CN105432695A - Novel pesticide, and preparation method and application thereof - Google Patents
Novel pesticide, and preparation method and application thereof Download PDFInfo
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- CN105432695A CN105432695A CN201510937613.2A CN201510937613A CN105432695A CN 105432695 A CN105432695 A CN 105432695A CN 201510937613 A CN201510937613 A CN 201510937613A CN 105432695 A CN105432695 A CN 105432695A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses a novel pesticide, and a preparation method and an application thereof, and belongs to the technical field of preparation of pesticides. The novel pesticide comprises, by weight, leaves of Salix babylonica.L, Piper methysticum Forst, Camellia Sinensis leaf, Anabasis aphylla L., paulownia leaf, Derris fordii Oliv., garlic, neem, horseradish, Pterocarya stenoptera leaves, Cortex Fraxini, Sophora flavescens, Euphorbia soongarica, pyrethrum, onion, patrinia herb, purslane, Radix Scutellariae, aloe, Cortex Magnoliae Officinalis and water, and the novel pesticide is prepared through the steps of medicine solution extraction, concentration, drying, crushing, sieving and disinfection. The novel pesticide has the advantages of nontoxic component, no residue, no nuisance, simple production method, low cost and good application effect, can effectively prevent and treat yellow spiders, Parlatoria pergandii Comstock, papilios, leaf miner and other plant pests, has a primary killing rate reaching 96.06% or above, has no medicine resistance, and can be used for 4-6 years.
Description
Technical field
The invention belongs to insecticide preparing technical field, be specifically related to a kind of novel pesticide, preparation method and application thereof.
Background technology
Current control pest all use chemical insecticide mostly, along with the raising of living standards of the people, require high, not only will eat, and will eat health agricultural product quality.The Pesticide Residue that high malicious chemical pesticide causes more and more becomes the focus of social concerns.High-toxic pesticide is the core and the key that affect agricultural product quality and safety, not only affects agricultural product quality, directly endangers the healthy of the people, also affects increasing peasant income.Because the toxicity of high-toxic pesticide is large, the event of person poultry poisoning was caused to happen occasionally in the past.Very big on the impact of women and children, the children that teratogenesis is disabled are a lot.In addition, along with the protective awareness of countries in the world to environment for human survival and natural, ecological strengthens day by day, high malicious high residue insecticide will be restricted further.The quality safety of unreasonable use to agricultural product of agricultural chemicals constitutes a threat to, therefore, reduce Pesticide use particularly high-toxic pesticide use, to raising agricultural product quality and the market competitiveness, promote China's agricultural sustainable development, ensure the life security of broad masses of the people and very great meaning of building a harmonious society.
Because chemical pesticide is easy to the pesticide resistance causing insect; dosage is made in order to control efficiency well constantly increases; a lot of natural enemy and beneficial organism are murdered; and pollute us and to depend on for existence living environment; the more and more attention of Environmental protection; will be further strict to the Detecting Pesticide in agricultural product, therefore, greatly develop the direction that non-toxic and non-pollution high-efficiency plant source pesticide is Agrochemicals from now on.
Summary of the invention
The invention provides a kind of novel pesticide, preparation method and application thereof, use chemical pesticide control insect to cause the problem such as pest resistance to insecticide and contaminated environment to solve, novel pesticide composition of the present invention is nontoxic, and noresidue is nuisanceless, environmental protection; New type disinsection agent and process for producing same of the present invention is simple, and cost is low, and effect is good; Novel pesticide of the present invention effectively can prevent and treat the plant insects such as yellow spider, chaff sheet a red-spotted lizard, swallowtail butterfly, leaf miner, and one time killing rate all reaches more than 96.06%, and does not have drug resistance.
For solving above technical problem, the present invention by the following technical solutions:
A kind of novel pesticide, in units of weight portion, comprise following raw material: weeping willow leaf 40-60 part, kawakaw 40-60 part, tea free 40-60 part, Herba Anabasis aphyllae 30-50 part, paulownia leaves 30-50 part, poison trifoliate jewelvine 30-50 part, garlic 20-40 part, print chinaberry 20-40 part, horseradish 20-40 part, leaf of Pterocarya Stenoptera 20-30 part, bark of ash 20-30 part, kuh-seng 20-30 part, Roots of Euphorbia soongarica 20-30 part, Dalmatian chrysanthemum 15-25 part, onion 15-25 part, field pennycress 15-25 part, kitchen garden 15-25 part, root of large-flowered skullcap 10-20 part, aloe 10-20 part, bark of official magnolia 10-20 part, water 2000-7000 part.
Preferably, described novel pesticide, in units of weight portion, comprise following raw material: weeping willow leaf 45-55 part, kawakaw 45-55 part, tea free 45-55 part, Herba Anabasis aphyllae 35-45 part, paulownia leaves 35-45 part, poison trifoliate jewelvine 35-45 part, garlic 25-35 part, print chinaberry 25-35 part, horseradish 25-35 part, leaf of Pterocarya Stenoptera 22-28 part, bark of ash 22-28 part, kuh-seng 22-28 part, Roots of Euphorbia soongarica 22-28 part, Dalmatian chrysanthemum 18-22 part, onion 18-22 part, field pennycress 18-22 part, kitchen garden 18-22 part, root of large-flowered skullcap 12-18 part, aloe 12-18 part, bark of official magnolia 12-18 part, water 3000-6000 part.
Preferably, described novel pesticide, in units of weight portion, comprise following raw material: 50 parts, weeping willow leaf, kawakaw 50 parts, tea free 50 parts, Herba Anabasis aphyllae 40 parts, paulownia leaves 40 parts, malicious trifoliate jewelvine 40 parts, 30 parts, garlic, print chinaberry 30 parts, horseradish 30 parts, leaf of Pterocarya Stenoptera 25 parts, the bark of ash 25 parts, kuh-seng 25 parts, Roots of Euphorbia soongarica 25 parts, Dalmatian chrysanthemum 20 parts, onion 20 parts, field pennycress 20 parts, kitchen garden 20 parts, the root of large-flowered skullcap 15 parts, aloe 15 parts, the bark of official magnolia 15 parts, 4500 parts, water.
The present invention also provides a kind of preparation method of novel pesticide, it is characterized in that, comprises the following steps:
S1: by weeping willow leaf, kawakaw, tea free, Herba Anabasis aphyllae, paulownia leaves, malicious trifoliate jewelvine, garlic, print chinaberry, horseradish, leaf of Pterocarya Stenoptera, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Dalmatian chrysanthemum, onion, field pennycress, kitchen garden, the root of large-flowered skullcap, aloe, bark of official magnolia co-grinding, obtain mixture A, mixture A is added to the water, under ultrasonic assistant extraction method, extracts liquid;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained novel pesticide.
Preferably, step S2 herb liquid filters, and is concentrated into water content≤25%.
Preferably, in step S2, mixture B is dry at 90-100 DEG C.
More preferably, described mixture B is dried to water content≤6% at 90-100 DEG C.
Preferably, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
Preferably, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
The application of described novel pesticide in one or more plant insects of control yellow spider, chaff sheet a red-spotted lizard, swallowtail butterfly, leaf miner.
Pharmacology of the present invention is as follows:
Weeping willow leaf has the effect such as clearing heat and detoxicating, expelling wind and removing dampness, anti-inflammation, maggot of going out, infanticide Jue.
Kawakaw contains multiple Ginkgolide Component, has the multiple physiological and pharmacological effects such as anti-spasm, anti-top epilepsy, local anaesthesia, anti-inflammatory, Antifungi, desinsection, has stronger inhibitory action to shigella dysenteriae, typhoid bacillus and Escherichia coli.
The extract of tea free has potent bactericidal action, and tea tree can effectively tackle for various mycotic infection, can kill staphylococcus aureus, diphtheria bacillus.
Herba Anabasis aphyllae belongs to chenopod, is dicotyledon, has the effects such as clearing heat and detoxicating, anti-inflammation, pain relieving desinsection, can be used for rural area preparation agricultural chemicals of eliminating the four pests--rats, bedbugs, flies and mosquitoes, the use of disinfestation and deratization.
Paulownia leaves extract has antibacterial and antivirus action, propyl alcohol extract all has antibacterial activity, In vitro Bactericidal Experiments proves, paulownia leaves extract is stronger to staphylococcus aureus, hay bacillus effect, extract panlownin and sesamin, kill insect (fly, the mosquito etc.) effect of this binary to pyrethrins and allyl cinerin has synergistic effect.
Poison trifoliate jewelvine dicotyledon medicine leguminous plant, extract bitter, very toxic, there is killing parasites to relieve itshing, by effects such as arthritis with fixed pain caused by dampness.
In garlic, sulfur-containing compound has strong antibacterial and anti-inflammation functions, all has suppression and killing action to multiple coccus, bacillus, fungi and virus etc., is the one that in the natural plants found at present, antibacterial action is the strongest.
Print Melia, in Meliaceae, comes from Southeast Asia, and containing print chinaberry, solannin etc., have good disinsection efficiency, insect is once contact, and growth will be suppressed.
Pungent thing in horseradish has strong antibacterial killing ability, particularly has obvious effect to cholera bacteria, typhoid fever bacterium, colon bacillus, diphtheria bacterium, staphylococcus aureus etc.
Chinese ash has the effects such as antibacterial, desinsection, removing toxic substances, and leaf is poisonous, can used as pesticides insecticide.
The bark of ash has antibacterial insecticidal action, has obvious inhibitory action, be usually used in controlling bacillary dysentery clinically to staphylococcus aureus, bacillus subtilis, Escherichia coli, brewer's yeast, bacterium wine yeast etc., enteritis, leukorrhea, chronic bronchitis, red eye, swell pain etc.
Kuh-seng belongs to herbaceos perennial; Be taken as the substitute of monkshood and radix aconiti agrestis at the Northwest's kuh-seng and use, simultaneously the traditional medicine of the ethnic group such as Ye Shi Kazak, the Hui ethnic group, is mainly used in pain relieving, dehumidifying, cold-dispelling.
Roots of Euphorbia soongarica is herbaceos perennial, main product in Gansu, the ground such as Xinjiang and Russia, the substitute in new thick area as the root of Beijing euphorbia uses, and has effect of removing water retention by purgation, dispersing swelling and dissipating binds.
Dalmatian chrysanthemum containing 4 kinds of insecticidal constituents, pyrethrin (pyrethrin) I, II and cinerin (cinerin) I, II, Dalmatian chrysanthemum to various insects as mosquito, fly, bedbug and cockroach etc. have toxic action.
Onion is warm in nature, acrid-sweet flavor, eliminate the phlegm, diuresis, stomach-invigorating intestine-moisturizing, the function such as removing toxic substances desinsection, staphylococcus aureus, diphtheria bacillus can be killed.
Field pennycress, with root-like stock and root, all herbal medicine, belongs to antipyretic and antidotal type medicine in Chinese medicine, cool in nature, taste is pungent, bitter.Return liver, stomach, large intestine channel, have effect that is clearing heat and detoxicating, removing blood stasis and expelling pus.Modern pharmacy is thought, it is containing volatile oil, Patrinia scaniosaefolia saponin and β-sterol glucose formula, have anti-inflammatory, antibacterial, calm, protect the liver the effect with cardiac stimulant diuresis.Field pennycress has suppression or killing action to staphylococcus aureus, shigella dysenteriae, typhoid bacillus, Pseudomonas aeruginosa.
Kitchen garden is cold in nature, the sweet acid of taste, and have clearing heat and detoxicating, Li Shui dries, and loose blood detumescence, dust-collection sterilization, anti-inflammatory analgetic, effects such as cool blood of stopping blooding, have stronger inhibitory action to shigella dysenteriae, typhoid bacillus and Escherichia coli.
The root of large-flowered skullcap is labiate, and its active ingredient is 5 kinds of flavone components such as baicalein, baicalin, wogonin, neobaicalein.In addition, still containing cupreol, benzoic acid, baicalinase etc.Have antibacterial, desinsection, antiviral, calm, diuresis, guarantor's courage, protect the liver, detoxify, anti-inflammatory and make the effects such as blood sugar rising.
Aloe contains the multiple nutritional components such as lignin, aloietic acid, saponin, anthraquinone, aloin, vitamin, oxidase, lipase, amylase, lysine, leucine, threonine, isoleucine, phenyl alanine, valine.Extract component tinctura aloes in aloe is the material that antibiotic property is very strong, the germs such as energy killing fungus, mould, bacterium, virus, the growth breeding of suppression and eliminating pathogen, the germ class of aloe antibiotic sterilization has: the germ of the diseases such as diphtheria bacterium, tetanolysin, pulmonitis strain, lactic acid bacteria, dysentery bacillus, colon bacillus, plague bacterium, cholera bacteria and initiation tympanitis, cystitis, pyesis, measles, rabies, polio, epidemic encephalitis.
The ether of the bark of official magnolia and methanolic extract have strong antibacterial action to cariogenic bacteria streptococcus mutans (Streptococusmatuans), and its Antibacterial Constituents is defined as Magnolol and Honokiol.Both are 6.3 μ g/ml to the minimum inhibitory concentration (MIC) of streptococcus mutans, and its antibacterial action (to streptococcus mutans) is stronger than berberine.The first deduction of the bark of official magnolia divides magnocurarine and Cortex Magnoliae Officinalis volatile oil saturated aqueous solution to have certain bacteriostasis to staphylococcus aureus, sarcine and hay bacillus, and the bark of official magnolia also has antibacterial activity to Diplococcus pneumopniae and shigella dysenteriae.
The present invention has following beneficial effect:
(1) novel pesticide composition of the present invention is nontoxic, and noresidue is nuisanceless, environmental protection, can not bring environmental pollution;
(2) novel pesticide of the present invention effectively can prevent and treat the plant insects such as yellow spider, chaff sheet a red-spotted lizard, swallowtail butterfly, leaf miner, and one time killing rate all reaches more than 96.06%, and does not have resistance to medical, can use by 4-6;
(3) new type disinsection agent and process for producing same of the present invention is simple, and cost is low, easy to use, and effect is good, is conducive to applying.
Embodiment
Be specifically described below in conjunction with specific embodiment.
Embodiment 1
A kind of novel pesticide, in units of weight portion, comprise following raw material: 40 parts, weeping willow leaf, kawakaw 40 parts, tea free 40 parts, Herba Anabasis aphyllae 30 parts, paulownia leaves 30 parts, malicious trifoliate jewelvine 30 parts, 20 parts, garlic, print chinaberry 20 parts, horseradish 20 parts, leaf of Pterocarya Stenoptera 20 parts, the bark of ash 20 parts, kuh-seng 20 parts, Roots of Euphorbia soongarica 20 parts, Dalmatian chrysanthemum 15 parts, onion 15 parts, field pennycress 15 parts, kitchen garden 15 parts, the root of large-flowered skullcap 10 parts, aloe 10 parts, the bark of official magnolia 10 parts, 2000 parts, water.
The preparation method of described novel pesticide, comprises the following steps:
S1: by weeping willow leaf, kawakaw, tea free, Herba Anabasis aphyllae, paulownia leaves, malicious trifoliate jewelvine, garlic, print chinaberry, horseradish, leaf of Pterocarya Stenoptera, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Dalmatian chrysanthemum, onion, field pennycress, kitchen garden, the root of large-flowered skullcap, aloe, bark of official magnolia co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 140W, concentration of alcohol is 55%, Extracting temperature is 55 DEG C, and extraction time is 50min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 25%, and obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, pressure is sterilizing 5min under 210KPa, obtained novel pesticide.
Embodiment 2
A kind of novel pesticide, in units of weight portion, comprise following raw material: 60 parts, weeping willow leaf, kawakaw 60 parts, tea free 60 parts, Herba Anabasis aphyllae 50 parts, paulownia leaves 50 parts, malicious trifoliate jewelvine 50 parts, 40 parts, garlic, print chinaberry 40 parts, horseradish 40 parts, leaf of Pterocarya Stenoptera 30 parts, the bark of ash 30 parts, kuh-seng 30 parts, Roots of Euphorbia soongarica 30 parts, Dalmatian chrysanthemum 25 parts, onion 25 parts, field pennycress 25 parts, kitchen garden 25 parts, the root of large-flowered skullcap 20 parts, aloe 20 parts, the bark of official magnolia 20 parts, 7000 parts, water.
The preparation method of described novel pesticide, comprises the following steps:
S1: by weeping willow leaf, kawakaw, tea free, Herba Anabasis aphyllae, paulownia leaves, malicious trifoliate jewelvine, garlic, print chinaberry, horseradish, leaf of Pterocarya Stenoptera, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Dalmatian chrysanthemum, onion, field pennycress, kitchen garden, the root of large-flowered skullcap, aloe, bark of official magnolia co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 180W, concentration of alcohol is 75%, Extracting temperature is 65 DEG C, and extraction time is 30min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 18%, and obtain mixture B, it is 4% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained novel pesticide.
Embodiment 3
A kind of novel pesticide, in units of weight portion, comprise following raw material: 50 parts, weeping willow leaf, kawakaw 50 parts, tea free 50 parts, Herba Anabasis aphyllae 40 parts, paulownia leaves 40 parts, malicious trifoliate jewelvine 40 parts, 30 parts, garlic, print chinaberry 30 parts, horseradish 30 parts, leaf of Pterocarya Stenoptera 25 parts, the bark of ash 25 parts, kuh-seng 25 parts, Roots of Euphorbia soongarica 25 parts, Dalmatian chrysanthemum 20 parts, onion 20 parts, field pennycress 20 parts, kitchen garden 20 parts, the root of large-flowered skullcap 15 parts, aloe 15 parts, the bark of official magnolia 15 parts, 4500 parts, water.
The preparation method of described novel pesticide, comprises the following steps:
S1: by weeping willow leaf, kawakaw, tea free, Herba Anabasis aphyllae, paulownia leaves, malicious trifoliate jewelvine, garlic, print chinaberry, horseradish, leaf of Pterocarya Stenoptera, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Dalmatian chrysanthemum, onion, field pennycress, kitchen garden, the root of large-flowered skullcap, aloe, bark of official magnolia co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 65%, Extracting temperature is 60 DEG C, and extraction time is 40min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 135 DEG C in temperature, pressure is sterilizing 4min under 220KPa, obtained novel pesticide.
Embodiment 4
A kind of novel pesticide, in units of weight portion, comprise following raw material: 45 parts, weeping willow leaf, kawakaw 45 parts, tea free 45 parts, Herba Anabasis aphyllae 35 parts, paulownia leaves 35 parts, malicious trifoliate jewelvine 35 parts, 25 parts, garlic, print chinaberry 25 parts, horseradish 25 parts, leaf of Pterocarya Stenoptera 22 parts, the bark of ash 22 parts, kuh-seng 22 parts, Roots of Euphorbia soongarica 22 parts, Dalmatian chrysanthemum 18 parts, onion 18 parts, field pennycress 18 parts, kitchen garden 18 parts, the root of large-flowered skullcap 12 parts, aloe 12 parts, the bark of official magnolia 12 parts, 3000 parts, water.
The preparation method of described novel pesticide, comprises the following steps:
S1: by weeping willow leaf, kawakaw, tea free, Herba Anabasis aphyllae, paulownia leaves, malicious trifoliate jewelvine, garlic, print chinaberry, horseradish, leaf of Pterocarya Stenoptera, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Dalmatian chrysanthemum, onion, field pennycress, kitchen garden, the root of large-flowered skullcap, aloe, bark of official magnolia co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 150W, concentration of alcohol is 60%, Extracting temperature is 55 DEG C, and extraction time is 45min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 22%, and obtain mixture B, it is 6% that gained mixture B is dried to water content at 90 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 134 DEG C in temperature, pressure is sterilizing 5min under 210KPa, obtained novel pesticide.
Embodiment 5
A kind of novel pesticide, in units of weight portion, comprise following raw material: 55 parts, weeping willow leaf, kawakaw 55 parts, tea free 55 parts, Herba Anabasis aphyllae 45 parts, paulownia leaves 45 parts, malicious trifoliate jewelvine 45 parts, 35 parts, garlic, print chinaberry 35 parts, horseradish 35 parts, leaf of Pterocarya Stenoptera 28 parts, the bark of ash 28 parts, kuh-seng 28 parts, Roots of Euphorbia soongarica 28 parts, Dalmatian chrysanthemum 22 parts, onion 22 parts, field pennycress 22 parts, kitchen garden 22 parts, the root of large-flowered skullcap 18 parts, aloe 18 parts, the bark of official magnolia 18 parts, 6000 parts, water.
The preparation method of described novel pesticide, comprises the following steps:
S1: by weeping willow leaf, kawakaw, tea free, Herba Anabasis aphyllae, paulownia leaves, malicious trifoliate jewelvine, garlic, print chinaberry, horseradish, leaf of Pterocarya Stenoptera, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Dalmatian chrysanthemum, onion, field pennycress, kitchen garden, the root of large-flowered skullcap, aloe, bark of official magnolia co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 170W, concentration of alcohol is 70%, Extracting temperature is 65 DEG C, and extraction time is 35min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 20%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 100 DEG C, then pulverize, cross 200 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained novel pesticide.
Embodiment 6
A kind of novel pesticide, in units of weight portion, comprise following raw material: 58 parts, weeping willow leaf, kawakaw 58 parts, tea free 58 parts, Herba Anabasis aphyllae 46 parts, paulownia leaves 46 parts, malicious trifoliate jewelvine 46 parts, 35 parts, garlic, print chinaberry 35 parts, horseradish 35 parts, leaf of Pterocarya Stenoptera 28 parts, the bark of ash 28 parts, kuh-seng 28 parts, Roots of Euphorbia soongarica 28 parts, Dalmatian chrysanthemum 23 parts, onion 23 parts, field pennycress 23 parts, kitchen garden 23 parts, the root of large-flowered skullcap 18 parts, aloe 18 parts, the bark of official magnolia 18 parts, 6500 parts, water.
The preparation method of described novel pesticide, comprises the following steps:
S1: by weeping willow leaf, kawakaw, tea free, Herba Anabasis aphyllae, paulownia leaves, malicious trifoliate jewelvine, garlic, print chinaberry, horseradish, leaf of Pterocarya Stenoptera, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Dalmatian chrysanthemum, onion, field pennycress, kitchen garden, the root of large-flowered skullcap, aloe, bark of official magnolia co-grinding, obtain mixture A, mixture A is added to the water, liquid is extracted under ultrasonic assistant extraction method, condition is: ultrasonic power is 160W, concentration of alcohol is 70%, Extracting temperature is 60 DEG C, and extraction time is 45min;
S2: by medical filtration obtained for step S1, to be concentrated into water content be 23%, and obtain mixture B, it is 5% that gained mixture B is dried to water content at 95 DEG C, then pulverize, cross 100 mesh sieve, gained powder is 136 DEG C in temperature, pressure is sterilizing 3min under 230KPa, obtained novel pesticide.
For verifying the effect of novel pesticide of the present invention, by following experimental verification.
Adopt the novel pesticide of embodiment 1-6, the ratio of joining 40g water in 1g novel pesticide uses, and once prevents and treats the test of the plant insects such as yellow spider, chaff sheet a red-spotted lizard, swallowtail butterfly, leaf miner, the results are shown in following table.
From upper table, the novel pesticide of embodiment of the present invention 1-6 is to a killing rate of the plant insects such as yellow spider, chaff sheet a red-spotted lizard, swallowtail butterfly, leaf miner all more than 96.06%, and result of use is good.Due to novel pesticide nonhazardous of the present invention, do not pollute, do not remain, it is efficient to add control efficiency, therefore, can widely popularize application.
Above content can not assert that the present invention specifically implements to be confined to these explanations; for general technical staff of the technical field of the invention; do not departing under concept thereof of the present invention; some simple deduction or replace can also be made, all should be considered as belonging to the scope of patent protection that the present invention is determined by submitted to claims.
Claims (10)
1. a novel pesticide, it is characterized in that, in units of weight portion, comprise following raw material: weeping willow leaf 40-60 part, kawakaw 40-60 part, tea free 40-60 part, Herba Anabasis aphyllae 30-50 part, paulownia leaves 30-50 part, poison trifoliate jewelvine 30-50 part, garlic 20-40 part, print chinaberry 20-40 part, horseradish 20-40 part, leaf of Pterocarya Stenoptera 20-30 part, bark of ash 20-30 part, kuh-seng 20-30 part, Roots of Euphorbia soongarica 20-30 part, Dalmatian chrysanthemum 15-25 part, onion 15-25 part, field pennycress 15-25 part, kitchen garden 15-25 part, root of large-flowered skullcap 10-20 part, aloe 10-20 part, bark of official magnolia 10-20 part, water 2000-7000 part.
2. novel pesticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: weeping willow leaf 45-55 part, kawakaw 45-55 part, tea free 45-55 part, Herba Anabasis aphyllae 35-45 part, paulownia leaves 35-45 part, poison trifoliate jewelvine 35-45 part, garlic 25-35 part, print chinaberry 25-35 part, horseradish 25-35 part, leaf of Pterocarya Stenoptera 22-28 part, bark of ash 22-28 part, kuh-seng 22-28 part, Roots of Euphorbia soongarica 22-28 part, Dalmatian chrysanthemum 18-22 part, onion 18-22 part, field pennycress 18-22 part, kitchen garden 18-22 part, root of large-flowered skullcap 12-18 part, aloe 12-18 part, bark of official magnolia 12-18 part, water 3000-6000 part.
3. novel pesticide according to claim 1, it is characterized in that, in units of weight portion, comprise following raw material: 50 parts, weeping willow leaf, kawakaw 50 parts, tea free 50 parts, Herba Anabasis aphyllae 40 parts, paulownia leaves 40 parts, malicious trifoliate jewelvine 40 parts, 30 parts, garlic, print chinaberry 30 parts, horseradish 30 parts, leaf of Pterocarya Stenoptera 25 parts, the bark of ash 25 parts, kuh-seng 25 parts, Roots of Euphorbia soongarica 25 parts, Dalmatian chrysanthemum 20 parts, onion 20 parts, field pennycress 20 parts, kitchen garden 20 parts, the root of large-flowered skullcap 15 parts, aloe 15 parts, the bark of official magnolia 15 parts, 4500 parts, water.
4. a preparation method for the novel pesticide according to any one of claim 1-3, is characterized in that, comprises the following steps:
S1: by weeping willow leaf, kawakaw, tea free, Herba Anabasis aphyllae, paulownia leaves, malicious trifoliate jewelvine, garlic, print chinaberry, horseradish, leaf of Pterocarya Stenoptera, the bark of ash, kuh-seng, Roots of Euphorbia soongarica, Dalmatian chrysanthemum, onion, field pennycress, kitchen garden, the root of large-flowered skullcap, aloe, bark of official magnolia co-grinding, obtain mixture A, mixture A is added to the water, under ultrasonic assistant extraction method, extracts liquid;
S2: by medical filtration obtained for step S1, concentrated, obtain mixture B, gained mixture B be dry, pulverize, sieve, sterilizing, obtained novel pesticide.
5. the preparation method of novel pesticide according to claim 4, it is characterized in that, the condition that the extraction method of ultrasonic assistant described in step S1 extracts liquid is, condition is: ultrasonic power is 140-180W, concentration of alcohol is 55%-75%, Extracting temperature is 55-65 DEG C, and extraction time is 30-50min; Step S2 herb liquid filters, and is concentrated into water content≤25%.
6. the preparation method of novel pesticide according to claim 4, is characterized in that, in step S2, mixture B is dry at 90-100 DEG C.
7. the preparation method of novel pesticide according to claim 6, is characterized in that, described mixture B is dried to water content≤6% at 90-100 DEG C.
8. the preparation method of novel pesticide according to claim 4, is characterized in that, the condition of sieving in step S2 is: cross 100-200 mesh sieve.
9. the preparation method of novel pesticide according to claim 4, is characterized in that, the condition of sterilizing in step S2 is: temperature is 134-136 DEG C, and pressure is 210-230KPa, and the time is 3-5min.
10. the application of the novel pesticide according to any one of claim 1-3 in one or more plant insects of control yellow spider, chaff sheet a red-spotted lizard, swallowtail butterfly, leaf miner.。
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| CN201510937613.2A CN105432695A (en) | 2015-12-16 | 2015-12-16 | Novel pesticide, and preparation method and application thereof |
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| CN201510937613.2A CN105432695A (en) | 2015-12-16 | 2015-12-16 | Novel pesticide, and preparation method and application thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105935065A (en) * | 2016-05-30 | 2016-09-14 | 铜陵东晟生态农业科技有限公司 | Fruit tree pesticide |
| CN105994412A (en) * | 2016-06-01 | 2016-10-12 | 蚌埠市宝煦家庭农场 | Insecticide for control of black currant plume moth pest |
| CN106212557A (en) * | 2016-07-20 | 2016-12-14 | 无锡市厚桥中东桃梨专业合作社 | A kind of medicine based on herbs preventing and treating anthracnose of peach |
| CN106342911A (en) * | 2016-08-01 | 2017-01-25 | 韦波 | Botanical insecticide |
| CN106538617A (en) * | 2016-09-22 | 2017-03-29 | 广西汇智生产力促进中心有限公司 | A kind of sweet bean insecticide |
| CN106561730A (en) * | 2016-10-31 | 2017-04-19 | 钟山县昱成水果种植专业合作社 | Efficient pharmaceutical composition for preventing and treating black rot of citrus gonggan and preparation method thereof |
| KR20220011886A (en) | 2020-07-22 | 2022-02-03 | 한국화학연구원 | Composition for controlling plant diseases including Pterocarya tonkinensis extract or fraction thereof, and method of controlling plant diseases using the same |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1111478A (en) * | 1994-11-01 | 1995-11-15 | 吴日章 | Multivariate Chinese herbal medicine plant insecticide and preparation method thereof |
| CN1385077A (en) * | 2001-07-02 | 2002-12-18 | 梁军强 | Plant foliage fertilizer |
| CN101491259A (en) * | 2008-01-25 | 2009-07-29 | 郝素平 | Nuisance free pesticide |
| CN104026176A (en) * | 2014-06-25 | 2014-09-10 | 无锡市崇安区科技创业服务中心 | Natural organic pesticide composition and preparation method thereof |
| CN102775238B (en) * | 2012-08-22 | 2015-06-24 | 乌鲁木齐木易联华生物科技有限公司 | Organic plant pesticide fertilizer with pesticidal and bactericidal effects and production technique thereof |
-
2015
- 2015-12-16 CN CN201510937613.2A patent/CN105432695A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1111478A (en) * | 1994-11-01 | 1995-11-15 | 吴日章 | Multivariate Chinese herbal medicine plant insecticide and preparation method thereof |
| CN1385077A (en) * | 2001-07-02 | 2002-12-18 | 梁军强 | Plant foliage fertilizer |
| CN101491259A (en) * | 2008-01-25 | 2009-07-29 | 郝素平 | Nuisance free pesticide |
| CN102775238B (en) * | 2012-08-22 | 2015-06-24 | 乌鲁木齐木易联华生物科技有限公司 | Organic plant pesticide fertilizer with pesticidal and bactericidal effects and production technique thereof |
| CN104026176A (en) * | 2014-06-25 | 2014-09-10 | 无锡市崇安区科技创业服务中心 | Natural organic pesticide composition and preparation method thereof |
Non-Patent Citations (5)
| Title |
|---|
| 伍有声等 编: "《实用新农药指南》", 31 August 1991 * |
| 刘强等 主编: "《中药新产品开发》", 31 March 2013 * |
| 蔡明段: "《柑橘病虫害原色图鉴》", 30 November 2011 * |
| 谭仁祥: "《植物成分功能》", 31 October 2003 * |
| 邱立新: "《林业药剂药械使用技术》", 31 January 2011 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105935065A (en) * | 2016-05-30 | 2016-09-14 | 铜陵东晟生态农业科技有限公司 | Fruit tree pesticide |
| CN105994412A (en) * | 2016-06-01 | 2016-10-12 | 蚌埠市宝煦家庭农场 | Insecticide for control of black currant plume moth pest |
| CN106212557A (en) * | 2016-07-20 | 2016-12-14 | 无锡市厚桥中东桃梨专业合作社 | A kind of medicine based on herbs preventing and treating anthracnose of peach |
| CN106342911A (en) * | 2016-08-01 | 2017-01-25 | 韦波 | Botanical insecticide |
| CN106538617A (en) * | 2016-09-22 | 2017-03-29 | 广西汇智生产力促进中心有限公司 | A kind of sweet bean insecticide |
| CN106561730A (en) * | 2016-10-31 | 2017-04-19 | 钟山县昱成水果种植专业合作社 | Efficient pharmaceutical composition for preventing and treating black rot of citrus gonggan and preparation method thereof |
| KR20220011886A (en) | 2020-07-22 | 2022-02-03 | 한국화학연구원 | Composition for controlling plant diseases including Pterocarya tonkinensis extract or fraction thereof, and method of controlling plant diseases using the same |
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