CN104026176B - A kind of natural organic agricultural chemical composition and preparation method thereof - Google Patents
A kind of natural organic agricultural chemical composition and preparation method thereof Download PDFInfo
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- CN104026176B CN104026176B CN201410291344.2A CN201410291344A CN104026176B CN 104026176 B CN104026176 B CN 104026176B CN 201410291344 A CN201410291344 A CN 201410291344A CN 104026176 B CN104026176 B CN 104026176B
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- 239000000203 mixture Substances 0.000 title claims abstract description 15
- 239000003905 agrochemical Substances 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 50
- 238000009835 boiling Methods 0.000 claims abstract description 46
- 239000000706 filtrate Substances 0.000 claims abstract description 46
- 239000000575 pesticide Substances 0.000 claims abstract description 41
- 241000250966 Tanacetum cinerariifolium Species 0.000 claims abstract description 27
- ROVGZAWFACYCSP-MQBLHHJJSA-N [2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OC1C(C)=C(C\C=C/C=C)C(=O)C1 ROVGZAWFACYCSP-MQBLHHJJSA-N 0.000 claims abstract description 27
- 229940015367 pyrethrum Drugs 0.000 claims abstract description 27
- 239000012141 concentrate Substances 0.000 claims abstract description 23
- 238000001816 cooling Methods 0.000 claims abstract description 23
- 238000001914 filtration Methods 0.000 claims abstract description 23
- 238000007654 immersion Methods 0.000 claims abstract description 23
- 238000002156 mixing Methods 0.000 claims abstract description 23
- 239000011550 stock solution Substances 0.000 claims abstract description 16
- 239000012567 medical material Substances 0.000 claims description 4
- 238000011017 operating method Methods 0.000 claims description 2
- 241000607479 Yersinia pestis Species 0.000 abstract description 5
- 238000001228 spectrum Methods 0.000 abstract description 4
- 241000196324 Embryophyta Species 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 2
- 238000007865 diluting Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 description 11
- 239000000126 substance Substances 0.000 description 6
- 241000238631 Hexapoda Species 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 230000001629 suppression Effects 0.000 description 4
- 230000000749 insecticidal effect Effects 0.000 description 3
- 241000239290 Araneae Species 0.000 description 2
- 241000258937 Hemiptera Species 0.000 description 2
- 239000006272 natural pesticide Substances 0.000 description 2
- 241000195493 Cryptophyta Species 0.000 description 1
- 206010059866 Drug resistance Diseases 0.000 description 1
- 241000907661 Pieris rapae Species 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 229940088710 antibiotic agent Drugs 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of natural organic agricultural chemical composition and preparation method thereof, this composition pesticide includes following components by weight: Folium Meliae 100 parts, Pyrethrum 30 ~ 50 parts, Herba Artemisiae Annuae 18 ~ 28 parts, 20 ~ 30 parts of Bulbus Allii, 20 ~ 30 parts of Fructus Capsici, 5 ~ 15 parts of Rhizoma Zingiberis Recens.Preparation method is: weigh Folium Meliae, Bulbus Allii, Fructus Capsici and Rhizoma Zingiberis Recens in proportion, grinds, and adds clear water and soaks 12 ~ 24 hours, it is heated to 90 ~ 100 DEG C, keep slight boiling condition 0.5 ~ 1 hour, filtered while hot, filtrate stands cooling, filtering residue adds water immersion 2 ~ 3 hours, refiltering after boiling 0.5 ~ 1 hour, twice filtrate mixing, cryogenic vacuum concentrates, obtaining pesticide stock solution, diluting 1000 ~ 2000 times can come into operation.The composition pesticide of the present invention, pest-resistant spectrum is wide, and raw material natural environmental-protective is the most harmless to human body and environment, can be widely used for the plantation of nuisance-free plant, and preparation method is simple, easily realizes industrialization.
Description
Technical field
The invention belongs to pesticide production technology field, be specifically related to a kind of natural organic agricultural chemical composition and preparation method thereof.
Background technology
In agricultural production, insect can disturb the growth of crops, both have impact on the yield of crops, and had also caused food safety tired
Disturb.Therefore, most peasants can select chemical pesticide to carry out pest control.But in recent years, owing to abusing what chemical pesticide caused
Problem is increasingly subject to pay attention to.First, abuse chemical pesticide can make the Drug resistance of insect increase, it is reported that, conventional pesticide has
Effectiveness amount 10 years is general rises three times, so on, insect pasts medical help and not paints an alarming picture of the situation just to scare the audience.Secondly, although the using of chemical pesticide
Improve the yield of crops, but difficulty dispelled by the chemical pesticide of residual, healthy to people causes the biggest threat.Finally,
After unnecessary chemical pesticide flows into river, meeting severe contamination water quality, not only can not drink, also can form algae and spread unchecked, ecological mistake
The disastrous effect of weighing apparatus.Therefore, Novel high-efficient pesticide is sought extremely urgent.
Natural organic agricultural chemicals is the natural pesticide being transformed by agricultural products, both can make full use of the agricultural resource of plantation, the most not
Can impact health and the environment of human body, putting forth effort to develop natural organic agricultural chemicals is a main trend.
Summary of the invention
Based on foregoing, the present invention uses various plants source extract combination to form natural organic agricultural chemicals, has the pest-resistant of wide spectrum
Effect, can be widely applied to the pest control of veterinary antibiotics, Chinese crude drug, has the chemistry such as notable, the green safety of insecticidal effect
The effect that pesticide is not replaced.
An object of the present invention is to provide a kind of natural organic agricultural chemical composition, includes following components by weight: Folium Meliae
100 parts, Pyrethrum 30～50 parts, Herba Artemisiae Annuae 18～28 parts, Bulbus Allii 20～30 parts, Fructus Capsici 20～30 parts, Rhizoma Zingiberis Recens 5～15 parts.
Preferably, include following components by weight: Folium Meliae 100 parts, Pyrethrum 35～45 parts, Herba Artemisiae Annuae 22～24 parts,
Bulbus Allii 20～25 parts, Fructus Capsici 25～30 parts, Rhizoma Zingiberis Recens 8～12 parts.
It is highly preferred that include following components by weight: Folium Meliae 100 parts, Pyrethrum 40 parts, Herba Artemisiae Annuae 23 parts, Bulbus Allii
25 parts, 28 parts of Fructus Capsici, 10 parts of Rhizoma Zingiberis Recens.
Another object of the present invention is to provide the preparation method of a kind of natural organic agricultural chemical composition, including following operating procedure:
Weigh Folium Meliae, Pyrethrum, Herba Artemisiae Annuae, Bulbus Allii, Fructus Capsici and Rhizoma Zingiberis Recens by weight, grind, add clear water immersion 12～24 little
Time, it being heated to 90～100 DEG C, holding slight boiling condition 0.5～1 hour, filtered while hot, filtrate stands cooling, and filtering residue adds water leaching
Steeping 2～3 hours, refilter after boiling 0.5～1 hour, twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide stock solution, dilute
Release 1000～2000 times can come into operation.
Described clear water addition is as the criterion to cover medical material.
Containing 1g medical material in every milliliter of described pesticide stock solution.
The present invention each component insecticide is all had stronger tag, stomach kills effect.
The natural organic agricultural chemical composition of one that the present invention provides, pest-resistant spectrum is wide, raw material natural environmental-protective, after using, to human body and
Environment is the most harmless, can be widely used for the plantation of nuisance-free plant, and preparation method is simple, easily realizes industrialization.
Detailed description of the invention
Embodiment 1
Weigh Folium Meliae 100 parts, Pyrethrum 30 parts, Herba Artemisiae Annuae 18 parts, 20 parts of Bulbus Allii, 20 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 12 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 2 hours, refilters after boiling 0.5 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide
Stock solution.
Embodiment 2
Weigh Folium Meliae 100 parts, Pyrethrum 30 parts, Herba Artemisiae Annuae 18 parts, 22 parts of Bulbus Allii, 20 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 14 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 2 hours, refilters after boiling 0.5 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide
Stock solution.
Embodiment 3
Weigh Folium Meliae 100 parts, Pyrethrum 31 parts, Herba Artemisiae Annuae 19 parts, 24 parts of Bulbus Allii, 20 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 16 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 2.5 hours, refilters after boiling 0.5 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide
Stock solution.
Embodiment 4
Weigh Folium Meliae 100 parts, Pyrethrum 32 parts, Herba Artemisiae Annuae 19 parts, 25 parts of Bulbus Allii, 20 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 18 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 2.5 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide
Stock solution.
Embodiment 5
Weigh Folium Meliae 100 parts, Pyrethrum 32 parts, Herba Artemisiae Annuae 20 parts, 26 parts of Bulbus Allii, 20 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 20 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 6
Weigh Folium Meliae 100 parts, Pyrethrum 32 parts, Herba Artemisiae Annuae 20 parts, 28 parts of Bulbus Allii, 20 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 22 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 7
Weigh Folium Meliae 100 parts, Pyrethrum 32 parts, Herba Artemisiae Annuae 21 parts, 30 parts of Bulbus Allii, 20 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 2.5 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide
Stock solution.
Embodiment 8
Weigh Folium Meliae 100 parts, Pyrethrum 32 parts, Herba Artemisiae Annuae 21 parts, 25 parts of Bulbus Allii, 22 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 20 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 2.5 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide
Stock solution.
Embodiment 9
Weigh Folium Meliae 100 parts, Pyrethrum 32 parts, Herba Artemisiae Annuae 22 parts, 25 parts of Bulbus Allii, 24 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 22 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 2.5 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide
Stock solution.
Embodiment 10
Weigh Folium Meliae 100 parts, Pyrethrum 34 parts, Herba Artemisiae Annuae 22 parts, 25 parts of Bulbus Allii, 26 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 11
Weigh Folium Meliae 100 parts, Pyrethrum 36 parts, Herba Artemisiae Annuae 23 parts, 25 parts of Bulbus Allii, 27 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 2.5 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide
Stock solution.
Embodiment 12
Weigh Folium Meliae 100 parts, Pyrethrum 36 parts, Herba Artemisiae Annuae 23 parts, 25 parts of Bulbus Allii, 28 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 13
Weigh Folium Meliae 100 parts, Pyrethrum 38 parts, Herba Artemisiae Annuae 23 parts, 25 parts of Bulbus Allii, 30 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 14
Weigh Folium Meliae 100 parts, Pyrethrum 38 parts, Herba Artemisiae Annuae 24 parts, 25 parts of Bulbus Allii, 28 parts of Fructus Capsici and 5 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 2.5 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide
Stock solution.
Embodiment 15
Weigh Folium Meliae 100 parts, Pyrethrum 40 parts, Herba Artemisiae Annuae 20 parts, 25 parts of Bulbus Allii, 28 parts of Fructus Capsici and 7 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 20 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 16
Weigh Folium Meliae 100 parts, Pyrethrum 40 parts, Herba Artemisiae Annuae 22 parts, 25 parts of Bulbus Allii, 28 parts of Fructus Capsici and 9 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 22 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 17
Weigh Folium Meliae 100 parts, Pyrethrum 40 parts, Herba Artemisiae Annuae 23 parts, 25 parts of Bulbus Allii, 28 parts of Fructus Capsici and 10 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 18
Weigh Folium Meliae 100 parts, Pyrethrum 44 parts, Herba Artemisiae Annuae 26 parts, 25 parts of Bulbus Allii, 28 parts of Fructus Capsici and 11 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 19
Weigh Folium Meliae 100 parts, Pyrethrum 48 parts, Herba Artemisiae Annuae 27 parts, 25 parts of Bulbus Allii, 28 parts of Fructus Capsici and 13 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Embodiment 20
Weigh Folium Meliae 100 parts, Pyrethrum 50 parts, Herba Artemisiae Annuae 28 parts, 25 parts of Bulbus Allii, 28 parts of Fructus Capsici and 15 parts of Rhizoma Zingiberis Recens, grind
Mill, adds clear water and soaks 24 hours, be heated to 95 DEG C, keep slight boiling condition 0.5 hour, filtered while hot, and filtrate stands cooling,
Filtering residue adds water immersion 3 hours, refilters after boiling 1 hour, and twice filtrate mixing, cryogenic vacuum concentrates, obtains pesticide former
Liquid.
Experimental example
The pesticide stock solution that embodiment 1～20 is prepared dilute with water 1000 times respectively, 1500 times, 2000 times, and test variant
Concentration pesticide, to scale insect, spider mite, sugar moth, heart-eating worm, leaf folder, Pieris rapae, the suppression ratio of wood louse, is shown in Table 1.
Suppression ratio (%) to various insects after the pesticide dilution that table 1 embodiment 1～20 prepares
As can be seen from Table 1, the natural pesticide compositions of the present invention has an insecticidal effect of wide spectrum, wherein for scale insect, six
The suppression ratio of some yellow spider and sugar moth is the highest, and the insect suppression ratio in embodiment 17 is the highest, is the optimal choice of inventive formulation.
Additionally, same pesticide stock solution extension rate is the lowest, insecticidal effect is the strongest.
Claims (3)
1. a natural organic agricultural chemical composition, it is characterized in that, include following components by weight: Folium Meliae 100 parts, Pyrethrum 40 parts, Herba Artemisiae Annuae 23 parts, 25 parts of Bulbus Allii, 28 parts of Fructus Capsici, 10 parts of Rhizoma Zingiberis Recens, the preparation method of described natural organic agricultural chemical composition includes following operating procedure: weigh Folium Meliae, Pyrethrum, Herba Artemisiae Annuae, Bulbus Allii, Fructus Capsici and Rhizoma Zingiberis Recens by weight, grind, add clear water and soak 12 ~ 24
Hour, it is heated to 90 ~ 100 DEG C, keeps slight boiling condition 0.5 ~ 1 hour, filtered while hot, filtrate stands cooling, and filtering residue adds water immersion 2 ~ 3 hours, refilters after boiling 0.5 ~ 1 hour, twice filtrate mixing, cryogenic vacuum concentrates, and obtains pesticide stock solution, dilutes 1000 ~ 2000
Can come into operation again.
The natural organic agricultural chemical composition of one the most according to claim 1, it is characterised in that in described preparation method, clear water addition is as the criterion to cover medical material.
The natural organic agricultural chemical composition of one the most according to claim 1, it is characterised in that in described preparation method, containing 1g medical material in every milliliter of described pesticide stock solution.
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