CN103585783B - Honeysuckle extraction is steamed extraction element and method - Google Patents
Honeysuckle extraction is steamed extraction element and method Download PDFInfo
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- CN103585783B CN103585783B CN201310619771.4A CN201310619771A CN103585783B CN 103585783 B CN103585783 B CN 103585783B CN 201310619771 A CN201310619771 A CN 201310619771A CN 103585783 B CN103585783 B CN 103585783B
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Abstract
The present invention relates to a kind of honeysuckle extraction and steam extraction element and method, steaming pot be will extract and heater and condenser will be equipped with, cooler serial connection heater, by extracting and distilling compatible process, honeysuckle raw material enters extraction steaming pot from feed inlet and outlet, the hot water that extraction steaming pot top passes into directly sprays in extraction on honeysuckle raw material through diffusing net and steams, in extraction steaming process, the honeysuckle effective ingredient feed liquid that gaseous, liquid coexists is the tubulation to condenser by carrier pipe, be cooled to below 40 DEG C by the normal-temperature water outside tubulation, being converted into liquid collects from liquid outlet, normal-temperature water outside tubulation is replaced as hot water, and be delivered to heater, steam hot water is provided for extraction steaming pot honeysuckle extraction again, so iterative cycles, reach energy-efficient. the present invention can larger limit extract outside effective ingredient of honeysuckle chlorogenic acid and flavonoids etc., can all reclaim again the contained volatile ingredient honeysuckle wet goods active ingredient of volatilization gas, improve chlorogenic acid extract yield, improve making full use of of effective ingredient of honeysuckle.
Description
Technical field
The invention belongs to Chinese medicine and extract manufacture field, particularly relate to a kind of honeysuckle extraction and steam extraction element and method.
Background technology
Honeysuckle is the dry flower of caprifoliaceae plant honeysuckle or the flower that band is just opened, herb all can be used as medicine, bud contains volatility honeysuckle aromatic oil, inositol, saponin(e, chlorogenic acid, the compounds such as flavonoids, cinnamic acid, nerol, jasmine arrives aldehyde etc., in stem, contain biological salty, he is rhinoceros element etc. in leaf, to contain lonicerin, wherein, chlorogenic acid is the main pharmacodynamics active component of honeysuckle, also have the compounds such as flavonoids, other volatility honeysuckle wet goods active ingredient also has medical value, also be one of traditional Chinese medicine material, have clearing heat and detoxicating, wind-heat dissipating, effect of hepatic cholagogic, the swollen sore for the treatment of of carbuncle, larynx numbness, anemopyretic colds etc. all have good curative effect, chlorogenic acid is to digestive system, hematological system and reproductive system all have pharmacological action, there is anti-inflammation widely, cholagogic, the effect that white blood cell count is increased in hemostasis. at present, from honeysuckle extracting method and from honeysuckle the method for chlorogenic acid extracting, mainly contain water extraction, water extract-alcohol precipitation, rare alcohol extracting etc., adopt the combined-enzyme method new technology chlorogenic acid extracting of cellulase and pectase as Chinese patent CN201010124495.0 discloses " a kind of method that adopts combined-enzyme method to extract Chlorogenic Acid of Flos Lonicerae " proposition.
Chinese patent CN201210308017.4 discloses " a kind of from honeysuckle-leaf chlorogenic acid extracting and Hyperoside method " and has proposed one and utilize crystallization and recrystallization method large-scale production chlorogenic acid and Hyperoside from fresh honeysuckle-leaf.
Chinese patent 201110292709.X discloses a kind of method of chlorogenic acid extracting in honeysuckle that " from honeysuckle rapidly and efficiently the method for chlorogenic acid extracting " discloses rapid extraction and be not destroyed in the biologically active of leaching process Content of Chlorogenic Acid and chemical constitution.
Chinese patent CN01144170.4 discloses " method for extraction and purification of Chlorogenic Acid of Flos Lonicerae " and has adopted Diluted Alcohol to carry out secondary back extraction to honeysuckle, concentrated extract, again with the preliminary edulcoration purification of flocculence, finally adopts Amberlyst process or acid ethyl acetate extraction purification refine.
In described patent and patent application or prior art, round the technology of extracting chlorogenci acid from honeysuckle main component, research honeysuckle main component chlorogenic acid extract yield, and the limitation of extraction process, and some other active ingredient has been left in the basket, the abundant extraction and application of less research effective ingredient of honeysuckle, as volatility honeysuckle wet goods active ingredient also has medical value.
And obviously there is drawback in these process for extracting, the active ingredient of honeysuckle can not obtain release and the utilization of larger limit, and the infiltration adopting is distilled while extracting processing method, also only limit to extract main component chlorogenic acid etc., as needs extract other active ingredient, processing technology is extracted in the infiltration distillation adopting, it is very slow that it adds man-hour distillation speed, be difficult to form production capacity, research displaces outside effective ingredient of honeysuckle chlorogenic acid and flavonoids etc., reclaim the contained active ingredient of volatilization gas, improve honeysuckle the making full use of of active ingredient in leaching process, improving production capacity is the problem that urgent need is researched and solved.
Summary of the invention
Object of the present invention is exactly the problem in order to solve prior art, provide a kind of honeysuckle extraction to steam extraction element and method, by the technique of extraction and way of distillation compatibility, can larger limit extract outside effective ingredient of honeysuckle chlorogenic acid and flavonoids etc., can all reclaim again the contained volatile ingredient honeysuckle wet goods active ingredient of volatilization gas, improve chlorogenic acid extract yield, improve making full use of of effective ingredient of honeysuckle, improve production capacity.
Another object of the present invention is to provide a kind of steaming pot honeysuckle extraction that extracts and steams the process that uses circulating hot water, be connected in series heater by cooler, steaming through extraction steaming pot extraction the effective ingredient of honeysuckle feed liquid of extracting is high temperature, by cooling by normal-temperature water in condenser, normal-temperature water is replaced as hot water and is sent to again heater and makes solvent hot water, through Steam Heating, is that extraction steaming pot honeysuckle extraction is steamed and used, so iterative cycles, reaches and extracts complete, energy-efficient object.
The technical solution adopted in the present invention is: a kind of honeysuckle extraction is steamed extraction element, hermetically sealed extraction steaming pot upper end is provided with hot water inlet, extraction steaming pot one side is provided with feed inlet and outlet, diffusing net is set in extraction steaming pot above, screen pack is set below, extraction steaming pot bottom is respectively equipped with sewage draining exit, liquid outlet, and liquid outlet accesses condenser by carrier pipe;
Described upper end of condenser is connected to hot water out pipe, and a side is provided with cooling water inlet, and bottom is provided with liquid outlet, is vertically arranged with tubulation in condenser, carrier pipe access tubulation, tubulation access liquid outlet.
Described hot water out pipe access heater, arranges tubulation in heater, heater is provided with steam inlet, and bottom is provided with hot water outlet, and hot water outlet accesses hot water inlet by hot-water line.
A kind of honeysuckle extraction is steamed extracting method, and concrete steps are as follows:
1) solvent heating, hot water enters heater from water inlet, flow to tubulation in heater, passes into steam simultaneously, continues hot water in heating tubulation by steam, and hot water temperature remains on more than 90 DEG C, flow to extraction steaming pot from hot water outlet;
2) extraction is steamed, honeysuckle raw material enters extraction steaming pot from feed inlet and outlet, and place on screen pack, the hot water that extraction steaming pot top passes into directly sprays in extraction on honeysuckle raw material through diffusing net and steams, honeysuckle raw material 50-60kg, extraction steaming time 90-140 minute, in extraction steaming process, the effective ingredient of honeysuckle feed liquid that gaseous, liquid coexists is by carrier pipe to condenser, and dirt is discharged from sewage draining exit;
3) cooling, the honeysuckle effective ingredient feed liquid that gas-liquid coexists by carrier pipe to the tubulation in condenser, being cooled to 40 DEG C by the normal-temperature water outside pipe is converted into below liquid and collects from liquid outlet, the replaced amount of normal-temperature water outside tubulation becomes hot water, water temperature is increased to the circulating hot water of 70-80 DEG C and is sent to again heater by hot water out pipe and does solvent heating, and the honeysuckle of extraction is collected liquid and comprises chlorogenic acid and honeysuckle wet goods effective ingredient.
Technique scheme of the present invention, has the following advantages:
1, the present invention adopts honeysuckle extraction to steam process for extracting, extraction steaming pot is equipped with to heater and cooler, in collecting extract, hot dipping is carried to gas (volatile ingredient) and all give cooling recovery, extraction steaming pot passes into hot water and directly sprays in extraction steaming on honeysuckle raw material through diffusing net, in extraction steaming process, the effective ingredient of honeysuckle feed liquid that gaseous, liquid coexists by carrier pipe to condenser, steam technique by extraction and extracted the whole active ingredient feed liquids that honeysuckle comprises liquid and gaseous state, normal-temperature water in condenser is cooled to below 40 DEG C, the effective ingredient of honeysuckle feed liquid that gaseous, liquid coexists all converts liquid to, comprise and extract honeysuckle main component chlorogenic acid, also reclaimed the contained lonicera oil of other active ingredient escaping gas of honeysuckle simultaneously, improve making full use of of effective ingredient of honeysuckle.
2, the present invention adopts honeysuckle extraction to steam process for extracting, by extraction steaming pot below built-in screen pack, honeysuckle is distributed in extraction steaming pot, by built-in diffusing net above extraction steaming pot, make on honeysuckle raw material, to extract steaming through direct uniform spray by the hot water of extraction steaming pot, make honeysuckle extraction steam extraction process and more divide fully.
3, the present invention extracts steaming pot by employing and is set to hermetically sealed, liquid outlet is set below, and directly deliver in condenser by carrier pipe, ensure the honeysuckle effective ingredient feed liquid that honeysuckle extraction steaming extraction process realization collection gaseous state, liquid state coexist, and by the cooling effective ingredient of honeysuckle liquid of collecting of condenser, by the technique that adds of extraction and way of distillation compatibility, improve chlorogenic acid extract yield, realize honeysuckle material effective component and all make full use of.
4, the present invention adopts condenser inside that tubulation is longitudinally set, the honeysuckle effective ingredient feed liquid that gas-liquid coexists accesses tubulation by carrier pipe, longitudinally tubulation is uniform in condenser inside, has ensured that feed liquid is fully cooling in condenser, collects effective ingredient of honeysuckle effect liquid better.
5, the present invention is owing on adopting process equipment, heater and cooler being connected in series, adopt extraction steaming pot honeysuckle extraction to steam the method that uses circulating hot water, making full use of the effective ingredient of honeysuckle feed liquid of extracting through the steaming of extraction steaming pot extraction is high temperature, by cooling by normal-temperature water in condenser, and normal-temperature water is replaced as hot water and is sent to heater and makes solvent hot water, transform by heat energy, steaming to use for extraction steaming pot honeysuckle extraction provides hot water, so iterative cycles, reaches extraction complete, energy-efficient.
Brief description of the drawings
Fig. 1 is that a kind of honeysuckle extraction of the present invention is steamed extraction element structural representation.
Fig. 2 is that a kind of honeysuckle extraction of the present invention is steamed extracting method process flow diagram.
Extract steaming pot 1, hot water inlet 2, feed inlet and outlet 3, diffusing net 4, screen pack 5, sewage draining exit 6, liquid outlet 7, cross carrier pipe 8, condenser 9, condenser 9, hot water out pipe 10, cooling water inlet 11, liquid outlet 12, condenser 9, tubulation 13, heater 14, steam inlet 15, tubulation 16, hot water outlet 17, hot-water line 18.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in more detail.
As shown in Figure 1, 2, a kind of honeysuckle extraction is steamed extraction element, will extract steaming pot and be equipped with heater and condenser. Extraction steaming pot 1 is made hermetically sealed, extraction steaming pot 1 top has hot water inlet 2, extraction steaming pot 1 one sides have feed inlet and outlet 3, extraction steaming pot 1 bottom is provided with sewage draining exit 6, liquid outlet 7, in extraction steaming pot 1, extraction steaming pot 1 arranges diffusing net 4 above, and extraction steaming pot 1 arranges screen pack 5 below, and liquid outlet 7 accesses condenser 9 by carrier pipe 8;
Condenser 9 upper ends are connected to hot water out pipe 10, one sides and are provided with cooling water inlet 11, and bottom is provided with liquid outlet 12, are vertically arranged with tubulation 13 in condenser 9, and carrier pipe 8 accesses tubulation 13, and tubulation 13 accesses liquid outlet 12.
Hot water out pipe 10 accesses heater 14, and heater 14 is interior longitudinally arranges tubulation 16, or horizontally set tubulation 16, is connected to steam inlet 15 on heater 14, and bottom is connected to hot water outlet 17, and hot water outlet 17 accesses hot water inlet 2 by hot-water line 18.
Honeysuckle extraction is steamed extracting method, and hot water enters heater from water inlet, flow to tubulation in heater, passes into steam simultaneously, continues hot water in heating tubulation by steam, and hot water temperature remains on more than 90 DEG C, flow to extraction steaming pot from hot water outlet; Honeysuckle raw material enters extraction steaming pot from feed inlet and outlet, and place on screen pack, the hot water that extraction steaming pot top passes into directly sprays in extraction on honeysuckle raw material through diffusing net and steams, honeysuckle raw material 50-60kg, extraction steaming time 90-140 minute, in extraction steaming process, the honeysuckle effective ingredient feed liquid that gaseous, liquid coexists is by carrier pipe to condenser, and dirt is discharged from sewage draining exit; The honeysuckle effective ingredient feed liquid that gas-liquid coexists by carrier pipe to the tubulation in condenser, the honeysuckle effective ingredient feed liquid that gaseous state, liquid state coexist is cooled to 40 DEG C and is converted into below liquid and collects from liquid outlet, the replaced heat of normal-temperature water outside tubulation becomes hot water, water temperature is increased to the circulating hot water of 70-80 DEG C and is sent to again heater by hot water out pipe and does solvent heating, and the honeysuckle of extraction is collected liquid and comprises chlorogenic acid and honeysuckle wet goods effective ingredient.
Embodiment:
Above-described embodiment is used for illustrating the present invention, is not limitation of the invention.
Claims (1)
1. honeysuckle extraction is steamed an extraction element, it is characterized in that: this honeysuckle extraction is steamed extraction element and had hermetically sealed extraction steaming pot (1), described inExtraction steaming pot (1) upper end is provided with hot water inlet (2), and described extraction steaming pot (1) one side is provided with feed inlet and outlet (3), in described extraction steaming pot (1)Diffusing net (4) is set above, screen pack (5) is set in described extraction steaming pot (1) below, described extraction steaming pot (1) bottom is respectively equipped with blowdownMouth (6), gas liquid outlet (7), described gas liquid outlet (7) is by carrier pipe (8) access condenser (9);
Described condenser (9) upper end is connected to hot water out pipe (10), and described condenser (9) one sides are provided with cooling water inlet (11), described condensationDevice (9) bottom is provided with liquid outlet (12), is vertically arranged with the second tubulation (13) in described condenser (9), and described carrier pipe (8) connectsEnter described the second tubulation (13), described the second tubulation (13) access liquid outlet (12);
Described hot water out pipe (10) access heater (14), arranges the first tubulation (16), described heater in described heater (14)(14) be provided with steam inlet (15), described heater (14) bottom is provided with hot water outlet (17), and described hot water outlet (17) connectsConnect hot-water line (18) and access again extraction steaming pot (1);
The extraction that this honeysuckle extraction is steamed extraction element is steamed the method for extracting honeysuckle, and concrete steps are as follows:
1) solvent heating, hot water enters heater from water inlet, flow to the first tubulation in heater, passes into steam simultaneously, continues to add by steamHot water in heat the first tubulation, hot water temperature remains on more than 90 DEG C, flow to extraction steaming pot from hot water outlet;
2) extraction is steamed, and honeysuckle raw material enters extraction steaming pot from feed inlet and outlet, and places on screen pack, and the hot water that extraction steaming pot top passes into is straight through diffusing netConnect spray extraction on honeysuckle raw material and steam, honeysuckle raw material 50-60kg, extraction steaming time 90-140 minute, in extraction steaming process, gaseous, liquid is commonThe honeysuckle effective ingredient feed liquid of depositing is by carrier pipe to condenser, and dirt is discharged from sewage draining exit;
3) cooling, the honeysuckle effective ingredient feed liquid that gas-liquid coexists, is cooled to by the normal-temperature water outside pipe to the second tubulation in condenser by carrier pipe40 DEG C are converted into below liquid and collect from liquid outlet, and the replaced amount of normal-temperature water outside the second tubulation becomes hot water, and water temperature is increased to the circulation of 70-80 DEG CHot water is sent to again heater by hot water out pipe and does solvent heating, and the honeysuckle of extraction is collected liquid and comprises chlorogenic acid and lonicera oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310619771.4A CN103585783B (en) | 2013-11-29 | 2013-11-29 | Honeysuckle extraction is steamed extraction element and method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310619771.4A CN103585783B (en) | 2013-11-29 | 2013-11-29 | Honeysuckle extraction is steamed extraction element and method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103585783A CN103585783A (en) | 2014-02-19 |
| CN103585783B true CN103585783B (en) | 2016-05-11 |
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| CN106362433B (en) * | 2016-08-30 | 2019-02-05 | 江苏康缘药业股份有限公司 | A kind of control method and device of the green medicinal extract extraction process of gold |
| CN107950845A (en) * | 2017-11-16 | 2018-04-24 | 湖北瀚思生物科技有限公司 | Honeysuckle functional beverage and its production method |
| CN113563973B (en) * | 2021-08-06 | 2024-05-03 | 温州阳羽机械科技有限公司 | Low-temperature extraction equipment and process for rose petal water |
| CN117099984B (en) * | 2023-08-02 | 2024-07-16 | 真奥金银花药业有限公司 | Honeysuckle beverage production equipment and preparation method thereof |
| CN116889584A (en) * | 2023-08-28 | 2023-10-17 | 真奥金银花药业有限公司 | Continuous extraction process of honeysuckle |
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| CN201415068Y (en) * | 2009-06-16 | 2010-03-03 | 江苏七〇七天然制药有限公司 | Device for extracting and concentrating effective ingredient of traditional Chinese medicine |
| JP5042508B2 (en) * | 2006-02-28 | 2012-10-03 | 湘南香料株式会社 | Method for producing extract |
| CN202526937U (en) * | 2012-04-12 | 2012-11-14 | 成都科尔医药技术有限公司 | Dynamic extracting and concentrating integrated device for traditional Chinese medicines |
| CN202671521U (en) * | 2012-06-30 | 2013-01-16 | 安徽皖峰蜂业集团有限公司 | Honeysuckle distillation extraction device |
| CN203620286U (en) * | 2013-11-29 | 2014-06-04 | 湖北瀚思生物科技有限公司 | Honeysuckle extraction-steaming extraction device |
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| WO2002072743A1 (en) * | 2001-03-13 | 2002-09-19 | Council Of Scientific And Industrial Research | A simple portable mini distillation apparatus for the production of essential oils and hydrosols |
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| JP5042508B2 (en) * | 2006-02-28 | 2012-10-03 | 湘南香料株式会社 | Method for producing extract |
| CN201415068Y (en) * | 2009-06-16 | 2010-03-03 | 江苏七〇七天然制药有限公司 | Device for extracting and concentrating effective ingredient of traditional Chinese medicine |
| CN202526937U (en) * | 2012-04-12 | 2012-11-14 | 成都科尔医药技术有限公司 | Dynamic extracting and concentrating integrated device for traditional Chinese medicines |
| CN202671521U (en) * | 2012-06-30 | 2013-01-16 | 安徽皖峰蜂业集团有限公司 | Honeysuckle distillation extraction device |
| CN203620286U (en) * | 2013-11-29 | 2014-06-04 | 湖北瀚思生物科技有限公司 | Honeysuckle extraction-steaming extraction device |
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