CN104194429B - A kind of acrylate zero diopter exterior coating - Google Patents
A kind of acrylate zero diopter exterior coating Download PDFInfo
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- CN104194429B CN104194429B CN201410482749.4A CN201410482749A CN104194429B CN 104194429 B CN104194429 B CN 104194429B CN 201410482749 A CN201410482749 A CN 201410482749A CN 104194429 B CN104194429 B CN 104194429B
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- acrylate
- exterior coating
- zero diopter
- coating
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- 238000000576 coating method Methods 0.000 title claims abstract description 35
- 239000011248 coating agent Substances 0.000 title claims abstract description 34
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 title claims abstract description 16
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 29
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims abstract description 21
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000000126 substance Substances 0.000 claims abstract description 11
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims abstract description 10
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000008367 deionised water Substances 0.000 claims abstract description 10
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 10
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 10
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims abstract description 9
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229920003063 hydroxymethyl cellulose Polymers 0.000 claims abstract description 7
- 229940031574 hydroxymethyl cellulose Drugs 0.000 claims abstract description 7
- 239000003112 inhibitor Substances 0.000 claims abstract description 6
- 239000004014 plasticizer Substances 0.000 claims abstract description 6
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 4
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 4
- WSFQLUVWDKCYSW-UHFFFAOYSA-M sodium;2-hydroxy-3-morpholin-4-ylpropane-1-sulfonate Chemical compound [Na+].[O-]S(=O)(=O)CC(O)CN1CCOCC1 WSFQLUVWDKCYSW-UHFFFAOYSA-M 0.000 claims description 8
- CJFLBOQMPJCWLR-UHFFFAOYSA-N bis(6-methylheptyl) hexanedioate Chemical compound CC(C)CCCCCOC(=O)CCCCC(=O)OCCCCCC(C)C CJFLBOQMPJCWLR-UHFFFAOYSA-N 0.000 claims description 4
- 239000000020 Nitrocellulose Substances 0.000 claims 1
- FJWGYAHXMCUOOM-QHOUIDNNSA-N [(2s,3r,4s,5r,6r)-2-[(2r,3r,4s,5r,6s)-4,5-dinitrooxy-2-(nitrooxymethyl)-6-[(2r,3r,4s,5r,6s)-4,5,6-trinitrooxy-2-(nitrooxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-3,5-dinitrooxy-6-(nitrooxymethyl)oxan-4-yl] nitrate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O)O[C@H]1[C@@H]([C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@@H](CO[N+]([O-])=O)O1)O[N+]([O-])=O)CO[N+](=O)[O-])[C@@H]1[C@@H](CO[N+]([O-])=O)O[C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O FJWGYAHXMCUOOM-QHOUIDNNSA-N 0.000 claims 1
- 229920001220 nitrocellulos Polymers 0.000 claims 1
- 229940079938 nitrocellulose Drugs 0.000 claims 1
- 238000005187 foaming Methods 0.000 abstract description 8
- 239000000463 material Substances 0.000 abstract description 8
- 230000001680 brushing effect Effects 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 6
- 239000003513 alkali Substances 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000000498 ball milling Methods 0.000 description 14
- 239000003973 paint Substances 0.000 description 9
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 8
- 239000001361 adipic acid Substances 0.000 description 4
- 235000011037 adipic acid Nutrition 0.000 description 4
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 102000004895 Lipoproteins Human genes 0.000 description 3
- 108090001030 Lipoproteins Proteins 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 3
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 230000005587 bubbling Effects 0.000 description 2
- 238000005034 decoration Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000002283 diesel fuel Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 1
- 239000003502 gasoline Substances 0.000 description 1
- 239000003350 kerosene Substances 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000001846 repelling effect Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
A kind of acrylate zero diopter exterior coating, its raw materials by weight portion proportioning is as follows: acrylic resin soln 100 parts；NC Nitroncellulose 20 40 parts；Styrene 20 30 parts；Tricresyl phosphate 5 10 parts；Rubber chemicals 25 45 parts；Ethyl acetate 5 15 parts；Methacrylic acid 10 20 parts；15 20 parts of plasticizer；MS 1 emulsifying agent 15 25 parts；Butyl acetate 5 25 parts；Deionized water 50 60 parts；Mould inhibitor 10 20 parts；Hydroxymethyl cellulose 25 35 parts；Toluene 30 40 parts；Product viscosity 120 150s, does not lumps；Surface drying time 1 2h, soaks nothing foaming, dry linting phenomenon after 15 25d in water；Alkali resistance is good, soaks that 48 72h are non-foaming, comes off in buck；Film brushing resistance 1,500 1800 times, can be with the widespread production not division of history into periods for current material.
Description
Technical field
The application belongs to paint field, particularly relates to a kind of acrylate zero diopter exterior coating.
Background technology
Coating, at the entitled paint of Chinese tradition.So-called coating is to be coated in be protected or filled
The body surface of decorations, and can be with the continuous film of coated article formation firm attachment, it is common that with tree
Fat or oil or emulsion are main, add or without pigment, filler, add corresponding additive,
With the formulated thick liquid of organic solvent or rubber chemicals.China's coating circle is more authoritative
" coating process " book is defined such that " coating is a kind of material, and this material is permissible
Be coated in object surface by different construction technologies, formed adhere to firmly, have some strength,
Continuous print solid film.The film common name film so formed, also known as paint film or coating." coating
Cover with paint, lacquer, colour wash, etc. and can very well bond with matrix material in body surface and form complete and tough and tensile diaphragm
Material, referred to as coating.Coating and paint are identical concepts.Paint is people's habits used for a long time
Used title, after introducing China, utilizes in building trade the most always.The effect of coating can be general
Including is three aspects: protective effect, decoration function, specific function effect.General group of coating
Become: comprise film forming matter, color stuffing, solvent, auxiliary agent.
China's paint industry grows stronger day by day under the promotion of downstream industry, and as one of them point
The building coating propped up, have also been obtained significant progress.Statistics shows, China in 2011
Building coating amounts to yield about 351.82 ten thousand tons, increases by more than 30% on a year-on-year basis.As can be seen here,
Although Chinese architecture paint industry experienced by the impact of global financial crisis in 2008, former material
Material rise in price and Central Bank increase the interest the pressure brought, but its growth momentum does not subtracts, and also protect
Hold higher growth rate.Coating is thickness oil colour, the most dry in the case of inflammable, do not dissolve in
Water, is slightly soluble in fat, dissolves in alcohol, aldehyde, ether, benzene, alkane, be soluble in gasoline, kerosene,
Diesel oil.
Exterior coating, for brushing the outer wall face of building, so a most important index
It is exactly ultraviolet radiation resisting, it is desirable to reach to irradiate for a long time nondiscolouring.Exterior coating has also required
Water repelling property, it is desirable to have from washing property.Paint film wants hard and smooth, dirty once rushing.Exterior wall is coated with
Material can be used for interior wall brushing and use and be because it and also have a water resisting property energy；And interior wall coating does not has
Standby anti-solarization function, so can not use interior wall coating when exterior coating.And along with humanity concept
Universal, and the composition of novel harmonious society, design a kind of viscosity high short and excellent water resistance
Acrylate zero diopter exterior coating is very important.
Summary of the invention
Solve the technical problem that:
The application is for above-mentioned technical problem, it is provided that a kind of acrylate zero diopter exterior coating, solves
Certainly existing acrylate zero diopter exterior coating resistance to water and viscosity is low, length drying time, be weak to brush
The technical problem such as wash.
Technical scheme:
A kind of acrylate zero diopter exterior coating, the raw material of described acrylate zero diopter exterior coating
Proportioning by weight is as follows: acrylic resin soln 100 parts；NC Nitroncellulose 20-40 part；
Styrene 20-30 part；Tricresyl phosphate 5-10 part；Rubber chemicals 25-45 part；Acetic acid
Ethyl ester 5-15 part；Methacrylic acid 10-20 part；Plasticizer 15-20 part；MS-1 emulsifying agent
15-25 part；Butyl acetate 5-25 part；Deionized water 50-60 part；Mould inhibitor 10-20 part；
Hydroxymethyl cellulose 25-35 part；Toluene 30-40 part.
As a preferred technical solution of the present invention: described acrylate zero diopter exterior coating
Raw materials by weight portion proportioning is as follows: acrylic resin soln 100 parts；NC Nitroncellulose 30
Part；Styrene 25 parts；Tricresyl phosphate 8 parts；Rubber chemicals 35 parts；Ethyl acetate
10 parts；Methacrylic acid 15 parts；17 parts of plasticizer；MS-1 emulsifying agent 20 parts；Acetic acid fourth
Ester 15 parts；Deionized water 55 parts；Mould inhibitor 15 parts；Hydroxymethyl cellulose 30 parts；Toluene
35 parts.
As a preferred technical solution of the present invention: described plasticizer uses adipic acid two different pungent
Ester.
As a preferred technical solution of the present invention: described mould inhibitor uses zinc naphthenate.
Beneficial effect:
A kind of acrylate zero diopter exterior coating of the present invention uses above technical scheme with existing
There is technology to compare, have following technical effect that 1, product viscosity 120-150s, in a reservoir
Do not lump；2, surface drying time 1-2h, soak after 15-25d without bubbling in water, dry linting existing
As；3, alkali resistance is good, soaks that 48-72h is non-foaming, come off in buck；4, film is resistance to
Scrubbability 1500-1800 time, can be with the widespread production not division of history into periods for current material.
Detailed description of the invention
Embodiment 1:
A kind of acrylate zero diopter exterior coating, its raw materials by weight portion proportioning is as follows: propylene
Acid resin solution 100 parts；NC Nitroncellulose 20 parts；Styrene 20 parts；Tricresyl phosphate
5 parts；Rubber chemicals 25 parts；Ethyl acetate 5 parts；Methacrylic acid 10 parts；Adipic acid two
Different monooctyl ester 15 parts；MS-1 emulsifying agent 15 parts；Butyl acetate 5 parts；Deionized water 50 parts；
Zinc naphthenate 10 parts；Hydroxymethyl cellulose 25 parts；Toluene 30 parts.
By NC Nitroncellulose, styrene, tricresyl phosphate, rubber chemicals, ethyl acetate and
Methacrylic acid loads in ball milling, and ball milling 30min is subsequently adding diisooctyl adipate, MS-1
Emulsifying agent, butyl acetate, deionized water and zinc naphthenate, add acrylic acid tree after ball milling 30min
Lipoprotein solution, continues ball milling 4h, finally, remaining raw material is all put into ball milling in ball mill
30min, had both obtained finished product.
Product viscosity 120s, surface drying time 2h, soaks nothing foaming, dry linting after 15d in water
Phenomenon；Alkali resistance is good, soaks that 48h is non-foaming, come off in buck；Film brushing resistance
1500 times.
Embodiment 2:
A kind of acrylate zero diopter exterior coating, its raw materials by weight portion proportioning is as follows: propylene
Acid resin solution 100 parts；NC Nitroncellulose 40 parts；Styrene 30 parts；Tricresyl phosphate
10 parts；Rubber chemicals 45 parts；Ethyl acetate 15 parts；Methacrylic acid 20 parts；Adipic acid
Di-isooctyl 20 parts；MS-1 emulsifying agent 25 parts；Butyl acetate 25 parts；Deionized water 60
Part；Zinc naphthenate 20 parts；Hydroxymethyl cellulose 35 parts；Toluene 40 parts.
By NC Nitroncellulose, styrene, tricresyl phosphate, rubber chemicals, ethyl acetate and
Methacrylic acid loads in ball milling, and ball milling 30min is subsequently adding diisooctyl adipate, MS-1
Emulsifying agent, butyl acetate, deionized water and zinc naphthenate, add acrylic acid tree after ball milling 30min
Lipoprotein solution, continues ball milling 5h, finally, remaining raw material is all put into ball milling in ball mill
30min, had both obtained finished product.
Product viscosity 135s, surface drying time 1.5h, without bubbling, falling in water after soaking 20d
Powder phenomenon；Alkali resistance is good, soaks that 60h is non-foaming, come off in buck；Film brushing resistance
1650 times.
Embodiment 3:
A kind of acrylate zero diopter exterior coating, its raw materials by weight portion proportioning is as follows: propylene
Acid resin solution 100 parts；NC Nitroncellulose 30 parts；Styrene 25 parts；Tricresyl phosphate
8 parts；Rubber chemicals 35 parts；Ethyl acetate 10 parts；Methacrylic acid 15 parts；Adipic acid
Di-isooctyl 17 parts；MS-1 emulsifying agent 20 parts；Butyl acetate 15 parts；Deionized water 55
Part；Zinc naphthenate 15 parts；Hydroxymethyl cellulose 30 parts；Toluene 35 parts.
By NC Nitroncellulose, styrene, tricresyl phosphate, rubber chemicals, ethyl acetate and
Methacrylic acid loads in ball milling, and ball milling 30min is subsequently adding diisooctyl adipate, MS-1
Emulsifying agent, butyl acetate, deionized water and zinc naphthenate, add acrylic acid tree after ball milling 30min
Lipoprotein solution, continues ball milling 4.5h, finally, remaining raw material is all put into ball in ball mill
Mill 30min, had both obtained finished product.
Product viscosity 150s, surface drying time 1h, soaks nothing foaming, dry linting after 25d in water
Phenomenon；Alkali resistance is good, soaks that 72h is non-foaming, come off in buck；Film brushing resistance
1800 times.
Composition all components in above example all can be commercially available.
Above-described embodiment is only intended to be illustrated present disclosure rather than limit, because of
This any change in the implication suitable with claims of the present invention and scope, all should
It is considered to be included within the scope of the claims.
Claims (1)
1. an acrylate zero diopter exterior coating, it is characterised in that described acrylate zero diopter
The raw materials by weight portion proportioning of exterior coating is as follows: acrylic resin soln 100 parts；Nitro
Cellulose 30 parts；Styrene 25 parts；Tricresyl phosphate 8 parts；Rubber chemicals 35 parts；
Ethyl acetate 10 parts；Methacrylic acid 15 parts；17 parts of plasticizer；MS-1 emulsifying agent 20
Part；Butyl acetate 15 parts；Deionized water 55 parts；Mould inhibitor 15 parts；Hydroxymethyl cellulose
30 parts；Toluene 35 parts；
Described plasticizer uses diisooctyl adipate；
Described mould inhibitor uses zinc naphthenate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410482749.4A CN104194429B (en) | 2014-09-19 | 2014-09-19 | A kind of acrylate zero diopter exterior coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410482749.4A CN104194429B (en) | 2014-09-19 | 2014-09-19 | A kind of acrylate zero diopter exterior coating |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104194429A CN104194429A (en) | 2014-12-10 |
| CN104194429B true CN104194429B (en) | 2016-09-07 |
Family
ID=52079809
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410482749.4A Active CN104194429B (en) | 2014-09-19 | 2014-09-19 | A kind of acrylate zero diopter exterior coating |
Country Status (1)
| Country | Link |
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| CN (1) | CN104194429B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106009939A (en) * | 2016-08-01 | 2016-10-12 | 安庆瑞泰化工有限公司 | Mildew proof water-based paint and preparation method thereof |
| CN107118675A (en) * | 2017-06-22 | 2017-09-01 | 合肥易美特建材有限公司 | A kind of zero diopter exterior coating and preparation method |
| CN109880458A (en) * | 2019-02-18 | 2019-06-14 | 南通市乐佳涂料有限公司 | A kind of cement water-proof cold-resistant coating and the preparation method and application thereof |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386727B (en) * | 2008-10-24 | 2011-05-11 | 深圳市广田环保涂料有限公司 | Yellowing-resistant nitro white matt finish and preparation method thereof, use method |
| CN102391758A (en) * | 2011-09-21 | 2012-03-28 | 谢利荣 | Enamel paint used for automobiles |
| CN102604489B (en) * | 2012-03-20 | 2013-11-13 | 惠州市长润发涂料有限公司 | Water-based environment-friendly nitrolacquer and construction method for same |
| CN102675942A (en) * | 2012-06-21 | 2012-09-19 | 南通顺阳化工有限公司 | Cold-resistant paint |
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2014
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| CN104194429A (en) | 2014-12-10 |
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Inventor after: Shen Yang Inventor before: Ma Zhiming |
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Effective date of registration: 20160805 Address after: 225300, Jiangsu province Taizhou Hailing Industrial Park District Street to build a standard workshop No. 37 Applicant after: Jiangsu Baidai Energy-Saving Building Materials Co.,Ltd. Address before: Zhujiang Road Wuzhong District Mudu town of Suzhou city in Jiangsu Province Tianlong 215101 No. 378 building room 4722 Applicant before: SUZHOU LUOTELAN NEW MATERIAL TECHNOLOGY CO., LTD. |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Acrylate flat-gloss exterior wall coating material Effective date of registration: 20170922 Granted publication date: 20160907 Pledgee: Bank of China Limited by Share Ltd Taizhou branch Pledgor: Jiangsu Baidai Energy-Saving Building Materials Co.,Ltd. Registration number: 2017320000030 |
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Date of cancellation: 20190604 Granted publication date: 20160907 Pledgee: Bank of China Limited by Share Ltd Taizhou branch Pledgor: Jiangsu Baidai Energy-Saving Building Materials Co.,Ltd. Registration number: 2017320000030 |