CN103766545A - Preparation method of cordyceps militaris extractive-rich cordyceps militaris tea - Google Patents
Preparation method of cordyceps militaris extractive-rich cordyceps militaris tea Download PDFInfo
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- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 241001122767 Theaceae Species 0.000 title abstract 5
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- 239000012141 concentrate Substances 0.000 claims abstract description 27
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000000926 separation method Methods 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000009835 boiling Methods 0.000 claims abstract description 12
- 238000000605 extraction Methods 0.000 claims abstract description 8
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- 150000004676 glycans Chemical class 0.000 claims description 18
- 229920001282 polysaccharide Polymers 0.000 claims description 18
- 239000005017 polysaccharide Substances 0.000 claims description 18
- 241000233866 Fungi Species 0.000 claims description 14
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- 239000000203 mixture Substances 0.000 claims description 13
- 239000007787 solid Substances 0.000 claims description 11
- 238000004821 distillation Methods 0.000 claims description 10
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 230000003750 conditioning effect Effects 0.000 claims description 6
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- 235000019634 flavors Nutrition 0.000 claims description 6
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- 239000013049 sediment Substances 0.000 claims description 5
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- 238000010298 pulverizing process Methods 0.000 claims description 4
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- 235000009917 Crataegus X brevipes Nutrition 0.000 claims description 3
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- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims description 3
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- 235000012907 honey Nutrition 0.000 claims description 3
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 claims description 3
- 240000000171 Crataegus monogyna Species 0.000 claims 1
- 230000000050 nutritive effect Effects 0.000 abstract description 5
- 238000003809 water extraction Methods 0.000 abstract description 5
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- KQLDDLUWUFBQHP-UHFFFAOYSA-N Cordycepin Natural products C1=NC=2C(N)=NC=NC=2N1C1OCC(CO)C1O KQLDDLUWUFBQHP-UHFFFAOYSA-N 0.000 description 1
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 description 1
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- OFEZSBMBBKLLBJ-BAJZRUMYSA-N cordycepin Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@@H]1O[C@H](CO)C[C@H]1O OFEZSBMBBKLLBJ-BAJZRUMYSA-N 0.000 description 1
- OFEZSBMBBKLLBJ-UHFFFAOYSA-N cordycepine Natural products C1=NC=2C(N)=NC=NC=2N1C1OC(CO)CC1O OFEZSBMBBKLLBJ-UHFFFAOYSA-N 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention discloses a preparation method of cordyceps militaris extractive-rich cordyceps militaris tea. The preparation method of the cordyceps militaris extractive-rich cordyceps militaris tea comprises the following steps: preparing two parts of cordyceps militaris fruiting bodies with the same mass, adding one part of fruiting bodies to an ethanol solution for extraction, carrying out solid-liquid separation, distilling liquid at reduced pressure to concentrate so as to obtain a concentrated solution; putting the fruiting bodies subjected to alcohol extraction and separation in boiling water for extraction, carrying out solid-liquid separation, distilling liquid at reduced pressure to concentrate so as to obtain extractum; drying and crushing the fruiting bodies subjected to alcohol extraction and water extraction, adding water, heating till boiling, extracting, centrifuging and filtering so as to obtain cordyceps militaris fruiting body precipitates; concentrating liquid so as to obtain a concentrated solution; and mixing the prepared concentrated solution and the extractum with the other part of dried cordyceps militaris fruiting bodies, drying, subpackaging, and sterilizing, thus obtaining the nutrition enhancement type cordyceps militaris tea. The cordyceps militaris extractive-rich cordyceps militaris tea has very high nutritive value and treatment effect and is convenient to carry and eat; active ingredients of cordyceps militaris are furthest utilized.
Description
Technical field
The invention belongs to Cordyceps militaris tea preparing technical field, relate in particular to a kind of preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea.
Background technology
Cordyceps militaris, is commonly called as northern Chinese caterpillar fungus, and its medical value is similar to Cordyceps sinensis, therefore be recited as again " northern Chinese caterpillar Fungus " in pharmacopeia.It not only has high nutritive value, and has high health care.Contain the various bioactivators such as cordycepic acid, cordycepin, Flavonoid substances and SOD, Cordyceps sinensis polysaccharide and rich in protein and amino acid etc. because of Cordyceps militaris; so it is in anti-cancer; anticancer; reducing blood lipid, prevents and treats artery sclerosis, the protection heart, brain tissue; tranquilizing soporific; reduce phlegm, relieving asthma, protect the aspects such as lung kidney-nourishing and there is adjuvant treatment efficacy.
Above-mentioned Cordyceps militaris function factor (nutrient) can be by steeping in wine, for the stripping of the mode such as tea-drinking, Baoshang, directly absorbed and bring into play its function by human body.But, not all active material can all extract by a kind of separate mode, different active materials are separated by diverse ways, only have the multiple separation method of employing and according to successively rational separation sequence, could maximum keep the active material in Cordyceps militaris.Some function factor must be by modern separation technology processing, and body could absorb and bring into play its function.For example Cordyceps sinensis polysaccharide, this material is the constituent of Cordyceps militaris cell membrane, combines closely with other materials in cell membrane, if without separation of polysaccharides technical finesse, this function factor can not absorbed by body.And Cordyceps sinensis polysaccharide all has important health care.The multiple biologically actives such as antitumor, antiviral, anti-ageing, anti-oxidant, hypoglycemic and immunoregulation effect that Polysaccharides in Cultured Cordyceps militaris has, measurement result shows, Polysaccharides in Cultured Cordyceps militaris content is 32.30-60.32mg/g.
Fruiting bodies of cordyceps militaris is approved as new resource food on March 16th, 2009 by the Ministry of Public Health, stipulates that its scope of application is: directly edible, drinks, can, flavouring, beverage.Take Cordyceps militaris as raw material or directly to produce the patented product of " alternative tea " or " health protection tea " increasing, its mode of production can be divided into type: pulverize mixed matching: fruiting bodies of cordyceps militaris or mycelia and other auxiliary materials are pulverized 1., then carry out mixture according to certain ratio, between main ingredient, cooperatively interact and reach the effect that strengthens or increase some function; 2. extract processing type: in this processing type, be divided into again two kinds, (1) feature of this series products is first fruiting bodies of cordyceps militaris or unclassified stores to be carried out to alcohol extracting or water extraction, then with dry fruiting bodies of cordyceps militaris or unclassified stores, alcohol extract or water extraction liquid are adsorbed to the dry finished product that obtains.(2) feature of this series products is first fruiting bodies of cordyceps militaris or unclassified stores to be carried out to alcohol extracting or water extraction, then by alcohol extract or the dry finished product that obtains of water extraction liquid.The feature of this series products is that instant capacity is good, has the feature of the first type products concurrently simultaneously; 3. the processing type of getting a lift: fruiting bodies of cordyceps militaris or mycelium are directly sneaked in green tea or black tea raw material, and together processed according to the processing technology of green tea or black tea and tealeaves, its products characteristics is the concept of having used Chinese caterpillar fungus, has ignored the functional of Chinese caterpillar fungus.
The function factor of the Cordyceps militaris that existing Cordyceps militaris series products manufacture exists can not extract completely, has reduced nutritive value and the therapeutic efficiency of Cordyceps militaris series products.
Summary of the invention
The object of the embodiment of the present invention is to provide a kind of preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea, the function factor that is intended to the Cordyceps militaris that solves existing Cordyceps militaris series products manufacture existence can not extract completely, has reduced the nutritive value of Cordyceps militaris series products and the problem of therapeutic efficiency.
The embodiment of the present invention is achieved in that a kind of preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea, and this preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea comprises the following steps:
Step 1, gets weight fruiting bodies of cordyceps militaris m1, the m2 (m1=m2) such as two parts;
Step 2, get Cordyceps militaris, add 20%～95% ethanol water solution lixiviate according to volume ratio, solid-liquid ratio is 1: 4～6 (weight per volume), lixiviate 3 hours～6 hours under 40 ℃ of vacuum conditions, Separation of Solid and Liquid, repeat aforesaid operations once, merge alcohol extract twice, by liquid pressure-reducing Distillation recovery ethanol, and obtain the concentrate of original volume 1/4～1/6;
Step 3, the Cordyceps militaris that step 2 is obtained is placed in boiling water and extracts, and solid-liquid ratio is 1: 4～6 (weight per volume), and 100 ℃ are boiled 3 hours～6 hours, and Separation of Solid and Liquid, by liquid pressure-reducing distillation, obtains the concentrate of original volume 1/4～1/8;
Step 4, the Cordyceps militaris that step 3 is obtained is dry, pulverizing, adds water, and solid-liquid ratio is 1: 6～10 (weight per volume), and is heated to boiling extraction, keeps 3h, and centrifugal filtering, repeats last time and operates twice, obtains Cordyceps militaris sediment; Liquid concentration, to 1/6～1/10 of original volume, is obtained to the thick polysaccharide concentrate of Chinese caterpillar fungus;
Step 5, concentrate, step 3 obtain obtains the thick polysaccharide concentrate of Cordyceps militaris that concentrate, step 4 obtain and mix with the drying fruiting bodies of cordyceps militaris of m2 equivalent for obtaining that step 2 is obtained, can in mixture, add local flavor conditioning agent, mixture is dry, packing, sterilizing obtain the reinforced Cordyceps militaris tea of differently flavoured nutrition.
Further, in step 1, Cordyceps militaris can be selected one or more in fruiting bodies of cordyceps militaris, cordyceps mycelium, Cordyceps militaris polypide and Chinese caterpillar fungus culture medium.
Further, Cordyceps militaris is preferably fruiting bodies of cordyceps militaris.
Further, in step 4, Cordyceps militaris is crushed to 50 order～100 orders.
Further, in step 5, local flavor conditioning agent can be citric acid, dextrin, cyclodextrin, hawthorn, honey etc.
The preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea provided by the invention, adopt modern bioseparation technology, various function factors in fruiting bodies of cordyceps militaris (can be also the mixture of mycelium, polypide, culture medium or above-mentioned substance) are more effectively extracted, then various extracts and Cordyceps militaris are mixed and made into the reinforced Cordyceps militaris tea of nutrition.Preparation method of the present invention can extract the function factor in Cordyceps militaris completely, the Cordyceps militaris active ingredient obtaining, the all function factors of Cordyceps militaris are comprised, there is high nutritive value and therapeutic efficiency, the active component of Cordyceps militaris is got the maximum use, and be convenient for carrying with edible.The reinforced Cordyceps militaris tea of nutrition provided by the invention, commodity value also exceeds common Chinese caterpillar fungus several times, has significant economic benefit and social benefit.
Accompanying drawing explanation
Fig. 1 is the preparation method's flow chart that is rich in Cordyceps militaris extract Cordyceps militaris tea that the embodiment of the present invention provides.
The specific embodiment
In order to make object of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not intended to limit the present invention.
Below in conjunction with drawings and the specific embodiments, application principle of the present invention is further described.
As shown in Figure 1, the preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea of the embodiment of the present invention comprises the following steps:
S101: get fruiting bodies of cordyceps militaris and add ethanolic solution lixiviate, Separation of Solid and Liquid, obtains concentrate by liquid pressure-reducing distillation and concentration;
S102: the solid content obtaining is placed in to boiling water and extracts, Separation of Solid and Liquid, becomes medicinal extract by liquid pressure-reducing distillation and concentration;
S103: by dry the fructification obtaining, pulverizing, add water and be heated to boiling and extract, centrifugal filtering, obtains fruiting bodies of cordyceps militaris sediment; By liquid concentration, obtain concentrate;
S104: by obtain obtain concentrate and medicinal extract mixes with drying fruiting bodies of cordyceps militaris, is dried, packing, sterilizing obtain being rich in Cordyceps militaris extract Cordyceps militaris tea.
The present invention specifically comprises the steps:
Step 1, gets weight fruiting bodies of cordyceps militaris m1, the m2 (m1=m2) such as two parts;
Step 2, get Cordyceps militaris, add 20%～95% ethanol water solution lixiviate according to volume ratio, solid-liquid ratio is 1: 4～6 (weight per volume), lixiviate 3 hours～6 hours under 40 ℃ of vacuum conditions, Separation of Solid and Liquid, repeat aforesaid operations once, merge alcohol extract twice, by liquid pressure-reducing Distillation recovery ethanol, and obtain the concentrate of original volume 1/4～1/6;
Step 3, the Cordyceps militaris that step 2 is obtained is placed in boiling water and extracts, and solid-liquid ratio is 1: 4～6 (weight per volume), and 100 ℃ are boiled 3 hours～6 hours, and Separation of Solid and Liquid, by liquid pressure-reducing distillation, obtains the concentrate of original volume 1/4～1/8;
Step 4, the Cordyceps militaris that step 3 is obtained is dry, pulverizing, adds water, and solid-liquid ratio is 1: 6～10 (weight per volume), and is heated to boiling extraction, keeps 3h, and centrifugal filtering, repeats last time and operates twice, obtains Cordyceps militaris sediment; Liquid concentration, to 1/6～1/10 of original volume, is obtained to the thick polysaccharide concentrate of Chinese caterpillar fungus;
Step 5, concentrate, step 3 obtain obtains the thick polysaccharide concentrate of Cordyceps militaris that concentrate, step 4 obtain and mix with the drying fruiting bodies of cordyceps militaris of m2 equivalent for obtaining that step 2 is obtained, can in mixture, add local flavor conditioning agent, mixture is dry, packing, sterilizing obtain the reinforced Cordyceps militaris tea of differently flavoured nutrition.
Further, in step 1, Cordyceps militaris can be selected one or more in fruiting bodies of cordyceps militaris, cordyceps mycelium, Cordyceps militaris polypide and Chinese caterpillar fungus culture medium.
Further, Cordyceps militaris is preferably fruiting bodies of cordyceps militaris.
Further, in step 4, Cordyceps militaris is crushed to 50 order～100 orders.
Further, in step 5, local flavor conditioning agent can be citric acid, dextrin, cyclodextrin, hawthorn, honey etc.
In conjunction with embodiments of the invention, the present invention is described further:
Embodiment 1,
1) get weight fruiting bodies of cordyceps militaris m1, the m2 (m1=m2) such as two parts;
2) get Cordyceps militaris (m1), add the lixiviate of 30% (volume ratio) ethanol water solution, solid-liquid ratio is 1: 4 (weight/volume), lixiviate 3 hours under 40 ℃ of vacuum conditions, and Separation of Solid and Liquid, repeats aforesaid operations once.Merge alcohol extract twice, by liquid pressure-reducing Distillation recovery ethanol, and obtain the concentrate of original volume 1/4;
3) by step 2) Cordyceps militaris that obtains is placed in boiling water and extracts, and solid-liquid ratio is 1: 4 (weight/volume), and 100 ℃ are boiled 3 hours, and Separation of Solid and Liquid, by liquid pressure-reducing distillation, obtains the concentrate of original volume 1/8;
4) by step 3) Cordyceps militaris that obtains is dry, pulverize, add water, solid-liquid ratio 1: 10 (weight/volume), and be heated to boiling and extract, keeping 3h, centrifugal filtering, repeats last time and operates twice, obtains Cordyceps militaris sediment; Liquid concentration, to 1/10 of original volume, is added to 95% (volume ratio) ethanol water of 3 times of amounts, under 4 ℃ of conditions static 12 hours, the centrifugal thick polysaccharide of Cordyceps militaris that obtains;
5) by step 2) obtain obtain concentrate, step 3) obtain obtain concentrate, step 4) the thick polysaccharide of Cordyceps militaris that obtains mixes with m2 equivalent freeze-drying fruiting bodies of cordyceps militaris, add 5% dextrin, mixture is dry, packing, sterilizing obtain the reinforced Cordyceps militaris tea of differently flavoured nutrition.
Fruiting bodies of cordyceps militaris be rich in Cordyceps militaris extract cordyceps tea Contents of Main Components contrast table
Note: with 90 ℃ of above-mentioned two product data measureds of water soaking.
In a word, key of the present invention is first with ethanol, heat-sensitive substance in fruiting bodies of cordyceps militaris to be extracted; Then carry out water extract extraction, finally by fructification drying and crushing, extract the thick polysaccharide of Cordyceps militaris, take after said method, both retained the heat-sensitive substance of Chinese caterpillar fungus, increase again the composition (Cordyceps sinensis polysaccharide must adopt the mode of poach to obtain, and adopting the mode of making tea is to obtain Cordyceps sinensis polysaccharide) of Cordyceps sinensis polysaccharide.
Chinese caterpillar fungus that the present invention adopts is not limited to Cordyceps militaris, also comprises other Chinese caterpillar fungus kinds of Cordyceps.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any modifications of doing within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in protection scope of the present invention.
Claims (5)
1. a preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea, is characterized in that, this preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea comprises the following steps:
Step 1, gets weight fruiting bodies of cordyceps militaris m1, the m2 such as two parts, m1=m2;
Step 2, get fruiting bodies of cordyceps militaris m1, add 20%～95% ethanol water solution lixiviate according to volume ratio, the weight or volume ratio of feed liquid is lixiviate 3 hours～6 hours under 1: 4～6,40 ℃ vacuum conditions, Separation of Solid and Liquid, repeat aforesaid operations once, merge alcohol extract twice, by liquid pressure-reducing Distillation recovery ethanol, and obtain the concentrate of original volume 1/4～1/6;
Step 3, the Cordyceps militaris that step 2 is obtained is placed in boiling water and extracts, and feed liquid weight or volume ratio is 1: 4～6,100 ℃ and boils 3 hours～6 hours, and Separation of Solid and Liquid, by liquid pressure-reducing distillation, obtains the concentrate of original volume 1/4～1/8;
Step 4, the Cordyceps militaris that step 3 is obtained is dry, pulverizing, adds water, and feed liquid weight or volume ratio is 1: 6～10, and is heated to boiling extraction, keeps 3h, and centrifugal filtering, repeats last time and operates twice, obtains Cordyceps militaris sediment; Liquid concentration, to 1/6～1/10 of original volume, is obtained to the thick polysaccharide concentrate of Chinese caterpillar fungus;
Step 5, concentrate, step 3 obtain obtains the thick polysaccharide concentrate of Cordyceps militaris that concentrate, step 4 obtain and mix with the drying fruiting bodies of cordyceps militaris of m2 equivalent for obtaining that step 2 is obtained, also can in mixture, add local flavor conditioning agent, mixture is dry, packing, sterilizing obtain the reinforced Cordyceps militaris tea of differently flavoured nutrition.
2. the preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea as claimed in claim 1, it is characterized in that, in step 1, Cordyceps militaris can be selected one or more in fruiting bodies of cordyceps militaris, cordyceps mycelium, Cordyceps militaris polypide and Chinese caterpillar fungus culture medium.
3. the preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea as claimed in claim 2, is characterized in that, Cordyceps militaris is preferably fruiting bodies of cordyceps militaris.
4. the preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea as claimed in claim 1, is characterized in that, in step 4, Cordyceps militaris is crushed to 50 order～100 orders.
5. the preparation method who is rich in Cordyceps militaris extract Cordyceps militaris tea as claimed in claim 1, is characterized in that, in step 5, local flavor conditioning agent can be citric acid, dextrin, cyclodextrin, hawthorn, honey.
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| CN107485584A (en) * | 2017-07-28 | 2017-12-19 | 鹰仕达（中国）有限公司 | A kind of oral care composition |
| CN107595750A (en) * | 2017-07-28 | 2018-01-19 | Dj健康产业集团 | A kind of active inflammation-diminishing toothpaste |
| CN107616500A (en) * | 2017-10-27 | 2018-01-23 | 吉林农业大学 | Cordyceps militaris Fructooligosaccharidcomposition composition and its preparation method and application |
| CN107712160A (en) * | 2017-11-22 | 2018-02-23 | 恭城福茂生油茶文化产业发展有限公司 | A kind of preparation method of portable oil tea |
| CN107889904A (en) * | 2017-11-22 | 2018-04-10 | 恭城福茂生油茶文化产业发展有限公司 | A kind of preparation method of portable oil tea |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101124988A (en) * | 2007-09-25 | 2008-02-20 | 江苏瑞迪生科技有限公司 | Method for extracting refined cordycepin and cordyceps polysaccharide from Cordyceps militaris |
| CN101229199A (en) * | 2008-01-15 | 2008-07-30 | 重庆和润生物工程有限公司 | Integrative extract method of multi-active ingredient in cordyceps militaris mycelium |
| CN101580755A (en) * | 2009-06-11 | 2009-11-18 | 湖南农业大学 | Process for continuously extracting cordyceps militaris essential oil, cordycepin, cordycepic acid and cordyceps militaris polysaccharide from cordyceps militaris |
| CN101613390A (en) * | 2009-07-21 | 2009-12-30 | 贵州大学 | A method for separating and purifying high-purity cordycepin |
| CN101755976A (en) * | 2010-02-26 | 2010-06-30 | 上海科立特农科（集团）有限公司 | Phellinus linteus and Cordyeps militaris health protection tea and preparation method thereof |
| CN101906127A (en) * | 2010-07-23 | 2010-12-08 | 上海国宝企业发展中心 | Method for extracting cordycepin and cordyceps polysaccharides from residue of cordyceps militaris culture medium |
| CN102432656A (en) * | 2011-12-23 | 2012-05-02 | 辽宁省农业科学院大连生物技术研究所 | A method for extracting and purifying cordycepin from fruiting bodies of Cordyceps militaris |
| CN102558264A (en) * | 2012-01-18 | 2012-07-11 | 辽宁仙榆湾北冬虫夏草（集团）有限公司 | Method for extracting cordycepin and cordyceps polysaccharide from cordyceps militaris |
| CN103431095A (en) * | 2013-08-17 | 2013-12-11 | 刘润成 | Cordycepsmilitaris health tea and manufacturing method thereof |
-
2014
- 2014-01-02 CN CN201410009360.8A patent/CN103766545A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101124988A (en) * | 2007-09-25 | 2008-02-20 | 江苏瑞迪生科技有限公司 | Method for extracting refined cordycepin and cordyceps polysaccharide from Cordyceps militaris |
| CN101229199A (en) * | 2008-01-15 | 2008-07-30 | 重庆和润生物工程有限公司 | Integrative extract method of multi-active ingredient in cordyceps militaris mycelium |
| CN101580755A (en) * | 2009-06-11 | 2009-11-18 | 湖南农业大学 | Process for continuously extracting cordyceps militaris essential oil, cordycepin, cordycepic acid and cordyceps militaris polysaccharide from cordyceps militaris |
| CN101613390A (en) * | 2009-07-21 | 2009-12-30 | 贵州大学 | A method for separating and purifying high-purity cordycepin |
| CN101755976A (en) * | 2010-02-26 | 2010-06-30 | 上海科立特农科（集团）有限公司 | Phellinus linteus and Cordyeps militaris health protection tea and preparation method thereof |
| CN101906127A (en) * | 2010-07-23 | 2010-12-08 | 上海国宝企业发展中心 | Method for extracting cordycepin and cordyceps polysaccharides from residue of cordyceps militaris culture medium |
| CN102432656A (en) * | 2011-12-23 | 2012-05-02 | 辽宁省农业科学院大连生物技术研究所 | A method for extracting and purifying cordycepin from fruiting bodies of Cordyceps militaris |
| CN102558264A (en) * | 2012-01-18 | 2012-07-11 | 辽宁仙榆湾北冬虫夏草（集团）有限公司 | Method for extracting cordycepin and cordyceps polysaccharide from cordyceps militaris |
| CN103431095A (en) * | 2013-08-17 | 2013-12-11 | 刘润成 | Cordycepsmilitaris health tea and manufacturing method thereof |
Non-Patent Citations (4)
| Title |
|---|
| 刘汉清主编: "《中药药剂实验与指导》", 31 January 2002, 中国医药科技出版社 * |
| 曹月梅主编: "《中药制药专门技术》", 31 August 2006, 河海大学出版社 * |
| 王英娟等: "蛹虫草中虫草素、虫草多糖综合提取工艺研究", 《西北植物学报》 * |
| 祁波: "蛹虫草虫草素和虫草多糖综合提取工艺的研究", 《科技信息》 * |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105901681A (en) * | 2016-04-20 | 2016-08-31 | 浙江农林大学 | Preparation methods for extract liquid, fermentation extracellular liquid and fermentation intracellular liquid of dictyophora, and application thereof |
| CN107281013A (en) * | 2017-07-28 | 2017-10-24 | 鹰仕达（中国）有限公司 | One kind removes tooth stain and suppresses bacterial plaque toothpaste |
| CN107362112A (en) * | 2017-07-28 | 2017-11-21 | 鹰仕达（中国）有限公司 | One kind shield gum healing toothpaste |
| CN107468553A (en) * | 2017-07-28 | 2017-12-15 | 鹰仕达（中国）有限公司 | A kind of anti-caries toothpaste |
| CN107485584A (en) * | 2017-07-28 | 2017-12-19 | 鹰仕达（中国）有限公司 | A kind of oral care composition |
| CN107595750A (en) * | 2017-07-28 | 2018-01-19 | Dj健康产业集团 | A kind of active inflammation-diminishing toothpaste |
| CN107595750B (en) * | 2017-07-28 | 2020-07-14 | Dj健康产业集团 | Active anti-inflammation toothpaste |
| CN107616500A (en) * | 2017-10-27 | 2018-01-23 | 吉林农业大学 | Cordyceps militaris Fructooligosaccharidcomposition composition and its preparation method and application |
| CN107712160A (en) * | 2017-11-22 | 2018-02-23 | 恭城福茂生油茶文化产业发展有限公司 | A kind of preparation method of portable oil tea |
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