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CN103528934A - Mutual correlation technology for measuring permeability stress sensitivity of ultra-low permeability rocks - Google Patents

Mutual correlation technology for measuring permeability stress sensitivity of ultra-low permeability rocks Download PDF

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CN103528934A
CN103528934A CN201310518094.7A CN201310518094A CN103528934A CN 103528934 A CN103528934 A CN 103528934A CN 201310518094 A CN201310518094 A CN 201310518094A CN 103528934 A CN103528934 A CN 103528934A
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permeability
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CN103528934B (en
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王小琼
葛洪魁
申颍浩
汪道兵
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China University of Petroleum Beijing
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Abstract

本发明提供了一种测量超低渗岩石渗透率应力敏感性的互相关技术。该技术包括下列步骤:a)选取页岩或致密砂岩等超低渗岩心,将其加工成圆柱体试件;b)加工一个圆柱体钢块标准试件,用于系统标定;c)采用周期振荡法进行超低渗透率的测量,孔隙介质可采用气体或水。钢块测量结果用于标定系统;d)将岩心放于夹持器中,施加围压、孔隙压,对岩心进行饱和,施加上游正弦压力波并保持不变,测量不同围压的下游压力波响应;e)对不同围压的下游压力波形进行互相关分析,获得渗透率随围压的变化。本发明结合超低渗透岩石渗透率测量的周期振荡法,对渗透率测量的压力波形进行互相关分析,提高渗透率变化测量的精度,解决超低渗透率应力敏感性测量难题。

Figure 201310518094

The invention provides a cross-correlation technique for measuring the stress sensitivity of ultra-low permeability rock permeability. The technology includes the following steps: a) select ultra-low permeability cores such as shale or tight sandstone, and process them into cylindrical specimens; b) process a cylindrical steel block standard specimen for system calibration; c) use periodic Oscillation method is used to measure ultra-low permeability, and the porous medium can be gas or water. The measurement results of the steel block are used to calibrate the system; d) Put the core in the holder, apply confining pressure and pore pressure, saturate the core, apply the upstream sinusoidal pressure wave and keep it constant, and measure the downstream pressure wave of different confining pressure Response; e) Perform cross-correlation analysis on the downstream pressure waveforms of different confining pressures to obtain the variation of permeability with confining pressure. The present invention combines the periodic oscillation method of ultra-low permeability rock permeability measurement to perform cross-correlation analysis on the pressure waveform of permeability measurement, improves the accuracy of permeability change measurement, and solves the problem of ultra-low permeability stress sensitivity measurement.

Figure 201310518094

Description

一种测量超低渗岩石渗透率应力敏感性的互相关技术A cross-correlation technique for measuring the stress sensitivity of ultra-low permeability rock permeability

技术领域technical field

本发明是关于超低渗透率材料应力敏感性测试的技术,特别是关于一种超低渗岩石渗透率应力敏感性的互相关测试技术。本发明可为非常规油气储层、核废料储层的渗透率应力敏感性测试提供技术支持。The invention relates to a technology for testing stress sensitivity of ultra-low permeability materials, in particular to a cross-correlation testing technology for ultra-low permeability rock permeability stress sensitivity. The invention can provide technical support for the permeability stress sensitivity test of unconventional oil and gas reservoirs and nuclear waste reservoirs.

背景技术Background technique

渗透率是储层最重要的物性参数,也是油气开发的基础。近年来随着页岩气、致密砂岩油气等非常规油气的开发,迫切需要开展超低渗透率(<0.1×10-3μm2)测试,这对测试方法和仪器都提出了挑战,是非常规油气开发研究的难点。目前我国石油工业中主要采用稳态法和脉冲衰减法进行超低渗透率测试,在测试精度、稳定性和测试周期方面还存在不足,发展高精度超低渗透率的方法十分重要。Permeability is the most important physical parameter of reservoir and the basis of oil and gas development. In recent years, with the development of unconventional oil and gas such as shale gas and tight sandstone oil and gas, there is an urgent need to carry out ultra-low permeability (<0.1×10 -3 μm 2 ) testing, which poses challenges to both testing methods and instruments, and is unconventional. Difficulties in oil and gas development research. At present, the steady-state method and pulse decay method are mainly used in my country's petroleum industry to test ultra-low permeability, but there are still shortcomings in test accuracy, stability and test cycle. It is very important to develop high-precision ultra-low permeability methods.

影响渗透率测量的因素主要可分为外因和内因两大类,内因即岩石的矿物成分、孔隙结构、颗粒大小等。外因主要有压力、温度及流体的性质。在实验室中对于超低渗岩心,尤其是对于渗透率低于0.1×10-3μm2的岩心样品,渗透率测量耗时长,有的长达数周到数月,因此首先对压机的压力泵以及孔隙压力泵等仪器提出了较高的要求,需要仪器的精度高,稳定性好,可以保持某一应力状态长达数日至数月以测量某一应力状态下的渗透率值。其次,无论是孔隙压力泵原因还是测量渗透率方法的原因,孔隙压力的扰动也要非常小。实验过程中无论是输入的孔隙压力还是输出的测试压力都存在噪声,如低频的温度扰动、高频的泵和压力传感器的噪音、以及其他高频的电信号等高低频噪音,这些噪音对测试结果具有重要影响,随着测试样品渗透率的降低而增大。特别是针对超低渗的岩心,仪器恒定温度至关重要。否则很小的温度及环境扰动都可能导致孔隙压力曲线难以拟合。目前常用的稳态法和脉冲衰减法测量超低渗透率稳定性不够好、精度也受温度噪音等影响,更难测量渗透率的应力敏感性。The factors affecting the measurement of permeability can be mainly divided into two categories: external factors and internal factors. The internal factors are the mineral composition, pore structure, and particle size of rocks. External factors mainly include pressure, temperature and fluid properties. For ultra-low permeability cores in the laboratory, especially for core samples with a permeability lower than 0.1×10 -3 μm 2 , the measurement of permeability takes a long time, some as long as several weeks to several months, so the pressure of the press Instruments such as pumps and pore pressure pumps put forward higher requirements. The instruments need to have high precision and good stability, and can maintain a certain stress state for several days to several months to measure the permeability value under a certain stress state. Second, the perturbation of the pore pressure, whether due to the pore pressure pump or the method of measuring the permeability, should be very small. During the experiment, there are noises in both the input pore pressure and the output test pressure, such as low-frequency temperature disturbance, high-frequency pump and pressure sensor noise, and other high-frequency electrical signals and other high- and low-frequency noises. The results have significant effects, which increase with decreasing permeability of the test sample. Especially for cores with ultra-low permeability, the constant temperature of the instrument is very important. Otherwise, small temperature and environmental disturbances may make it difficult to fit the pore pressure curve. The commonly used steady-state method and pulse decay method are not stable enough to measure ultra-low permeability, and the accuracy is also affected by temperature noise, which makes it more difficult to measure the stress sensitivity of permeability.

相对于目前广泛应用的脉冲衰减法,周期振荡法对实验条件、环境等要求低,具有用时短,结果稳定、精度高的优点。周期振荡法只用了岩石两端孔隙压力信号的振幅比和相位差,对绝对值没有要求,因此一定程度上降低了环境变化对测量结果的影响。并且周期振荡法的孔隙压力波具备波形特征,可应用快速富里叶变换(FFT)、互谱法等数字信号处理方法处理周期振荡法的数据,从而能大幅度地提高信噪比,以达到精细测量超低渗透率的要求。本发明结合超低渗透岩石渗透率测量的周期振荡法,将波形互相关方法用于渗透率变化测量,大幅度提高渗透率变化测量的精度和稳定性,解决超低渗透岩石渗透率应力敏感性测量难题。该方法原理为:两列波形的互相关可高精度地获得波形相位差异,属于波形干涉测量,在信号检测领域获得广泛应用。本发明将波形互相关方法用于渗透率变化测量,对渗透率测量的压力波形进行互相关分析,获得渗透率随围压的变化,评价超低渗透岩石渗透率的应力敏感性。为非常规油气储层、核废料储层的渗透率应力敏感性测试提供技术支持Compared with the pulse attenuation method widely used at present, the periodic oscillation method has lower requirements on experimental conditions and environment, and has the advantages of short time, stable results and high precision. The periodic oscillation method only uses the amplitude ratio and phase difference of the pore pressure signals at both ends of the rock, and does not require absolute values, so the influence of environmental changes on the measurement results is reduced to a certain extent. Moreover, the pore pressure wave of the periodic oscillation method has waveform characteristics, and digital signal processing methods such as fast Fourier transform (FFT) and cross-spectrum method can be used to process the data of the periodic oscillation method, so that the signal-to-noise ratio can be greatly improved to achieve fine Measuring ultra-low permeability requirements. The present invention combines the periodic oscillation method of ultra-low permeability rock permeability measurement, uses the waveform cross-correlation method for permeability change measurement, greatly improves the accuracy and stability of permeability change measurement, and solves the ultra-low permeability rock permeability stress sensitivity Measurement conundrum. The principle of the method is: the cross-correlation of two columns of waveforms can obtain the waveform phase difference with high precision, which belongs to waveform interferometry and is widely used in the field of signal detection. The invention uses the waveform cross-correlation method for permeability change measurement, carries out cross-correlation analysis on the pressure waveform of permeability measurement, obtains the change of permeability with confining pressure, and evaluates the stress sensitivity of ultra-low permeability rock permeability. Provide technical support for the permeability stress sensitivity test of unconventional oil and gas reservoirs and nuclear waste reservoirs

发明内容Contents of the invention

本发明的目的是提供一种测量超低渗岩石渗透率应力敏感性的互相关技术,该技术综合体现了非常规储层低孔、低渗的特征,并在实验设备及数据处理上做了创新性的发明。从而进行超低渗岩心渗透率应力敏感性监测。The purpose of the present invention is to provide a cross-correlation technology for measuring the stress sensitivity of ultra-low permeability rock permeability. Innovative invention. In order to monitor the stress sensitivity of ultra-low permeability core permeability.

为实现上述目的,本发明提供了一种超低渗岩石渗透率应力敏感性的互相关技术,该技术包括下列步骤:a)选取页岩或致密砂岩等超低渗岩心,将其加工成圆柱体试件;b)加工一个圆柱体钢块标准试件,用于系统标定;c)采用周期振荡法进行超低渗透率的测量,孔隙介质可采用气体或水。首先将钢块试件放于岩心夹持器中,夹持器由两个伺服压力泵通过阀门分别给岩心施加围压、正弦孔隙压力波。钢块测量结果用于标定系统;d)将岩心放于夹持器中,施加围压、孔隙压,对岩心进行水饱和或气饱和。岩心饱和后,施加上游正弦压力波,测量下游正弦压力波响应。保持上游正弦压力波不变,变围压,测量不同围压的下游压力波的响应;e)将波形互相关方法用于渗透率变化测量,对不同围压下渗透率测量的压力波形进行互相关分析,获得渗透率随围压的变化,评价超低渗透岩石渗透率的应力敏感性。In order to achieve the above object, the present invention provides a cross-correlation technology of ultra-low permeability rock permeability stress sensitivity, which comprises the following steps: a) select ultra-low permeability rock cores such as shale or tight sandstone, and process them into cylindrical b) process a cylindrical steel block standard sample for system calibration; c) use periodic oscillation method for ultra-low permeability measurement, and the porous medium can be gas or water. First, the steel block specimen is placed in the core holder, and the holder uses two servo pressure pumps to respectively apply confining pressure and sinusoidal pore pressure wave to the core through the valve. The measurement results of the steel block are used to calibrate the system; d) Put the core in the holder, apply confining pressure and pore pressure, and saturate the core with water or gas. After the core is saturated, an upstream sinusoidal pressure wave is applied and the downstream sinusoidal pressure wave response is measured. Keep the upstream sinusoidal pressure wave unchanged, change the confining pressure, and measure the response of the downstream pressure wave at different confining pressures; e) use the waveform cross-correlation method for the measurement of permeability changes, and perform cross-correlation on the pressure waveforms of permeability measurements under different confining pressures. Through correlation analysis, the change of permeability with confining pressure is obtained, and the stress sensitivity of ultra-low permeability rock permeability is evaluated.

进一步地,在步骤a)中,选取的页岩、致密砂岩等岩心取自所开发储层的全直径岩心或相同层位的露头,具有超低渗透率。将所述岩心加工成直径为2.5cm,高度为3-4cm的标准圆柱体。Further, in step a), the selected cores such as shale and tight sandstone are taken from full-diameter cores of the developed reservoir or outcrops of the same horizon, and have ultra-low permeability. The core is processed into a standard cylinder with a diameter of 2.5 cm and a height of 3-4 cm.

进一步地,在步骤b)中,加工一个与岩心同尺度的圆柱体钢块试件。钢块的孔隙度和渗透率理论上为零。Further, in step b), a cylindrical steel block specimen with the same scale as the core is processed. The porosity and permeability of steel blocks are theoretically zero.

进一步地,在步骤c)中,将钢块试件放于夹持器中,分别给钢块试件施加围压、孔隙压。并在钢块试件上游施加正弦孔隙压力波,测量下游孔隙压力波响应。该测量结果用于对系统比储流率等值进行标定。Further, in step c), the steel block test piece is placed in the holder, and the confining pressure and pore pressure are respectively applied to the steel block test piece. A sinusoidal pore pressure wave is applied upstream of the steel block specimen, and the downstream pore pressure wave response is measured. The measurement results are used to calibrate the system specific storage rate equivalent.

进一步地,在步骤d)中,采用周期振荡法进行页岩、致密砂岩等超低渗岩心渗透率的测量。施加围压、孔隙压对岩心进行饱和后,施加上游正弦压力波,测量下游正弦压力波响应。保持上游正弦压力波不变,变围压,测量不同围压的下游压力波的响应。Further, in step d), the periodic oscillation method is used to measure the permeability of ultra-low permeability cores such as shale and tight sandstone. After applying confining pressure and pore pressure to saturate the core, an upstream sinusoidal pressure wave is applied, and the downstream sinusoidal pressure wave response is measured. Keep the upstream sinusoidal pressure wave constant, change the confining pressure, and measure the response of the downstream pressure wave with different confining pressure.

进一步地,在步骤e)中,在周期振荡法数据处理中采用互相关技术,选择某一围压的下游孔隙压力波为参考压力波形,通过不同围压下下游压力波与参考压力波的互相关处理,获得相对的压力波形幅值比及相位差。Further, in step e), the cross-correlation technique is adopted in the data processing of the periodic oscillation method, and the downstream pore pressure wave of a certain confining pressure is selected as the reference pressure waveform, and the correlation between the downstream pressure wave and the reference pressure wave under different confining pressures is used to Correlation processing to obtain the relative pressure waveform amplitude ratio and phase difference.

进一步地,在夹持器中输运孔隙流体的管道内径非常小,约为0.7mm,出夹持器以后通过阀门将管道连接到内径3mm的大管道。以减少比储流率对超低渗岩心渗透率测试的影响。Further, the inner diameter of the pipe transporting the pore fluid in the holder is very small, about 0.7 mm, and after exiting the holder, the pipe is connected to a large pipe with an inner diameter of 3 mm through a valve. In order to reduce the impact of the specific storage rate on the ultra-low permeability core permeability test.

进一步地,保持上游孔隙压力波形不变,即保持上游孔隙压力波形相同的振幅及频率。Further, keep the waveform of the upstream pore pressure unchanged, that is, keep the same amplitude and frequency of the upstream pore pressure waveform.

进一步地,选择某一围压条件下的下游压力波为参考波形,选择某一围压条件下的渗透率为参考渗透率。Further, the downstream pressure wave under a certain confining pressure is selected as the reference waveform, and the permeability under a certain confining pressure is selected as the reference permeability.

本发明的有益效果在于,结合超低渗透岩石渗透率测量的周期振荡法,将波形互相关方法用于渗透率变化测量,对渗透率测量的压力波形进行互相关分析,大幅度提高渗透率变化测量的精度和稳定性,获得渗透率随围压的变化,解决超低渗透岩石渗透率应力敏感性测量难题,以评价超低渗透岩石渗透率的应力敏感性。该方法在非常规油气开发、核废料储层研究中将会应力潜力较大。The beneficial effect of the present invention is that, in combination with the periodical oscillation method of ultra-low permeability rock permeability measurement, the waveform cross-correlation method is used for the permeability change measurement, and the cross-correlation analysis is performed on the pressure waveform of the permeability measurement, which greatly improves the permeability change. The accuracy and stability of the measurement can obtain the change of permeability with the confining pressure, and solve the problem of stress sensitivity measurement of ultra-low permeability rock permeability, so as to evaluate the stress sensitivity of ultra-low permeability rock permeability. This method will have great stress potential in unconventional oil and gas development and nuclear waste reservoir research.

附图说明Description of drawings

为了更清楚地说明本发明实施例,下面将对实施例描述中所需要使用的附图作简单地介绍。在附图中:In order to illustrate the embodiments of the present invention more clearly, the following briefly introduces the accompanying drawings that are used in the description of the embodiments. In the attached picture:

图1为本发明实施例一种测量超低渗岩石渗透率应力敏感性的互相关技术的实验流程图;Fig. 1 is an experimental flow chart of a cross-correlation technique for measuring ultra-low permeability rock permeability stress sensitivity in an embodiment of the present invention;

图2为本发明实施例一种测量超低渗岩石渗透率应力敏感性的互相关技术的实验装置结构示意图;Fig. 2 is a schematic diagram of the experimental device structure of a cross-correlation technique for measuring the stress sensitivity of ultra-low permeability rock permeability in an embodiment of the present invention;

图3为本发明实施例超低渗岩石渗透率应力敏感性测量的互相关技术示意图;3 is a cross-correlation technical schematic diagram of ultra-low permeability rock permeability stress sensitivity measurement in an embodiment of the present invention;

具体实施方式Detailed ways

为使本发明实施例的目的、技术方案和优点更加清楚明白,下面结合附图对本发明实施例做进一步详细说明。在此,本发明的示意性实施例及其说明用于解释本发明,但并不作为对本发明的限定。In order to make the purpose, technical solutions and advantages of the embodiments of the present invention more clear, the embodiments of the present invention will be further described in detail below in conjunction with the accompanying drawings. Here, the exemplary embodiments and descriptions of the present invention are used to explain the present invention, but not to limit the present invention.

现有的技术测量超低渗透率主要存在的问题是测量时间长、精度低、稳定性不好,因此更难测量超低渗岩心的渗透率应力敏感性。为了克服以上困难,本发明提供了一种测量超低渗岩石渗透率应力敏感性的互相关技术。如图1所示,该方法包括下列步骤:The main problems of existing technologies for measuring ultra-low permeability are long measurement time, low precision, and poor stability. Therefore, it is more difficult to measure the permeability stress sensitivity of ultra-low permeability cores. In order to overcome the above difficulties, the present invention provides a cross-correlation technique for measuring the stress sensitivity of ultra-low permeability rock permeability. As shown in Figure 1, the method includes the following steps:

步骤S101:选取页岩或致密砂岩等超低渗岩心,将其加工成圆柱体试件;Step S101: select ultra-low permeability cores such as shale or tight sandstone, and process them into cylindrical specimens;

步骤S102:加工一个圆柱体钢块标准试件,用于系统标定;Step S102: Process a cylindrical steel block standard test piece for system calibration;

步骤S103:采用周期振荡法进行超低渗透率的测量,孔隙介质可采用气体或水。首先将钢块试件放于岩心夹持器中,夹持器由两个伺服压力泵通过阀门分别给岩心施加围压、正弦孔隙压力波。钢块测量结果用于标定系统;Step S103: The periodical oscillation method is used to measure the ultra-low permeability, and the porous medium can be gas or water. First, the steel block specimen is placed in the core holder, and the holder uses two servo pressure pumps to respectively apply confining pressure and sinusoidal pore pressure wave to the core through the valve. The steel block measurement results are used to calibrate the system;

步骤S104:将岩心放于夹持器中,施加围压、孔隙压,对岩心进行水饱和或气饱和。岩心饱和后,施加上游正弦压力波,测量下游正弦压力波响应。保持上游正弦压力波不变,变围压,测量不同围压的下游压力波的响应;Step S104: Put the core in the holder, apply confining pressure and pore pressure, and saturate the core with water or gas. After the core is saturated, an upstream sinusoidal pressure wave is applied and the downstream sinusoidal pressure wave response is measured. Keep the upstream sinusoidal pressure wave unchanged, change the confining pressure, and measure the response of the downstream pressure wave with different confining pressure;

步骤S105:将波形互相关方法用于渗透率变化测量,对不同围压下渗透率测量的压力波形进行互相关分析,获得渗透率随围压的变化,评价超低渗透岩石渗透率的应力敏感性。Step S105: Apply the waveform cross-correlation method to the measurement of permeability change, perform cross-correlation analysis on the pressure waveforms of permeability measurements under different confining pressures, obtain the change of permeability with confining pressure, and evaluate the stress sensitivity of ultra-low permeability rock permeability sex.

由上所述,对于超低渗的非常规储层,通过该仪器设备可以对系统的比储流率进行标定和校正,从而大幅度提高渗透率的测量精度。结合超低渗透岩石渗透率测量的周期振荡法,将波形互相关方法用于渗透率变化测量,对渗透率测量的压力波形进行互相关分析,可以获得渗透率随围压的变化,评价超低渗透岩石渗透率的应力敏感性。As mentioned above, for unconventional reservoirs with ultra-low permeability, the specific storage flow rate of the system can be calibrated and corrected through this instrument and equipment, thereby greatly improving the measurement accuracy of permeability. Combined with the periodic oscillation method of ultra-low permeability rock permeability measurement, the waveform cross-correlation method is used to measure the permeability change, and the cross-correlation analysis of the pressure waveform of the permeability measurement can obtain the change of the permeability with the confining pressure, and evaluate the ultra-low permeability. Stress Sensitivity of Permeable Rock Permeability.

在实验室中对于超低渗岩心,尤其是对于渗透率低于0.1×10-3μm2的岩心样品,渗透率测量耗时长,对压机的压力泵以及孔隙压力泵等仪器提出了较高的要求,需要仪器的精度高,稳定性好,可以保持某一应力状态长达数日至数月以测量某一应力状态下的渗透率值。另外,由于非常规储层的渗透率极低,输运孔隙流体的管道的比储流率对渗透率测量结果的影响就变得很大,为了克服不足,采用了管道变内径输运孔隙流体,在夹持器中的管道内径约为0.7mm,出夹持器以后通过阀门将管道连接到内径为3mm的大管道。如图2所示,1为岩心室,2、3分别为孔隙压伺服泵和围压控制泵,给岩心施加孔隙压和围压。4、5、6分别为上游孔隙压传感器、下游孔隙压传感器、围压传感器。采用周期振荡法测试岩心渗透率时,在岩心上游施加一个正弦孔隙压力波,观测岩心下游孔隙压力的响应。7为控制阀门,8为输运孔隙流体的内径为0.7mm的管道,9是输运孔隙流体的内径为3mm的管道。所测试的岩心加工成直径为2.5cm,高度为3-4cm的标准圆柱体,放置于岩心室1处。实验设备能进行变围压测量。为了解决岩心夹持器比储流率对超低渗透率精度的影响,加工了一个与岩心同尺度的圆柱体钢块试件。钢块的孔隙度和渗透率理论上为零。将钢块试件放于夹持器中,分别给钢块施加围压、孔隙压,在钢块上游施加一个正弦孔隙压力波,测量下游压力波响应,该测量结果用于对岩心渗透率测量结果进行标定。For ultra-low permeability cores in the laboratory, especially for core samples with a permeability lower than 0.1×10 -3 μm 2 , the measurement of permeability takes a long time, and the pressure pump of the press and the pore pressure pump and other instruments have higher requirements. The requirement of the instrument requires high precision and good stability, and it can maintain a certain stress state for several days to several months to measure the permeability value under a certain stress state. In addition, due to the extremely low permeability of unconventional reservoirs, the specific storage flow rate of the pipeline transporting pore fluids has a great influence on the measurement results of permeability. , the inner diameter of the pipe in the holder is about 0.7mm, and the pipe is connected to a large pipe with an inner diameter of 3mm through a valve after exiting the holder. As shown in Figure 2, 1 is the core chamber, 2 and 3 are the pore pressure servo pump and the confining pressure control pump respectively, which apply pore pressure and confining pressure to the core. 4, 5, and 6 are the upstream pore pressure sensor, the downstream pore pressure sensor, and the confining pressure sensor respectively. When the periodic oscillation method is used to test the permeability of the core, a sinusoidal pore pressure wave is applied upstream of the core, and the response of the pore pressure downstream of the core is observed. 7 is a control valve, 8 is a pipeline with an inner diameter of 0.7 mm for transporting pore fluid, and 9 is a pipeline with an inner diameter of 3 mm for transporting pore fluid. The tested rock core is processed into a standard cylinder with a diameter of 2.5 cm and a height of 3-4 cm, and placed in the core chamber 1. The experimental equipment can measure the variable confining pressure. In order to solve the influence of the specific storage rate of the core holder on the accuracy of ultra-low permeability, a cylindrical steel block specimen with the same scale as the core was processed. The porosity and permeability of steel blocks are theoretically zero. Put the steel block specimen in the holder, respectively apply confining pressure and pore pressure to the steel block, apply a sinusoidal pore pressure wave to the upstream of the steel block, and measure the downstream pressure wave response. The measurement results are used to measure the core permeability. The results are calibrated.

为了测量渗透率的相对变化,采用互相关技术对周期振荡法的波形数据进行分析。该技术原理为:两列波形的互相关可高精度地获得波形相位差异,属于波形干涉测量,在信号检测领域获得广泛应用。互相关函数定义为:To measure the relative change in permeability, the waveform data from the periodic oscillation method were analyzed using cross-correlation techniques. The principle of this technology is: the cross-correlation of two columns of waveforms can obtain the waveform phase difference with high precision, which belongs to waveform interferometry and has been widely used in the field of signal detection. The cross-correlation function is defined as:

RR (( tt ,, tt ww )) (( tt SS )) &equiv;&equiv; &Integral;&Integral; tt -- tt ww tt ++ tt ww uu unpunp (( tt &prime;&prime; )) uu perper (( tt &prime;&prime; ++ tt sthe s )) dd tt &prime;&prime; (( &Integral;&Integral; tt -- tt ww tt ++ tt ww uu unpunp 22 (( tt &prime;&prime; )) dd tt &prime;&prime; &Integral;&Integral; tt -- tt ww tt ++ tt ww uu perper 22 (( tt &prime;&prime; )) dd tt &prime;&prime; )) 11 22

式中,时间窗长度为2tw,t为窗的中心位置。ts是互相关中用到的移动时间,uunp代表参考波场,uper表示不同围压下的波场。互相关函数的最大值(Rmax)代表了两列波的相似程度,对应于Rmax的时间延迟(δt)代表了不同相位的变化。In the formula, the length of the time window is 2t w , and t is the center position of the window. t s is the moving time used in cross-correlation, uunp represents the reference wave field, and uper represents the wave field under different confining pressures. The maximum value (R max ) of the cross-correlation function represents the similarity of two waves, and the time delay (δ t ) corresponding to R max represents the change of different phases.

本发明结合超低渗透岩石渗透率测量的周期振荡法,将波形互相关技术用于渗透率变化测量。利用互相关技术,比较两列相似波列的相位差以获得渗透率变化的高精度测量。周期振荡法渗透率变化测量的互相关技术是利用下游波形的互相关获得不同应力状态下的相位差。如图3所示,1为岩心上游孔隙压力波,不论围压怎么变化,始终保持上游压力波形相同,具备相同的振幅、频率。2为岩心,具有超低渗透性。3是不同围压下岩心下游孔隙压力响应波形。由于上游孔隙压力波具有相同的振幅、频率,因此可以通过对下游孔隙压力波的互相关获得不同围压条件下的振幅比及相位差。图3中4为不同围压条件下,下游孔隙压力波的相位差,5是不同围压条件下,下游孔隙压力波的振幅比。由不同围压条件下,下游孔隙压力波形的振幅比及相位差获得渗透率随围压的变化,评价超低渗透岩石渗透率的应力敏感性。The invention combines the periodic oscillation method of ultra-low permeability rock permeability measurement, and uses waveform cross-correlation technology for permeability change measurement. Using cross-correlation techniques, the phase differences of two similar wave trains are compared to obtain high-precision measurements of permeability changes. The cross-correlation technique of the periodic oscillation method for permeability change measurement is to use the cross-correlation of downstream waveforms to obtain the phase difference under different stress states. As shown in Fig. 3, 1 is the upstream pore pressure wave of the core, no matter how the confining pressure changes, the upstream pressure waveform always remains the same, with the same amplitude and frequency. 2 is a core with ultra-low permeability. 3 is the response waveform of the downstream pore pressure of the core under different confining pressures. Since the upstream pore pressure waves have the same amplitude and frequency, the amplitude ratio and phase difference under different confining pressure conditions can be obtained by cross-correlating the downstream pore pressure waves. In Fig. 3, 4 is the phase difference of downstream pore pressure waves under different confining pressure conditions, and 5 is the amplitude ratio of downstream pore pressure waves under different confining pressure conditions. The variation of permeability with confining pressure is obtained from the amplitude ratio and phase difference of downstream pore pressure waveforms under different confining pressure conditions, and the stress sensitivity of ultra-low permeability rock permeability is evaluated.

以上所述的具体实施例,对本发明的目的、技术方案和有益效果进行了进一步详细说明,所应理解的是,以上所述仅为本发明的具体实施例而已,并不用于限定本发明的保护范围,凡在本发明的精神和原则之内,所做的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The specific embodiments described above have further described the purpose, technical solutions and beneficial effects of the present invention in detail. It should be understood that the above descriptions are only specific embodiments of the present invention and are not intended to limit the scope of the present invention. Protection scope, within the spirit and principles of the present invention, any modification, equivalent replacement, improvement, etc., shall be included in the protection scope of the present invention.

Claims (10)

1.一种测量超低渗岩石渗透率应力敏感性的互相关技术.其特征在于将波形互相关方法用于渗透率变化测量,大幅度提高渗透率变化测量的精度和稳定性,解决超低渗透岩石渗透率应力敏感性测量难题。该方法原理为:两列波形的互相关可高精度地获得波形相位差异,属于波形干涉测量,在信号检测领域获得广泛应用。本发明结合超低渗透岩石渗透率测量的周期振荡法,将波形互相关方法用于渗透率变化测量,对渗透率测量的压力波形进行互相关分析,获得渗透率随围压的变化,评价超低渗透岩石渗透率的应力敏感性。1. A cross-correlation technology for measuring the stress sensitivity of ultra-low permeability rock permeability. It is characterized in that the waveform cross-correlation method is used for the measurement of permeability change, which greatly improves the accuracy and stability of permeability change measurement, and solves the problem of ultra-low permeability. Difficulties in measuring the stress sensitivity of permeability rock permeability. The principle of the method is: the cross-correlation of two columns of waveforms can obtain the waveform phase difference with high precision, which belongs to waveform interferometry and is widely used in the field of signal detection. The present invention combines the periodic oscillation method of ultra-low permeability rock permeability measurement, uses the waveform cross-correlation method for the permeability change measurement, and performs cross-correlation analysis on the pressure waveform of the permeability measurement to obtain the change of the permeability with the confining pressure, and evaluate the ultra-low permeability. Stress Sensitivity of Low Permeability Rock Permeability. 该技术包括下列步骤:The technique includes the following steps: a)选取页岩或致密砂岩等超低渗岩心,将其加工成圆柱体试件;a) select ultra-low permeability cores such as shale or tight sandstone, and process them into cylindrical specimens; b)加工一个圆柱体钢块标准试件,用于系统标定;b) Process a cylindrical steel block standard test piece for system calibration; c)采用周期振荡法进行超低渗透率的测量,孔隙介质可采用气体或水。首先将钢块试件放于岩心夹持器中,夹持器由两个伺服压力泵通过阀门分别给岩心施加围压、正弦孔隙压力波。钢块测量结果用于标定系统;c) The periodical oscillation method is used to measure the ultra-low permeability, and the porous medium can be gas or water. First, the steel block specimen is placed in the core holder, and the holder uses two servo pressure pumps to respectively apply confining pressure and sinusoidal pore pressure wave to the core through the valve. The steel block measurement results are used to calibrate the system; d)将岩心放于夹持器中,施加围压、孔隙压,对岩心进行水饱和或气饱和。岩心饱和后,施加上游正弦压力波,测量下游正弦压力波响应。保持上游正弦压力波不变,变围压,测量不同围压的下游压力波的响应;d) Put the core in the holder, apply confining pressure and pore pressure, and saturate the core with water or gas. After the core is saturated, an upstream sinusoidal pressure wave is applied and the downstream sinusoidal pressure wave response is measured. Keep the upstream sinusoidal pressure wave unchanged, change the confining pressure, and measure the response of the downstream pressure wave with different confining pressure; e)将波形互相关方法用于渗透率变化测量,对不同围压下渗透率测量的压力波形进行互相关分析,获得渗透率随围压的变化,评价超低渗透岩石渗透率的应力敏感性。e) Apply the waveform cross-correlation method to the measurement of permeability change, conduct cross-correlation analysis on the pressure waveforms of permeability measurements under different confining pressures, obtain the change of permeability with confining pressure, and evaluate the stress sensitivity of ultra-low permeability rock permeability . 2.如权利要求1所述的测量超低渗岩石渗透率应力敏感性的互相关技术,其特征在于,在步骤a)中,选取的页岩、致密砂岩等岩心取自所开发储层的全直径岩心或相同层位的露头,具有超低渗透率,将所述岩心加工成直径为2.5cm,高度为3-4cm的标准圆柱体。2. the cross-correlation technique of measuring ultra-low permeability rock permeability stress sensitivity as claimed in claim 1, is characterized in that, in step a), the rock cores such as selected shale, tight sandstone are taken from the developed reservoir Full-diameter cores or outcrops of the same horizon, with ultra-low permeability, are machined into standard cylinders with a diameter of 2.5 cm and a height of 3-4 cm. 3.如权利要求1所述的测量超低渗岩石渗透率应力敏感性的互相关技术,其特征在于,在步骤b)中,加工一个与岩心同尺度的圆柱体钢块试件,钢块的孔隙度和渗透率理论上为零。3. the cross-correlation technique of measuring ultra-low permeability rock permeability stress sensitivity as claimed in claim 1, is characterized in that, in step b), process a cylindrical steel block specimen with the same scale as rock core, steel block The porosity and permeability are theoretically zero. 4.如权利要求1所述的测量超低渗岩石渗透率应力敏感性的互相关技术,其特征在于,在步骤c)中,将钢块试件放于夹持器中,分别给钢块试件施加围压、孔隙压,并在钢块试件上游施加正弦孔隙压力波,测量下游孔隙压力波响应,该测量结果用于对系统比储流率等值进行标定。4. the cross-correlation technique of measuring ultra-low permeability rock permeability stress sensitivity as claimed in claim 1, is characterized in that, in step c), steel block specimen is placed in the holder, respectively gives steel block Confining pressure and pore pressure are applied to the specimen, and a sinusoidal pore pressure wave is applied upstream of the steel block specimen, and the response of the downstream pore pressure wave is measured. The measurement results are used to calibrate the equivalent value of the system specific storage flow rate. 5.如权利要求1所述的测量超低渗岩石渗透率应力敏感性的互相关技术,其特征在于,在步骤c)中,夹持器中输运上、下游孔隙介质的两根管道内径很小,约为0.7mm,以减少比储流率对超低渗岩心渗透率测试的影响。5. the cross-correlation technique of measuring ultra-low permeability rock permeability stress sensitivity as claimed in claim 1, is characterized in that, in step c), in the holder, the two pipe inner diameters of transporting upper and lower pore media It is very small, about 0.7mm, to reduce the influence of the specific storage rate on the ultra-low permeability core permeability test. 6.如权利要求1所述的测量超低渗岩石渗透率应力敏感性的互相关技术,其特征在于,在步骤d)中,采用周期振荡法进行页岩、致密砂岩等超低渗岩心渗透率的测量,施加围压、孔隙压对岩心进行饱和后,施加上游正弦压力波,测量下游正弦压力波响应,保持上游正弦压力波不变,变围压,测量不同围压的下游压力波的响应。6. the cross-correlation technique of measuring ultra-low permeability rock permeability stress sensitivity as claimed in claim 1, is characterized in that, in step d), adopts periodic oscillation method to carry out ultra-low permeability rock cores such as shale, tight sandstone infiltration Rate measurement, apply confining pressure and pore pressure to saturate the core, apply upstream sinusoidal pressure wave, measure downstream sinusoidal pressure wave response, keep upstream sinusoidal pressure wave unchanged, change confining pressure, measure downstream pressure wave of different confining pressure response. 7.如权利要求1所述的测量超低渗岩石渗透率应力敏感性的互相关技术,其特征在于,在步骤e)中,在周期振荡法数据处理中采用互相关技术,选择某一围压的下游孔隙压力波为参考压力波形,通过不同围压下下游压力波与参考压力波的互相关处理,获得相对的压力波形幅值比及相位差。7. the cross-correlation technology of measuring ultra-low permeability rock permeability stress sensitivity as claimed in claim 1, is characterized in that, in step e), adopts cross-correlation technology in period oscillation method data processing, selects a certain range The downstream pore pressure wave under different confining pressures is the reference pressure waveform, and the relative pressure waveform amplitude ratio and phase difference are obtained through cross-correlation processing between the downstream pressure wave and the reference pressure wave under different confining pressures. 8.如权利要求5所述的测量超低渗岩石渗透率应力敏感性的互相关技术,其特征在于,在夹持器中输运孔隙流体的管道内径非常小,约为0.7mm,出夹持器以后通过阀门将管道连接到内径3mm的大管道。8. The cross-correlation technique for measuring the stress sensitivity of ultra-low permeability rock permeability as claimed in claim 5, characterized in that, the internal diameter of the pipe transporting pore fluid in the holder is very small, about 0.7mm, The holder is then connected to a large pipe with an inner diameter of 3 mm through a valve. 9.如权利要求6所述的测量超低渗岩石渗透率应力敏感性的互相关技术,其特征在于,保持上游孔隙压力波形不变,即保持上游孔隙压力波形相同的振幅及频率。9. The cross-correlation technique for measuring the stress sensitivity of ultra-low permeability rock permeability as claimed in claim 6, wherein the upstream pore pressure waveform is kept constant, that is, the same amplitude and frequency of the upstream pore pressure waveform are kept. 10.如权利要求7所述的测量超低渗岩石渗透率应力敏感性的互相关技术,其特征在于,选择某一围压条件下的下游压力波为参考波形,选择某一围压条件下的渗透率为参考渗透率。10. the cross-correlation technique of measuring ultra-low permeability rock permeability stress sensitivity as claimed in claim 7, is characterized in that, selects the downstream pressure wave under a certain confining pressure condition as reference waveform, selects under a certain confining pressure condition The permeability is the reference permeability.
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CN110470581A (en) * 2019-08-02 2019-11-19 中国石油大学(北京) Determine the method, apparatus and storage medium of reservoir stress sensitive degree
CN111024585A (en) * 2019-12-31 2020-04-17 国家地质实验测试中心 Metal standard for low or ultra-low permeability test
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CN111141654A (en) * 2019-12-31 2020-05-12 国家地质实验测试中心 Preparation method of metal standard substance
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