CN103708959B - A kind of Double-control sustained-release fertilizer and production method thereof - Google Patents
A kind of Double-control sustained-release fertilizer and production method thereof Download PDFInfo
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- CN103708959B CN103708959B CN201310722177.8A CN201310722177A CN103708959B CN 103708959 B CN103708959 B CN 103708959B CN 201310722177 A CN201310722177 A CN 201310722177A CN 103708959 B CN103708959 B CN 103708959B
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- 238000013268 sustained release Methods 0.000 title claims abstract description 19
- 239000012730 sustained-release form Substances 0.000 title claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- 239000000463 material Substances 0.000 claims abstract description 18
- 150000001875 compounds Chemical class 0.000 claims abstract description 15
- 238000010521 absorption reaction Methods 0.000 claims abstract description 13
- 239000002245 particle Substances 0.000 claims abstract description 7
- 238000005507 spraying Methods 0.000 claims description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 11
- 239000003795 chemical substances by application Substances 0.000 claims description 9
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- 241000487918 Acacia argyrodendron Species 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000002199 base oil Substances 0.000 claims description 6
- 239000002374 bone meal Substances 0.000 claims description 6
- 235000011222 chang cao shi Nutrition 0.000 claims description 6
- 239000002904 solvent Substances 0.000 claims description 6
- 239000010902 straw Substances 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- 229940036811 bone meal Drugs 0.000 claims description 5
- 239000003610 charcoal Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 3
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- 239000004208 shellac Substances 0.000 claims description 3
- ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 claims description 3
- 229940113147 shellac Drugs 0.000 claims description 3
- 235000013874 shellac Nutrition 0.000 claims description 3
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 10
- 235000015097 nutrients Nutrition 0.000 abstract description 10
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 abstract description 9
- 235000002017 Zea mays subsp mays Nutrition 0.000 abstract description 9
- 235000005822 corn Nutrition 0.000 abstract description 9
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract description 5
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 5
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 5
- 239000011574 phosphorus Substances 0.000 abstract description 5
- 239000011591 potassium Substances 0.000 abstract description 4
- 229910052700 potassium Inorganic materials 0.000 abstract description 4
- 230000012010 growth Effects 0.000 abstract description 3
- 239000002131 composite material Substances 0.000 abstract description 2
- 230000001276 controlling effect Effects 0.000 abstract description 2
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- 239000011347 resin Substances 0.000 abstract description 2
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- 238000013270 controlled release Methods 0.000 description 7
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 6
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- 238000003912 environmental pollution Methods 0.000 description 5
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- 230000008901 benefit Effects 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 239000000618 nitrogen fertilizer Substances 0.000 description 3
- 239000002689 soil Substances 0.000 description 3
- GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 210000003608 fece Anatomy 0.000 description 2
- 239000010871 livestock manure Substances 0.000 description 2
- 241000309551 Arthraxon hispidus Species 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 239000005696 Diammonium phosphate Substances 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- MMDJDBSEMBIJBB-UHFFFAOYSA-N [O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[NH6+3] Chemical compound [O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[NH6+3] MMDJDBSEMBIJBB-UHFFFAOYSA-N 0.000 description 1
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
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- 239000002734 clay mineral Substances 0.000 description 1
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- 230000007423 decrease Effects 0.000 description 1
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 1
- 229910000388 diammonium phosphate Inorganic materials 0.000 description 1
- 235000019838 diammonium phosphate Nutrition 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
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- 230000007613 environmental effect Effects 0.000 description 1
- 238000012851 eutrophication Methods 0.000 description 1
- 230000004720 fertilization Effects 0.000 description 1
- 208000000509 infertility Diseases 0.000 description 1
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- 231100000535 infertility Toxicity 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
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- 229920000642 polymer Polymers 0.000 description 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 description 1
- 229910052939 potassium sulfate Inorganic materials 0.000 description 1
- 239000001120 potassium sulphate Substances 0.000 description 1
- 235000011151 potassium sulphates Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000002352 surface water Substances 0.000 description 1
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- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- Fertilizers (AREA)
Abstract
The invention discloses a kind of Double-control sustained-release fertilizer and production method thereof, this Double-control sustained-release fertilizer comprises ternary compound fertilizer material component, absorption bonding component and dressing component three part, the composite organic-inorganic fertilizer particle that to be the absorption bonding component researched and developed voluntarily with my company and dressing component produce for sustained release dosage is for core core, the macroelement molecule such as nitrogen, phosphorus, potassium of core in-core is adsorbed bonding component and is adsorbed, according to plant growth needs, slow releasing; Recycling dressing component wraps up this slow-release fertilizer core core and forms release membranes, realizes the dual-sustained-release regulating and controlling of nutrient, overcomes that the nutrient slowly-released property of resin coated fertilizer is good but price is high, the material coated cost of inorganic nutrients is low but the shortcoming of nutrient slowly-released property difference.Through testing on corn, volume increase 14.9%, mu increases income 165.4 yuan, and the whole growth and development stage of corn all shows healthy and strong tall and straight, and the middle and later periods is without de-fertile phenomenon.
Description
Technical field
The present invention relates to a kind of slow release fertilizer, particularly relate to a kind of Double-control sustained-release fertilizer and production method thereof.
Background technology
Chemical fertilizer is one of agriculture most important production means.China's chemical fertilizer consumption amount accounts for the 20-30% of world Fertilizer total quantity consumed, ranks first in the world.The contribution rate increased grain according to expert calculation China Fertilizer Industry is to about 35%, and huge contribution has been made in the existence developing into China and even the people of the world of Fertilizer Industry.
But also occurred the phenomenon of the quick growth of unit grain fertilizer amount while China's Fertilizer Industry fast development, fertilising un-reasonable phenomenon is very outstanding, utilization rate of fertilizer is low, the wasting of resources, environmental pollution and agriculture production cost increase.The usage quantity of China's chemical fertilizer is considerably beyond international average level, and current China amount of application of nitrogen fertilizer is 3 times of the U.S., French 1.5 times, German 1.6 times.Chemical fertilizer utilization ratio is well below world standard.America utilization rate of fertilizer reaches 52%, and European utilization ratio reaches 68%.And China's utilization ratio is only 30 ~ 35%, so low utilization rate of fertilizer, wastes a large amount of financial resources and resource.The elements such as a large amount of nitrogen, phosphorus, potassium residue in soil, enter underground water and surface water or be discharged in air, bring serious environmental pollution.According to statistics, China's nitrogen fertilizer production accounts for 5% of national energy consumption, the carbonic acid gas of discharge accounts for 8% of national total emission volumn, agricultural pollution accounts for 60% of gross contamination source, a large amount of fertilizer losses, person remain in inside soil, and the hardening soil is degenerated, and cause agricultural product quality to decline, environmental pollution, ecological damage.
Chemical fertilizer is maximum in China's agriculture production economy expenditure, and due to the combined influence of fertilizer character and edatope condition, utilization rate of fertilizer is low has become ubiquitous problem on fertilizer application.This season utilization ratio of current China nitrogenous fertilizer is only 30%-35%, is equivalent to lose 1,900 ten thousand tons of urea every year.Except direct financial loss, some areas cause environmental pollution because of improper fertilization, occur the problems such as in earth's surface eutrophication, underground water and vegetables, nitrate nitrogen content exceeds standard, the increase of nitrous oxide emission amount.
Improve the aspects such as utilization rate of fertilizer, saving cost, minimizing environmental pollution and have very large development space, slow release fertilizer can improve utilization rate of fertilizer, improves utilization rate of fertilizer, reduces rate of fertilizer application, saves labor of fertilizer application power, seems particularly important.Slow-release fertilizer makes it to absorb with crop nutrition content basic synchronised by the regulation and control to nutrient release rate, greatly can improve fertilizer nutrient utilization, reduces widespread pollution from the overuse of fertilizers and pesticides in rural area.
Coated fertilizer is a type of sustained-controll-release fertiliser, can be divided into organic coated fertilizer and inorganic coating fertilizer by the character of mould material; The existing sulphur coated urea of inorganic coating fertilizer, clay mineral coated fertilizer; Organic coated fertilizer mainly refers to polymer coated fertilizer.Inorganic coating fertilizer general cost is lower, pollution-free, but controlled release period is shorter; The controlled release period of organic coated fertilizer is long, but cost is high, uses in a large number and may bring risk to edatope.
Summary of the invention
The object of this invention is to provide one and integrate adsorption sustained-release and coated slow-release effect, Environmental Safety, the Double-control sustained-release fertilizer of increase yield significantly.
Another object of the present invention is to provide a kind of raw material and is easy to get, and production cost is low, the production method of the simple slow release fertilizer of technique.
The object of the invention is to be achieved through the following technical solutions, this Double-control sustained-release fertilizer comprises ternary compound fertilizer material component, absorption bonding component and dressing component three part, and described ternary compound fertilizer material component comprises nitrogen, phosphorus, potassium macroelement; Described absorption bonding component comprises straw biological black wood charcoal, deglued bone meal, tackiness agent; Described tackiness agent is the mixture of shellac and rosin, and the blending ratio of mixture is equal proportion, take ethanol as solvent, is dissolved with 80-100 gram of solute in often liter of solvent; Described dressing component comprises base oil, mud, diatomite.
In described absorption bonding component, the ratio of weight and number of straw biological black wood charcoal, deglued bone meal, tackiness agent is 10: 5: 2;
In described dressing component, base oil, mud, diatomaceous ratio of weight and number are 2: 10: 7;
The production method of Double-control sustained-release fertilizer of the present invention, comprises the following steps:
1. be the ratio mixing of 10: 5: 1 by ratio of weight and the number of copies by straw biological black wood charcoal, deglued bone meal, tackiness agent, add appropriate water, stir being heated at the temperature of 50-60 DEG C, make homogeneous absorption bonding spray coating liquor;
2. the spray coating liquor adopting the method for spraying step 1. to be obtained sprays to granulation on ternary compound fertilizer material, and the ratio of weight and number that ternary compound fertilizer material bonds spray coating liquor with absorption is 100: 15-20, spraying temperature 60-70 DEG C;
3. 10 parts of mud, 7 parts of diatomite are added suitable quantity of water and stir, be heated to 40-50 DEG C, then add 2 parts of base oils, fully stir, make dressing spray coating liquor;
4. the dressing spray coating liquor that on the ternary compound fertilizer material particle adopting heat spraying method 2. to obtain in step, 3. spraying process obtains, spraying temperature is 55-65 DEG C, and the ratio of weight and number of ternary compound fertilizer material particle and dressing spray coating liquor is 100: 8-10;
Advantage of the present invention:
Double-control sustained-release fertilizer, the composite organic-inorganic fertilizer particle that to be the absorption bonding component researched and developed voluntarily with my company and dressing component produce for sustained release dosage is for core core, the macroelement molecule such as nitrogen, phosphorus, potassium of core in-core is adsorbed bonding component and is adsorbed, according to plant growth needs, and slow releasing; Recycling dressing component wraps up this slow-release fertilizer core core and forms release membranes, realize the dual-sustained-release regulating and controlling of nutrient, overcome that the nutrient slowly-released property of resin coated fertilizer is good but price is high, the material coated cost of inorganic nutrients is low but the shortcoming of nutrient slowly-released property difference, have that production cost is low, had good sustained release effect, fertilizer are residual without film, the advantage such as suitable field crop application especially.
Embodiment
Double-control sustained-release fertilizer of the present invention comprises ternary compound fertilizer material component, absorption bonding component and dressing component three part, and ternary compound fertilizer material component comprises nitrogen, phosphorus, potassium macroelement, can add other trace element as required; Absorption bonding component comprises straw biological black wood charcoal, deglued bone meal, tackiness agent, and its consumption is 10: 5: 2 by weight; Tackiness agent is the mixture of shellac and rosin, and the blending ratio of mixture is equal proportion, take ethanol as solvent, is dissolved with 90 grams of solutes in often liter of solvent; Dressing component comprises base oil, mud, diatomite, and its consumption is 2: 10: 7 by weight.
The production method of Double-control sustained-release fertilizer of the present invention, comprises the following steps:
(1) adopt vapor heated method by 10 kilograms of straw biological black wood charcoals, 5 kilograms of deglued bone meals, 1 kilogram of tackiness agents mixing, add appropriate water, stir being heated at the temperature of 55 DEG C, make homogeneous absorption bonding spray coating liquor;
(2) adopt the method for spraying that the spray coating liquor 18 kilograms that step (1) is obtained is sprayed to granulation on 100 kilograms of ternary compound fertilizer material, spraying temperature 60-70 DEG C;
(3) 10 kilograms of mud, 7 kilograms of diatomite are added suitable quantity of water and stir, be heated to 40-50 DEG C, then add 2 kilograms of base oils, fully stir, make dressing spray coating liquor;
(4) the dressing spray coating liquor 9 kilograms that on the ternary compound fertilizer material particle adopting heat spraying method to obtain in step (2), 3. spraying process obtains, spraying temperature is 55-65 DEG C.
The field test data of Double-control sustained-release fertilizer on corn
1. test process
Process 1: mu Controlled Release Fertilizer 15kg makees base manure; Before head water, disposable mu again chases after Controlled Release Fertilizer 10kg and adds urea 20kg.
Process 2: mu diammonium phosphate 20kg adds urea 8kg and adds potassium sulphate fertilizer 5kg and make base manure, and before head water, disposable mu chases after urea 25kg.
2. experimental field basic condition
Experimental field be selected in Linyi City Yinan County Soviet Union villages and small towns, test area is 10.5 mu, and conventional fertilizer application area is 6.5 mu, and Controlled Release Fertilizer test area is 4 mu.April 30 was sowed, and May 11 emerged, pour water the time of infertility 5 times (30/6,11/7,24/7,5/8,1/9), intertillage secondary.Before conventional fertilizer application joint head water, mu chases after urea 25kg.Controlled Release Fertilizer every mu chases after 5kg.October 20 gathered in the crops.
3. test result analysis
(1) different treatment is on the impact of corn character
Corn slow-release or control-release fertilizer as can be seen from Table 1, plant height, Ear height, spike length are all high than conventional fertilizer application, and bald sharp rate is lower than contrast.
The field investigation of table 1 different treatment and indoor species test situation
(2) different treatment is on the impact of corn yield
From grain number per spike, Ear weight, thousand seed weight and seed-producing rate (see table 1), execute corn slow-release or control-release fertilizer process more than conventional fertilizer application 23.8 successively, heavy 18.5g, 25.6g and exceed 0.2 percentage point, finally fall in output, execute corn Controlled Release Fertilizer than conventional fertilizer application mu volume increase 129.7kg, amount of increase in production is 14.9%.
4 Economic and Efficiency Analysis
Table 2 shows, execute fewer than conventional fertilizer application 10.6 yuan of slow-release or control-release fertilizer mu cost, and per mu yield value is higher than conventional fertilizer application 154.8 yuan.It is 165.4 yuan that mu has a net increase of benefit.
Table 2 applies fertilizer Economic and Efficiency Analysis
Under this test conditions, use dual control slow-release or control-release fertilizer, there is obvious production-increasing function and economic benefit; Meanwhile, the whole growth and development stage of corn all shows healthy and strong tall and straight, and the middle and later periods is without de-fertile phenomenon.Can promote by large-scale demonstration.
Claims (1)
1. a production method for Double-control sustained-release fertilizer, is characterized in that comprising the following steps:
1. be the ratio mixing of 10: 5: 1 by ratio of weight and the number of copies by straw biological black wood charcoal, deglued bone meal, tackiness agent, add appropriate water, stir being heated at the temperature of 50-60 DEG C, make homogeneous absorption bonding spray coating liquor;
2. the spray coating liquor adopting the method for spraying step 1. to be obtained sprays to granulation on ternary compound fertilizer material, and the ratio of weight and number that ternary compound fertilizer material bonds spray coating liquor with absorption is 100: 15-20, spraying temperature 60-70 DEG C;
3. 10 parts of mud, 7 parts of diatomite are added suitable quantity of water and stir, be heated to 40-50 DEG C, then add 2 parts of base oils, fully stir, make dressing spray coating liquor;
4. the dressing spray coating liquor that on the ternary compound fertilizer material particle adopting heat spraying method 2. to obtain in step, 3. spraying process obtains, spraying temperature is 55-65 DEG C, the ratio of weight and number of ternary compound fertilizer material particle and dressing spray coating liquor is 100: 8-10, described tackiness agent take ethanol as solvent, be dissolved with 80-100 gram of solute in often liter of solvent, its solute is the mixture of the equal proportion of shellac and rosin.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310722177.8A CN103708959B (en) | 2013-12-15 | 2013-12-15 | A kind of Double-control sustained-release fertilizer and production method thereof |
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| CN201310722177.8A CN103708959B (en) | 2013-12-15 | 2013-12-15 | A kind of Double-control sustained-release fertilizer and production method thereof |
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| CN103708959A CN103708959A (en) | 2014-04-09 |
| CN103708959B true CN103708959B (en) | 2015-12-09 |
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| CN104447029B (en) * | 2014-12-14 | 2017-03-08 | 青岛锐志农业技术服务有限公司 | A kind of environment-friendlyplant plant slow-release compound fertilizer |
| CN107056407A (en) * | 2016-12-30 | 2017-08-18 | 华南农业大学 | A kind of film-coated and slow release fertilizer using municipal sludge as raw material and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1524832A (en) * | 2003-03-02 | 2004-09-01 | 吴永常 | Envelope technology and method for controllable slow-release fertilizer |
| CN2771202Y (en) * | 2003-04-21 | 2006-04-12 | 冯树杰 | Two-cladding-layer, two-film-layer spherical fertilizer |
| CN101165013A (en) * | 2007-09-22 | 2008-04-23 | 李涛 | Special fertilizer for lawn and granulating method thereof |
| CN103058789A (en) * | 2012-12-29 | 2013-04-24 | 广东中迅农科股份有限公司 | Cartap fertilizer granules and preparation method thereof |
| CN103351209A (en) * | 2013-06-07 | 2013-10-16 | 安徽金阳环保肥业有限公司 | Slow-release fertilizer special for cotton and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100946937B1 (en) * | 2007-10-31 | 2010-03-09 | 주식회사 동부하이텍 | Biodegradable slow-release coating fertilizer |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1524832A (en) * | 2003-03-02 | 2004-09-01 | 吴永常 | Envelope technology and method for controllable slow-release fertilizer |
| CN2771202Y (en) * | 2003-04-21 | 2006-04-12 | 冯树杰 | Two-cladding-layer, two-film-layer spherical fertilizer |
| CN101165013A (en) * | 2007-09-22 | 2008-04-23 | 李涛 | Special fertilizer for lawn and granulating method thereof |
| CN103058789A (en) * | 2012-12-29 | 2013-04-24 | 广东中迅农科股份有限公司 | Cartap fertilizer granules and preparation method thereof |
| CN103351209A (en) * | 2013-06-07 | 2013-10-16 | 安徽金阳环保肥业有限公司 | Slow-release fertilizer special for cotton and preparation method thereof |
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