CN104027829A - Solid freshener containing lemon tea tree essential oil component and preparation method of solid freshener - Google Patents
Solid freshener containing lemon tea tree essential oil component and preparation method of solid freshener Download PDFInfo
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- CN104027829A CN104027829A CN201410252619.1A CN201410252619A CN104027829A CN 104027829 A CN104027829 A CN 104027829A CN 201410252619 A CN201410252619 A CN 201410252619A CN 104027829 A CN104027829 A CN 104027829A
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- essential oil
- fructus citri
- citri limoniae
- solid freshener
- tea tree
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 46
- 239000007787 solid Substances 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 240000002184 Leptospermum petersonii Species 0.000 title abstract 5
- 235000003658 Leptospermum petersonii Nutrition 0.000 title abstract 5
- 239000007788 liquid Substances 0.000 claims abstract description 31
- 238000003756 stirring Methods 0.000 claims abstract description 30
- 235000009024 Ceanothus sanguineus Nutrition 0.000 claims abstract description 24
- 240000003553 Leptospermum scoparium Species 0.000 claims abstract description 24
- 235000015459 Lycium barbarum Nutrition 0.000 claims abstract description 24
- 239000000843 powder Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 230000001954 sterilising effect Effects 0.000 claims abstract description 9
- 239000002904 solvent Substances 0.000 claims abstract description 8
- 125000003118 aryl group Chemical group 0.000 claims abstract description 4
- 244000269722 Thea sinensis Species 0.000 claims description 16
- 235000006468 Thea sinensis Nutrition 0.000 claims description 16
- 239000000047 product Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 12
- 239000003292 glue Substances 0.000 claims description 11
- 239000002131 composite material Substances 0.000 claims description 10
- 239000000499 gel Substances 0.000 claims description 9
- 238000004659 sterilization and disinfection Methods 0.000 claims description 9
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 claims description 8
- 229920002148 Gellan gum Polymers 0.000 claims description 7
- 230000002421 anti-septic effect Effects 0.000 claims description 7
- 239000012752 auxiliary agent Substances 0.000 claims description 7
- 235000010418 carrageenan Nutrition 0.000 claims description 7
- 239000000679 carrageenan Substances 0.000 claims description 7
- 229920001525 carrageenan Polymers 0.000 claims description 7
- 229940113118 carrageenan Drugs 0.000 claims description 7
- 239000004359 castor oil Substances 0.000 claims description 7
- 235000019438 castor oil Nutrition 0.000 claims description 7
- 239000000216 gellan gum Substances 0.000 claims description 7
- 235000010492 gellan gum Nutrition 0.000 claims description 7
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 7
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 7
- 229940100555 2-methyl-4-isothiazolin-3-one Drugs 0.000 claims description 6
- BEGLCMHJXHIJLR-UHFFFAOYSA-N methylisothiazolinone Chemical compound CN1SC=CC1=O BEGLCMHJXHIJLR-UHFFFAOYSA-N 0.000 claims description 6
- 239000003963 antioxidant agent Substances 0.000 claims description 5
- 230000003078 antioxidant effect Effects 0.000 claims description 5
- 239000003921 oil Substances 0.000 claims description 5
- 239000000049 pigment Substances 0.000 claims description 5
- LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 claims description 4
- 244000247812 Amorphophallus rivieri Species 0.000 claims description 4
- 235000001206 Amorphophallus rivieri Nutrition 0.000 claims description 4
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 4
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 claims description 4
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 claims description 4
- 229920002581 Glucomannan Polymers 0.000 claims description 4
- 229920002752 Konjac Polymers 0.000 claims description 4
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 4
- 239000001110 calcium chloride Substances 0.000 claims description 4
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 4
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 claims description 4
- 239000001527 calcium lactate Substances 0.000 claims description 4
- 229960002401 calcium lactate Drugs 0.000 claims description 4
- 235000011086 calcium lactate Nutrition 0.000 claims description 4
- NEHNMFOYXAPHSD-UHFFFAOYSA-N citronellal Chemical compound O=CCC(C)CCC=C(C)C NEHNMFOYXAPHSD-UHFFFAOYSA-N 0.000 claims description 4
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 claims description 4
- 229940046240 glucomannan Drugs 0.000 claims description 4
- 239000000252 konjac Substances 0.000 claims description 4
- 235000010485 konjac Nutrition 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- 229920000161 Locust bean gum Polymers 0.000 claims description 3
- 235000010420 locust bean gum Nutrition 0.000 claims description 3
- 239000000711 locust bean gum Substances 0.000 claims description 3
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 claims description 2
- 229920001817 Agar Polymers 0.000 claims description 2
- 241000134874 Geraniales Species 0.000 claims description 2
- 239000005792 Geraniol Substances 0.000 claims description 2
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 claims description 2
- 239000008272 agar Substances 0.000 claims description 2
- 235000010419 agar Nutrition 0.000 claims description 2
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 claims description 2
- LLEMOWNGBBNAJR-UHFFFAOYSA-N biphenyl-2-ol Chemical compound OC1=CC=CC=C1C1=CC=CC=C1 LLEMOWNGBBNAJR-UHFFFAOYSA-N 0.000 claims description 2
- WTEVQBCEXWBHNA-YFHOEESVSA-N citral B Natural products CC(C)=CCC\C(C)=C/C=O WTEVQBCEXWBHNA-YFHOEESVSA-N 0.000 claims description 2
- 229930003633 citronellal Natural products 0.000 claims description 2
- 235000000983 citronellal Nutrition 0.000 claims description 2
- 235000000484 citronellol Nutrition 0.000 claims description 2
- 239000012467 final product Substances 0.000 claims description 2
- 229940113087 geraniol Drugs 0.000 claims description 2
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 2
- 229920000053 polysorbate 80 Polymers 0.000 claims description 2
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 2
- 235000010234 sodium benzoate Nutrition 0.000 claims description 2
- 239000004299 sodium benzoate Substances 0.000 claims description 2
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 239000001509 sodium citrate Substances 0.000 claims description 2
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 2
- 239000004611 light stabiliser Substances 0.000 claims 1
- 239000008367 deionised water Substances 0.000 abstract description 3
- 229910021641 deionized water Inorganic materials 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract description 2
- 239000000654 additive Substances 0.000 abstract 2
- 230000000996 additive effect Effects 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 239000003755 preservative agent Substances 0.000 abstract 2
- 230000002335 preservative effect Effects 0.000 abstract 2
- 230000001580 bacterial effect Effects 0.000 abstract 1
- 238000009924 canning Methods 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 230000000249 desinfective effect Effects 0.000 abstract 1
- 238000007599 discharging Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 230000002401 inhibitory effect Effects 0.000 abstract 1
- 238000007689 inspection Methods 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 239000002386 air freshener Substances 0.000 description 22
- 239000003205 fragrance Substances 0.000 description 8
- 230000000844 anti-bacterial effect Effects 0.000 description 6
- 230000002159 abnormal effect Effects 0.000 description 5
- 230000035943 smell Effects 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 4
- 238000009472 formulation Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 3
- 230000007613 environmental effect Effects 0.000 description 3
- 150000004676 glycans Chemical class 0.000 description 3
- 235000013599 spices Nutrition 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 208000036142 Viral infection Diseases 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
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- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- WZYRMLAWNVOIEX-MOJAZDJTSA-N (2s)-2-[(2r,3r,4s)-3,4-dihydroxyoxolan-2-yl]-2-hydroxyacetaldehyde Chemical compound O=C[C@@H](O)[C@@H]1OC[C@H](O)[C@H]1O WZYRMLAWNVOIEX-MOJAZDJTSA-N 0.000 description 1
- KFGWEMFTDGCYSK-UHFFFAOYSA-N 3-methyl-1,2-thiazole 1-oxide Chemical compound CC=1C=CS(=O)N=1 KFGWEMFTDGCYSK-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- SHZGCJCMOBCMKK-UHFFFAOYSA-N D-mannomethylose Natural products CC1OC(O)C(O)C(O)C1O SHZGCJCMOBCMKK-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- PNNNRSAQSRJVSB-UHFFFAOYSA-N L-rhamnose Natural products CC(O)C(O)C(O)C(O)C=O PNNNRSAQSRJVSB-UHFFFAOYSA-N 0.000 description 1
- 244000131316 Panax pseudoginseng Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 208000033809 Suppuration Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- PNNNRSAQSRJVSB-BXKVDMCESA-N aldehydo-L-rhamnose Chemical compound C[C@H](O)[C@H](O)[C@@H](O)[C@@H](O)C=O PNNNRSAQSRJVSB-BXKVDMCESA-N 0.000 description 1
- WQZGKKKJIJFFOK-PHYPRBDBSA-N alpha-D-galactose Chemical compound OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@H]1O WQZGKKKJIJFFOK-PHYPRBDBSA-N 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
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- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000002354 daily effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- DNJIEGIFACGWOD-UHFFFAOYSA-N ethanethiol Chemical compound CCS DNJIEGIFACGWOD-UHFFFAOYSA-N 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 229930182830 galactose Natural products 0.000 description 1
- 238000001879 gelation Methods 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000008297 liquid dosage form Substances 0.000 description 1
- 239000001289 litsea cubeba fruit oil Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000003340 mental effect Effects 0.000 description 1
- 230000004630 mental health Effects 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- -1 saccharide compound Chemical class 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 230000007928 solubilization Effects 0.000 description 1
- 238000005063 solubilization Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 239000010677 tea tree oil Substances 0.000 description 1
- 229940111630 tea tree oil Drugs 0.000 description 1
- 230000009385 viral infection Effects 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Plant Substances (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention relates to a solid freshener containing a lemon tea tree essential oil component. The solid freshener comprises the following main components in percentage by weight: 0.5-3% of compound rubber powder, 0.1-1% of a gel additive, 1-10% of lemon tea tree essential oil, 2-15% of a solubilizer, 0.1-0.5% of a sterilizing preservative, 0.01-0.1% of other components and the balance of deionized water. The invention further discloses a preparation method of the solid freshener containing the lemon tea tree essential oil component. The preparation method comprises the following steps: 1) firstly, fully stirring the compound rubber powder in hot water a 90-95 DEG C till the hot water becomes a transparent solution, adding the gel additive and fully stirring, then, cooling to 60-65 DEG C, and insulating and stirring to obtain a liquid A; 2) mixing the lemon tea tree essential oil and the solubilizer and uniformly stirring to obtain a liquid B; and 3) adding the liquid B into the liquid A, uniformly stirring, then, adding the sterilizing preservative and other components and uniformly stirring, and filtering, discharging and canning, and packaging finished products after passed inspection. By taking tea tree essential oil as the aromatic component, the solid freshener not only is fresh and natural in odor and refreshing, but also has the bacterial-inhibiting and disinfecting function.
Description
Technical field
The present invention relates to a kind of air freshener, belong to daily chemical product technical field, be specifically related to a kind of solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil and preparation method thereof.
Background technology
In recent years, along with improving constantly of China's lives of the people level, people also more and more pay attention to healthy and domestic environment.Air quality has become the focus of the another concern after food safety.Keeping the clean and pure and fresh of air and environment, is everyone hope.Have pure and fresh air, can eliminate the fatigue of one day, lax nervous body and mind, is of value to human body physical and mental health.But along with life in work in physical product abundantization with variation, environment around and air are contaminated.In order to improve air quality and deaeration abnormal flavour, air freshener has become the needs of life, and increasing consumer brings into use air freshener to improve air quality.
For bringing into play to greatest extent the effect of preparation and improving the use impression of consumer, every technology such as emulsifying, solubilization, gelation, slow-releasing in air freshener manufacture, have been used.The technology of applying in air freshener is mainly in order to compose perfume (or spice), smelly eliminating, inhibition stench generation and antibacterial.The air freshener of selling on the market at present from form mainly contain liquid type, three kinds of aerosol-type and gel-types.Wherein common and the most practical is gel-type, can slowly discharge fragrant abnormal smells from the patient, easy to use.At present in Chinese market, a lot of consumers worry to use air freshener dangerous, worry to use essence that air freshener uses to allocate for chemosynthesis, use meeting damages human body, affect health, use air freshener can cause air " secondary pollution ", thereby refusal is used air freshener.This also hinders by being the reason that air freshener market further develops.Therefore the air freshener that, need to develop natural series meets different consumer demands.
Chinese patent CN1524585A discloses a kind of all natural air freshener, it adopts litsea cubeba oil, Oleum Rosae Rugosae as fragrance ingredient, compare with conventional air freshener, adopted the volatile oil of natural origin, more natural, safety, but form is liquid dosage form, uses inconvenient, and the ginseng of multiple quintessence oil is joined, the feature fragrance of original quintessence oil that scatters and disappears possibly.Chinese patent CN1799635A discloses a kind of long effective air freshener, and it has adopted hydroexpansivity resin and the preparation of long-acting gel can obtain gel-type air freshener, and spice is able to slow release.But still take spice as aromatic composition, add the auxiliary agents such as the virose ethylene glycol of tool simultaneously, its safety needs to be investigated.
Along with people's living standard is more and more higher, also more and more higher to the requirement of product.Therefore, how developing a good air freshener not only possesses and purifies air, pleasant mental and body, but also will be safely, have no side effect, storage and easy to use, there is the effects such as certain antibacterial, deodorization, be the technical barrier that one of ordinary skill in the art face.
Summary of the invention
In order to overcome the above-mentioned deficiency of existing air freshener, the object of the present invention is to provide a kind of solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil, take Fructus Citri Limoniae tea tree ethereal oil as fragrant functional component, not only abnormal smells from the patient is fresh and clean, refreshment, and there is antibacterial, disinfection efficacy, compare with conventional air freshener, product also environmental protection more in use, green, healthy, safety.
The present invention is achieved by the following technical solutions.
A kind of Fructus Citri Limoniae Camellia sinensis derived essential oil solid freshener, each raw material components that comprises following percentage by weight: composite glue powder 0.5-3% of containing that the present invention proposes; Gel auxiliary agent 0.1-1%; Fructus Citri Limoniae tea tree ethereal oil 1-10%; Solubilizing agent 1-15%; Sterilization antiseptic 0.1-0.5%; Other component 0.01-0.1%; Surplus is deionized water.
Furthermore, a kind of Fructus Citri Limoniae Camellia sinensis derived essential oil solid freshener, each raw material components that comprises following percentage by weight: composite glue powder 0.6～2.0% of containing that the present invention proposes; Gel auxiliary agent 0.3～0.8%; Fructus Citri Limoniae tea tree ethereal oil 2.0～6.0%; Solubilizing agent 2.0～8.0%; Sterilization antiseptic 0.1～0.3%; Other component 0.05～0.1%; Surplus is deionized water.
Composite glue powder of the present invention is gellan gum, carrageenan, locust bean gum, agar, Konjac glucomannan, wherein more preferred gellan gum card and draw one or both mixing in any proportion in glue.Gellan gum is a kind of novel microbial extracellular polysaccharide, is to be followed successively by by four glycan molecules the macromolecule saccharide compound that D-Glucose, D-Glucose aldehydic acid, D-Glucose, L-rhamnose are formed by connecting by glycosidic bond, has superior gelling performance.Carrageenan is a kind of hydrophilic gel, calcium, potassium, sodium, the ammonium salt of the polysaccharide sulfuric ester being comprised of galactose and Anhydrogalactose..Gellan gum and carrageenan are all the natural hydrophilic gels in source, are widely used in grocery trade.
Gel auxiliary agent of the present invention is any or two or more mixture in calcium chloride, calcium lactate, sodium chloride, sodium citrate, wherein more preferred calcium lactate.
Fructus Citri Limoniae tea tree ethereal oil of the present invention is natural aromatic quintessence oil, the pure and fresh fragrance that it had both had as Fructus Citri Limoniae pleasant, has rouse oneself, be described as " the happy oil " in Australia state, have again the sterilizing ability stronger than traditional tea tree oil, can efficiently resist skin viral infection, send out the symptoms such as pus, redness, consoling skin simultaneously, reduce and stimulate, is natural antibacterial, antiseptic and antiinflammatory.Its component comprises geranial (22-30%), neral (23-27%), geraniol, citronellal (9-28%) and citronellol.
Solubilizing agent of the present invention has castor oil hydrogenated, fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-7, this kind-60, the mixture of one or more in tween 80, wherein more preferred castor oil hydrogenated.
Sterilization antiseptic of the present invention has one or more the mixture in sodium benzoate, Methylisothiazolinone, phenyl phenol, wherein preferable methyl isothiazolone more.
In addition, the invention allows for a kind of preparation method of the above-mentioned type solid pleasant smell agent that contains Fructus Citri Limoniae Camellia sinensis derived essential oil, comprise the following steps:
1) first composite glue powder is stirred well to clear solution in 90-95 ℃ of hot water, adds gel auxiliary agent, stir fully, be then cooled to 60-65 ℃, insulated and stirred, obtains A liquid;
2) Fructus Citri Limoniae tea tree ethereal oil, solubilizing agent are mixed, stir, obtain B liquid;
3) B liquid is joined in A liquid and mixed, stir.Then add sterilization antiseptic, other component, stir; Filter out batch can dress, be up to the standards and get final product packed products.
Solid freshener of the present invention has following advantage and beneficial effect than prior art:
The Fructus Citri Limoniae tea tree ethereal oil of natural origin of take is fragrant functional component, and not only abnormal smells from the patient is fresh and clean, refreshment, and there is antibacterial, disinfection efficacy.Compare with traditional liquid type air freshener, it is just sustainable fragrant more than 25 days, easy to use that product opens wide placement.Product is also environmental protection more in use, healthy, safety.Meet consumer to green, pure and fresh, the natural requirement of air.
The specific embodiment
By concrete preferred embodiment, in conjunction with comparative test example, the solid freshener that contains Fructus Citri Limoniae tea tree ethereal oil of the present invention is described in further detail below, but the present invention is not limited in following embodiment.
The solid freshener performance test methods that contains Fructus Citri Limoniae tea tree ethereal oil of the present invention is as follows:
1, fragrance preference degree evaluation methodology.
Evaluation methodology: the sample of preparation is placed in to confined space (about 3m
3) middle placement 2 hours, selected totally 10 of tested volunteer men and women (22 years old-55 years old age), carry out sensory evaluation to sample, mark to evaluate fragrance fancy grade: 10 minutes, enjoy a lot by following 4 degree; 8 minutes, prefer; 6 minutes, general; 0 minute, do not like;
2, evaluation methodology service time
The sample (about 70g) parallel (2 groups) of preparation is positioned over to volatilization naturally in half ventilated environment, records origination date.Observe and weigh every day, until the complete exhaustion of sample or weight constant weight are judged as and finish using, record date, calculates and use natural law.
embodiment 1～3
According to the formulation content of table 1, prepare respectively the solid freshener that contains Fructus Citri Limoniae tea tree ethereal oil of embodiment 1～3, its preparation method is: the composite glue powder first carrageenan, Konjac glucomannan being formed is stirred well to clear solution in 90-95 ℃ of hot water, add calcium chloride, stir fully, then be cooled to 60-65 ℃, insulated and stirred, obtains A liquid; Fructus Citri Limoniae tea tree ethereal oil, antioxidant, castor oil hydrogenated are mixed, stir.Obtain B liquid; B liquid is joined in A liquid and mixed, stir.Then add Methylisothiazolinone, pigment, stir.Filter out batch can dress.Draw samples is also tested by quality standard, is up to the standards and can be packaged into product.
The formula of the Fructus Citri Limoniae tea tree ethereal oil solid freshener of table 1 embodiment 1～3 forms
embodiment 4～6
According to table 2 formulation content, prepare respectively embodiment 4～6 Fructus Citri Limoniae tea tree ethereal oil solid fresheners, its preparation method is: the composite glue powder first carrageenan, locust bean gum being formed is stirred well to clear solution in 90-95 ℃ of hot water, add calcium lactate, stir fully, then be cooled to 60-65 ℃, insulated and stirred, obtains A liquid; Fructus Citri Limoniae tea tree ethereal oil, antioxidant, castor oil hydrogenated and AEO9 are mixed, stir.Obtain B liquid; B liquid is joined in A liquid and mixed, stir.Then add Methylisothiazolinone, pigment, stir.Filter out batch can dress.Draw samples is also tested by quality standard, is up to the standards and can be packaged into product.
The formula of the Fructus Citri Limoniae tea tree ethereal oil solid freshener of table 2 embodiment 4～6 forms
embodiment 7～9
According to table 3 formulation content, prepare respectively embodiment 7～9 Fructus Citri Limoniae tea tree ethereal oil solid fresheners, its preparation method is: the composite glue powder first Konjac glucomannan, gellan gum being formed is stirred well to clear solution in 90-95 ℃ of hot water, add potassium chloride, stir fully, then be cooled to 60-65 ℃, insulated and stirred, obtains A liquid; Fructus Citri Limoniae tea tree ethereal oil, antioxidant, castor oil hydrogenated are mixed, stir.Obtain B liquid; B liquid is joined in A liquid and mixed, stir.Then add Methylisothiazolinone, pigment, stir.Filter out batch can dress.Draw samples is also tested by quality standard, is up to the standards and can be packaged into product.
The formula of the Fructus Citri Limoniae tea tree ethereal oil solid freshener of table 3 embodiment 7～9 forms
embodiment 10～12
According to table 4 formulation content, prepare respectively embodiment 10～12 Fructus Citri Limoniae tea tree ethereal oil solid fresheners, its preparation method is: the composite glue powder first carrageenan, gellan gum being formed is stirred well to clear solution in 90-95 ℃ of hot water, add calcium chloride, stir fully, then be cooled to 60-65 ℃, insulated and stirred, obtains A liquid; Fructus Citri Limoniae tea tree ethereal oil, antioxidant, castor oil hydrogenated are mixed, stir.Obtain B liquid; B liquid is joined in A liquid and mixed, stir.Then add Methylisothiazolinone, pigment, stir.Filter out batch can dress.Draw samples is also tested by quality standard, is up to the standards and can be packaged into product.
The formula of the Fructus Citri Limoniae tea tree ethereal oil solid freshener of table 4 embodiment 10～12 forms
By above-described embodiment, contrast commercially available air freshener, carried out fragrance preference degree assessment and test service time, experimental result in Table 5, table 6.
Table 5 fragrance preference degree and service time result
Table 6 fragrance preference degree and service time result
Consolidated statement 6～table 7 test data can find out, uses consumer's fancy grade of each embodiment product and service time all higher than commercially available prod.
The feature of the solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil of the present invention is:
It is fragrant functional component that the present invention uses the Fructus Citri Limoniae tea tree ethereal oil of natural origin, and not only abnormal smells from the patient is fresh and clean, refreshment.And there is antibacterial, disinfection efficacy.Compare with traditional liquid type air freshener, it is just sustainable fragrant more than 25 days, easy to use that product opens wide placement.Product also environmental protection more in use, healthy, safety.Meet consumer to green, pure and fresh, the natural requirement of air.
The above, it is only preferred embodiment of the present invention, not the present invention is done to any pro forma restriction, therefore every, do not depart from technical solution of the present invention content, any simple modification, equivalent variations and the modification the above embodiment done according to technical spirit of the present invention, all still belong in the scope of technical solution of the present invention.
Claims (9)
1. a solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil, is characterized in that each raw material components that contains following percentage by weight:
2. the solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil according to claim 1, is characterized in that each raw material components that contains following percentage by weight:
3. the solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil according to claim 1, is characterized in that: described composite glue powder is any or two or more mixture in gellan gum, carrageenan, locust bean gum, agar, Konjac glucomannan.
4. the solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil according to claim 1, is characterized in that: described gel auxiliary agent is any or two or more mixture in calcium chloride, calcium lactate, sodium chloride, sodium citrate.
5. the solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil according to claim 1, it is characterized in that: described Fructus Citri Limoniae tea tree ethereal oil is natural aromatic quintessence oil, its component comprises geranial (22-30%), neral (23-27%), geraniol, citronellal (9-28%) and citronellol.
6. the solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil according to claim 1, it is characterized in that: described solubilizing agent is castor oil hydrogenated, fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-7, this kind-60, the mixture of one or more in tween 80.
7. the solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil according to claim 1, is characterized in that: described sterilization antiseptic is one or more the mixture in sodium benzoate, Methylisothiazolinone, phenyl phenol.
8. the solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil according to claim 1, is characterized in that: described other component is light stabilizer, antioxidant, pigment, and these components are universaling component, and kind is not done specific limited.
9. the preparation method of a kind of solid freshener that contains Fructus Citri Limoniae Camellia sinensis derived essential oil described in any one in claim 1-8, is characterized in that comprising the following steps:
1) first composite glue powder is stirred well to clear solution in 90-95 ℃ of hot water, adds gel auxiliary agent, stir fully, be then cooled to 60-65 ℃, insulated and stirred obtains A liquid;
2) Fructus Citri Limoniae tea tree ethereal oil, solubilizing agent are mixed, B liquid stirs to obtain;
3) B liquid is joined in A liquid and mixed, stir; Then add sterilization antiseptic, other component, stir; Filter out batch can dress, be up to the standards and get final product packed products.
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