CN103114445A - Shrink-proof finishing agent for wool fabrics and preparation method thereof - Google Patents
Shrink-proof finishing agent for wool fabrics and preparation method thereof Download PDFInfo
- Publication number
- CN103114445A CN103114445A CN 201210442861 CN201210442861A CN103114445A CN 103114445 A CN103114445 A CN 103114445A CN 201210442861 CN201210442861 CN 201210442861 CN 201210442861 A CN201210442861 A CN 201210442861A CN 103114445 A CN103114445 A CN 103114445A
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- CN
- China
- Prior art keywords
- parts
- shrink
- ethylene glycol
- preparation
- citric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 210000002268 wool Anatomy 0.000 title claims abstract description 28
- 239000004744 fabric Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 36
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 36
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims abstract description 24
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims abstract description 18
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910001629 magnesium chloride Inorganic materials 0.000 claims abstract description 9
- 239000000661 sodium alginate Substances 0.000 claims abstract description 9
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 9
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 9
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 16
- 229920002101 Chitin Polymers 0.000 claims description 11
- 239000000047 product Substances 0.000 claims description 9
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 8
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 8
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 8
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 8
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 8
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 3
- 229920001661 Chitosan Polymers 0.000 abstract 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 abstract 1
- SNAAJJQQZSMGQD-UHFFFAOYSA-N aluminum magnesium Chemical compound [Mg].[Al] SNAAJJQQZSMGQD-UHFFFAOYSA-N 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 229920003063 hydroxymethyl cellulose Polymers 0.000 abstract 1
- 229940031574 hydroxymethyl cellulose Drugs 0.000 abstract 1
- 238000011282 treatment Methods 0.000 description 3
- 239000000835 fiber Substances 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000009950 felting Methods 0.000 description 1
- 210000004209 hair Anatomy 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a shrink-proof finishing agent for wool fabrics and a preparation method thereof. The shrink-proof finishing agent for wool fabrics is prepared from the following components in parts by weight: 3-5 parts of citric acid, 3-6 parts of magnesium chloride, 1-3 parts of hydroxymethyl cellulose, 1-3 parts of sodium alginate, 2-5 parts of magnesium aluminum silicate, 10-30 parts of chitosan, 2-5 parts of sodium bicarbonate, 10-20 parts of ethylene glycol, 1-3 parts of dibutyl phthalate and 100-180 parts of water. Compared with the prior art, the shrink-proof finishing agent for wool fabrics does not need pretreatment, and has favorable compatibility with dye assistants for wool; and the preparation method has the advantages of simple technique and low cost.
Description
Technical field
The invention belongs to the textile auxiliary technical field, more specifically relate to a kind of wool fabric shrink-resistant agent and preparation method thereof.
Background technology
Wool fibre has many premium properties, and its shortcoming is that wool fabric felting and fluffiness can occur when washing, and main cause is that wool surface has Microstructure of epidermal scale.Therefore, the shiinkproof finish of wool scale layer structure is the important research object of wool processing.The shiinkproof finish of wool fabric mainly contains two kinds of methods, and the one, adopt chemical treatments the phosphorus sheet of wool surface partly to be removed or removed fully, be called for short subtraction; Next is to adopt polymer treatment, and the scale on wool top layer is wrapped by, and mutually bonding between fiber, thereby gives its shrink resistance, is called for short addition.
Summary of the invention
The object of the invention is to overcome the deficiency that prior art exists, a kind of wool fabric shrink-resistant agent is provided.
Another object of the present invention is to provide the preparation method of this wool fabric shrink-resistant agent.
For achieving the above object, the present invention has taked following technical scheme:
A kind of wool fabric shrink-resistant agent in weight portion, consists of the following composition:
Citric acid: 3～5, magnesium chloride: 3～6, Carboxymethyl Cellulose: 1～3,
Sodium alginate: 1～3, Magnesiumaluminumsilicate: 2～5, chitin: 10～30,
Sodium bicarbonate: 2～5, ethylene glycol: 10～20, dibutyl phthalate: 1～3,
Water: 100～180.
In technique scheme, the preparation technology of described wool fabric shrink-resistant agent is as follows:
(1) dibutyl phthalate is added to the water, mixes;
(2) citric acid, chitin, ethylene glycol are mixed, stir;
(3) product with step (1) mixes with the product of step (2), stirring reaction 1～3 hour;
(4) add all the other components, get final product to get product after mixing.
Compared with prior art, the present invention has following beneficial effect:
(1) need not preliminary treatment, and good with the compatibility of color additive with hair;
(2) preparation technology is easy, and is with low cost.
The specific embodiment
The invention will be further described below in conjunction with specific embodiment, but the present invention's scope required for protection is not limited to the scope that embodiment describes.
Embodiment 1
A kind of wool fabric shrink-resistant agent in weight portion, consists of the following composition:
Citric acid: 3, magnesium chloride: 3, Carboxymethyl Cellulose: 1,
Sodium alginate: 1, Magnesiumaluminumsilicate: 2, chitin: 10,
Sodium bicarbonate: 2, ethylene glycol: 10, dibutyl phthalate: 1, water: 100.
Embodiment 2
A kind of wool fabric shrink-resistant agent in weight portion, consists of the following composition:
Citric acid: 5, magnesium chloride: 6, Carboxymethyl Cellulose: 3,
Sodium alginate: 3, Magnesiumaluminumsilicate: 5, chitin: 30,
Sodium bicarbonate: 5, ethylene glycol: 20, dibutyl phthalate: 3, water: 180.
Embodiment 3
A kind of wool fabric shrink-resistant agent in weight portion, consists of the following composition:
Citric acid: 4, magnesium chloride: 5, Carboxymethyl Cellulose: 2,
Sodium alginate: 2, Magnesiumaluminumsilicate: 4, chitin: 20,
Sodium bicarbonate: 3, ethylene glycol: 16, dibutyl phthalate: 2, water: 160.
In above-described embodiment, the preparation method of described a kind of wool fabric shrink-resistant agent comprises the steps:
(1) dibutyl phthalate is added to the water, mixes;
(2) citric acid, chitin, ethylene glycol are mixed, stir;
(3) product with step (1) mixes with the product of step (2), stirring reaction 1～3 hour;
(4) add all the other components, get final product to get product after mixing.
Claims (5)
1. a wool fabric shrink-resistant agent, is characterized in that, in weight portion, consists of the following composition:
Citric acid: 3～5, magnesium chloride: 3～6, Carboxymethyl Cellulose: 1～3,
Sodium alginate: 1～3, Magnesiumaluminumsilicate: 2～5, chitin: 10～30,
Sodium bicarbonate: 2～5, ethylene glycol: 10～20, dibutyl phthalate: 1～3,
Water: 100～180.
2. a kind of wool fabric shrink-resistant agent according to claim 1, is characterized in that, in weight portion, consists of the following composition:
Citric acid: 3, magnesium chloride: 3, Carboxymethyl Cellulose: 1,
Sodium alginate: 1, Magnesiumaluminumsilicate: 2, chitin: 10,
Sodium bicarbonate: 2, ethylene glycol: 10, dibutyl phthalate: 1, water: 100.
3. a kind of wool fabric shrink-resistant agent according to claim 1, is characterized in that, in weight portion, consists of the following composition:
Citric acid: 5, magnesium chloride: 6, Carboxymethyl Cellulose: 3,
Sodium alginate: 3, Magnesiumaluminumsilicate: 5, chitin: 30,
Sodium bicarbonate: 5, ethylene glycol: 20, dibutyl phthalate: 3, water: 180.
4. a kind of wool fabric shrink-resistant agent according to claim 1, is characterized in that, in weight portion, consists of the following composition:
Citric acid: 4, magnesium chloride: 5, Carboxymethyl Cellulose: 2,
Sodium alginate: 2, Magnesiumaluminumsilicate: 4, chitin: 20,
Sodium bicarbonate: 3, ethylene glycol: 16, dibutyl phthalate: 2, water: 160.
5. the preparation method of a kind of wool fabric shrink-resistant agent claimed in claim 1, is characterized in that, comprises the steps:
(1) dibutyl phthalate is added to the water, mixes;
(2) citric acid, chitin, ethylene glycol are mixed, stir;
(3) product with step (1) mixes with the product of step (2), stirring reaction 1～3 hour;
(4) add all the other components, get final product to get product after mixing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210442861 CN103114445A (en) | 2012-11-08 | 2012-11-08 | Shrink-proof finishing agent for wool fabrics and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210442861 CN103114445A (en) | 2012-11-08 | 2012-11-08 | Shrink-proof finishing agent for wool fabrics and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103114445A true CN103114445A (en) | 2013-05-22 |
Family
ID=48412866
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201210442861 Withdrawn CN103114445A (en) | 2012-11-08 | 2012-11-08 | Shrink-proof finishing agent for wool fabrics and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103114445A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103422349A (en) * | 2013-08-02 | 2013-12-04 | 吴江市七都镇庙港雅迪针织制衣厂 | Woolen sweater treating liquid containing sodium alginate |
| CN103741452A (en) * | 2013-12-17 | 2014-04-23 | 江苏金太阳纺织科技有限公司 | Shirt finishing liquid and preparation method |
| CN105648779A (en) * | 2016-04-01 | 2016-06-08 | 吴江福汇缘家纺有限公司 | Anti-hairfalling antistatic finishing agent and preparation method thereof |
| CN105638757A (en) * | 2016-01-19 | 2016-06-08 | 黄伟洪 | Clothing drying and mold preventing bactericide |
| CN109610156A (en) * | 2018-12-04 | 2019-04-12 | 山东如意科技集团有限公司 | A kind of worsted cashmere facing anti-crease finishing technique |
-
2012
- 2012-11-08 CN CN 201210442861 patent/CN103114445A/en not_active Withdrawn
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103422349A (en) * | 2013-08-02 | 2013-12-04 | 吴江市七都镇庙港雅迪针织制衣厂 | Woolen sweater treating liquid containing sodium alginate |
| CN103741452A (en) * | 2013-12-17 | 2014-04-23 | 江苏金太阳纺织科技有限公司 | Shirt finishing liquid and preparation method |
| CN103741452B (en) * | 2013-12-17 | 2015-09-30 | 顾祥茂 | A kind of shirt dressing liquid and preparation method thereof |
| CN105638757A (en) * | 2016-01-19 | 2016-06-08 | 黄伟洪 | Clothing drying and mold preventing bactericide |
| CN105648779A (en) * | 2016-04-01 | 2016-06-08 | 吴江福汇缘家纺有限公司 | Anti-hairfalling antistatic finishing agent and preparation method thereof |
| CN109610156A (en) * | 2018-12-04 | 2019-04-12 | 山东如意科技集团有限公司 | A kind of worsted cashmere facing anti-crease finishing technique |
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| PB01 | Publication | ||
| C04 | Withdrawal of patent application after publication (patent law 2001) | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20130522 |