CN103271868A - Honey extractive, manufacturing technology thereof and infant wet tissues - Google Patents
Honey extractive, manufacturing technology thereof and infant wet tissues Download PDFInfo
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- CN103271868A CN103271868A CN2013102480916A CN201310248091A CN103271868A CN 103271868 A CN103271868 A CN 103271868A CN 2013102480916 A CN2013102480916 A CN 2013102480916A CN 201310248091 A CN201310248091 A CN 201310248091A CN 103271868 A CN103271868 A CN 103271868A
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Abstract
The invention discloses a manufacturing method for honey extractive used for wet tissue additive solution, which comprises the following steps: 1) removing impurities in propolis, and freezing the propolis for 45 to 52 hours at the temperature of minus 5 DEG C, 2) quickly crushing and screening the freezed propolis, 3) adding the screened propolis into ethanol solution to be impregnated for 5 to 7 hours at the temperature of 22 to 26 DEG C, then still-standing for 1.5 to 2.5 hours, extracting supernatant liquid, adding ethanol solution to continue impregnating and still standing the material left, repeating at least three times like that, then combining the supernatant liquid gained before, and cooling the supernatant liquid to below 5 DEG C, 4) filtering, heating and evaporating the filter liquor below the temperature of 50 DEG C, and gaining honey extracting liquid, and 5) diluting the honey extracting liquid until the sugar degree is 40 to 50, then concentrating until the sugar degree is 78 to 79 under low pressure, and then filtering to gain the honey extractive. The honey extractive, manufactured by the invention, can be taken as a natural preservative agent to be added to the additive solution of infant wet tissues, and greatly improves the use safety of the infant wet tissues.
Description
Technical field
The present invention relates to a kind of manufacture technology field of wet tissue, relate in particular to a kind of Mel extract and preparation method thereof and add the infant wet tissue that time Mel extract is made.
Background technology
Foster in the process at infant, often need the skin of infant is nursed.Traditional nursing care mode is come wiping infant skin for the cloth that adopts some quality softnesses, but this mode needs often to clean cloth, and owing to repeatedly use, is easy to generate antibacterial, and the health of infant is worked the mischief.Along with development, the progress of technology, wet tissue begins more and more to popularize, and becomes people's article of everyday use, and some wet tissue that are specifically designed to the infant skin nursing also begin to appear on the market.Because the antibacterial ability that the ratio that infant bears a pretty, delicate skin and infant itself has adult is more weak, people are when making the wet tissue that is used for infant, need to consider more the safety of use, and some infant wet tissue at present, the annex solution that adds to the wet tissue base material often adds the chemical material of some synthetic, and this health to infant can impact.
This shows, how prior art is improved, a kind of substance of adding to infant wet tissue annex solution that is applicable to is provided, the annex solution that obtains is safer, annex solution can better be nursed infant skin after forming the infant wet tissue thus, and this is the present technical issues that need to address in this area.
Summary of the invention
In order to solve above-mentioned the deficiencies in the prior art, the objective of the invention is to, a kind of Mel extract for the wet tissue annex solution and processing technology thereof are provided, the Mel extract that obtains can be used in the infant wet tissue annex solution, improves the safety that wet tissue uses.
For solving above technical problem, technical scheme of the present invention is:
A kind of manufacture method of the Mel extract for the wet tissue annex solution comprises the steps:
1) propolis is removed behind the impurity freezing 45h～52h under the temperature below-5 ℃;
2) then with broken, the screening fast of the propolis after freezing;
3) propolis after will sieving adds alcoholic solution and flood 5h～7h under 22 ℃～26 ℃ temperature, take out the upper strata stillness of night after then leaving standstill 1.5h～2.5h, remaining material adds alcoholic solution again to be continued dipping, leaves standstill, so repeat at least three times, merge the upper strata stillness of night that each time obtain then to cool to below 5 ℃;
4) the cooled upper strata stillness of night is filtered, filtrate carrying out heating evaporation below 50 ℃, is namely got the Mel essence;
5) diluting this Mel essence to its pol is 40-50, and under low pressure being concentrated into pol then is 78～79, namely gets Mel extract after refiltering.
Preferably, in the step 3), the volume ratio of propolis and ethanol is 1:3～1:5.
Preferably, in the step 3), the mass percent concentration of used alcoholic solution is 85%～95%.
Preferably, in the step 4), heating is carried out in decompression evaporator, adopts heating in water bath; Filtration is carried out in the plate and frame filter.
Preferably, in the step 3), cooling is carried out in the cooling reactor.
Preferably, in the step 1), freezing 48h under-18 ℃ temperature.
Preferably, step 2) in, screening is carried out in 14 purpose reciprocating sieves, returns again freezing greater than 14 purpose granules.
Preferably, in the step 4), the alcohol vapour that evaporates is recovered to the storage tank recirculation through condenser uses.
A kind of Mel extract of the present invention is made by aforesaid manufacture method.
A kind of infant wet tissue of the present invention comprises base material, is added with annex solution in the described base material, contains foregoing Mel extract in the described annex solution.
Compared with prior art, the present invention with propolis as raw material, design by the series of process step, making obtains Mel extract, this Mel extract can be used as natural antiseptic to be added in the infant wet tissue annex solution, make the infant wet tissue, replace the chemosynthesis antiseptic harmful to the infant health, improved the safety in utilization of infant wet tissue greatly; In addition, because Mel extract is at room temperature placed the several years can be not corrupt, show that its antisepsis is extremely strong, and studies have shown that by experiment, Mel has stronger inhibitory action to gram positive bacterias such as streptococcus, staphylococcus, diphtheria corynebacteriums, so add the infant wet tissue that makes after annex solution that Mel extract of the present invention makes is used, can clean, moisten the infant skin, improve immunity, reach good infant skin nursing efficacy.
Infant wet tissue of the present invention aims at baby's tender and lovely skin design, the Mel extract that contains, and salubrious moistening improved body immunity, and be gentle non-stimulated.
The specific embodiment
For making technical scheme of the present invention clearer, the present invention is described in detail below in conjunction with coming by specific embodiment.
The manufacture method of the Mel extract for the wet tissue annex solution of the present invention comprises the steps:
1) propolis is removed behind the impurity freezing 45h～52h under the temperature below-5 ℃;
2) then with broken, the screening fast of the propolis after freezing;
3) propolis after will sieving adds alcoholic solution flood 5h～7h under 22 ℃～26 ℃ temperature, take out the upper strata stillness of night after then leaving standstill 1.5h～2.5h, remaining material adds alcoholic solution again to be continued dipping, leaves standstill, so repeat at least three times, merge the upper strata stillness of night that each time obtain then to cool to below 5 ℃;
4) the cooled supernatant is filtered, filtrate carrying out heating evaporation below 50 ℃, is namely got the Mel essence;
5) diluting this Mel essence to its pol is 40-50, and under low pressure being concentrated into pol then is 78～79, namely gets Mel extract after refiltering.
The physical property of propolis has determined it to be in semi plastic stage at normal temperatures, is difficult to fragmentation, and the technical scheme in the step 1), behind freezing 45h～52h under the temperature below-5 ℃, then propolis can become broken easily with propolis.
Temperature remains on about 22 ℃～26 ℃ in the dipping process, and temperature too high (as greater than 26 ℃) can cause that then Cera Flava dissolves in a large number, causes filtration difficulty; Temperature low excessively (as less than 22 ℃), then the dissolubility reduction causes time lengthening, and solvent load strengthens.
A kind of Mel extract of the present invention is made by aforesaid manufacture method.
A kind of infant wet tissue of the present invention comprises base material, is added with annex solution in the described base material, contains foregoing Mel extract in the described annex solution.
Embodiment one
The manufacture method of the Mel extract that is used for the wet tissue annex solution of present embodiment comprises the steps:
1, propolis raw material is removed impurity through the preliminary election classification;
2, the raw material after the preliminary election is put into refrigerator, place freezing 48h under-18 ℃ of temperature;
3, the raw material after freezing is put into the disintegrating machine fragmentation rapidly;
4, the raw material after the fragmentation is entered immediately reciprocating sieve (14 order), return refrigerator greater than 14 purpose granules;
5, the raw material behind the crushing and screening is put into the dipping still, the dipping still is preferably selected the reactor of joining reflux condenser for use, again in propolis: the ethanol volume ratio is that the ratio of 1:4 adds 90% ethanol, dipping, and constantly stirring at normal temperatures, behind the 6h, stop to stir, leave standstill 2h, emit the supernatant, add 90% ethanol such as above-mentioned technology again and repeat 3 times, merge solution;
6, the solution that merging is obtained enters the cooling reactor, feeds cooling water circulation cooling in reacting kettle jacketing, and mechanical agitation is cooled to below 5 ℃;
7, the solution after the cooling is taken advantage of and is coldly entered the plate and frame filter by pump and filter, and solution temperature remains on below 5 ℃, can make the Cera Flava that dissolves in the alcoholic solution separate out and leach with filtering residue like this;
8, filtrate enters decompression evaporator, adopts heating in water bath; Remain on below 50 ℃ in this phase temperature, can reduce evaporation and the effective ingredient heated denaturalization of volatile oil like this;
9, the ethanol steam that evaporates reclaims through condenser and injects solvent tanker, recycles;
10, the evaporation after the propolis casting after pure Mel essence;
11, the pure Mel essence of dilution gained, making its pol is 40, under low pressure being concentrated into pol is 78-79, filters at last and obtains Mel extract.
Embodiment two
The manufacture method of the Mel extract that is used for the wet tissue annex solution of present embodiment comprises the steps:
1, propolis raw material is removed impurity through the preliminary election classification;
2, the raw material after the preliminary election is put into refrigerator, place freezing 50h under-15 ℃ of temperature;
3, the raw material after freezing is put into the disintegrating machine fragmentation rapidly.
4, the raw material after the fragmentation is entered immediately reciprocating sieve (14 order), return refrigerator greater than 14 purpose granules;
5, the raw material behind the crushing and screening is put into the dipping still, the dipping still is preferably selected the reactor of joining reflux condenser for use, and again in propolis: the ethanol volume ratio is that the ratio of 1:3 adds 90% ethanol, dipping, and constantly stirring at normal temperatures.Behind the 7h, stop to stir, leave standstill 2.5h, emit the supernatant, add 90% ethanol such as above-mentioned technology again and repeat 3 times, merge solution;
6, the solution that merging is obtained enters the cooling reactor, feeds cooling water circulation cooling in reacting kettle jacketing, and mechanical agitation is cooled to below 5 ℃;
7, the solution after the cooling is taken advantage of and is coldly entered the plate and frame filter by pump and filter.Solution temperature keeps can making the Cera Flava that dissolves in the alcoholic solution separate out and leach with filtering residue like this below 5 ℃.
8, filtrate enters decompression evaporator, adopts heating in water bath.Remain on below 50 ℃ in this phase temperature, can reduce evaporation and the effective ingredient heated denaturalization of volatile oil like this;
9, the ethanol steam that evaporates reclaims through condenser and injects solvent tanker, recycles;
10, the evaporation after the propolis casting after pure Mel essence;
11, the pure Mel essence of dilution gained, making its pol is 50, under low pressure being concentrated into pol is 79, filters at last and obtains Mel extract.
Embodiment three
The manufacture method of the Mel extract that is used for the wet tissue annex solution of present embodiment comprises the steps:
1, propolis raw material is removed impurity through the preliminary election classification;
2, the raw material after the preliminary election is put into refrigerator, place freezing 52h under-10 ℃ of temperature;
3, the raw material after freezing is put into the disintegrating machine fragmentation rapidly;
4, the raw material after the fragmentation is entered immediately reciprocating sieve (14 order), return refrigerator greater than 14 purpose granules;
5, the raw material behind the crushing and screening is put into the dipping still, the dipping still is preferably selected the reactor of joining reflux condenser for use.Again in propolis: the ethanol volume ratio is that the ratio of 1:5 adds 90% ethanol, dipping, and constantly stirring at normal temperatures.Behind the 5h, stop to stir, leave standstill 1.5h, emit supernatant, add 90% ethanol such as above-mentioned technology again and repeat 3 times, merge solution;
6, the solution that merging is obtained enters the cooling reactor, feeds cooling water circulation cooling in reacting kettle jacketing, and mechanical agitation is cooled to below 5 ℃;
7, the solution after the cooling is taken advantage of and is coldly entered the plate and frame filter by pump and filter.Solution temperature keeps can making the Cera Flava that dissolves in the alcoholic solution separate out and leach with filtering residue like this below 5 ℃;
8, filtrate enters decompression evaporator, adopts heating in water bath.Remain on below 50 ℃ in this phase temperature, can reduce evaporation and the effective ingredient heated denaturalization of volatile oil like this;
9, the ethanol steam that evaporates reclaims through condenser and injects solvent tanker, recycles;
10, the evaporation after the propolis casting after pure Mel essence;
11, the pure Mel essence of dilution gained, making its pol is 45, under low pressure being concentrated into pol is 79, filters at last and obtains Mel extract.
Embodiment four
The manufacture method of the Mel extract that is used for the wet tissue annex solution of present embodiment comprises the steps:
1, propolis raw material is removed impurity through the preliminary election classification;
2, the raw material after the preliminary election is put into refrigerator, place freezing 52h under-5 ℃ of temperature;
3, the raw material after freezing is put into the disintegrating machine fragmentation rapidly;
4, the raw material after the fragmentation is entered immediately reciprocating sieve (14 order), return refrigerator greater than 14 purpose granules;
5, the raw material behind the crushing and screening is put into the dipping still, the dipping still is preferably selected the reactor of joining reflux condenser for use.Again in propolis: ethanol is that the ratio of 1:3 adds 90% ethanol, dipping, and constantly stirring at normal temperatures.6.5h after, stop to stir, leave standstill 1.5h, emit the supernatant, add 90% ethanol such as above-mentioned technology again and repeat 3 times, merge solution;
6, the solution that merging is obtained enters the cooling reactor, feeds cooling water circulation cooling in reacting kettle jacketing, and mechanical agitation is cooled to below 5 ℃;
7, the solution after the cooling is taken advantage of and is coldly entered the plate and frame filter by pump and filter.Solution temperature should keep below 5 ℃, can make the Cera Flava that dissolves in the alcoholic solution separate out and leach with filtering residue like this;
8, filtrate enters decompression evaporator, adopts heating in water bath.Should remain on below 50 ℃ in this phase temperature, can reduce evaporation and the effective ingredient heated denaturalization of volatile oil like this;
9, the ethanol steam that evaporates reclaims through condenser and injects solvent tanker, recycles;
10, the evaporation after the propolis casting after pure Mel essence;
11, the pure Mel essence of dilution gained, making its pol is 48, under low pressure being concentrated into pol is 78, filters at last and obtains Mel extract.
Embodiment five
The manufacture method of the Mel extract that is used for the wet tissue annex solution of present embodiment comprises the steps:
1, propolis raw material is removed impurity through the preliminary election classification;
2, the raw material after the preliminary election is put into refrigerator, place freezing 52h under-8 ℃ of temperature;
3, the raw material after freezing is put into the disintegrating machine fragmentation rapidly;
4, the raw material after the fragmentation is entered immediately reciprocating sieve (14 order), return refrigerator greater than 14 purpose granules;
5, the raw material behind the crushing and screening is put into the dipping still, the dipping still is preferably selected the reactor of joining reflux condenser for use.Again in propolis: ethanol is that the ratio of 1:4 adds 90% ethanol, dipping, and constantly stirring at normal temperatures.Behind the 7h, stop to stir, leave standstill 2.5h, emit the supernatant, add 90% ethanol such as above-mentioned technology again and repeat 3 times, merge solution;
6, the solution that merging is obtained enters the cooling reactor, feeds cooling water circulation cooling in reacting kettle jacketing, and mechanical agitation is cooled to below 5 ℃;
7, the solution after the cooling is taken advantage of and is coldly entered the plate and frame filter by pump and filter.Solution temperature should keep below 5 ℃, can make the Cera Flava that dissolves in the alcoholic solution separate out and leach with filtering residue like this;
8, filtrate enters decompression evaporator, adopts heating in water bath.Should remain on below 50 ℃ in this phase temperature, can reduce evaporation and the effective ingredient heated denaturalization of volatile oil like this;
9, the ethanol steam that evaporates reclaims through condenser and injects solvent tanker, recycles;
10, the evaporation after the propolis casting after pure Mel essence;
11, the pure Mel essence of dilution gained, making its pol is 48, under low pressure being concentrated into pol is 78, filters at last and obtains Mel extract.
Infant wet tissue annex solution of the present invention, made by the material of following percentage by weight:
Natural honey extract 4%～5%; Wetting agent 2%～3%; Emollient 0.05%～0.3%; PH value regulator 0.01%～0.053%; PGG-40 castor oil hydrogenated 1%～2%; Antibacterial 0.02%～0.1%; Surplus is pure water; Wherein, described wetting agent is any one or the two or more mixture in sorbitol, propylene glycol, the glycerol; Described emollient is any one or the two or more mixture in Jojoba wax PEG-120 ester, lanoline, water-soluble silicon oil, the PEG-7 glycerol coconut oil fat; Described pH value regulator is lactic acid or citric acid.Wherein, the natural honey extract makes for the method by aforementioned any embodiment; Wherein, antibacterial is benzethonium chloride.
The processing technology of aforesaid infant wet tissue annex solution comprises the steps:
1) at normal temperatures the antibacterial of whole formula ratios is added in the pure water, stir;
2) add natural honey extract, the wetting agent of whole formula ratios more while stirring, make mixed liquor become uniform clear liquor state;
3) the PGG-40 castor oil hydrogenated is heated to 50 ℃～60 ℃, adds the emollient of whole formula ratios then while stirring, together join step 2 again) in mixed liquor in;
4) add the pure water of pH value regulator and surplus at last, stir namely;
More than in each step, the speed of stirring is 30r/min～50r/min, mixing time is 5min～10min.
Wherein, among the above embodiment, benzethonium chloride in other embodiments, also can adopt other material as antibacterial as antibacterial.
Wherein, the PGG-40 castor oil hydrogenated of above embodiment is as synergist.
The annex solution that above embodiment is made is used in the making of wet tissue, then the wet tissue that makes is carried out the skin moisture measurement, and test result shows that the skin water content is 39% before not using Mel elite water, and the skin water content is promoted to 51.5% after use.In addition, after testing, the pH value of this wet tissue is acidity on the weak side, and the PH reagent paper is presented on about 5.5, and suitable fully skin uses at any time.
The wet tissue that makes is LD50＞5000mg/kgBW to the striving property acute oral toxicity of male and female NIH mice, belongs to nontoxic level, meets " disinfection technology standard ";
The wet tissue that makes carries out the intact skin irritant test one time: the result shows that the wet tissue that makes belongs to nonirritant to the stimulation of skin, meets " disinfection technology standard ".
Only be preferred implementation of the present invention below, should be pointed out that above-mentioned preferred implementation should not be considered as limitation of the present invention, protection scope of the present invention should be as the criterion with claim institute restricted portion.For those skilled in the art, without departing from the spirit and scope of the present invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (10)
1. a manufacture method that is used for the Mel extract of wet tissue annex solution is characterized in that, comprises the steps:
1) propolis is removed behind the impurity freezing 45h～52h under the temperature below-5 ℃;
2) then with broken, the screening fast of the propolis after freezing;
3) propolis after will sieving adds alcoholic solution and flood 5h～7h under 22 ℃～26 ℃ temperature, take out the upper strata stillness of night after then leaving standstill 1.5h～2.5h, remaining material adds alcoholic solution again to be continued dipping, leaves standstill, so repeat at least three times, merge the upper strata stillness of night that each time obtain then to cool to below 5 ℃;
4) the cooled upper strata stillness of night is filtered, filtrate carrying out heating evaporation below 50 ℃, is namely got the Mel essence;
5) diluting this Mel essence to its pol is 40-50, and under low pressure being concentrated into pol then is 78～79, namely gets Mel extract after refiltering.
2. the manufacture method of the Mel extract for the wet tissue annex solution as claimed in claim 1 is characterized in that in the step 3), the volume ratio of propolis and ethanol is 1:3～1:5.
3. the manufacture method of the Mel extract for the wet tissue annex solution as claimed in claim 1 is characterized in that in the step 3), the mass percent concentration of used alcoholic solution is 85%～95%.
4. the manufacture method of the Mel extract for the wet tissue annex solution as claimed in claim 1 is characterized in that, in the step 4), heating is carried out in decompression evaporator, adopts heating in water bath; Filtration is carried out in the plate and frame filter.
5. the manufacture method of the Mel extract for the wet tissue annex solution as claimed in claim 1 is characterized in that, in the step 3), cooling is carried out in the cooling reactor.
6. the manufacture method of the Mel extract for the wet tissue annex solution as claimed in claim 1 is characterized in that, in the step 1), and freezing 48h under-18 ℃ temperature.
7. the manufacture method of the Mel extract for the wet tissue annex solution as claimed in claim 1 is characterized in that step 2) in, screening is carried out in 14 purpose reciprocating sieves, returns again freezing greater than 14 purpose granules.
8. the manufacture method of the Mel extract for the wet tissue annex solution as claimed in claim 1 is characterized in that, in the step 4), the alcohol vapour that evaporates is recovered to the storage tank recirculation through condenser uses.
9. a Mel extract is characterized in that, is made by each described manufacture method of claim 1～8.
10. an infant wet tissue comprises base material, is added with annex solution in the described base material, it is characterized in that, contains the described Mel extract of claim 9 in the described annex solution.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310248091.6A CN103271868B (en) | 2013-06-20 | 2013-06-20 | Honey extractive, manufacturing technology thereof and infant wet tissues |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310248091.6A CN103271868B (en) | 2013-06-20 | 2013-06-20 | Honey extractive, manufacturing technology thereof and infant wet tissues |
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| CN103271868A true CN103271868A (en) | 2013-09-04 |
| CN103271868B CN103271868B (en) | 2014-09-10 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106692024A (en) * | 2017-03-29 | 2017-05-24 | 广州极雅生物科技有限公司 | Baby skin cream |
| CN114191454A (en) * | 2022-01-23 | 2022-03-18 | 吉林蜂道馆健康产业有限公司 | Preparation method of bee therapy product for reducing blood fat |
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| US5922324A (en) * | 1995-01-31 | 1999-07-13 | Kabushiki Kaisha Hayashibara Seibutsu Kagaku Kenkyujo | Propolis extract with improved water-solubility |
| CN102283866A (en) * | 2011-06-16 | 2011-12-21 | 张大辉 | Method for extracting propolis containing high-purity flavones |
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2013
- 2013-06-20 CN CN201310248091.6A patent/CN103271868B/en active Active
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5922324A (en) * | 1995-01-31 | 1999-07-13 | Kabushiki Kaisha Hayashibara Seibutsu Kagaku Kenkyujo | Propolis extract with improved water-solubility |
| CN102283866A (en) * | 2011-06-16 | 2011-12-21 | 张大辉 | Method for extracting propolis containing high-purity flavones |
Non-Patent Citations (1)
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| 张巧鸣: "蜂蜜提取物在化妆品中的应用", 《日用化学品科学》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106692024A (en) * | 2017-03-29 | 2017-05-24 | 广州极雅生物科技有限公司 | Baby skin cream |
| CN114191454A (en) * | 2022-01-23 | 2022-03-18 | 吉林蜂道馆健康产业有限公司 | Preparation method of bee therapy product for reducing blood fat |
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| CN103271868B (en) | 2014-09-10 |
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Address after: 528000 Guicheng, Foshan, Nanhai District, East Street, No. 23 gem Patentee after: KINGDOM HEALTHCARE HOLDINGS CO., LTD., GUANGDONG Address before: 528200 Foshan, Nanhai, Guicheng, South China Sea, North Road, Hang Seng Bank Building, No. 8, building 50, No. Patentee before: Kingdom Sanitary Products Co., Ltd. |