CN103131297A - Powder coating with trioctyl trimellitate - Google Patents
Powder coating with trioctyl trimellitate Download PDFInfo
- Publication number
- CN103131297A CN103131297A CN2013100406398A CN201310040639A CN103131297A CN 103131297 A CN103131297 A CN 103131297A CN 2013100406398 A CN2013100406398 A CN 2013100406398A CN 201310040639 A CN201310040639 A CN 201310040639A CN 103131297 A CN103131297 A CN 103131297A
- Authority
- CN
- China
- Prior art keywords
- parts
- trioctyl trimellitate
- powder coating
- rev
- crossed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention discloses powder coating with trioctyl trimellitate. The powder coating with the trioctyl trimellitate is prepared from the following materials, by weight, 90-95 parts of bisphenols A type epoxy resin, 20-30 parts of polyving alcohol, 20-25 parts of 2402 phenolic resin, 1.5-3 parts of hydroxypropyl methyl cellulose, 100-110 parts of inorganic filler, 3-5 parts of nano calcium carbonate, 1-2 parts of fumed silica, 0.5-1.3 parts of acrylate flow ping agent, 1-2 parts of organic silicon defoamer, 0.5-1.5 parts of benzoin, 1-2 parts of rice hull ash, 1-2 parts of antimonous oxide, 1-2 parts of aluminium hydroxide, 6-8 parts of 4 methoxy methyl urea, 1-2 parts of trioctyl trimellitate, and 1-2 parts of antioxygen168. The powder coating with the trioctyl trimellitate is environment-friendly, high in mechanical strength, convenient to use, poison-free, harmless, inflaming retarding, and strong in weather resistance.
Description
Technical field
The present invention relates to paint field, is exactly a kind of powder coating that contains trioctyl trimellitate.
Background technology
Powder coating is a kind of novel solvent 100% solid powdery coating that do not contain.Have solvent-free, pollution-free, recyclable, environmental protection, the saving energy and resource, the physical strength high reduces labor intensity and films.Powder coating is and the diverse form of general coating, and it is that state with fines exists.Owing to not using solvent, so be called powder coating.The principal feature of powder coating has: the characteristics with nuisanceless, high-level efficiency, saving resource.
Summary of the invention
The object of the present invention is to provide a kind of powder coating that contains trioctyl trimellitate.
Above-mentioned purpose realizes by following scheme:
a kind of powder coating that contains trioctyl trimellitate, it is characterized in that, that raw material by following weight parts makes: bisphenol A type epoxy resin 90-95, polyvinyl alcohol 20-30, 2402 resol 20-25, Vltra tears 1.5-3, mineral filler 100-110, nano-calcium carbonate 3-5, aerosil 1-2, acrylate flow agent 0.5-1.3, silicone antifoam agent 1-2, st-yrax 0.5-1.5, rice hull ash 1-2, antimonous oxide 1-2, aluminium hydroxide 1-2, tetramethoxymethylglycoluril 6-8, trioctyl trimellitate 1-2, irgasfos 168 1-2.
Described a kind of powder coating that contains trioctyl trimellitate, it is characterized in that: described mineral filler is comprised of the raw material of following weight parts: ground barium sulfate 20-22, Modified Iron slag 10-12, modified Nano wilkinite 10-15;
Described modified Nano preparation method for bentonite is: wilkinite was calcined 4-6 hour under 700-800 ℃, after cooling, the 100-200 mesh sieve is crossed in fragmentation, then soak after 5-7 hour in the acetic acid solution of 8-10%, take out, deionized water wash adds to neutral the stearic acid that is equivalent to wilkinite weight 1-2%, after mixing, oven dry grinds to form nanometer powder, and get final product;
The preparation method of described Modified Iron slag is: Iron-ore Slag is soaked 5-7 hour in the acetic acid solution of 8-10% after, take out, deionized water wash was calcined 4-6 hour under 600-700 ℃ afterwards to neutral, after cooling, the 100-200 mesh sieve is crossed in fragmentation, then adds the stearic acid that is equivalent to Iron-ore Slag weight 1-2%, after mixing, oven dry grinds to form nanometer powder, and get final product.
Described a kind of powder coating that contains trioctyl trimellitate is characterized in that:
The preparation method comprises the following steps:
(1), by described each raw material of weight part accurate weighing, mix 3-4 minute under 500-600 rev/min, mix 8-10 minute under 3800-4500 rev/min, mix 1-2 minute afterwards under 400-500 rev/min, stop stirring, get mixture;
(2), mixture is extruded at the temperature of 100-115 ℃ with forcing machine, get extruded stock;
(3), extruded stock is crossed the 100-200 mesh sieve after pulverizing, and be get final product.
Described a kind of powder coating that contains trioctyl trimellitate is characterized in that:
Described silicone antifoam agent solid content is 25%.
Beneficial effect of the present invention is: environmental protection of the present invention, and physical strength is high; Both easy to use, nontoxic fire-retardant again, weathering resistance is strong.
Embodiment
A kind of powder coating that contains trioctyl trimellitate, that raw material by following weight parts (kg) makes: bisphenol A type epoxy resin 95, polyvinyl alcohol 30,2402 resol 25, Vltra tears 3, mineral filler 110, nano-calcium carbonate 5, aerosil 2, acrylate flow agent 1.3, solid content are 25% silicone antifoam agent 2, st-yrax 1.1, rice hull ash 1, antimonous oxide 2, aluminium hydroxide 2, tetramethoxymethylglycoluril 8, trioctyl trimellitate 2, irgasfos 168 1.
Described mineral filler is comprised of the raw material of following weight parts: ground barium sulfate 22, Modified Iron slag 12, modified Nano wilkinite 10;
Described modified Nano preparation method for bentonite is: wilkinite was calcined 6 hours under 750 ℃, after cooling, 100 mesh sieves are crossed in fragmentation, then soak after 5 hours in 8% acetic acid solution, take out, deionized water wash adds to neutral the stearic acid that is equivalent to wilkinite weight 1%, after mixing, oven dry grinds to form nanometer powder, and get final product;
The preparation method of described Modified Iron slag is: Iron-ore Slag is soaked 5 hours in 10% acetic acid solution after, take out, deionized water wash was calcined 6 hours under 700 ℃ afterwards to neutral, after cooling, 200 mesh sieves are crossed in fragmentation, then add the stearic acid that is equivalent to Iron-ore Slag weight 2%, after mixing, oven dry grinds to form nanometer powder, and get final product.
Described a kind of powder coating that contains trioctyl trimellitate,
The preparation method comprises the following steps:
(1), by described each raw material of weight part accurate weighing, mix 3 minutes under 600 rev/mins, mix 9 minutes under 4500 rev/mins, mix 2 minutes afterwards under 500 rev/mins, stop stirring, get mixture;
(2), mixture is extruded at the temperature of 115 ℃ with forcing machine, get extruded stock;
(3), extruded stock is crossed 200 mesh sieves after pulverizing, and be get final product.
Adopt high pressure electrostatic painting on foundry goods the present embodiment gained coating, voltage is 60KV, and average film thickness is the 65-75 micron, and condition of cure is 180 ℃ of bakings 20 minutes;
Performance index are as follows:
According to GB/T1732 test, shock resistance 〉=50kg.cm;
According to GB/T6739 test, pencil hardness 〉=H level;
480h QUV-B accelerated light ageing experimental test gets, and protects the light rate and reaches 89%.
The gained coatingsurface is smooth, without bubble, and particle, shrinkage cavity, pin hole.
Claims (4)
1. powder coating that contains trioctyl trimellitate, it is characterized in that, that raw material by following weight parts makes: bisphenol A type epoxy resin 90-95, polyvinyl alcohol 20-30, 2402 resol 20-25, Vltra tears 1.5-3, mineral filler 100-110, nano-calcium carbonate 3-5, aerosil 1-2, acrylate flow agent 0.5-1.3, silicone antifoam agent 1-2, st-yrax 0.5-1.5, rice hull ash 1-2, antimonous oxide 1-2, aluminium hydroxide 1-2, tetramethoxymethylglycoluril 6-8, trioctyl trimellitate 1-2, irgasfos 168 1-2.
2. a kind of powder coating that contains trioctyl trimellitate according to claim 1, it is characterized in that: described mineral filler is comprised of the raw material of following weight parts: ground barium sulfate 20-22, Modified Iron slag 10-12, modified Nano wilkinite 10-15;
Described modified Nano preparation method for bentonite is: wilkinite was calcined 4-6 hour under 700-800 ℃, after cooling, the 100-200 mesh sieve is crossed in fragmentation, then soak after 5-7 hour in the acetic acid solution of 8-10%, take out, deionized water wash adds to neutral the stearic acid that is equivalent to wilkinite weight 1-2%, after mixing, oven dry grinds to form nanometer powder, and get final product;
The preparation method of described Modified Iron slag is: Iron-ore Slag is soaked 5-7 hour in the acetic acid solution of 8-10% after, take out, deionized water wash was calcined 4-6 hour under 600-700 ℃ afterwards to neutral, after cooling, the 100-200 mesh sieve is crossed in fragmentation, then adds the stearic acid that is equivalent to Iron-ore Slag weight 1-2%, after mixing, oven dry grinds to form nanometer powder, and get final product.
3. a kind of powder coating that contains trioctyl trimellitate according to claim 1 is characterized in that:
The preparation method comprises the following steps:
(1), by described each raw material of weight part accurate weighing, mix 3-4 minute under 500-600 rev/min, mix 8-10 minute under 3800-4500 rev/min, mix 1-2 minute afterwards under 400-500 rev/min, stop stirring, get mixture;
(2), mixture is extruded at the temperature of 100-115 ℃ with forcing machine, get extruded stock;
(3), extruded stock is crossed the 100-200 mesh sieve after pulverizing, and be get final product.
4. a kind of powder coating that contains trioctyl trimellitate according to claim 1 is characterized in that:
Described silicone antifoam agent solid content is 25%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310040639.8A CN103131297B (en) | 2013-02-03 | 2013-02-03 | A kind of powder coating containing trioctyl trimellitate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310040639.8A CN103131297B (en) | 2013-02-03 | 2013-02-03 | A kind of powder coating containing trioctyl trimellitate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103131297A true CN103131297A (en) | 2013-06-05 |
| CN103131297B CN103131297B (en) | 2016-03-30 |
Family
ID=48491770
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310040639.8A Expired - Fee Related CN103131297B (en) | 2013-02-03 | 2013-02-03 | A kind of powder coating containing trioctyl trimellitate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103131297B (en) |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103483952A (en) * | 2013-09-03 | 2014-01-01 | 安徽精一机械设备有限公司 | Acrylic transparent powder paint |
| CN104017408A (en) * | 2014-06-24 | 2014-09-03 | 玉石塑粉有限公司 | Thermosetting powder coating additive and preparation process thereof as well as coating containing thermosetting powder coating additive |
| CN104177988A (en) * | 2014-07-11 | 2014-12-03 | 安徽桑瑞斯环保新材料有限公司 | Power coating for metal bonding |
| CN104946036A (en) * | 2015-06-25 | 2015-09-30 | 安徽华辉塑业科技有限公司 | Flame-retarding type decorative powder coating material |
| CN105482629A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Powder coating for aluminium profile |
| CN105482630A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Powder coating with high chemical stability |
| CN105482627A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Wear-resisting powder coating |
| CN105482626A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Powder coating for metal plate |
| CN105482628A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Antistatic antiflaming powder coating |
| CN105542618A (en) * | 2015-12-23 | 2016-05-04 | 铜陵市肆得科技有限责任公司 | Powder coating with high performance and high stability |
| CN105985704A (en) * | 2015-12-23 | 2016-10-05 | 铜陵市肆得科技有限责任公司 | High-impact-resistance powder coating |
| CN107474688A (en) * | 2017-08-03 | 2017-12-15 | 安徽真信涂料有限公司 | A kind of interior wall powdery paints |
| CN107815211A (en) * | 2017-10-05 | 2018-03-20 | 镇江泽枫霖建筑材料有限公司 | A kind of preparation technology with high weatherability building materials |
| CN107815212A (en) * | 2017-10-05 | 2018-03-20 | 镇江泽枫霖建筑材料有限公司 | A kind of coating with weather resistance |
| CN107936298A (en) * | 2017-12-12 | 2018-04-20 | 马鞍山市东方仪表有限公司 | A kind of instrument plastic casing filler |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1712473A (en) * | 2004-06-24 | 2005-12-28 | 徐州正菱涂装有限公司 | Epoxy zinc-enriched antiseptic powdery paint and production thereof |
| CN1733853A (en) * | 2005-06-01 | 2006-02-15 | 兰州理工大学 | FBE phenolic modified epoxy powder coating and preparation method thereof |
-
2013
- 2013-02-03 CN CN201310040639.8A patent/CN103131297B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1712473A (en) * | 2004-06-24 | 2005-12-28 | 徐州正菱涂装有限公司 | Epoxy zinc-enriched antiseptic powdery paint and production thereof |
| CN1733853A (en) * | 2005-06-01 | 2006-02-15 | 兰州理工大学 | FBE phenolic modified epoxy powder coating and preparation method thereof |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103483952A (en) * | 2013-09-03 | 2014-01-01 | 安徽精一机械设备有限公司 | Acrylic transparent powder paint |
| CN103483952B (en) * | 2013-09-03 | 2016-06-22 | 安徽精一机械设备有限公司 | A kind of Acrylic transparent powder paint |
| CN104017408A (en) * | 2014-06-24 | 2014-09-03 | 玉石塑粉有限公司 | Thermosetting powder coating additive and preparation process thereof as well as coating containing thermosetting powder coating additive |
| CN104017408B (en) * | 2014-06-24 | 2016-03-02 | 玉石塑粉有限公司 | A kind of thermosetting powder coating(s) auxiliary agent and a kind of coating comprising this auxiliary agent |
| CN104177988A (en) * | 2014-07-11 | 2014-12-03 | 安徽桑瑞斯环保新材料有限公司 | Power coating for metal bonding |
| CN104946036A (en) * | 2015-06-25 | 2015-09-30 | 安徽华辉塑业科技有限公司 | Flame-retarding type decorative powder coating material |
| CN105482626A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Powder coating for metal plate |
| CN105482627A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Wear-resisting powder coating |
| CN105482630A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Powder coating with high chemical stability |
| CN105482628A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Antistatic antiflaming powder coating |
| CN105542618A (en) * | 2015-12-23 | 2016-05-04 | 铜陵市肆得科技有限责任公司 | Powder coating with high performance and high stability |
| CN105482629A (en) * | 2015-12-23 | 2016-04-13 | 铜陵市肆得科技有限责任公司 | Powder coating for aluminium profile |
| CN105985704A (en) * | 2015-12-23 | 2016-10-05 | 铜陵市肆得科技有限责任公司 | High-impact-resistance powder coating |
| CN107474688A (en) * | 2017-08-03 | 2017-12-15 | 安徽真信涂料有限公司 | A kind of interior wall powdery paints |
| CN107815211A (en) * | 2017-10-05 | 2018-03-20 | 镇江泽枫霖建筑材料有限公司 | A kind of preparation technology with high weatherability building materials |
| CN107815212A (en) * | 2017-10-05 | 2018-03-20 | 镇江泽枫霖建筑材料有限公司 | A kind of coating with weather resistance |
| CN107936298A (en) * | 2017-12-12 | 2018-04-20 | 马鞍山市东方仪表有限公司 | A kind of instrument plastic casing filler |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103131297B (en) | 2016-03-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103131297A (en) | Powder coating with trioctyl trimellitate | |
| CN103131298B (en) | A kind of Flame Retardant Powder Coatings containing hydration zinc borate | |
| CN103131301B (en) | A kind of preparation method of the powder coating containing polyvinyl alcohol | |
| CN103131299B (en) | A kind of powder coating containing nano titanium oxide | |
| CN103571413B (en) | Dry-hanging stone curtain wall epoxy adhesive and preparation method thereof | |
| CN103131302A (en) | Powder coating with hydroxypropyl methyl cellulose | |
| CN105176002B (en) | A kind of impervious leakage-stopping environment-friendly epoxy grouting material | |
| CN103131304B (en) | Powder coating containing modified carbide slag | |
| CN103483993A (en) | Low-temperature curing powder paint | |
| CN103289535A (en) | Powdery paint containing bamboo charcoal powder | |
| CN103131303A (en) | Powder coating with fungacetin | |
| CN103205177B (en) | A kind of preparation method of powder coating containing dibutyl phthalate | |
| CN102977768B (en) | Metal antirust paint prepared from modified phenolic resin, and its preparation method | |
| CN103289539A (en) | Preparation method of modified fluorite slag-containing powdery paint | |
| CN110015863B (en) | Modifier for water glass for casting sand mold of electric melting brick and modified water glass prepared by modifier | |
| CN104355591B (en) | A kind of green heat-insulation wall plate and preparation method thereof | |
| CN103289536A (en) | Powdery paint containing tree ash | |
| CN106281029A (en) | A kind of macromolecule high resiliency environment-friendly materials | |
| CN103205178A (en) | Preparation method for powder coating containing ethyl acetate | |
| CN103497633A (en) | Constructional powdery paint | |
| CN103289537A (en) | Powdery paint containing butyl acrylate monomer | |
| CN103131300B (en) | A kind of preparation method of the powder coating containing terpine resin T110 | |
| CN106281030A (en) | A kind of environment-friendly type multiple-effect high-molecular damping material | |
| CN103696285B (en) | A kind of random grain gas mold materials pigment liquid and application thereof | |
| CN103555149A (en) | Powder coating for radiator shell |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160224 Address after: 1101, room 230022, building A, Sino Swiss building, 9 Hongfeng Road, Hefei, Anhui Applicant after: Chuzhou Xincai Printing Co., Ltd. Address before: The new town of Anhui province Wuhu City fan 241200 Fanchang County Economic Development Office Applicant before: Ni Jinpei |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Huang Tao Inventor after: Ren Hailan Inventor before: Ni Jinpei |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170725 Address after: South West Road 519050 South Town Guangdong city Zhuhai province 596 No. 10 building 101-20 room Patentee after: Zhuhai United New Material Co. Ltd. Gaolan Address before: 1101, room 230022, building A, Sino Swiss building, 9 Hongfeng Road, Hefei, Anhui Patentee before: ANHUI VMWAY INFORMATION TECHNOLOGY CO.,LTD. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160330 Termination date: 20210203 |