CN103750573B - Electronic cigarette tobacco tar and preparation method thereof - Google Patents
Electronic cigarette tobacco tar and preparation method thereof Download PDFInfo
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- CN103750573B CN103750573B CN201410030927.XA CN201410030927A CN103750573B CN 103750573 B CN103750573 B CN 103750573B CN 201410030927 A CN201410030927 A CN 201410030927A CN 103750573 B CN103750573 B CN 103750573B
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- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 235000002637 Nicotiana tabacum Nutrition 0.000 title description 4
- 241000208125 Nicotiana Species 0.000 title 1
- 239000007788 liquid Substances 0.000 claims abstract description 16
- 241000202807 Glycyrrhiza Species 0.000 claims abstract description 10
- 235000001453 Glycyrrhiza echinata Nutrition 0.000 claims abstract description 10
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 claims abstract description 10
- 235000017382 Glycyrrhiza lepidota Nutrition 0.000 claims abstract description 10
- 238000000605 extraction Methods 0.000 claims abstract description 10
- 229940010454 licorice Drugs 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000706 filtrate Substances 0.000 claims abstract description 6
- 239000000047 product Substances 0.000 claims abstract description 6
- 238000000034 method Methods 0.000 claims abstract description 5
- 239000012634 fragment Substances 0.000 claims abstract description 4
- 238000010992 reflux Methods 0.000 claims abstract description 4
- 239000002893 slag Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims abstract description 4
- 150000001298 alcohols Chemical class 0.000 claims description 7
- BEVWMRQFVUOPJT-UHFFFAOYSA-N 2,4-dimethyl-1,3-thiazole-5-carboxamide Chemical compound CC1=NC(C)=C(C(N)=O)S1 BEVWMRQFVUOPJT-UHFFFAOYSA-N 0.000 claims description 4
- UWHCKJMYHZGTIT-UHFFFAOYSA-N Tetraethylene glycol, Natural products OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 claims description 4
- GLZWNFNQMJAZGY-UHFFFAOYSA-N octaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCOCCOCCO GLZWNFNQMJAZGY-UHFFFAOYSA-N 0.000 claims description 4
- JLFNLZLINWHATN-UHFFFAOYSA-N pentaethylene glycol Chemical compound OCCOCCOCCOCCOCCO JLFNLZLINWHATN-UHFFFAOYSA-N 0.000 claims description 4
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 4
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims description 3
- 239000012141 concentrate Substances 0.000 claims description 3
- IIRDTKBZINWQAW-UHFFFAOYSA-N hexaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCO IIRDTKBZINWQAW-UHFFFAOYSA-N 0.000 claims description 3
- 229960002715 nicotine Drugs 0.000 claims description 3
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims description 3
- 235000013599 spices Nutrition 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- -1 diethyl alcohol Chemical compound 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- 206010011224 Cough Diseases 0.000 abstract description 3
- 206010062717 Increased upper airway secretion Diseases 0.000 abstract description 3
- 208000026435 phlegm Diseases 0.000 abstract description 3
- 210000000952 spleen Anatomy 0.000 abstract description 3
- 238000001784 detoxification Methods 0.000 abstract description 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 244000061176 Nicotiana tabacum Species 0.000 description 3
- 238000001914 filtration Methods 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
- 229920001223 polyethylene glycol Polymers 0.000 description 2
- 230000005586 smoking cessation Effects 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007407 health benefit Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
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Abstract
本发明涉及电子烟，公开了一种电子烟烟油的制备方法，包括以下步骤:（1）选择干燥的甘草，先将其清洗并切碎；（2）将上一步骤中的碎片投入至提取容器中，并按1kg碎甘草加入5‑10L的比例加入75‑95％的食用酒精；（3）对上一步骤中提取容器内的原料进行加热回流提取，提取8‑10小时，然后静置、冷却至室温；（4）对上一步骤中的原料进行过滤、去渣，得到提取液；（5）将上一步骤中得到的提取液过滤，所得滤液经浓缩罐浓缩至密度在1.0以上，得到组合物A；（6）将上一步骤中所得组合物A按重量百分比0.8‑3.5%加入普通电子烟烟油中，搅拌均匀得到成品。本发明还公开了这种方法所制备的电子烟烟油。本发明的电子烟烟油具有补脾益气、清热解毒、祛痰止咳等保健效果的优点。The present invention relates to electronic cigarettes, and discloses a preparation method of electronic cigarette oil, which includes the following steps: (1) select dry licorice, first wash and chop it; (2) put the fragments in the previous step into In the extraction container, add 75-95% edible alcohol at a ratio of 5-10L to 1kg of crushed licorice; (3) Heat and reflux the raw materials in the extraction container in the previous step, extract for 8-10 hours, and then statically (4) Filter the raw materials in the previous step and remove slag to obtain the extract; (5) Filter the extract obtained in the previous step, and the obtained filtrate is concentrated in a concentration tank to a density of 1.0 As above, the composition A is obtained; (6) The composition A obtained in the previous step is added into the ordinary e-cigarette oil at a weight percentage of 0.8-3.5%, and the finished product is obtained by stirring evenly. The invention also discloses the electronic cigarette liquid prepared by the method. The e-cigarette liquid of the present invention has the advantages of invigorating the spleen and replenishing qi, clearing away heat and detoxification, eliminating phlegm and relieving cough and other health care effects.
Description
技术领域technical field
本发明涉及电子烟，尤其是涉及一种电子烟用的电子烟烟油及其制备方法。The invention relates to electronic cigarettes, in particular to an electronic cigarette liquid used in electronic cigarettes and a preparation method thereof.
背景技术Background technique
在我国，有近1/4的人口都在抽烟，毫不夸张地说中国吸烟的人数比某些国家的人口总数还要多，近年来，中国控烟力度也在不断加强，不仅从2011年5月1日起在公共场所全面禁烟，还加大了对戒烟控烟产品开发的支持力度，电子烟作为其中一种重要的戒烟控烟产品得到政府的大力支持和推广，该技术发展势不可挡。In my country, nearly 1/4 of the population is smoking. It is no exaggeration to say that the number of smokers in China is more than the total population of some countries. Smoking will be completely banned in public places from March 1, and support for the development of smoking cessation and tobacco control products has also been increased. As one of the important smoking cessation and tobacco control products, electronic cigarettes have been strongly supported and promoted by the government, and the development of this technology is unstoppable.
作为电子烟的原料——烟油，大部分是从烟草植物或其它物质中提取的，也有一些采用化学合成的方法制备得到，这种烟油只是一种香烟替代物，对人体也没有什么保健的效果。As the raw material of e-cigarettes, e-liquid is mostly extracted from tobacco plants or other substances, and some are prepared by chemical synthesis. This kind of e-liquid is only a substitute for cigarettes and has no health benefits for the human body. Effect.
发明内容Contents of the invention
为克服现有电子烟的缺点，本发明目的在于提供一种电子烟用的具有保健效果的电子烟烟油及其制备方法。In order to overcome the shortcomings of the existing electronic cigarettes, the purpose of the present invention is to provide an electronic cigarette oil for electronic cigarettes with health care effects and a preparation method thereof.
本发明通过以下技术措施实现的，一种电子烟烟油的制备方法，包括以下步骤:The present invention is realized through the following technical measures, a preparation method of electronic cigarette liquid, comprising the following steps:
（1）选择干燥的甘草，先将其清洗并切碎；(1) Choose dry licorice, wash and chop it first;
（2）将上一步骤中的碎片投入至提取容器中，并按1kg碎甘草加入5-10L的比例加入75-95％的食用酒精；(2) Put the fragments in the previous step into the extraction container, and add 75-95% edible alcohol at the ratio of 1kg of crushed licorice to 5-10L;
（3）对上一步骤中提取容器内的原料进行加热回流提取，提取8-10小时，然后静置、冷却至室温；(3) Heat and reflux the raw materials in the extraction container in the previous step for extraction for 8-10 hours, then let stand and cool to room temperature;
（4）对上一步骤中的原料进行过滤、去渣，得到提取液；(4) Filtering and removing slag from the raw materials in the previous step to obtain an extract;
（5）将上一步骤中得到的提取液过滤，所得滤液经浓缩罐浓缩至密度在1.0以上，得到组合物A；(5) Filtrate the extract obtained in the previous step, and concentrate the obtained filtrate through a concentration tank to a density above 1.0 to obtain composition A;
（6）将上一步骤中所得组合物A按重量百分比0.8-3.5%加入普通电子烟烟油中，搅拌均匀得到成品。(6) Add 0.8-3.5% by weight of the composition A obtained in the previous step into the ordinary e-cigarette oil, and stir evenly to obtain the finished product.
作为一种优选方式，所述普通电子烟烟油包括以下重量份额的各组份：水20-40份、醇类50-80份、香料或尼古丁少量。As a preferred manner, the common e-cigarette liquid includes the following components by weight: 20-40 parts of water, 50-80 parts of alcohols, and a small amount of spices or nicotine.
作为一种优选方式，所述醇类为丙二醇或甘油。As a preferred manner, the alcohols are propylene glycol or glycerin.
作为一种优选方式，所述醇类包括以下重量份额的各组份：2,2-氧联双乙醇（C4H10O3）1-5份、三甘醇（C6H14O4）5-30份、四甘醇（C8H18O5）20-40份、五甘醇（C10H22O6）15-35份、六甘醇（C12H26O7）5-25份、七甘醇（C14H30O8）3-15份、八甘醇（C16H34O9）1-5份。As a preferred method, the alcohols include the following components by weight: 1-5 parts of 2,2-oxybis-bis-ethanol (C 4 H 10 O 3 ), 1-5 parts of triethylene glycol (C 6 H 14 O 4 ) 5-30 parts, tetraethylene glycol (C 8 H 18 O 5 ) 20-40 parts, pentaethylene glycol (C 10 H 22 O 6 ) 15-35 parts, hexaethylene glycol (C 12 H 26 O 7 ) 5 -25 parts, 3-15 parts of heptaethylene glycol (C 14 H 30 O 8 ), 1-5 parts of octaethylene glycol (C 16 H 34 O 9 ).
本发明还公开了一种利用上述方法所制备的电子烟烟油。The invention also discloses an electronic cigarette liquid prepared by the method.
本发明利用甘草的提取物加入至普通电子烟烟油中形成新的烟油，这种新的烟油的具有补脾益气、清热解毒、祛痰止咳的效果。In the present invention, the extract of licorice is added to the common e-cigarette oil to form a new oil. The new oil has the effects of invigorating spleen and Qi, clearing heat and detoxification, eliminating phlegm and relieving cough.
具体实施方式detailed description
下面结合实施例对本发明作进一步详细说明。The present invention is described in further detail below in conjunction with embodiment.
一种电子烟烟油，其制备方法包括以下步骤:A kind of electronic cigarette liquid, its preparation method comprises the following steps:
（1）选择干燥的甘草，先将其清洗并切碎；(1) Choose dry licorice, wash and chop it first;
（2）将上一步骤中的碎片投入至提取容器中，并按1kg碎甘草加入5-10L的比例加入75-95％的食用酒精；(2) Put the fragments in the previous step into the extraction container, and add 75-95% edible alcohol at the ratio of 1kg of crushed licorice to 5-10L;
（3）对上一步骤中提取容器内的原料进行加热回流提取，提取8-10小时，然后静置、冷却至室温；(3) Heat and reflux the raw materials in the extraction container in the previous step for extraction for 8-10 hours, then let stand and cool to room temperature;
（4）对上一步骤中的原料进行过滤、去渣，得到提取液；(4) Filtering and removing slag from the raw materials in the previous step to obtain an extract;
（5）将上一步骤中得到的提取液过滤，所得滤液经浓缩罐浓缩至密度在1.0以上，得到组合物A；(5) Filtrate the extract obtained in the previous step, and concentrate the obtained filtrate through a concentration tank to a density above 1.0 to obtain composition A;
（6）将上一步骤中所得组合物A按重量百分比0.8-3.5%加入普通电子烟烟油中，搅拌均匀得到成品。(6) Add 0.8-3.5% by weight of the composition A obtained in the previous step into the ordinary e-cigarette oil, and stir evenly to obtain the finished product.
本烟油利用甘草的提取物加入至普通电子烟烟油中形成新的烟油，这种新的烟油的具有补脾益气、清热解毒、祛痰止咳的效果。In the e-liquid, the extract of licorice is added to common e-cigarette e-liquid to form a new e-liquid. The new e-liquid has the effects of invigorating the spleen and replenishing qi, clearing heat and detoxifying, eliminating phlegm and relieving cough.
本发明的电子烟烟油，在前面技术方案的基础上，具体的是普通电子烟烟油包括以下重量份额的各组份：水20-40份、醇类50-80份、香料或尼古丁少量。The e-cigarette oil of the present invention, on the basis of the previous technical solution, specifically, the ordinary e-cigarette oil includes the following components by weight: 20-40 parts of water, 50-80 parts of alcohols, a small amount of spices or nicotine .
本发明的电子烟烟油，在前面技术方案的基础上，具体的是醇类为丙二醇或甘油。The e-cigarette oil of the present invention, on the basis of the previous technical solution, specifically, the alcohol is propylene glycol or glycerin.
本发明的电子烟烟油，在前面技术方案的基础上，具体的是醇类包括以下重量份额的各组份：2,2-氧联双乙醇（C4H10O3）1-5份、三甘醇（C6H14O4）5-30份、四甘醇（C8H18O5）20-40份、五甘醇（C10H22O6）15-35份、六甘醇（C12H26O7）5-25份、七甘醇（C14H30O8）3-15份、八甘醇（C16H34O9）1-5份。采用复合聚低碳醇（2,2-氧联双乙醇、三甘醇、四甘醇、五甘醇、六甘醇、七甘醇、八甘醇），可以提高雾化效果和去除传统的甜腻味道。The e-cigarette liquid of the present invention, on the basis of the previous technical scheme, specifically, the alcohols include the following components by weight: 1-5 parts of 2,2-oxybis-bis-ethanol (C 4 H 10 O 3 ) , triethylene glycol (C 6 H 14 O 4 ) 5-30 parts, tetraethylene glycol (C 8 H 18 O 5 ) 20-40 parts, pentaethylene glycol (C 10 H 22 O 6 ) 15-35 parts, six 5-25 parts of glycol (C 12 H 26 O 7 ), 3-15 parts of heptaethylene glycol (C 14 H 30 O 8 ), 1-5 parts of octaethylene glycol (C 16 H 34 O 9 ). The use of compound polylower carbon alcohols (2,2-oxodiethylene glycol, triethylene glycol, tetraethylene glycol, pentaethylene glycol, hexaethylene glycol, heptaethylene glycol, octaethylene glycol) can improve the atomization effect and remove traditional Sweet taste.
以上是对本发明电子烟烟油的制备方法及其加工方法进行了阐述，用于帮助理解本发明，但本发明的实施方式并不受上述实施例的限制，任何未背离本发明原理下所作的改变、修饰、替代、组合、简化，均应为等效的置换方式，都包含在本发明的保护范围之内。The above is the elaboration of the preparation method and processing method of the e-cigarette oil of the present invention, which is used to help understand the present invention, but the implementation of the present invention is not limited by the above examples. Changes, modifications, substitutions, combinations, and simplifications should all be equivalent replacements, and are all included within the protection scope of the present invention.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| GB2504075A (en) | 2012-07-16 | 2014-01-22 | Nicoventures Holdings Ltd | Electronic smoking device |
| GB2504076A (en) | 2012-07-16 | 2014-01-22 | Nicoventures Holdings Ltd | Electronic smoking device |
| GB2528673B (en) * | 2014-07-25 | 2020-07-01 | Nicoventures Holdings Ltd | Aerosol provision system |
| CN105326087A (en) * | 2014-08-12 | 2016-02-17 | 佛山市万绿素电子科技有限公司 | Electronic cigarette tobacco tar with functions of alleviating hangover and protecting liver |
| GB201505597D0 (en) | 2015-03-31 | 2015-05-13 | British American Tobacco Co | Article for use with apparatus for heating smokable material |
| GB201505595D0 (en) | 2015-03-31 | 2015-05-13 | British American Tobacco Co | Cartridge for use with apparatus for heating smokeable material |
| CN107653066A (en) * | 2017-09-28 | 2018-02-02 | 河南省新郑金叶香料有限公司 | A kind of licorice aroma component for tobacco and its extraction method and application |
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