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CN103351950A - Cigarette essence perfume containing coke hawthorn extract and cigarettes containing same - Google Patents

Cigarette essence perfume containing coke hawthorn extract and cigarettes containing same Download PDF

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Publication number
CN103351950A
CN103351950A CN2013102700494A CN201310270049A CN103351950A CN 103351950 A CN103351950 A CN 103351950A CN 2013102700494 A CN2013102700494 A CN 2013102700494A CN 201310270049 A CN201310270049 A CN 201310270049A CN 103351950 A CN103351950 A CN 103351950A
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Prior art keywords
tobacco
cigarette
fragrance
burnt
extract
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CN2013102700494A
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Chinese (zh)
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蹇顺华
陈�胜
齐富友
李星
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China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
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China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
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Abstract

本发明公开了一种含有焦山楂提取物的烟用香精香料,它是由下述成分组成的:焦山楂提取物20~40%、白兰叶油0.3~0.5%、葫芦巴酊0.3~0.5%、酸梅酊0.5~1.0%、杏仁酊0.1~0.2%、丙二醇1~10%、余量为水,所述焦山楂提取物制备方法是:取焦山楂,加入10~20倍30%~95%的乙醇,浸泡1~3h后,加热回流提取2~4次,每次1~4小时,过滤,合并滤液,减压浓缩至焦山楂重量的2~4倍。本发明还公开了含有该烟用香精香料的卷烟及其制备方法。本发明得到烟用香精香料中所含的自然香气与烟草协调,加入到烟草叶组配方后对烟气形态有较好的修饰作用,同时使香气变得更加丰富,烟气柔和细腻,降低喉部刺激,对烟草品质有很好的改善作用。The invention discloses a tobacco essence and fragrance containing burnt hawthorn extract, which is composed of the following components: burnt hawthorn extract 20-40%, white orchid leaf oil 0.3-0.5%, fenugreek tincture 0.3-0.5% , sour plum tincture 0.5~1.0%, almond tincture 0.1~0.2%, propylene glycol 1~10%, and the balance is water. The preparation method of the burnt hawthorn extract is: take burnt hawthorn, add 10~20 times 30%~95 % ethanol, after soaking for 1-3 hours, heat and reflux for extraction 2-4 times, each time for 1-4 hours, filter, combine the filtrate, and concentrate under reduced pressure to 2-4 times the weight of burnt hawthorn. The invention also discloses a cigarette containing the essence and fragrance for tobacco and a preparation method thereof. According to the present invention, the natural aroma contained in the essence and fragrance for tobacco is in harmony with tobacco, and after being added to the tobacco leaf group formula, it has a good modification effect on the shape of the smoke, and at the same time makes the aroma more abundant, the smoke is soft and delicate, and the throat is reduced. Internal stimulation, which has a good effect on improving the quality of tobacco.

Description

A kind of essence spice for cigarette and cigarette that contains Fructus Crataegi (parched to brown) extract
Technical field
The present invention relates to essence spice for cigarette, specifically a kind of essence spice for cigarette that contains Fructus Crataegi (parched to brown) extract the invention still further relates to a kind of cigarette that contains this essence spice for cigarette and preparation method thereof.
Background technology
Essence and flavoring agent is the soul of cigarette product, and the quality of cigarette is played keying action.Along with becoming increasingly conspicuous of smoking and health problem dispute, the significant challenge that tobacco industry faces is exactly when reducing cigarette tar content, makes again cigarette keep enough fragrance.At present, many cigar mills adopt the way that adds various essence and flavoring agents, to remedy the deficiency of cigarette fragrance when meticulously allocating cigarette composition.
In recent years, Chinese herbal medicine extract feeds in raw material in perfuming cigarette as additive application has become emphasis and the focus of tobacco industry research.Herbal medicine is the distinct Chinese characteristics products, and tobacco is combined with herbal medicine, is one of " Chinese-style cigarette " most characteristic style.China is the native place of herbal medicine, and the application of Chinese herb feed additive in Chinese-style cigarette is the peculiar advantage of Chinese Tobacco Industry.There is abundant Chinese herbal medicine resource in China, many kinds on Chemical Composition with the tobacco structural similitude, but performance is different, they can remedy the deficiency of tobacco in some aspects.
Fructus Crataegi (parched to brown) is a kind of Chinese medicine commonly used, is that the mature fruit heating process of preparing Chinese medicine of rosaceous plant hawthorn forms.The main chemical compositions of Fructus Crataegi (parched to brown) is Flavonoid substances, and cardiovascular systems is had obvious pharmacological action, and another kind of composition is triterpene substance, and cardiac stimulant is arranged, and increases coronary blood flow, improves the vital role such as microcirculation.Contain in addition organic acid such as chlorogenic acid, coffic acid and tannin, the acid anhydride of tanning, epicatechol, choline, vagusstoff, Sitosterolum, carotene and a large amount of Vit C etc.Modern pharmacology studies show that hawthorn decoction and ethanol extraction all have anti-microbial effect to shigella flexneri, sonne bacillus, Bacillus proteus, intestinal bacteria.The now development and use of Fructus Crataegi (parched to brown) are multiplex in medicine and food service industry, there is not yet relevant report in tobacco industry.
Summary of the invention
The purpose of this invention is to provide a kind of essence spice for cigarette that contains Fructus Crataegi (parched to brown) extract, the invention still further relates to a kind of cigarette that contains this essence spice for cigarette and preparation method thereof.This essence spice for cigarette fragrance matter is abundant, and the soft fine and smooth flue gas of energy reduces flue gas to the pungent stimulation of oral cavity and throat.
Above-mentioned purpose is achieved through the following technical solutions:
A kind of essence spice for cigarette that contains Fructus Crataegi (parched to brown) extract, it is that one-tenth by following weight per-cent is grouped into:
Figure BDA0000343342401
Surplus is water,
Described Fructus Crataegi (parched to brown) extract preparation method is: get Fructus Crataegi (parched to brown), add by weight 10 ~ 20 times of volume fractions and be 30% ~ 95% ethanol, after soaking 1 ~ 3h, heating and refluxing extraction 2 ~ 4 times, each 1 ~ 4 hour, filter merging filtrate, under 55 ~ 65 ℃ of temperature, be evaporated to 2 ~ 4 times of Fructus Crataegi (parched to brown) weight, and get final product.
Preferably, described essence spice for cigarette is that one-tenth by following weight per-cent is grouped into:
Figure BDA0000343342402
Surplus is water.
Preferably, described Fructus Crataegi (parched to brown) extract preparation method is: get Fructus Crataegi (parched to brown), add by weight 12 times of volume fractions and be 60% ethanol, soak 2h after, heating and refluxing extraction 3 times each 2 hours, is filtered, merging filtrate is evaporated to 3 times of Fructus Crataegi (parched to brown) weight, and get final product under 60 ℃ of temperature.
A kind of cigarette contains described essence spice for cigarette in the pipe tobacco of this cigarette.
A kind of method for preparing described cigarette: be evenly to be sprayed in the pipe tobacco behind 95% the dissolve with ethanol with described essence spice for cigarette volume fraction, then pipe tobacco is dried under 55 ~ 65 ℃ of conditions to water content be 12 ~ 16%, make cigarette, the consumption of described essence spice for cigarette is 0.01 ~ 0.1% of pipe tobacco dry weight.
The invention has the beneficial effects as follows:
1, the present invention obtains natural fragrance contained in the essence spice for cigarette and tobacco coordination, after joining the tobacco tobacco leaf formulation flue gas form there is preferably modification, makes simultaneously fragrance become abundanter, the soft exquisiteness of flue gas, reducing throat stimulates, and cigarette quality is had good improvement effect.
2, starting material of the present invention are originated and are easy to get, and preparation technology is simple, and cost is low, are beneficial to produce to transform.
Embodiment
The present invention is described in detail below in conjunction with embodiment.
Embodiment 1
A kind of essence spice for cigarette that contains Fructus Crataegi (parched to brown) extract, it is that one-tenth by following weight per-cent is grouped into:
Figure BDA0000343342403
Surplus is water.
Described Fructus Crataegi (parched to brown) extract preparation method is: get Fructus Crataegi (parched to brown), add by weight 12 times of volume fractions and be 60% ethanol, soak 2h after, heating and refluxing extraction 3 times each 2 hours, is filtered, merging filtrate is evaporated to 3 times of Fructus Crataegi (parched to brown) weight, and get final product under 60 ℃ of temperature.
Be evenly to be sprayed in the pipe tobacco behind 95% the dissolve with ethanol above-mentioned essence spice for cigarette volume fraction, the consumption of described essence spice for cigarette is 0.06% of pipe tobacco dry weight, then pipe tobacco is dried under 60 ℃ of conditions to water content be 14%, make cigarette.
Sensory evaluating smoking result shows: the pungency in the flue gas obviously descends, and oral cavity nasal cavity comfort level is obviously improved.
Embodiment 2
A kind of essence spice for cigarette that contains Fructus Crataegi (parched to brown) extract, it is that one-tenth by following weight per-cent is grouped into:
Figure BDA0000343342404
Surplus is water,
Described Fructus Crataegi (parched to brown) extract preparation method is: get Fructus Crataegi (parched to brown), add by weight 10 times of volume fractions and be 95% ethanol, soak 3h after, heating and refluxing extraction 4 times each 1 hour, is filtered, merging filtrate is evaporated to 4 times of Fructus Crataegi (parched to brown) weight, and get final product under 55 ℃ of temperature.
Be evenly to be sprayed in the pipe tobacco behind 95% the dissolve with ethanol above-mentioned essence spice for cigarette volume fraction, the consumption of described essence spice for cigarette is 0.1% of pipe tobacco dry weight, then pipe tobacco is dried under 55 ℃ of conditions to water content be 12%, make cigarette.
Embodiment 3
A kind of essence spice for cigarette that contains Fructus Crataegi (parched to brown) extract, it is that one-tenth by following weight per-cent is grouped into:
Figure BDA0000343342405
Surplus is water,
Described Fructus Crataegi (parched to brown) extract preparation method is: get Fructus Crataegi (parched to brown), add by weight 20 times of volume fractions and be 30% ethanol, soak 1h after, heating and refluxing extraction 2 times each 4 hours, is filtered, merging filtrate is evaporated to 2 times of Fructus Crataegi (parched to brown) weight, and get final product under 65 ℃ of temperature.
Be evenly to be sprayed in the pipe tobacco behind 95% the dissolve with ethanol above-mentioned essence spice for cigarette volume fraction, the consumption of described essence spice for cigarette is 0.01% of pipe tobacco dry weight, then pipe tobacco is dried under 65 ℃ of conditions to water content be 16%, make cigarette.

Claims (5)

1.一种含有焦山楂提取物的烟用香精香料,其特征在于它是由下述重量百分比的成分组成的:1. a flavoring and fragrance for tobacco that contains burnt hawthorn extract, is characterized in that it is made up of following composition by weight percentage:
Figure FDA0000343342391
Figure FDA0000343342391
余量为水,The balance is water, 所述焦山楂提取物制备方法是:取焦山楂,按重量加入10~20倍体积分数为30%~95%的乙醇,浸泡1~3h后,加热回流提取2~4次,每次1~4小时,过滤,合并滤液,在55~65℃温度下减压浓缩至焦山楂重量的2~4倍,即得。The preparation method of the burnt hawthorn extract is as follows: take burnt hawthorn, add 10-20 times of ethanol with a volume fraction of 30%-95% by weight, soak for 1-3 hours, heat and reflux extract 2-4 times, each time 1-20% After 4 hours, filter, combine the filtrates, and concentrate under reduced pressure at a temperature of 55-65°C to 2-4 times the weight of the burnt hawthorn.
2.根据权利要求1所述的含有焦山楂提取物的烟用香精香料,其特征在于它是由下述重量百分比的成分组成的:2. the flavoring and fragrance for tobacco that contains burnt hawthorn extract according to claim 1, is characterized in that it is made up of the composition of following percentage by weight:
Figure FDA0000343342392
Figure FDA0000343342392
余量为水。The balance is water.
3.根据权利要求1所述的含有焦山楂提取物的烟用香精香料,其特征在于所述焦山楂提取物制备方法是:取焦山楂,按重量加入12倍体积分数为60%的乙醇,浸泡2h后,加热回流提取3次,每次2小时,过滤,合并滤液,在60℃温度下减压浓缩至焦山楂重量的3倍,即得。3. The tobacco flavor and fragrance containing burnt hawthorn extract according to claim 1, characterized in that the preparation method of the burnt hawthorn extract is: take burnt hawthorn, add 12 times of ethanol with a volume fraction of 60% by weight, After soaking for 2 hours, extract under reflux for 3 times, each time for 2 hours, filter, combine the filtrates, concentrate under reduced pressure at 60°C to 3 times the weight of burnt hawthorn, and obtain the product. 4.一种卷烟,其特征在于所述卷烟的烟丝中含有权利要求1或2或3所述的烟用香精香料。4. A cigarette, characterized in that the shredded tobacco of the cigarette contains the flavor and fragrance for tobacco according to claim 1, 2 or 3. 5.一种制备权利要求4所述卷烟的方法,其特征在于:将所述烟用香精香料用体积分数为95%的乙醇溶解后均匀喷洒于烟丝中,然后将烟丝在55~65℃条件下烘干至含水量为12~16%,制成卷烟,所述烟用香精香料的用量为烟丝干重的0.01~0.1%。5. A method for preparing the cigarette according to claim 4, characterized in that: dissolving the flavor and fragrance for tobacco with ethanol with a volume fraction of 95% and evenly spraying it in shredded tobacco, and then drying the shredded tobacco at 55-65°C Dried down until the water content is 12-16%, and made into cigarettes, the amount of the flavor and fragrance for tobacco is 0.01-0.1% of the dry weight of shredded tobacco.
CN2013102700494A 2013-06-28 2013-06-28 Cigarette essence perfume containing coke hawthorn extract and cigarettes containing same Pending CN103351950A (en)

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Cited By (7)

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Publication number Priority date Publication date Assignee Title
CN103892454A (en) * 2014-03-18 2014-07-02 黄金珍 Pressure lowering and lipid lowering electronic cigarette atomized liquid and preparation method thereof
CN104232309A (en) * 2014-09-30 2014-12-24 云南中烟工业有限责任公司 Tobacco flavor prepared from phyllanthus emblica, plum, broadleaf holly leaf and tobacco and application of tobacco flavor
CN104371826A (en) * 2014-10-31 2015-02-25 湖北中烟工业有限责任公司 Natural cigarette flavoring with antiseptic effect
CN104762133A (en) * 2015-04-27 2015-07-08 湖北中烟工业有限责任公司 Preparation method for cigarette hawthorn extract
CN105011362A (en) * 2015-06-17 2015-11-04 云南中烟工业有限责任公司 Glyceryl triacetate extract of Chinese hawthorn fruit and application thereof to cigarette
JP2020533975A (en) * 2017-09-15 2020-11-26 エ− ブランソン、マイケル Plant products and injection methods infused with oil extracted from plants of the genus Cannabis
US11950623B2 (en) 2017-09-15 2024-04-09 Big 5 Properties Inc. Plant product infused with oil and method of infusion

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103892454A (en) * 2014-03-18 2014-07-02 黄金珍 Pressure lowering and lipid lowering electronic cigarette atomized liquid and preparation method thereof
CN103892454B (en) * 2014-03-18 2017-01-04 黄金珍 Hypertension and hyperlipemia electronic cigarette atomizing liquid and preparation method thereof
CN104232309A (en) * 2014-09-30 2014-12-24 云南中烟工业有限责任公司 Tobacco flavor prepared from phyllanthus emblica, plum, broadleaf holly leaf and tobacco and application of tobacco flavor
CN104371826A (en) * 2014-10-31 2015-02-25 湖北中烟工业有限责任公司 Natural cigarette flavoring with antiseptic effect
CN104762133A (en) * 2015-04-27 2015-07-08 湖北中烟工业有限责任公司 Preparation method for cigarette hawthorn extract
CN105011362A (en) * 2015-06-17 2015-11-04 云南中烟工业有限责任公司 Glyceryl triacetate extract of Chinese hawthorn fruit and application thereof to cigarette
JP2020533975A (en) * 2017-09-15 2020-11-26 エ− ブランソン、マイケル Plant products and injection methods infused with oil extracted from plants of the genus Cannabis
JP7019799B2 (en) 2017-09-15 2022-02-15 エ- ブランソン、マイケル How to make plant products infused with cannabis oil
AU2020202488B2 (en) * 2017-09-15 2022-08-25 Michael A. BRUNSON Plant product infused with oil and method of infusion
US11950623B2 (en) 2017-09-15 2024-04-09 Big 5 Properties Inc. Plant product infused with oil and method of infusion

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Application publication date: 20131016