring sleeve.

第一恒压恒速泵的泵出口端经管路与并联的第一活塞容器和第二活塞容器的活塞驱动力入口端相连;第一活塞容器和第二活塞容器的两个内容物输出端分别经过第一阀门和第二阀门控制通断后经管路汇流至电加热岩心夹持器的夹持器液流输入管,在所述管路进入夹持器液流输入管之前,管路上连接有流量计量器和第三阀门;The pump outlet end of the first constant pressure and constant speed pump is connected to the piston driving force inlet port of the first piston container and the second piston container in parallel through the pipeline; the two content output ports of the first piston container and the second piston container are respectively After being controlled on and off by the first valve and the second valve, it flows into the holder liquid flow input pipe of the electric heating core holder through the pipeline. Before the pipeline enters the holder liquid flow input pipe, a flow rate is connected to the pipeline meter and third valve;

第二恒压恒速泵的泵出口端经管路与电加热岩心夹持器上的环压导入管相连接,在所述管路进入环压导入管之前,管路上连接有第一压力传感器和第四阀门;电加热岩心夹持器的夹持器液流输出管经管路与所述回压阀上的进液口相连接,在所述管路进入进液口之前,管路上连接有第二压力传感器和第五阀门;所述回压阀上的出液口与量筒相连接。The pump outlet end of the second constant pressure constant speed pump is connected with the ring pressure introduction pipe on the electric heating core holder through the pipeline, before the pipeline enters the ring pressure introduction pipe, the first pressure sensor and the first pressure sensor are connected on the pipeline. The fourth valve: the holder liquid flow output pipe of the electric heating core holder is connected with the liquid inlet on the back pressure valve through the pipeline, before the pipeline enters the liquid inlet, the pipeline is connected with the first Two pressure sensors and a fifth valve; the liquid outlet on the back pressure valve is connected with the measuring cylinder.

一种利用权利要求1中所述装置在实验室内精确模拟岩心带压放置驱替的方法,该方法由如下步骤组成:A method for accurately simulating the displacement of rock cores under pressure in a laboratory using the device described in claim 1, the method is composed of the following steps:

第一步,关闭权利要求1中所述装置内的所有阀门,检查装置的密封性;The first step is to close all valves in the device described in claim 1, and check the tightness of the device;

第二步,调节权利要求1中所述电加热岩心夹持器的温度至接近地层温度,通过温度传感器监测其温度变化,保持其温度始终在地层温度附近;The second step is to adjust the temperature of the electrically heated core holder described in claim 1 to be close to the formation temperature, monitor its temperature change through a temperature sensor, and keep its temperature near the formation temperature;

第三步,向权利要求1中所述装置内第一活塞容器A和第二活塞容器B中分别装入一定量的水和油,使油和水分别充满第一阀门、第二阀门和第三阀门之间的管线;In the third step, a certain amount of water and oil are respectively filled into the first piston container A and the second piston container B in the device described in claim 1, so that the oil and water are respectively filled with the first valve, the second valve and the second valve. The pipeline between the three valves;

第四步,通过驱替压力梯度与流速的关系式得驱替压力梯度区间为In the fourth step, the interval of the displacement pressure gradient is obtained through the relationship between the displacement pressure gradient and the flow rate:

(1) (1)

式中:——渗流速度,cm/s;——驱替压力梯度,Mpa/cm;——启动压力梯度,Mpa/cm;a、b、c——二次多项式系数,主要与流度有关,可通过拟合岩心压差—流速实验数据求得;In the formula: ——seepage velocity, cm/s; ——displacement pressure gradient, Mpa/cm; ——starting pressure gradient, Mpa/cm; a, b, c——quadratic polynomial coefficients, mainly related to fluidity, which can be obtained by fitting core pressure difference-flow velocity experimental data;

合理驱替压力为:(2),式中——岩心长度,单位m;The reasonable displacement pressure is: (2), where —core length, in m;

第五步,为保证岩石孔隙度不变,按照岩石弹性变形中孔隙度变化公式,确定出进行驱替实验时的合理环压Pc:In the fifth step, in order to keep the porosity of the rock unchanged, the reasonable ring pressure P c during the displacement experiment is determined according to the porosity change formula in the elastic deformation of the rock:

(3) (3)

上式就是岩石弹性变形过程中孔隙度变化公式;The above formula is the porosity change formula in the rock elastic deformation process;

由该式可知孔隙度绝对变化量与孔隙度本身、有效孔隙压缩系数和净围压(Pc—P)有关;From this formula, it can be seen that the absolute change of porosity is related to the porosity itself, the effective pore compressibility coefficient and the net confining pressure ( Pc - P );

若保持净围压不变,孔隙度也不变;反之,孔隙度将发生变化;因此,通过计算得出驱替压力P,在其合理范围内,随着其不断增大,环压Pc也不断变化,这样就可以保证岩心在合理带压驱替情况下进行试验;If the net confining pressure remains constant, the porosity will also remain unchanged; otherwise, the porosity will change; therefore, the displacement pressure P is obtained through calculation. Within its reasonable range, as it increases continuously, the ring pressure P c is also constantly changing, so that the core can be tested under reasonable pressure displacement conditions;

式中:Vp—岩石表观体积,m3;Vb—孔隙体积,m3;Cbp—拟表观体积压缩系数,1/Mpa;Cbc—表观体积压缩系数,1/Mpa;Cpp—有效孔隙压缩系数,1/Mpa;Cr—岩石骨架颗粒体积压缩系数,1/Mpa;Pc—上覆压力(环压),Mpa;P—流体压力(驱替压力),Mpa;In the formula: Vp—apparent volume of rock, m3; Vb—pore volume, m3; Cbp—pseudo-apparent volume compressibility, 1/Mpa; Cbc—apparent volume compressibility, 1/Mpa; Cpp—effective pore compressibility , 1/Mpa; Cr—volume compressibility coefficient of rock skeleton particles, 1/Mpa; Pc—overburden pressure (ring pressure), Mpa; P—fluid pressure (displacement pressure), Mpa;

第六步,对位于权利要求1中所述装置内电加热岩心夹持器(6)内的岩心进行饱和油实验,打开第四阀门和第一阀门,启动第二恒压恒速泵向电加热岩心夹持器内的第一环套空间加入环压;The sixth step is to conduct a saturated oil experiment on the core located in the electrically heated core holder (6) in the device described in claim 1, open the fourth valve and the first valve, and start the second constant pressure and constant speed pump to the electric Heating the first ring space in the core holder to add ring pressure;

第七步,按照第四步和第五步中所得出的数值,确定出进行驱替实验时保证岩心孔隙度不发生改变的净围压数值The seventh step, according to the values obtained in the fourth and fifth steps, determine the net confining pressure value to ensure that the core porosity does not change when the displacement experiment is carried out ;

第八步,启动权利要求1中所述装置中第一恒压恒速泵,调节压力至第四步所获得驱替压力值P的中间值P ,打开第二活塞容器对应的第二阀门;In the eighth step, start the first constant pressure and constant speed pump in the device described in claim 1, adjust the pressure to the middle value P of the displacement pressure value P obtained in the fourth step, and open the second valve corresponding to the second piston container ;

第九步,打开权利要求1中所述装置中的回压阀,调节弹簧调整旋钮,使得所述回压阀内的回压值等于由第八步所获得的驱替压力P ,开始饱和油实验;The ninth step is to open the back pressure valve in the device described in claim 1, adjust the spring adjustment knob, so that the back pressure value in the back pressure valve is equal to the displacement pressure P obtained in the eighth step, and start to saturate oil experiment;

第十步,饱和完毕后,整个权利要求1中所述装置不拆卸,关闭第一恒压恒速泵(1)和活塞容器B的阀门,关闭第三阀门和第五阀门,加压放置24h;The tenth step, after the saturation is completed, the device described in claim 1 is not disassembled, the first constant pressure constant speed pump (1) and the valve of the piston container B are closed, the third valve and the fifth valve are closed, and the pressure is placed for 24 hours ;

第十一步,启动权利要求1中所述装置中的恒速恒压泵,打开第一活塞容器的阀门,打开阀门4和阀门11,开始驱油实验;当驱油实验开始时,驱替压力P取值为中间值P,回压阀也调节至P,此时压力传感器检测到驱替压力变化,通过与环压传感器检测到的压力进行对比,为保持净围压不变,手动启动恒速恒压泵进行增压,环压Pc为Pc;由公式(3)知:若始终保持环压与驱替压力的差值不变,就可保证岩心的孔隙度不变;In the eleventh step, start the constant speed and constant pressure pump in the device described in claim 1, open the valve of the first piston container, open the valve 4 and the valve 11, and start the oil displacement experiment; when the oil displacement experiment starts, the displacement The pressure P is taken as the middle value P , and the back pressure valve is also adjusted to P. At this time , the pressure sensor detects the displacement pressure change. By comparing with the pressure detected by the ring pressure sensor, in order to keep the net confining pressure unchanged, Manually start the constant speed and constant pressure pump to pressurize, and the ring pressure Pc is in Pc; from the formula (3): if the difference between the ring pressure and the displacement pressure is kept constant, the porosity of the core can be guaranteed to remain unchanged;

因此,调节驱替压力P的值为P,回压阀调节至P,则环压也在不断调节至Pc。此时关闭加热器,保证岩心实验在接近真实地层温度,压力条件下进行;待排出液全部是水时,驱油实验完毕;Therefore, if the value of the displacement pressure P is adjusted to the P end , and the back pressure valve is adjusted to the P end , the ring pressure is also continuously adjusted to the Pc end . At this time, turn off the heater to ensure that the core test is carried out under the conditions of close to the real formation temperature and pressure; when the discharged liquid is all water, the oil displacement test is completed;

第十二步,按照第十一步循环操作,多次调节驱替压力P,环压Pc以及回压阀压力值,进行试验;In the twelfth step, according to the cyclic operation of the eleventh step, adjust the displacement pressure P, the ring pressure Pc and the pressure value of the back pressure valve several times, and conduct the test;

第十三步,根据流量计量器的计量结果以及量筒的计量结果,计算每个驱替压力P的试验数据:岩心含油饱和度和孔隙度,渗透率等参数,求其平均值。The thirteenth step, according to the measurement results of the flow meter and the measurement cylinder, calculate the test data of each displacement pressure P: parameters such as core oil saturation, porosity, permeability, etc., find the average value.

本发明具有如下有益效果:通过驱替压力梯度与流速的关系式计算得出岩心驱替时所需的合理驱替压力;在放置、驱替实验时在出口端加回压阀,保持岩心夹持器内压力和环压压力稳定;再根据岩心孔隙度与净围压的关系,保持岩心所受应力不变;调节电加热岩心夹持器的温度接近地层温度,使整个岩心处于接近地层高温高压的实际环境。通过流量计量器精确计量通过流体的量,准确计算岩心的物性参数。应用此方法,可减少岩心驱替时的驱替误差,使得实验环境更接近实际地层情况,获得更准确的实验数据。The present invention has the following beneficial effects: the reasonable displacement pressure required for core displacement can be obtained by calculating the relationship between displacement pressure gradient and flow velocity; The internal pressure and ring pressure of the holder are stable; according to the relationship between the porosity of the core and the net confining pressure, the stress on the core is kept constant; the temperature of the electric heating core holder is adjusted to be close to the formation temperature, so that the whole core is at a high temperature close to the formation High pressure real environment. The flow meter is used to accurately measure the amount of passing fluid, and accurately calculate the physical parameters of the core. Applying this method can reduce the displacement error during core displacement, make the experimental environment closer to the actual formation conditions, and obtain more accurate experimental data.

附图说明:Description of drawings:

图1是本发明的整体结构示意图。Fig. 1 is a schematic diagram of the overall structure of the present invention.

图2是本发明所述电加热岩心夹持器与第二恒压恒速泵连接后的结构示意图;Fig. 2 is the structure diagram after the electric heating core holder of the present invention is connected with the second constant pressure and constant speed pump;

图3是本发明所述回压阀的结构示意图;Fig. 3 is a schematic structural view of the back pressure valve of the present invention;

图4是本发明所述电加热岩心夹持器的结构示意图。Fig. 4 is a schematic structural view of the electric heating core holder of the present invention.

具体实施方式:detailed description:

下面结合附图对本发明作进一步说明:The present invention will be further described below in conjunction with accompanying drawing:

由图1所示,该种用于实验室内精确模拟岩心带压放置驱替的装置,由第一恒压恒速泵1、第二恒压恒速泵9、第一活塞容器 A 、第二活塞容器 B 、流量计量器5、电加热岩心夹持器6、带有压力显示表的第一压力传感器8和第二压力传感器10、回压阀以及量筒17组成。As shown in Figure 1, this kind of device for accurately simulating the displacement of rock cores under pressure in the laboratory consists of a first constant pressure and constant speed pump 1, a second constant pressure and constant speed pump 9, a first piston container A, a second Two piston containers B, a flow meter 5, an electric heating core holder 6, a first pressure sensor 8 and a second pressure sensor 10 with a pressure display gauge, a back pressure valve and a measuring cylinder 17 are composed.

其中,所述回压阀的结构如图3所示,具有阀座12和回压容器腔13、进液口18、出液口19、活塞 22 、弹簧 23 以及弹簧调整旋钮 20 ,进液口 18 和出液口 19 位于回压容器腔 13 内的液流通道两端,弹簧 23 推动活塞 22 沿回压容器腔 13 的内腔向上运动,弹簧调整旋钮 20 用于调整弹簧 23 的弹性力。具体实现时,可以采用上海禹沪公司的ZZY型自力式压力调节阀,无需外加能源,利用被调介质自身能量为动力源引入执行机构控制阀芯位置,改变两端的压差和流量,使阀前或阀后压力稳定。自力式压力调节阀具有动作灵敏,密封性好,压力设定点波动力小等优点,自力式压力调节阀广泛应用于气体、液体及介质稳压或泄压稳压的自动控制。Wherein, the structure of the back pressure valve as shown in Figure 3, has a valve seat 12 and a back pressure container cavity 13, a liquid inlet 18, a liquid outlet 19, a piston 22, a spring 23 and a spring adjustment knob 20, and the liquid inlet 18 and liquid outlet 19 are located at both ends of the liquid flow channel in the back pressure container cavity 13, the spring 23 pushes the piston 22 to move upward along the inner cavity of the back pressure container cavity 13, and the spring adjustment knob 20 is used to adjust the elastic force of the spring 23. In actual implementation, the ZZY type self-operated pressure regulating valve of Shanghai Yuhu Company can be used. No external energy is needed, and the energy of the regulated medium itself is used as the power source to introduce the actuator to control the position of the valve core, changing the pressure difference and flow at both ends, so that the valve Stable pressure before or after the valve. The self-operated pressure regulating valve has the advantages of sensitive action, good sealing, and small fluctuation of the pressure set point. The self-operated pressure regulating valve is widely used in the automatic control of gas, liquid and medium pressure stabilization or pressure relief.

电加热岩心夹持器6的结构如图4所示,具有可封闭岩心31的内腔,所述内腔外套有耐高温高压的胶套29,所述内腔的两端通过带有密封塞的螺纹连接端封闭,并分别引出与所述内腔相连通的夹持器液流输入管33和夹持器液流输出管21;在所述两个螺纹连接端之间固定有密封的环形圆筒外壁27和环形圆筒内壁32;环形圆筒内壁32与胶套29之间形成第一环套空间30,环形圆筒外壁27与环形圆筒内壁32之间形成第二环套空间28,在第二环套空间28内置有电加热器26,电加热器26的调温装置25位于环形圆筒外壁27之外;经密封处理后贯穿环形圆筒外壁27和环形圆筒内壁32,固定有一根环压导入管24,环压导入管24的开口位于第一环套空间30内。The structure of the electric heating core holder 6 is as shown in Figure 4. It has an inner cavity that can close the rock core 31. The inner cavity is covered with a rubber sleeve 29 resistant to high temperature and high pressure. The two ends of the inner cavity are provided with sealing plugs. The threaded connection end of the clamper is closed, and the holder liquid flow input pipe 33 and the holder liquid flow output pipe 21 that are connected with the inner cavity are drawn out respectively; a sealed annular ring is fixed between the two threaded connection ends. The outer wall 27 of the cylinder and the inner wall 32 of the annular cylinder; the first annulus space 30 is formed between the inner wall 32 of the annular cylinder and the rubber sleeve 29, and the second annulus space 28 is formed between the outer wall 27 of the annular cylinder and the inner wall 32 of the annular cylinder , an electric heater 26 is built in the second ring sleeve space 28, and the temperature regulating device 25 of the electric heater 26 is located outside the outer wall 27 of the annular cylinder; after being sealed, it penetrates the outer wall 27 of the annular cylinder and the inner wall 32 of the annular cylinder, A ring pressure introduction pipe 24 is fixed, and the opening of the ring pressure introduction pipe 24 is located in the first ring sleeve space 30 .

第一恒压恒速泵1的泵出口端经管路与并联的第一活塞容器A和第二活塞容器B的活塞驱动力入口端相连;第一活塞容器A和第二活塞容器B的两个内容物输出端分别经过第一阀门2和第二阀门3控制通断后经管路汇流至电加热岩心夹持器6的夹持器液流输入管33,在所述管路进入夹持器液流输入管33之前,管路上连接有流量计量器5和第三阀门4。The pump outlet end of the first constant pressure and constant speed pump 1 is connected to the piston driving force inlet port of the first piston container A and the second piston container B in parallel through the pipeline; The output end of the content is controlled on and off by the first valve 2 and the second valve 3 respectively, and then flows into the holder liquid flow input pipe 33 of the electric heating core holder 6 through the pipeline, and enters the holder liquid flow in the pipeline Before the input pipe 33, a flow meter 5 and a third valve 4 are connected to the pipeline.

如图2所示,第二恒压恒速泵9的泵出口端经管路与电加热岩心夹持器6上的环压导入管24相连接,在所述管路进入环压导入管24之前,管路上连接有第一压力传感器8和第四阀门7;As shown in Figure 2, the pump outlet end of the second constant pressure and constant speed pump 9 is connected with the ring pressure introduction pipe 24 on the electric heating core holder 6 through the pipeline, before the pipeline enters the ring pressure introduction pipe 24 , the pipeline is connected with a first pressure sensor 8 and a fourth valve 7;

电加热岩心夹持器6的夹持器液流输出管21经管路与所述回压阀上的进液口18相连接,在所述管路进入进液口18之前,管路上连接有第二压力传感器10和第五阀门11;The holder liquid flow output pipe 21 of the electric heating core holder 6 is connected with the liquid inlet 18 on the back pressure valve through the pipeline, and before the pipeline enters the liquid inlet 18, the pipeline is connected with the first Two pressure sensors 10 and a fifth valve 11;

所述回压阀上的出液口19与量筒17相连接。The liquid outlet 19 on the back pressure valve is connected with the measuring cylinder 17 .

该种利用所述装置在实验室内精确模拟岩心带压放置驱替的方法,由如下步骤组成:The method for accurately simulating the displacement of the core under pressure in the laboratory by using the device is composed of the following steps:

第一步,关闭所述装置内的所有阀门,检查装置的密封性;The first step is to close all valves in the device and check the tightness of the device;

第二步,调节电加热岩心夹持器6的温度至接近地层温度,通过温度传感器监测其温度变化,保持其温度始终在地层温度附近;In the second step, adjust the temperature of the electrically heated core holder 6 to be close to the formation temperature, monitor its temperature change through a temperature sensor, and keep its temperature near the formation temperature;

第三步,向第一活塞容器A和第二活塞容器B中分别装入一定量的水和油,使油和水分别充满第一阀门2、第二阀门3和第三阀门4之间的管线;In the third step, a certain amount of water and oil are respectively loaded into the first piston container A and the second piston container B, so that the oil and water are filled with the space between the first valve 2, the second valve 3 and the third valve 4 respectively. pipeline;

第四步,通过驱替压力梯度与流速的关系式,即公式(1):The fourth step is to use the relationship between displacement pressure gradient and flow rate, that is, formula (1):

(1) (1)

式中:——渗流速度,cm/s;——驱替压力梯度,Mpa/cm;a、b、c——二次多项式系数,主要与流度有关,通过拟合岩心压差—流速实验数据求得。根据岩心压差-流速实验数据拟合二次多项式系数,得出二次多项式系数统计如表1所示:In the formula: ——seepage velocity, cm/s; —displacement pressure gradient, Mpa/cm; a, b, c—quadratic polynomial coefficients, mainly related to mobility, obtained by fitting core pressure difference-velocity experimental data. According to the core pressure difference-velocity experimental data fitting quadratic polynomial coefficients, the statistics of quadratic polynomial coefficients are shown in Table 1:

表1Table 1

通过驱替压力梯度与启动压力的关系式,即公式(2):Through the relationship between the displacement pressure gradient and the threshold pressure, that is, formula (2):

(2) (2)

式中:——启动压力梯度,Mpa/cm;In the formula: ——Start-up pressure gradient, Mpa/cm;

合并(1)式和(2)式,得Combining formula (1) and formula (2), we get

(3) (3)

求解(3)式,得Solving formula (3), we get

(4) (4)

所以驱替压力梯度区间为So the displacement pressure gradient interval is

(5) (5)

所以合理驱替压力为:(6),式中——岩心长度,单位m;So the reasonable displacement pressure is: (6), where —core length, in m;

第五步,为保证岩心孔隙度不变,按照岩石弹性变形中孔隙度变化公式得:In the fifth step, in order to ensure that the porosity of the core remains unchanged, according to the porosity change formula in rock elastic deformation:

(7) (7)

(8)but (8)

(9)again (9)

(10) (10)

将式(8)、(9)代入(7)式得Substituting (8) and (9) into (7) to get

(11) (11)

根据Cbc、Cbp、Cpc、Cpp四个压缩系数之间的关系,将式(11)整理得According to the relationship between the four compression coefficients of Cbc, Cbp, Cpc, and Cpp, formula (11) can be sorted into

(12) (12)

上式就是岩石弹性变形过程中孔隙度变化公式。由该式可知孔隙度绝对变化量与孔隙度本身、有效空隙压缩系数和净围压(Pc—P)有关。若保持净围压不变,孔隙度也不变;反之,孔隙度将发生变化。因此,将第五步中的驱替压力P,带入(12)计算合理环压Pc区间。式中:Vp—岩石表观体积,m3;Vb—孔隙体积,m3;Cbp—拟表观体积压缩系数,1/Mpa;Cbc—表观体积压缩系数,1/Mpa;Cpp—有效孔隙压缩系数,1/Mpa;Cr—岩石骨架颗粒体积压缩系数,1/Mpa;Pc—上覆压力(环压),Mpa;P—流体压力(驱替压力),Mpa。The above formula is the porosity change formula in the rock elastic deformation process. It can be seen from this formula that the absolute change in porosity is related to the porosity itself, the effective pore compressibility and the net confining pressure (Pc-P). If the net confining pressure is kept constant, the porosity will also remain unchanged; otherwise, the porosity will change. Therefore, the displacement pressure P in the fifth step is brought into (12) to calculate the reasonable ring pressure Pc interval. In the formula: Vp—apparent volume of rock, m3; Vb—pore volume, m3; Cbp—pseudo-apparent volume compressibility, 1/Mpa; Cbc—apparent volume compressibility, 1/Mpa; Cpp—effective pore compressibility , 1/Mpa; Cr—volume compressibility coefficient of rock skeleton particles, 1/Mpa; Pc—overburden pressure (ring pressure), Mpa; P—fluid pressure (displacement pressure), Mpa.

第六步,对位于电加热岩心夹持器(6)内的岩心(31)进行饱和油实验,打开第四阀门(7)和第一阀门(2),启动第二恒压恒速泵(9)向电加热岩心夹持器(6)内的第一环套空间(30)加入环压;The sixth step is to conduct saturated oil experiment on the core (31) located in the electric heating core holder (6), open the fourth valve (7) and the first valve (2), and start the second constant pressure and constant speed pump ( 9) Add ring pressure to the first ring space (30) in the electrically heated core holder (6);

第七步,按照第四步和第五步中所得出的数值,确定出进行驱替实验时保证岩心孔隙度不发生改变的净围压数值The seventh step, according to the values obtained in the fourth and fifth steps, determine the net confining pressure value to ensure that the core porosity does not change when the displacement experiment is carried out .

第八步,启动第一恒压恒速泵(1),调节压力至第四步所获得驱替压力值P的中间值P ,打开第二活塞容器(B)对应的第二阀门(3);In the eighth step, start the first constant pressure and constant speed pump (1), adjust the pressure to the middle value P of the displacement pressure value P obtained in the fourth step, and open the second valve (3) corresponding to the second piston container (B) );

第九步,打开所述回压阀,调节弹簧调整旋钮(20),使得所述回压阀内的回压值等于由第八步所获得的驱替压力P ,开始饱和油实验;In the ninth step, open the back pressure valve, adjust the spring adjustment knob (20), so that the back pressure value in the back pressure valve is equal to the displacement pressure P obtained in the eighth step, and start the saturated oil experiment;

第十步,饱和完毕后,整个装置不拆卸,关闭恒速恒压泵1和活塞容器B的阀门3,关闭阀门4和阀门11,加压放置24h;The tenth step, after the saturation is completed, the whole device is not disassembled, close the valve 3 of the constant speed and constant pressure pump 1 and the piston container B, close the valve 4 and valve 11, and place it under pressure for 24 hours;

第十一步,启动恒速恒压泵1,打开活塞容器A的阀门2,打开阀门4和阀门11,开始驱油实验。当驱油实验开始时,驱替压力P取值为中间值P,回压阀也调节至P,此时压力传感器检测到驱替压力变化,通过与环压传感器检测到的压力进行对比,为保持净围压不变,手动启动恒速恒压泵进行增压,环压Pc为Pc;由公式(12)知:若始终保持环压与驱替压力的差值不变,就可保证岩心的孔隙度不变。因此,调节驱替压力P的值为P,回压阀调节至P,则环压也在不断调节至Pc。此时关闭加热器,保证岩心实验在接近真实地层温度,压力条件下进行。待排出液全部是水时,驱油实验完毕。In the eleventh step, start the constant speed and constant pressure pump 1, open the valve 2 of the piston container A, open the valve 4 and the valve 11, and start the oil displacement experiment. When the oil displacement experiment starts, the displacement pressure P takes the middle value P , and the back pressure valve is also adjusted to P. At this time , the pressure sensor detects the displacement pressure change, and compares it with the pressure detected by the ring pressure sensor. , in order to keep the net confining pressure unchanged, the constant-speed constant-pressure pump is manually started to pressurize, and the ring pressure Pc is in Pc; from the formula (12): if the difference between the ring pressure and the displacement pressure is kept constant, then It can ensure that the porosity of the core remains unchanged. Therefore, if the value of the displacement pressure P is adjusted to the P end , and the back pressure valve is adjusted to the P end , the ring pressure is also continuously adjusted to the Pc end . Turn off the heater at this time to ensure that the core experiment is carried out under conditions close to the real formation temperature and pressure. When the discharged liquid is all water, the oil displacement experiment is completed.

第十二步, 按照第十一步循环操作,多次调节驱替压力P,环压Pc,回压阀压力值,进行试验。The twelfth step, according to the cyclical operation of the eleventh step, adjust the displacement pressure P, the ring pressure Pc, and the pressure value of the back pressure valve several times, and carry out the test.

第十三步,根据流量计量器的计量结果以及量筒的计量结果,计算每个驱替压力P的试验数据:岩心含油饱和度和孔隙度,渗透率等参数,求其平均值。The thirteenth step, according to the measurement results of the flowmeter and the measurement cylinder, calculate the test data of each displacement pressure P: parameters such as core oil saturation, porosity, permeability, etc., calculate the average value.

下面按照上述实施方案给出实验实例:Provide experimental example below according to above-mentioned embodiment scheme:

按照上述步骤连接实验装置,人造均质,2.5cm×2.5cm×50cm,有效渗透率为500mD。,测量岩心的孔渗数据。Connect the experimental device according to the above steps, artificial homogeneity, 2.5cm×2.5cm×50cm, effective permeability 500mD. , to measure the porosity and permeability data of the core.

第一步,关闭权利要求1中所述装置内的所有阀门,检查装置的密封性;The first step is to close all valves in the device described in claim 1, and check the tightness of the device;

第二步,调节电加热岩心夹持器 6 的温度至接近地层温度,通过温度传感器监测其温度变化,保持其温度始终在地层温度附近;The second step is to adjust the temperature of the electrically heated core holder 6 to be close to the formation temperature, monitor its temperature change through a temperature sensor, and keep its temperature close to the formation temperature;

第三步,向第一活塞容器 A 和第二活塞容器 B 中分别装入一定量的水和油,使油和水分别充满第一阀门 2 、第二阀门 3 和第三阀门 4 之间的管线;The third step is to put a certain amount of water and oil into the first piston container A and the second piston container B respectively, so that the oil and water fill the space between the first valve 2, the second valve 3 and the third valve 4 respectively. pipeline;

第四步,通过驱替压力梯度与流速的关系式,即公式(1):The fourth step is to use the relationship between displacement pressure gradient and flow rate, that is, formula (1):

(1) (1)

式中:——渗流速度,cm/s;——驱替压力梯度,Mpa/cm;a、b、c——二次多项式系数,主要与流度有关,通过拟合岩心压差—流速实验数据求得。根据岩心压差-流速实验数据拟合二次多项式系数,得出二次多项式系数统计表如下:In the formula: ——seepage velocity, cm/s; —displacement pressure gradient, Mpa/cm; a, b, c—quadratic polynomial coefficients, mainly related to mobility, obtained by fitting core pressure difference-velocity experimental data. According to the core pressure difference-velocity experimental data fitting quadratic polynomial coefficients, the statistical table of quadratic polynomial coefficients is obtained as follows:

通过驱替压力梯度与启动压力的关系式,即公式(2):Through the relationship between the displacement pressure gradient and the threshold pressure, that is, formula (2):

(2) (2)

式中:——启动压力梯度,Mpa/cm;In the formula: ——Start-up pressure gradient, Mpa/cm;

合并(1)式和(2)式,得Combining formula (1) and formula (2), we get

(3) (3)

求解(3)式,得Solving formula (3), we get

(4) (4)

所以驱替压力梯度区间为So the displacement pressure gradient interval is

(5) (5)

所以合理驱替压力为:(6),式中——岩心长度,单位m;So the reasonable displacement pressure is: (6), where —core length, in m;

所以合理驱替压力为;式中——岩心长度,m。So the reasonable displacement pressure is ; where —core length, m.

第五步,为保证岩石空隙度不变,按照岩石弹性变形中孔隙度变化公式得:In the fifth step, in order to ensure that the rock porosity remains unchanged, according to the porosity change formula in rock elastic deformation:

(7) (7)

(8)but (8)

(9)again (9)

(10) (10)

将式(8)、(9)代入(7)式得Substituting (8) and (9) into (7) to get

(11) (11)

根据Cbc、Cbp、Cpc、Cpp四个压缩系数之间的关系,将式(11)整理得According to the relationship between the four compression coefficients of Cbc, Cbp, Cpc, and Cpp, formula (11) can be sorted into

(12) (12)

由上述步骤计算得岩心体积为,驱动压力,则计算得出合理环压。由上式可知孔隙度绝对变化量与孔隙度本身、有效空隙压缩系数和净围压(Pc—P)有关。若保持净围压不变,孔隙度也不变;反之,孔隙度将发生变化。因此,通过计算得出驱替压力,在其合理范围内;环压,这样就可以保证岩心在合理带压驱替情况下进行试验。The core volume calculated by the above steps is , driving pressure , then the reasonable ring pressure can be calculated . It can be seen from the above formula that the absolute change of porosity is related to the porosity itself, the effective void compressibility coefficient and the net confining pressure (Pc-P). If the net confining pressure is kept constant, the porosity will also remain unchanged; otherwise, the porosity will change. Therefore, the displacement pressure is calculated by , within its reasonable range; ring pressure , so that the core can be tested under reasonable pressure displacement conditions.

第七步,按照第五步和第六步中所得出的数值,确定出进行驱替实验时保证岩心孔隙度不发生改变的净围压数值为4.8Mpa。In the seventh step, according to the values obtained in the fifth and sixth steps, it is determined that the net confining pressure value for ensuring that the core porosity does not change during the displacement experiment is 4.8Mpa.

第八步,启动第一恒压恒速泵1,调节压力至第五步所获得驱替压力值P范围内,打开第二活塞容器 B 对应的第二阀门3;In the eighth step, start the first constant pressure and constant speed pump 1, adjust the pressure to within the range of the displacement pressure value P obtained in the fifth step, and open the second valve 3 corresponding to the second piston container B;

第九步,打开所述回压阀,调节弹簧调整旋钮20,使得所述回压阀内的回压等于由第七步所获得的净围压,开始饱和油实验;In the ninth step, open the back pressure valve, adjust the spring adjustment knob 20, so that the back pressure in the back pressure valve is equal to the net confining pressure obtained in the seventh step, and start the saturated oil experiment;

第十步,饱和完毕后,整个装置不拆卸,关闭恒速恒压泵1和活塞容器B的阀门3,关闭阀门4和阀门11,加压放置24h,此时使岩心压力值与计算压力值一致;The tenth step, after the saturation is completed, the whole device is not disassembled, close the valve 3 of the constant speed and constant pressure pump 1 and the piston container B, close the valve 4 and valve 11, and place it under pressure for 24 hours. At this time, the core pressure value and the calculated pressure value consistent;

第十一步,启动恒速恒压泵1,打开活塞容器A的阀门2,打开阀门4和阀门11,开始驱油实验。当驱油实验开始时,驱替压力P取值为中间值,回压阀也调节至,此时压力传感器检测到驱替压力变化,通过与环压传感器检测到的压力进行对比,为保持净围压不变,手动启动恒速恒压泵进行增压,环压Pc为;由公式(12)知:若始终保持环压与驱替压力的差值不变,就可保证岩心的孔隙度不变。因此,调节驱替压力P的值为,回压阀调节至,则环压也在不断调节至。此时关闭加热器,保证岩心实验在接近真实地层温度,压力条件下进行。待排出液全部是水时,驱油实验完毕。In the eleventh step, start the constant speed and constant pressure pump 1, open the valve 2 of the piston container A, open the valve 4 and the valve 11, and start the oil displacement experiment. When the oil displacement experiment starts, the displacement pressure P takes an intermediate value , the back pressure valve is also adjusted to , at this time, the pressure sensor detects the change of displacement pressure. By comparing with the pressure detected by the ring pressure sensor, in order to keep the net confining pressure unchanged, the constant speed and constant pressure pump is manually started to increase the pressure. The ring pressure Pc is ; According to the formula (12): if the difference between the annular pressure and the displacement pressure is kept constant, the porosity of the core can be guaranteed to be constant. Therefore, the value of adjusting the displacement pressure P is , the back pressure valve is adjusted to , the ring pressure is constantly adjusted to . Turn off the heater at this time to ensure that the core experiment is carried out under conditions close to the real formation temperature and pressure. When the discharged liquid is all water, the oil displacement experiment is completed.

第十二步,按照第十一步循环操作,多次调节驱替压力P,环压Pc,回压阀压力值,进行试验。In the twelfth step, follow the cyclic operation of the eleventh step, adjust the displacement pressure P, the ring pressure Pc, and the pressure value of the back pressure valve several times, and carry out the test.

第十三步,根据流量计量器的计量结果以及量筒的计量结果,计算岩心渗透率和孔隙度等参数。为测得更精确的孔渗数据,按照上述实验步骤和操作方法做多组实验,求得其实验的平均渗透率0.0051um2和孔隙度0.15数据。而其它室内实验测得渗透率为0.0045um2,孔隙度为0.13,误差为11.76%,13.33%,该实验方法和装置测得实验数据更精确可靠。In the thirteenth step, parameters such as core permeability and porosity are calculated according to the measurement results of the flow meter and the measuring cylinder. In order to measure more accurate porosity and permeability data, several sets of experiments were done according to the above-mentioned experimental procedures and operation methods, and the data of the average permeability of 0.0051um 2 and porosity of 0.15 were obtained. While the permeability measured by other indoor experiments is 0.0045um 2 , the porosity is 0.13, and the error is 11.76%, 13.33%. The experimental data obtained by this experimental method and device are more accurate and reliable.

Claims (1)

1.一种在实验室内精确模拟岩心带压放置驱替的方法,该方法由如下步骤组成:1. A method for accurately simulating rock core displacement under pressure in a laboratory, the method consists of the following steps: 第一步,关闭模拟岩心带压放置驱替装置内的所有阀门,检查装置的密封性;The first step is to close all the valves in the pressure-placed displacement device of the simulated core, and check the tightness of the device; 第二步,调节模拟岩心带压放置驱替装置内电加热岩心夹持器(6)的温度至接近地层温度,通过温度传感器监测其温度变化,保持其温度始终在地层温度附近;The second step is to adjust the temperature of the electrically heated core holder (6) in the displacement device under pressure for the simulated core to be close to the formation temperature, monitor its temperature change through a temperature sensor, and keep its temperature near the formation temperature; 第三步,向模拟岩心带压放置驱替装置内第一活塞容器(A)和第二活塞容器(B)中分别装入一定量的水和油,使油和水分别充满第一阀门(2)、第二阀门(3)和第三阀门(4)之间的管线;In the third step, a certain amount of water and oil are respectively filled into the first piston container (A) and the second piston container (B) in the simulated rock core displacement device under pressure, so that the oil and water are respectively filled with the first valve ( 2), the pipeline between the second valve (3) and the third valve (4); 第四步,通过驱替压力梯度与流速的关系式得驱替压力梯度区间为In the fourth step, the interval of the displacement pressure gradient is obtained through the relationship between the displacement pressure gradient and the flow rate: KK μμ -- bb -- [[ bb -- KK μμ ]] 22 -- 44 aa [[ cc ++ KK μμ GG ]] 22 aa ≤≤ ΔΔ pp ≤≤ KK μμ -- bb ++ [[ bb -- KK μμ ]] 22 -- 44 aa [[ cc ++ KK μμ GG ]] 22 aa -- -- -- (( 11 )) 式中:K-岩心渗透率,10-3μm2;μ-流体粘度,mpa·s;△p-驱替压力梯度,Mpa/cm;G-启动压力梯度,Mpa/cm;a、b、c-二次多项式系数,主要与流度有关,可通过拟合岩心压差—流速实验数据求得;In the formula: K-core permeability, 10 -3 μm 2 ; μ-fluid viscosity, mpa s; △p-displacement pressure gradient, Mpa/cm; G-threshold pressure gradient, Mpa/cm; a, b, c-quadratic polynomial coefficient, mainly related to fluidity, can be obtained by fitting core pressure difference-velocity experimental data; 合理驱替压力为:p=△p·l(2),式中l-岩心长度,单位m;Reasonable displacement pressure is: p=△p·l(2), where l-core length, unit m; 第五步,为保证岩石孔隙度不变,按照岩石弹性变形中孔隙度变化公式,确定出进行驱替实验时的合理环压Pc:In the fifth step, in order to ensure that the rock porosity remains unchanged, the reasonable ring pressure Pc for the displacement experiment is determined according to the porosity change formula in rock elastic deformation: 上式就是岩石弹性变形过程中孔隙度变化公式;The above formula is the porosity change formula in the rock elastic deformation process; 由该式可知孔隙度绝对变化量与孔隙度本身、有效孔隙压缩系数和净围压(Pc-P)有关;From this formula, it can be seen that the absolute variation of porosity is related to porosity itself, effective pore compressibility and net confining pressure (Pc-P); 若保持净围压不变,孔隙度也不变;反之,孔隙度将发生变化;因此,通过计算得出驱替压力P,在其合理范围内,随着其不断增大,环压Pc也不断变化,这样就可以保证岩心在合理带压驱替情况下进行试验;If the net confining pressure remains constant, the porosity will also remain unchanged; otherwise, the porosity will change; therefore, the displacement pressure P is obtained through calculation. Within its reasonable range, as it continues to increase, the ring pressure Pc will also increase. Constantly changing, so that the core can be tested under reasonable pressure displacement conditions; 式中:Cpp—有效孔隙压缩系数,1/Mpa;Cr—岩石骨架颗粒体积压缩系数,1/Mpa;Pc—上覆压力,Mpa;P—流体压力,Mpa;In the formula: Cpp—effective pore compressibility, 1/Mpa; Cr—volume compressibility of rock skeleton particles, 1/Mpa; Pc—overburden pressure, Mpa; P—fluid pressure, Mpa; 第六步,对位于模拟岩心带压放置驱替装置内电加热岩心夹持器(6)内的岩心(31)进行饱和油实验,打开第四阀门(7)和第一阀门(2),启动第二恒压恒速泵(9)向电加热岩心夹持器(6)内的第一环套空间(30)加入环压;In the sixth step, the saturated oil experiment is carried out on the rock core (31) located in the electrically heated core holder (6) of the simulated rock core displacement device under pressure, and the fourth valve (7) and the first valve (2) are opened, Start the second constant pressure and constant speed pump (9) to add ring pressure to the first ring space (30) in the electric heating core holder (6); 第七步,按照第四步和第五步中所得出的数值,确定出进行驱替实验时保证岩心孔隙度不发生改变的净围压数值(pc-p);In the seventh step, according to the values obtained in the fourth and fifth steps, determine the net confining pressure value (p c -p) that ensures that the core porosity does not change when the displacement experiment is carried out; 第八步,启动模拟岩心带压放置驱替装置中第一恒压恒速泵(1),调节压力至第四步所获得驱替压力值P的中间值P,打开第二活塞容器(B)对应的第二阀门(3);In the eighth step, start the simulated rock core under pressure and place the first constant pressure constant speed pump (1) in the displacement device, adjust the pressure to the middle value P of the displacement pressure value P obtained in the fourth step, and open the second piston container ( B) the corresponding second valve (3); 第九步,打开模拟岩心带压放置驱替装置中的回压阀,调节弹簧调整旋钮(20),使得所述回压阀内的回压值等于由第八步所获得的驱替压力P,开始饱和油实验;In the ninth step, open the back pressure valve in the displacement device under pressure of the simulated rock core, adjust the spring adjustment knob (20), so that the back pressure value in the back pressure valve is equal to the displacement pressure P obtained in the eighth step , start the saturated oil experiment; 第十步,饱和完毕后,整个模拟岩心带压放置驱替装置不拆卸,关闭第一恒压恒速泵(1)和活塞容器B的阀门,关闭第三阀门(4)和第五阀门(11),加压放置24h;In the tenth step, after the saturation is completed, the whole simulated rock core is placed under pressure and the displacement device is not disassembled, and the first constant pressure and constant speed pump (1) and the valve of the piston container B are closed, and the third valve (4) and the fifth valve ( 11), placed under pressure for 24 hours; 第十一步,启动模拟岩心带压放置驱替装置中的第一恒压恒速泵,打开第一活塞容器(A)的阀门,打开第三阀门(4)和第五阀门(11),开始驱油实验;当驱油实验开始时,驱替压力P取值为中间值P,回压阀也调节至P,此时压力传感器检测到驱替压力变化,通过与环压传感器检测到的压力进行对比,为保持净围压不变,手动启动第二恒压恒速泵进行增压,环压Pc为Pc;由公式(3)知:若始终保持环压与驱替压力的差值不变,就可保证岩心的孔隙度不变;In the eleventh step, start the first constant-pressure and constant-speed pump in the pressure-placed displacement device of the simulated rock core, open the valve of the first piston container (A), open the third valve (4) and the fifth valve (11), Start the oil displacement experiment; when the oil displacement experiment starts, the displacement pressure P is the middle value P , and the back pressure valve is also adjusted to P , at this time, the pressure sensor detects the displacement pressure change, and the displacement pressure is detected by the ring pressure sensor. In order to keep the net confining pressure unchanged, the second constant pressure and constant speed pump is manually started to increase the pressure, and the ring pressure Pc is in Pc; from the formula (3): if the ring pressure and the displacement pressure are always kept The difference between the two values remains unchanged, which can ensure that the porosity of the core remains unchanged; 因此,调节驱替压力P的值为P,回压阀调节至P,则环压也在不断调节至Pc,此时关闭加热器,保证岩心实验在接近真实地层温度,压力条件下进行;待排出液全部是水时,驱油实验完毕;Therefore, adjust the value of the displacement pressure P to the P end , adjust the back pressure valve to the P end , and then adjust the ring pressure to the Pc end continuously. At this time, turn off the heater to ensure that the core test is close to the real formation temperature and pressure. Carry out; when the discharged liquid is all water, the oil displacement experiment is completed; 第十二步,按照第十一步循环操作,多次调节驱替压力P,环压Pc以及回压阀压力值,进行试验;In the twelfth step, according to the cyclic operation of the eleventh step, adjust the displacement pressure P, the ring pressure Pc and the pressure value of the back pressure valve several times, and carry out the test; 第十三步,根据流量计量器的计量结果以及量筒的计量结果,计算每个驱替压力P的试验数据,包括岩心含油饱和度、孔隙度和渗透率参数,求其平均值。In the thirteenth step, according to the measurement results of the flowmeter and the measuring cylinder, calculate the test data of each displacement pressure P, including the core oil saturation, porosity and permeability parameters, and calculate the average value.
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