CN103364176A - Testing system for laser induced damage threshold - Google Patents
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Abstract
本发明提供一种激光损伤阈值测试系统,包括高能激光损伤装置、高分辨率彩色CCD图像损伤判别装置、CCD辅助光源装置和样品台运动控制装置。该测试系统对经高能激光辐照后的待测样品,先后交替采用分别配有低倍和高倍率物镜光学系统的CCD采集单元进行初步快速损伤预判断和精确测量。采用本发明,不仅可有效地克服现有相衬显微法测量主观性强、测量误差大、测量时间长等缺点,而且还可同时满足1-on-1和R-on-1两种测量模式,既兼顾测量误差和测试效率、适用性强,又便于工业化应用。
The invention provides a laser damage threshold testing system, which includes a high-energy laser damage device, a high-resolution color CCD image damage judgment device, a CCD auxiliary light source device and a sample stage motion control device. The test system alternately uses CCD acquisition units equipped with low-magnification and high-magnification objective lens optical systems for preliminary rapid damage prediction and accurate measurement of the samples to be tested after high-energy laser irradiation. Adopting the present invention can not only effectively overcome the disadvantages of the existing phase contrast microscopy method, such as strong subjectivity, large measurement errors, and long measurement time, but also satisfy both 1-on-1 and R-on-1 measurements The mode not only takes into account the measurement error and test efficiency, but also has strong applicability and is convenient for industrial application.
Description
技术领域technical field
本发明涉及激光测试技术,尤其涉及一种采用相衬显微法的激光损伤阈值测试系统。The invention relates to laser testing technology, in particular to a laser damage threshold testing system using phase contrast microscopy.
背景技术Background technique
随着高功率激光器应用范围的不断扩大,光学薄膜或光学元件抗激光损伤性能的重要性日益突出,因此,激光损伤阈值已成为光学薄膜或光学元件不可缺少的一项性能指标。若要实现高性能、高激光损伤阈值的薄膜制备和探索研究,其关键还是在于准确测出光学元件或薄膜的激光损伤阈值。所以,在激光损伤阈值测试过程中,如何实现在线、实时、快速、准确地激光阈值损伤判别,以及在此基础上研制兼有激光阈值自动检测和数据信息处理功能的激光阈值智能化测试系统已成为研究的核心一环。With the continuous expansion of the application range of high-power lasers, the importance of the anti-laser damage performance of optical films or optical components has become increasingly prominent. Therefore, the laser damage threshold has become an indispensable performance index of optical films or optical components. To achieve high-performance, high laser damage threshold film preparation and research, the key is to accurately measure the laser damage threshold of optical components or films. Therefore, in the process of laser damage threshold testing, how to realize online, real-time, fast and accurate laser threshold damage discrimination, and on this basis, develop an intelligent laser threshold testing system with functions of automatic detection of laser threshold and data information processing. become a central part of the research.
近年来,国际标准化委员会颁布了ISO11254-1和ISO11254-2,这是对激光引起光学元件损伤而制定的国际标准。其所推荐的检测方法是相衬显微法,该检测方法采用放大倍率为100~150倍的显微镜对激光辐照后的光学元件或光学薄膜表面进行观察,以判别薄膜是否发生损伤。但是,该检测方法需要采用人工操作方式进行,存在明显的不足,主要表现在:In recent years, the International Standardization Committee has promulgated ISO11254-1 and ISO11254-2, which are international standards for damage to optical components caused by laser light. The recommended detection method is phase contrast microscopy, which uses a microscope with a magnification of 100 to 150 times to observe the surface of the optical element or optical film after laser irradiation to determine whether the film is damaged. However, this detection method needs to be carried out manually, and there are obvious deficiencies, which are mainly manifested in:
一、采用人工方式直接观察被测元件表面,主观性很强,且分辨率不高。此外,由于放大倍率较高,且测试点繁多,工作强度大;1. Using manual methods to directly observe the surface of the tested component is very subjective and the resolution is not high. In addition, due to the high magnification and the large number of test points, the work intensity is high;
二、需要人工控制待测样品在夹持台和测试台之间移动,不仅会引起较大的系统测量误差,而且需要有较洁净的实验环境以避免样品污损所引起的测量误差;2. It is necessary to manually control the movement of the sample to be tested between the clamping table and the test table, which will not only cause large system measurement errors, but also require a cleaner experimental environment to avoid measurement errors caused by sample contamination;
三、手工方式的检测方法效率低下,尤其是多点测试过程中,要实现各个测量点的聚焦定位和测量,要求测试人员必须具备娴熟的相衬显微镜方面的使用技能,因而测量过程耗时过长且无法实现整机的自动化。3. The manual detection method is inefficient, especially in the process of multi-point testing. In order to realize the focus positioning and measurement of each measurement point, the tester must have the skill of using the phase contrast microscope, so the measurement process is time-consuming. Long and unable to realize the automation of the complete machine.
是故,现有的激光损伤测试方法造成了极大的测量误差,很难保证光学元件或光学薄膜的损伤阈值高精度测量。有鉴于此,如何设计一种智能化的激光损伤阈值测试系统,以便有效克服现有测量方法的误差较大、测量过程耗时过长的缺陷,是相关技术人员亟待解决的一项课题。Therefore, the existing laser damage testing methods have caused huge measurement errors, and it is difficult to ensure high-precision measurement of the damage threshold of optical components or optical films. In view of this, how to design an intelligent laser damage threshold testing system to effectively overcome the defects of large errors in existing measurement methods and long time-consuming measurement processes is an urgent task for relevant technical personnel to solve.
发明内容Contents of the invention
针对现有技术中的激光损伤阈值测试方法所存在的上述缺陷,本发明提供了一种新颖的激光损伤阈值测试系统。Aiming at the above defects in the laser damage threshold testing method in the prior art, the present invention provides a novel laser damage threshold testing system.
依据本发明的一个方面,提供了一种激光损伤阈值测试系统,其中,该激光损伤阈值测试系统包括:According to one aspect of the present invention, a laser damage threshold testing system is provided, wherein the laser damage threshold testing system includes:
高能激光损伤装置,包括激光器、衰减器、聚焦透镜、分束器和高反镜,其中,所述激光器发出的激光依次经由所述衰减器、所述聚焦透镜、所述分束器和所述高反镜会聚在待测样品的表面,所述激光器发出高能量的、波长为1064nm、脉冲宽度为12ns的激光束,所述衰减器对发出的激光能量进行调整,使调整后的激光能量在2~200mJ范围内线性变化,所述聚焦透镜对调整后的激光束进行聚焦处理,所述分束器按100∶1的比例将小能量的激光导入激光测试分析单元进行能量光束分析;A high-energy laser damage device includes a laser, an attenuator, a focusing lens, a beam splitter, and a high reflection mirror, wherein the laser light emitted by the laser passes through the attenuator, the focusing lens, the beam splitter, and the The high reflection mirror converges on the surface of the sample to be tested. The laser emits a high-energy laser beam with a wavelength of 1064nm and a pulse width of 12ns. The attenuator adjusts the emitted laser energy so that the adjusted laser energy is Change linearly in the range of 2-200mJ, the focusing lens performs focusing processing on the adjusted laser beam, and the beam splitter guides the laser light with small energy into the laser test and analysis unit for energy beam analysis according to the ratio of 100:1;
高分辨率彩色CCD图像损伤判别装置,包括第一驱动步进电机、Z向运动机构、配有第一倍率物镜光学系统的CCD采集单元以及配有第二倍率物镜光学系统的CCD采集单元、CCD旋转夹持台,所述第二倍率高于所述第一倍率,其中,所述配有第一倍率物镜光学系统的CCD采集单元对来自高能激光损伤装置的激光辐照后的待测样品表面上的辐照点进行快速预判,筛选得到损伤测试点,然后通过配有第二倍率物镜光学系统的CCD采集单元对筛选后的未损伤测试点进行复检判断,所述CCD旋转夹持台用于实现配有第一倍率物镜光学系统的CCD采集单元以及配有第二倍率物镜光学系统的CCD采集单元在相同测试位置的旋转,所述Z向运动机构在所述第一驱动步进电机的作用下调整上述两个CCD采集单元的光路自动调焦;A high-resolution color CCD image damage discrimination device, including a first drive stepper motor, a Z-direction movement mechanism, a CCD acquisition unit equipped with a first magnification objective lens optical system, a CCD acquisition unit equipped with a second magnification objective lens optical system, and a CCD Rotate the clamping table, the second magnification is higher than the first magnification, wherein the CCD acquisition unit equipped with the first magnification objective lens optical system is used for the surface of the sample to be tested after being irradiated by the laser light from the high-energy laser damage device Rapid pre-judgment of the irradiated points on the screen to obtain the damaged test points, and then re-inspect and judge the screened undamaged test points through the CCD acquisition unit equipped with the second magnification objective lens optical system. The CCD rotating clamping table Used to realize the rotation of the CCD acquisition unit equipped with the first magnification objective lens optical system and the CCD acquisition unit equipped with the second magnification objective lens optical system at the same test position, the Z-direction motion mechanism drives the stepping motor at the first Under the effect of adjusting the optical path automatic focusing of the above two CCD acquisition units;
CCD辅助光源装置,包括角度可调光源夹持台和CCD辅助光源,所述角度可调光源夹持台用以控制所述CCD辅助光源的焦距;以及The CCD auxiliary light source device includes an angle-adjustable light source holder and a CCD auxiliary light source, and the angle-adjustable light source holder is used to control the focal length of the CCD auxiliary light source; and
样品台运动控制装置,包括第二驱动步进电机、样品工装台和XY方向二维平移台,所述第二驱动步进电机使所述XY方向二维平移台工作从而自动调整待测样品的工位,所述样品工装台用以放置所述待测样品。The sample stage motion control device includes a second drive stepper motor, a sample tooling table and a two-dimensional translation platform in the XY direction, and the second drive stepper motor makes the two-dimensional translation platform in the XY direction work so as to automatically adjust the position of the sample to be tested. Work station, the sample tooling platform is used to place the sample to be tested.
优选地,激光损伤阈值测试系统采用1-on-1模式对所述待测样品进行测试,首先通过所述配有第一倍率物镜光学系统的CCD采集单元记录i×j个测试点辐照前的初始图像,然后以给定的步长按照i个能级逐一在每个能级下对j个测试点进行激光辐照,并利用所述配有第一倍率物镜光学系统的CCD采集单元再次采集所述待测样品表面的i×j个测试点辐照后的图像,对比辐照前后的测试点图像从而筛选得到损伤测试点,最后通过所述配有第二倍率物镜光学系统的CCD采集单元对筛选后的未损伤测试点进行复检判断,其中,i、j为自然数。Preferably, the laser damage threshold test system adopts 1-on-1 mode to test the sample to be tested, and first records i×j test points before irradiation through the CCD acquisition unit equipped with the first magnification objective lens optical system The initial image of the first magnification objective lens optical system is used to irradiate j test points with laser light at each energy level one by one according to i energy levels at a given step size, and the CCD acquisition unit equipped with the first magnification objective lens optical system is used again Collect the irradiated images of i×j test points on the surface of the sample to be tested, compare the images of the test points before and after irradiation to obtain the damage test points, and finally collect them through the CCD equipped with the second magnification objective lens optical system The unit performs re-inspection and judgment on the screened undamaged test points, where i and j are natural numbers.
优选地,该激光损伤阈值测试系统采用R-on-1模式对所述待测样品进行测试,首先设定恒定的激光输出能量,使激光束以相同的时间间隔对待测样品表面的第一测试点进行多次辐照,然后通过所述配有第一倍率物镜光学系统的CCD采集单元对每次辐照后的所述第一测试点进行实时图像采集,并与未辐照时所采集图像进行比对,按预设判别标准认定损伤时即停止辐照并统计出辐照次数N,然后更换至所述待测样品表面的第二测试点,激光束以相同参数对所述第二测试点进行(N-1)次辐照,然后通过所述配有第二倍率物镜光学系统的CCD采集单元对所述第二测试点的表面进行观察,若无激光损伤则可判定损伤次数为N,若存在损伤则再次更换第三测试点,并经递减激光辐照次数后再通过所述配有第二倍率物镜光学系统的CCD采集单元对所述第三测试点表面进行观察,以此递减辐照次数n次后直至无激光损伤现象为止,记录该激光能量下导致损伤的次数为(N-n)次,其中,N、n为自然数。Preferably, the laser damage threshold testing system uses the R-on-1 mode to test the sample to be tested, and first sets a constant laser output energy so that the laser beam performs the first test on the surface of the sample to be tested at the same time interval Points are irradiated multiple times, and then the CCD acquisition unit equipped with the first magnification objective lens optical system is used for real-time image acquisition of the first test point after each irradiation, and compared with the image collected when not irradiated For comparison, when the damage is determined according to the preset judgment standard, the irradiation is stopped and the number of irradiations N is counted, and then replaced to the second test point on the surface of the sample to be tested, and the laser beam uses the same parameters for the second test point. Points are irradiated for (N-1) times, and then the surface of the second test point is observed through the CCD acquisition unit equipped with the second magnification objective lens optical system. If there is no laser damage, it can be determined that the number of damages is N , if there is damage, replace the third test point again, and observe the surface of the third test point through the CCD acquisition unit equipped with the second magnification objective lens optical system after decreasing the number of laser irradiation times, so as to decrease After n times of irradiation until there is no laser damage phenomenon, the number of damages caused by the laser energy is recorded as (N-n) times, where N and n are natural numbers.
优选地,该激光束的光斑直径介于0.6mm~1mm之间。Preferably, the spot diameter of the laser beam is between 0.6 mm and 1 mm.
优选地,待测样品的激光损伤阈值由所述激光测试分析单元进行能量光束分析所得到的输出激光能量、激光束光斑大小决定。Preferably, the laser damage threshold of the sample to be tested is determined by the output laser energy and the spot size of the laser beam obtained from the energy beam analysis performed by the laser test and analysis unit.
优选地,该激光损伤阈值测试系统还包括气流式表面清洁装置,包括清洗喷嘴、电磁阀、干燥过滤器、气阀和气源,其中,所述气源为氮气,打开气阀后,氮气进入所述干燥过滤器予以除湿,然后经过所述电磁阀来调节气压和流量,并利用所述清洗喷嘴射向所述待测样品的表面辐照点。Preferably, the laser damage threshold testing system also includes an airflow surface cleaning device, including a cleaning nozzle, a solenoid valve, a dry filter, an air valve and an air source, wherein the air source is nitrogen, and nitrogen enters the air after the air valve is opened. The drying filter is dehumidified, and then the air pressure and flow are adjusted through the solenoid valve, and the cleaning nozzle is used to irradiate the surface irradiation point of the sample to be tested.
优选地,该待测样品为光学元件、介质薄膜、金属薄膜或者半导体薄膜。Preferably, the sample to be tested is an optical element, a dielectric film, a metal film or a semiconductor film.
采用本发明的激光损伤阈值测试系统,不仅可有效地克服现有相衬显微法测量主观性强、测量误差大、测量时间长等缺点,而且还可同时满足1-on-1和R-on-1两种测量模式。具体地,该激光损伤阈值测试系统至少具有下列优点:Adopting the laser damage threshold testing system of the present invention can not only effectively overcome the disadvantages of strong subjectivity, large measurement error and long measurement time of the existing phase contrast microscopy method, but also satisfy the 1-on-1 and R- On-1 two measurement modes. Specifically, the laser damage threshold testing system has at least the following advantages:
1.兼顾测量误差和测试效率。本发明以相衬显微法为基础,在满足国际标准的前提下,有效地克服了手工测试过程中随机误差大、测试效率低的缺点。相比之下,现有技术采用单一CCD图像采集系统激光损伤测试方法,受限于高倍率CCD图像传感器物镜系统的调焦尺寸限制,只能通过牺牲物镜光学系统的放大倍率来提高测试效率,从而造成测试结果数值偏大。此外,本发明通过引入气流式自动清洁系统,对激光辐照后的样品表面进行清洗,可防止因损伤而产生的光学薄膜或元件材料粉末所引起的测量误差,进一步提高了测量的准确性。1. Taking into account the measurement error and test efficiency. Based on the phase-contrast microscopy method, the invention effectively overcomes the shortcomings of large random errors and low testing efficiency in the manual testing process under the premise of meeting international standards. In contrast, the existing technology uses a single CCD image acquisition system laser damage test method, which is limited by the focusing size of the high-magnification CCD image sensor objective system, and can only improve the test efficiency by sacrificing the magnification of the objective optical system. As a result, the value of the test result is too large. In addition, the present invention introduces an air-flow automatic cleaning system to clean the surface of the sample after laser irradiation, which can prevent measurement errors caused by optical films or component material powders caused by damage, and further improve measurement accuracy.
2.适用性强。本发明可同时实现1-on-1和R-on-1两种模式的激光损伤阈值测式方法,并且采用高分辨率的彩色CCD和与之匹配的图形采集系统可以直观地对经激光辐照后的光学薄膜或光学元件损伤形貌进行观察,既可用于对材料的抗激光损伤性能测试,又可用于材料的激光损伤分析。此外,本发明的待测样品可为各类光学元件、各类介质薄膜、金属薄膜或半导体薄膜。2. Strong applicability. The present invention can realize the laser damage threshold measuring method of two modes of 1-on-1 and R-on-1 at the same time, and adopt the high-resolution color CCD and the graphic acquisition system matching it to be able to visually monitor the laser damage threshold Observing the damage morphology of the optical film or optical element after irradiation can be used not only for the test of the anti-laser damage performance of the material, but also for the analysis of the laser damage of the material. In addition, the samples to be tested in the present invention can be various optical elements, various dielectric films, metal films or semiconductor films.
3.便于工业化应用。本发明的测试系统均可实现程序化控制,自动化程度高,同时各功能模块都具备较高的技术成熟度,因此可方便实现仪器化,用于工业生产实际。3. It is convenient for industrial application. The test system of the present invention can realize programmed control, has a high degree of automation, and at the same time, each functional module has a high degree of technical maturity, so it can be conveniently implemented as an instrument and used in actual industrial production.
附图说明Description of drawings
读者在参照附图阅读了本发明的具体实施方式以后,将会更清楚地了解本发明的各个方面。其中,Readers will have a clearer understanding of various aspects of the present invention after reading the detailed description of the present invention with reference to the accompanying drawings. in,
图1示出本发明的激光损伤阈值测试系统的结构示意图。FIG. 1 shows a schematic structural diagram of a laser damage threshold testing system of the present invention.
1-Nd:YAG激光器,2-可控衰减器,3-分束器,4-聚焦透镜,5-45度高反镜,6-激光测试分析单元,7-中央处理单元,8-CCD夹持台步进驱动电机,9-Z向运动机构,10-低倍率CCD图像采集单元,11-角度可调光源夹持台,12-辅助光源,13-高倍率CCD图像采集单元,14-CCD旋转夹持台,15-样品台驱动步进电机,16-样品工装台,17-待测样品,18-XY方向二维平移台,19-清洗喷嘴,20-电磁阀,21-气体干燥过滤器,22-气阀,23-清洗气源1-Nd:YAG laser, 2-controllable attenuator, 3-beam splitter, 4-focus lens, 5-45 degree high mirror, 6-laser test and analysis unit, 7-central processing unit, 8-CCD clip Holding stage stepping drive motor, 9-Z motion mechanism, 10-low magnification CCD image acquisition unit, 11-angle adjustable light source clamping platform, 12-auxiliary light source, 13-high magnification CCD image acquisition unit, 14-CCD Rotary clamping stage, 15-sample stage driving stepper motor, 16-sample tooling stage, 17-sample to be tested, 18-two-dimensional translation stage in XY direction, 19-cleaning nozzle, 20-solenoid valve, 21-gas drying and filtration Device, 22-air valve, 23-cleaning air source
具体实施方式Detailed ways
为了使本申请所揭示的技术内容更加详尽与完备,可参照附图以及本发明的下述各种具体实施例,附图中相同的标记代表相同或相似的组件。然而,本领域的普通技术人员应当理解,下文中所提供的实施例并非用来限制本发明所涵盖的范围。此外,附图仅仅用于示意性地加以说明,并未依照其原尺寸进行绘制。In order to make the technical content disclosed in this application more detailed and complete, reference may be made to the drawings and the following various specific embodiments of the present invention, and the same symbols in the drawings represent the same or similar components. However, those skilled in the art should understand that the examples provided below are not intended to limit the scope of the present invention. In addition, the drawings are only for schematic illustration and are not drawn according to their original scale.
在具体介绍本发明的激光损伤阈值测试系统前,首先简要说明激光损伤阈值的两种测试方式,即,R-on-1方式和1-on-1方式。Before specifically introducing the laser damage threshold testing system of the present invention, two testing methods for laser damage threshold, ie, the R-on-1 method and the 1-on-1 method, are first briefly described.
R-on-1损伤测试方式——对于被测样品上的同一点,用递增的激光能量重复照射样品,直到产生损伤为止。测试时要求初始激光能量远小于样品的损伤阈值,记录下造成样品损伤的脉冲激光能量,即认为是该点的损伤阈值。然后测出同一样品上多个点的损伤阈值,求出平均值即为被测样品的损伤阈值。R-on-1 damage test method - for the same point on the sample to be tested, the sample is repeatedly irradiated with increasing laser energy until damage occurs. During the test, the initial laser energy is required to be much smaller than the damage threshold of the sample, and the pulse laser energy that causes sample damage is recorded, which is considered as the damage threshold of the point. Then the damage threshold of multiple points on the same sample is measured, and the average value is obtained as the damage threshold of the tested sample.
1-on-1损伤测试方式——也称为零几率损伤法。使用同一能量的单脉冲激光照射m个点,记录下损伤的次数n。则每个能量激光辐照损伤概率P等于n/m。改变激光能量,再测出改变后的该激光能量下的损伤概率,包括损伤几率为0和100%的能量点。以激光能量为横轴,损伤几率为纵轴,得出损伤几率与激光能量点的分布,再用直线拟合并外推到零损伤几率,所对应的激光能量值即为被测样品的损伤阈值。1-on-1 damage test method - also known as zero-probability damage method. Use a single pulse laser with the same energy to irradiate m points, and record the number of damage n. Then the damage probability P of each energy laser irradiation is equal to n/m. Change the laser energy, and then measure the damage probability under the changed laser energy, including the energy points where the damage probability is 0 and 100%. Taking the laser energy as the horizontal axis and the damage probability as the vertical axis, the distribution of the damage probability and the laser energy point is obtained, and then fitted with a straight line and extrapolated to zero damage probability, the corresponding laser energy value is the damage of the tested sample threshold.
本发明的激光损伤阈值测试系统主要包括高能激光损伤装置、高分辨率彩色CCD图像损伤判别装置、CCD辅助光源装置和样品台运动控制装置。The laser damage threshold testing system of the present invention mainly includes a high-energy laser damage device, a high-resolution color CCD image damage discrimination device, a CCD auxiliary light source device and a sample stage motion control device.
本发明的高能激光损伤装置包括Nd:YAG激光器1、可控衰减器2、分束器4、聚焦透镜5和45°高反镜6组成。其中,激光器1发出的激光依次经由可控衰减器2、聚焦透镜5、分束器4和高反镜6会聚在待测样品的表面。其中,激光器1发出高能量的、波长为1064nm、脉冲宽度为12ns的激光束。可控衰减器2对激光器1发出的激光能量进行调整,使调整后的激光能量在2~200mJ范围内线性变化。针对脉冲激光的稳定性差可能带来的测量问题,高能激光损伤装置通过分束器4和激光测试分析单元3对输出激光的能量、束斑大小进行实时测量,并将其作为最终计算待测样品激光损伤阈值的依据。之后,激光束通过聚焦透镜5和45°高反镜6辐照到待测样品的表面。在此,聚焦透镜5对调整后的激光束进行聚焦处理。分束器按照100∶1的比例将小能量的激光导入激光测试分析单元3进行能量光束分析。The high-energy laser damage device of the present invention comprises a Nd:YAG laser 1 , a controllable attenuator 2 , a beam splitter 4 , a focusing lens 5 and a 45°
本发明的高分辨率彩色CCD图像损伤判别装置包括驱动步进电机8、Z向运动机构9、配有低倍率物镜光学系统的CCD采集单元12、配有高倍率物镜光学系统的CCD采集单元14、CCD旋转夹持台13。其中,配有低倍率物镜光学系统的CCD采集单元12可快速地对激光辐照后的待测样品表面上的辐照点进行快速预判,筛选得到损伤测试点,然后再采用高倍率物镜光学系统的CCD采集单元14对筛选后的未损伤测试点进行复检判断。CCD旋转夹持台13可快速地实现配有低倍率物镜光学系统的CCD采集单元12以及配有高倍率物镜光学系统的CCD采集单元14在相同测试位置的旋转。Z向运动机构9则可在驱动步进电机8的作用下调整上述两个CCD采集单元的光路自动调焦。The high-resolution color CCD image damage discrimination device of the present invention comprises a
本发明的CCD辅助光源装置包括角度可调光源夹持台10和CCD辅助光源11。该角度可调光源夹持台10用来控制CCD辅助光源11的焦距。例如,通过软件系统对CCD辅助光源11调整。The CCD auxiliary light source device of the present invention includes an angle-adjustable light
本发明的样品台运动控制装置包括样品台驱动步进电机15、样品工装台16和XY方向二维平移台18。样品台驱动步进电机15使XY方向二维平移台18工作从而自动调整待测样品的工位。样品工装台16用来放置该待测样品。例如,该样品工装台16通过编程控制,准确地将待测样品移动至激光辐照和CCD测试位置。The sample stage motion control device of the present invention includes a sample stage driving stepping
在一具体实施例中,该激光损伤阈值测试系统采用1-on-1模式对所述待测样品进行测试,首先通过所述配有第一倍率物镜光学系统的CCD采集单元记录i×j个测试点辐照前的初始图像,然后以给定的步长按照i个能级逐一在每个能级下对j个测试点进行激光辐照,并利用所述配有第一倍率物镜光学系统的CCD采集单元再次采集所述待测样品表面的i×j个测试点辐照后的图像,对比辐照前后的测试点图像从而筛选得到损伤测试点,最后通过所述配有第二倍率物镜光学系统的CCD采集单元对筛选后的未损伤测试点进行复检判断,其中,i、j为自然数。In a specific embodiment, the laser damage threshold testing system adopts 1-on-1 mode to test the sample to be tested, and first records i×j pieces of The initial image of the test point before irradiation, and then irradiate j test points with laser light at each energy level one by one according to i energy levels with a given step size, and use the optical system equipped with the first magnification objective lens The CCD acquisition unit collects again the images of the i×j test points on the surface of the sample to be tested after irradiation, compares the images of the test points before and after irradiation to screen the damage test points, and finally passes through the second magnification objective lens The CCD acquisition unit of the optical system performs re-inspection and judgment on the screened undamaged test points, where i and j are natural numbers.
在一具体实施例中,该激光损伤阈值测试系统采用R-on-1模式对所述待测样品进行测试,首先设定恒定的激光输出能量,使激光束以相同的时间间隔对待测样品表面的第一测试点进行多次辐照,然后通过所述配有第一倍率物镜光学系统的CCD采集单元对每次辐照后的所述第一测试点进行实时图像采集,并与未辐照时所采集图像进行比对,按预设判别标准认定损伤时即停止辐照并统计出辐照次数N,然后更换至所述待测样品表面的第二测试点,激光束以相同参数对所述第二测试点进行(N-1)次辐照,然后通过所述配有第二倍率物镜光学系统的CCD采集单元对所述第二测试点的表面进行观察,若无激光损伤则可判定损伤次数为N,若存在损伤则再次更换第三测试点,并经递减激光辐照次数后再通过所述配有第二倍率物镜光学系统的CCD采集单元对所述第三测试点表面进行观察,以此递减辐照次数n次后直至无激光损伤现象为止,记录该激光能量下导致损伤的次数为(N-n)次,其中,N、n为自然数。In a specific embodiment, the laser damage threshold testing system uses the R-on-1 mode to test the sample to be tested. First, a constant laser output energy is set so that the laser beam is tested on the surface of the sample at the same time interval. The first test point is irradiated multiple times, and then the CCD acquisition unit equipped with the first magnification objective lens optical system is used for real-time image acquisition of the first test point after each irradiation, and compared with the unirradiated The images collected during the test are compared, and when the damage is determined according to the preset judgment standard, the irradiation is stopped and the number of irradiations N is counted, and then it is replaced to the second test point on the surface of the sample to be tested. The second test point is irradiated for (N-1) times, and then the surface of the second test point is observed through the CCD acquisition unit equipped with the second magnification objective lens optical system. If there is no laser damage, it can be determined The number of damages is N. If there is damage, replace the third test point again, and observe the surface of the third test point through the CCD acquisition unit equipped with the second magnification objective lens optical system after decreasing the number of laser irradiation , after reducing the number of times of irradiation n times until there is no laser damage phenomenon, the number of damages caused by the laser energy is recorded as (N-n) times, where N and n are natural numbers.
此外,采用R-on-1模式或1-on-1模式对待测样品进行测试时,激光束的光斑直径介于0.6mm~1mm之间。In addition, when the sample to be tested is tested in the R-on-1 mode or 1-on-1 mode, the spot diameter of the laser beam is between 0.6 mm and 1 mm.
此外,待测样品的激光损伤阈值由激光测试分析单元进行能量光束分析所得到的输出激光能量、激光束光斑大小决定。In addition, the laser damage threshold of the sample to be tested is determined by the output laser energy and the spot size of the laser beam obtained from the energy beam analysis by the laser test and analysis unit.
在一具体实施例中,激光损伤阈值测试系统还包括气流式表面清洁装置。该气流式表面清洁装置包括清洗喷嘴19、电磁阀20、干燥过滤器21、气阀22和气源23。更详细地,气源为氮气,打开气阀22后,氮气进入干燥过滤器21予以除湿,然后经过电磁阀20来调节气压和流量,并利用清洗喷嘴19射向待测样品的表面辐照点,从而将激光辐照后的待测样品因损伤而产生的粉尘吹拭掉,防止其对CCD图像损伤判别产生影响。例如,待测样品可以为光学元件、介质薄膜、金属薄膜或者半导体薄膜。In a specific embodiment, the laser damage threshold testing system further includes an airflow surface cleaning device. The airflow type surface cleaning device includes a cleaning
实施例1:Example 1:
如图1所示,由Nd:YAG激光器1发出的高能量激光(波长1064nm,脉宽12ns,单脉冲能量可在200mJ范围调整)经过衰减器2、聚焦透镜3、分束器4和高反器5之后会聚在待测样品之上。利用多组衰减片组合衰减器2对输出激光能量进行调整,使其可在2~200mJ范围内线性变化。利用分束器按100∶1的比例将小能量的激光导入激光测试分析单元进行能量光束分析,实时测量其参数。As shown in Figure 1, the high-energy laser (wavelength 1064nm, pulse width 12ns, single pulse energy can be adjusted in the range of 200mJ) emitted by Nd:YAG laser 1 passes through attenuator 2, focusing
根据测试光学元件或薄膜样品的材料特性,设定测试激光能量范围,并将其10等分,按由高到底的次序每一能级辐照10个测试点。通过编程控制中央处理单元7,启动CCD夹持台步进驱动电机和样品台驱动步进电机,使-XY方向二维平移台18工作,自动调整待测样品的工位,并使其能方便地在辐照位置和CCD测试位置来回运动。与此同时,通过Z向运动机构9和角度可调光源夹持台利用软件系统控制辅助光源和CCD图像采集单元的聚焦系统。首先,利用低倍率CCD图像采集单元10对比激光辐照前后待测样品表面各测试点形貌变化,筛除明显得损伤点,之后再利用高倍率CCD图像采集单元13对其余各损伤点按辐照能级的高低,由高向低逐一进行测试,直至某一低能级下10个测试点均无损伤为止。其中,采用低倍率CCD图像采集单元的作用是利用其物镜系统与样品表面空间距离大的特点可实施实时图像采集,依次来提高测试速度,而采用高倍率CCD图像采集单元的目的是确保,所有的损伤点均能被检测到,从而使测量结果与相衬显微法测量国际标准相一致。According to the material properties of the test optical element or film sample, set the test laser energy range, and divide it into 10 equal parts, and irradiate 10 test points at each energy level in the order from high to low. Control the
在激光辐照实验进行的同时,开启气流式样品自清洁系统,打开气阀22,使清洗气源23中的氮气经过气体干燥过滤器21,电磁阀20进入到清洗喷嘴19,干燥的氮气以一定的压力对样品的经辐照后表面进行吹洗3~5秒钟,以免损伤后所产生的材料粉末污染(特别是附近测试点损伤后所产生的粉末污染)造成传感器误判。其中,电磁阀由程序控制,可对其流量、压力和开关进行控制。While the laser irradiation experiment is being carried out, the airflow type sample self-cleaning system is turned on, the
实施例2:Example 2:
根据待测样品的具体情况选定合适的激光能量,如图1所示,软件驱动各控制台,调整辅助光源、CCD图像采集单元焦距。采用相同能量和相同时间间隔对待测样品同一区域进行多次辐照处理(辐照次数设定在5~100次),并且在每次辐照在辐照同时,利用低倍率CCD图像采集单元实施观察待测样品辐照区域,当发现明显损伤后即停止辐照,记录其辐照次数为N。驱动XY方向二维平移台,将辐照区移动至另一位置,按相同能量和相同时间间隔对此区域辐照N-1次,之后将高倍率CCD图像采集单元切换至观察位置,观测损伤表面是否被损伤,若无损伤,则测试结束;若有损伤存在,则再次更换样品表面辐照区,按相同能量和相同时间间隔辐照N-1,采用高倍率CCD图像采集单元。测量后若仍有损伤,则再更换测试位置,按相同能量和时间间隔进行N-2辐照,如此方式,直到对待测元件表面第S个测量区域进行高倍率CCD图像单元测量未发现损伤为止,最终确定该能级下,其重复损伤次数为N-S+1。Select the appropriate laser energy according to the specific conditions of the sample to be tested. As shown in Figure 1, the software drives each console to adjust the focal length of the auxiliary light source and the CCD image acquisition unit. Use the same energy and the same time interval to perform multiple irradiation treatments on the same area of the sample to be tested (the number of irradiations is set at 5 to 100 times), and at the same time as each irradiation, use a low-magnification CCD image acquisition unit to implement Observe the irradiation area of the sample to be tested, stop the irradiation when obvious damage is found, and record the irradiation times as N. Drive the two-dimensional translation platform in the XY direction, move the irradiation area to another position, irradiate this area N-1 times with the same energy and the same time interval, and then switch the high-magnification CCD image acquisition unit to the observation position to observe the damage Whether the surface is damaged, if there is no damage, the test is over; if there is damage, replace the irradiation area on the sample surface again, irradiate N-1 at the same energy and time interval, and use a high-magnification CCD image acquisition unit. If there is still damage after the measurement, then change the test position, and carry out N-2 irradiation at the same energy and time interval, in this way, until no damage is found in the high-magnification CCD image unit measurement of the S-th measurement area on the surface of the component to be tested , it is finally determined that at this energy level, the number of repeated damages is N-S+1.
在上述条件下,气流式样品自清洁系统在每次辐照结束后可由软件控制工作,并且CCD进行图像采集时应在清洗结束之后。另外,在本实施例中,若待测元件的抗损伤性能较低,如针对一些金属薄膜或功能薄膜如类金刚石薄膜等材料,由于其辐照次数N较少,亦可直接采用高倍率CCD图像采集单元对辐照后测试点形貌进行观察,这样测试仅在待测样品表面某一点区域即可完成。Under the above conditions, the airflow sample self-cleaning system can be controlled by software after each irradiation, and the CCD image acquisition should be done after cleaning. In addition, in this embodiment, if the anti-damage performance of the element to be tested is low, such as for some metal thin films or functional thin films such as diamond-like films, due to the small number of irradiation N, high-magnification CCD can also be directly used The image acquisition unit observes the morphology of the test point after irradiation, so that the test can be completed only at a certain point on the surface of the sample to be tested.
采用本发明的激光损伤阈值测试系统,不仅可有效地克服现有相衬显微法测量主观性强、测量误差大、测量时间长等缺点,而且还可同时满足1-on-1和R-on-1两种测量模式。具体地,该激光损伤阈值测试系统至少具有下列优点:Adopting the laser damage threshold testing system of the present invention can not only effectively overcome the disadvantages of strong subjectivity, large measurement error and long measurement time of the existing phase contrast microscopy method, but also satisfy the 1-on-1 and R- On-1 two measurement modes. Specifically, the laser damage threshold testing system has at least the following advantages:
1.兼顾测量误差和测试效率。本发明以相衬显微法为基础,在满足国际标准的前提下,有效地克服了手工测试过程中随机误差大、测试效率低的缺点。相比之下,现有技术采用单一CCD图像采集系统激光损伤测试方法,受限于高倍率CCD图像传感器物镜系统的调焦尺寸限制,只能通过牺牲物镜光学系统的放大倍率来提高测试效率,从而造成测试结果数值偏大。此外,本发明通过引入气流式自动清洁系统,对激光辐照后的样品表面进行清洗,可防止因损伤而产生的光学薄膜或元件材料粉末所引起的测量误差,进一步提高了测量的准确性。1. Taking into account the measurement error and test efficiency. Based on the phase-contrast microscopy method, the invention effectively overcomes the shortcomings of large random errors and low testing efficiency in the manual testing process under the premise of meeting international standards. In contrast, the existing technology uses a single CCD image acquisition system laser damage test method, which is limited by the focusing size of the high-magnification CCD image sensor objective system, and can only improve the test efficiency by sacrificing the magnification of the objective optical system. As a result, the value of the test result is too large. In addition, the present invention introduces an air-flow automatic cleaning system to clean the surface of the sample after laser irradiation, which can prevent measurement errors caused by optical films or component material powders caused by damage, and further improve measurement accuracy.
2.适用性强。本发明可同时实现1-on-1和R-on-1两种模式的激光损伤阈值测式方法,并且采用高分辨率的彩色CCD和与之匹配的图形采集系统可以直观地对经激光辐照后的光学薄膜或光学元件损伤形貌进行观察,既可用于对材料的抗激光损伤性能测试,又可用于材料的激光损伤分析。此外,本发明的待测样品可为各类光学元件、各类介质薄膜、金属薄膜或半导体薄膜。2. Strong applicability. The present invention can realize the laser damage threshold measuring method of two modes of 1-on-1 and R-on-1 at the same time, and adopt the high-resolution color CCD and the graphic acquisition system matching it to be able to visually monitor the laser damage threshold Observing the damage morphology of the optical film or optical element after irradiation can be used not only for the test of the anti-laser damage performance of the material, but also for the analysis of the laser damage of the material. In addition, the samples to be tested in the present invention can be various optical elements, various dielectric films, metal films or semiconductor films.
3.便于工业化应用。本发明的测试系统均可实现程序化控制,自动化程度高,同时各功能模块都具备较高的技术成熟度,因此可方便实现仪器化,用于工业生产实际。3. It is convenient for industrial application. The test system of the present invention can realize programmed control, has a high degree of automation, and at the same time, each functional module has a high degree of technical maturity, so it can be conveniently implemented as an instrument and used in actual industrial production.
上文中,参照附图描述了本发明的具体实施方式。但是,本领域中的普通技术人员能够理解,在不偏离本发明的精神和范围的情况下,还可以对本发明的具体实施方式作各种变更和替换。这些变更和替换都落在本发明权利要求书所限定的范围内。Hereinbefore, specific embodiments of the present invention have been described with reference to the accompanying drawings. However, those skilled in the art can understand that without departing from the spirit and scope of the present invention, various changes and substitutions can be made to the specific embodiments of the present invention. These changes and substitutions all fall within the scope defined by the claims of the present invention.
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