CN102727658A - Chinese herbal extract with anti-dropping and oil-controlling effects, preparation method and application thereof - Google Patents
Chinese herbal extract with anti-dropping and oil-controlling effects, preparation method and application thereof Download PDFInfo
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Abstract
The invention discloses a Chinese herbal extract with anti-dropping and oil-controlling effects. Active components of the Chinese herbal extract are prepared from the following raw materials of: by weight, 10-20 parts of red sage root, 5-10 parts of Chinese angelica, 10-15 parts of sophora flavescens, 5-8 parts of Ligusticum wallichii, 5-8 parts of matrimony vine, 5-10 parts of pericarpium zanthoxyli, 4-8 parts of ligustrum lucidum, 10-15 parts of radix scrophulariae, 5-8 parts of bitter orange and 6-10 parts of root of kudzu vine. The Chinese herbal extract provided by the invention has good anti-dropping and oil-controlling effects. Its preparation method is simple. The product obtained is green and safe, has substantial efficacy, and is in favor of stimulating hair follicle, activating scalp cells and enhance blood circulation. The Chinese herbal extract itself has effects of invigorate blood circulation, promoting qi, preventing hair dropping and controlling oil, and especially has a better curative effect in allusion to seborrheic alopecia.
Description
Technical field
The present invention relates to a kind of Chinese medicine extract and preparation method thereof and application with anticreep control oil effect.
Background technology
Clinical common alopecia has two kinds of alopecia areata and seborrheic alopecia.Alopecia areata is claimed circular alopecia again, and the traditional Chinese medical science is called " alopecia areata ", " alopecia areata ", is a kind of speckle shape alopecia that takes place suddenly, the lighter's alopecia in the form of sheets, but weight person's alopecia totalis or alopecia universalis.It is relevant with autoimmune situation, heredity and Nervous and Mental Factors that pathogenic factor is thought.Seborrheic alopecia is called androgenetic alopecia again, is one of modal alopecia reason, and men and women's both sexes all have generation; Incidence rate is very high in male colony; Androgenetic alopecia can take place in the time of 50 years old in 50% male, though along with the increase occurrence probability at the age 70% seborrheic alopecia no conscious sympton that rises, bigger to alopecia people's psychological impact; And might influence its daily life along with growth in the living standard, people also more pay attention to alopeciaing therapeutic.
Chinese medicine mainly is the tincture of Chinese medicine being processed hair growth promoting to the external treatment of alopecia, makes medicine directly act on the affected part, and certain stimulation is played in the part; Thereby promote the blood circulation of local skin, improve trichotrophy, promote hair growth and drug absorption; Through Transdermal absorption, also can produce general action.General initial effect shows as hair strengthening, promptly stops alopecia or alopecia and reduces, and occurs hair growth promoting, long hair subsequently, promptly bears the fine hair on birds or animals galley proof earlier and sends out, and gradually becomes terminal hair again, or the fine hair on birds or animals galley proof is sent out blackening gradually, thick, hard, long.In addition scalp itch, dandruff, sebum too much all there is therapeutical effect in various degree.
Therefore, on safety, healthy health preserving basis, combine China's Chinese medicine theory,, prepare through compound recipe that to develop the anticreep hair care formulations with fine effect be the focus that those skilled in the art study according to monarch, minister, the traditional Chinese medical science thought helping, make.
Summary of the invention
The objective of the invention is to propose a kind of Chinese medicine composition and application thereof with the oily effect of good anticreep hair care control.
Compositions with the oily effect of anticreep hair care control provided by the present invention, its active component is processed by the former medicine of following portions by weight ratio:
Radix Salviae Miltiorrhizae 10～20 weight portions, Radix Angelicae Sinensis 5～10 weight portions, Radix Sophorae Flavescentis 10～15 weight portions, Rhizoma Chuanxiong 5～8 weight portions, Fructus Lycii 5～8 weight portions, Fructus Zanthoxyli 5～10 weight portions, Fructus Ligustri Lucidi 4～8 weight portions, Radix Scrophulariae 10～15 weight portions, Fructus Aurantii Immaturus 5～8 weight portions, Radix Puerariae 6～10 weight portions.
Its active component of said compositions is preferably processed by the former medicine of following portions by weight ratio:
Radix Salviae Miltiorrhizae 20 weight portions, Radix Angelicae Sinensis 10 weight portions, Radix Sophorae Flavescentis 15 weight portions, Rhizoma Chuanxiong 8 weight portions, Fructus Lycii 5 weight portions, Fructus Zanthoxyli 5 weight portions, Fructus Ligustri Lucidi 4 weight portions, Radix Scrophulariae 10 weight portions, Fructus Aurantii Immaturus 8 weight portions, Radix Puerariae 10 weight portions.
The present invention also provides above-mentioned method for preparing with Chinese medicine composition of the oily effect of anticreep hair care control.This method comprises the steps:
1) take by weighing each former medicine according to claim 1 or 2 described proportionings, after former medicine was mixed, pulverizer was pulverized;
2) the former medicine of Chinese medicine after pulverizing in the step 1) is joined in the alcoholic solution, soaked 1-2 hour;
3) agitating heating is extracted, and extracting temperature is 65-75 ℃, extracts 2 hours;
4) room temperature staticly settled 2-4 hour, got supernatant, and coarse filtration is centrifugal, gets supernatant, and the supernatant clarification is bright to be light red;
5) supernatant that step 4) is obtained places rotary evaporator to concentrate, and removes ethanol, is condensed into rare extractum shape, obtains peony to dark brown thick liquid, is Chinese medicine extract.
In the said step 1), said pulverizing is that said former medicated powder is broken to granular size is 20 orders-60 orders; Said step 2) in, the concentration expressed in percentage by volume of said alcoholic solution is 90-95%, is preferably 95%, and the ratio of former medicine of said Chinese medicine and alcoholic solution is 1g: (15-25) ml is preferably 1g:20ml.
Filter in the said step (4) is that 100～200 mesh filter screens filter; 5000 rev/mins of centrifugal rotational speeds, the time is 10 minutes.
In the said step (5), said spissated temperature is 55 ℃～60 ℃, specifically can be 55 ℃ or 60 ℃.
The hair care formulations that is active component with above-mentioned compositions with the oily effect of anticreep hair care control also belongs to protection scope of the present invention.Like tincture, shampoo or hair conditioner etc.
Wherein, said shampoo can be processed by following component:
Laureth sulfuric ester ammonium 20%; Fatty acid distribution of coconut oil single ethanol amide 1%; Dodecanamide propyl betanin 4%; Guar hydroxypropyltrimonium chloride 0.2%; Disodiumedetate 0.1%; Cetearyl alcohol 0.5%; Dimethyl siloxane 2%; Above-mentioned Chinese medicine composition 1-2%; Methylchloroisothiazandnone or Methylisothiazolinone 0.1%; Ethylene glycol stearate or glycol distearate 2%; Surplus is a water, and said % is meant the quality percentage composition.
The mass percent concentration in shampoo of above-mentioned Chinese medicine composition is preferably 1%.
The method for preparing of above-mentioned shampoo comprises the steps:
1) according to the component of above-mentioned shampoo, make material dissolution complete 60 ℃ of stirrings of heating in the laureth sulfuric ester ammonium adding part water;
2) according to the component of above-mentioned shampoo; With fatty acid distribution of coconut oil single ethanol amide, dodecanamide propyl betanin, guar hydroxypropyltrimonium chloride, disodiumedetate be added to stir in the part water after; Add in the solution of step 1) acquisition; Be heated to 80-85 ℃, homogenizing 3min stirs cooling; The cooling back adds the Chinese medicine composition of any preparation among cetearyl alcohol, dimethyl siloxane and cocamido propyl betaine, the claim 3-5; Stir; After adding methylchloroisothiazandnone or Methylisothiazolinone, ethylene glycol stearate or glycol distearate again; Supply water, mixing obtains shampoo.
Invention thinking of the present invention is: be the basis with the Chinese medical science theory; With human hair health is aim; According to monarch, minister, the traditional Chinese medical science prescription thought helping, make; With Chinese herbal medicine Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Chuanxiong, Fructus Lycii, Fructus Zanthoxyli, Fructus Ligustri Lucidi, Radix Scrophulariae, Fructus Aurantii Immaturus, Radix Puerariae effective combination together, and be main functional additive, be aided with the formulated Chinese medicine anticreep shampoo of matrix components commonly used in the shampoo with the prescription Chinese medicine extract.The natural gentleness of Chinese medicine treatment according to the invention, safe and non-stimulating, and, nourish transdermal very easily by skin absorbs, reach the effect that prevents alopecia, promotes hair growth and scalp control oil.
Beneficial effect of the present invention: Chinese medicine extract of the present invention has the oily effect of good anticreep hair care control, and method for preparing is easy, the products obtained therefrom green safety, and effect is remarkable, helps hair follicle stimulating, the activation scalp cells, and strengthen blood circulation.Chinese medicine extract itself has blood-activating and qi-promoting, prevents alopecia and controls oily effect, especially to seborrheic alopecia better therapeutic is arranged.
Description of drawings
Fig. 1 is Chinese medicine shampoo treatment alopecia 120 routine clinical observation result provided by the invention;
Fig. 2 is that Chinese medicine shampoo provided by the invention suppresses scalp fat secretion design sketch.
The specific embodiment
Embodiment 1, the present invention have the preparation of the Chinese medicine extract of anticreep control oil effect
1) take by weighing each crude drug according to following proportioning:
Radix Salviae Miltiorrhizae 20g, Radix Angelicae Sinensis 10g, Radix Sophorae Flavescentis 15g, Rhizoma Chuanxiong 8g, Fructus Lycii 5g, Fructus Zanthoxyli 5g, Fructus Ligustri Lucidi 4g, Radix Scrophulariae 10g, Fructus Aurantii Immaturus 8g, Radix Puerariae 10g;
2) after Chinese medicine mixed, pulverizer was pulverized, and is crushed to 20 orders-60 order.
3) to join concentration expressed in percentage by volume be that the ratio of Chinese medicine and alcoholic solution is 1g:20ml, soaks 1 hour in 95% the alcoholic solution to the Chinese medicine after will pulverizing.
4) agitating heating is extracted, and extracting temperature is 75 ℃, extracts 2h.
5) room temperature staticly settled 4 hours, got supernatant, 100 mesh filter screen coarse filtrations, and 5000 rev/mins, centrifugal 10 minutes, get supernatant, the supernatant clarification is bright to be light red.
6) supernatant that step 5) is obtained places rotary evaporator to concentrate, and removes ethanol, is condensed into rare extractum shape, is peony to dark brown thick liquid, and density is 1.10-1.30.The density calculation method is: Chinese medicine extract density=quality (g)/volume (ml).
The preparation of embodiment 2 Chinese medicine extract of the present invention
1) take by weighing each crude drug according to following proportioning:
Radix Salviae Miltiorrhizae 10g, Radix Angelicae Sinensis 5g, Radix Sophorae Flavescentis 10g, Rhizoma Chuanxiong 5g, Fructus Lycii 8g, Fructus Zanthoxyli 10g, Fructus Ligustri Lucidi 8g, Radix Scrophulariae 15g, Fructus Aurantii Immaturus 8g, Radix Puerariae 5g;
2) after Chinese medicine mixed, pulverizer was pulverized.Be crushed to 20 orders-60 order.
3) to join concentration expressed in percentage by volume be that the ratio of Chinese medicine and alcoholic solution is 1g:15ml, soaks 2 hours in 90% the alcoholic solution to the Chinese medicine after will pulverizing;
4) agitating heating is extracted, and extracting temperature is 70 ℃.Extract 2h.
Room temperature staticly settled 2 hours, got supernatant, 150 mesh filter screen coarse filtrations, 5000 rev/mins centrifugal 10 minutes, get supernatant, supernatant clarification is bright to be light red.
6) supernatant that step 5) is obtained places rotary evaporator to concentrate, and removes ethanol, is condensed into rare extractum shape, is peony to dark brown thick liquid, and density is 1.10-1.30; The density calculation method is: Chinese medicine extract density=quality (g)/volume (ml).
The preparation of embodiment 3 Chinese medicine extract of the present invention
1) take by weighing each crude drug according to following proportioning:
Radix Salviae Miltiorrhizae 15g, Radix Angelicae Sinensis 8g, Radix Sophorae Flavescentis 12g, Rhizoma Chuanxiong 7g, Fructus Lycii 6g, Fructus Zanthoxyli 8g, Fructus Ligustri Lucidi 6g, Radix Scrophulariae 12g, Fructus Aurantii Immaturus 6g, Radix Puerariae 8g;
2) after Chinese medicine mixed, pulverizer was pulverized.Be crushed to 20 orders-60 order.
3) to join concentration expressed in percentage by volume be that the ratio of Chinese medicine and alcoholic solution is 1g:25ml, soaks 2 hours in 95% the alcoholic solution to the Chinese medicine after will pulverizing;
4) agitating heating is extracted, and extracting temperature is 65 ℃.Extract 2h.
5) room temperature staticly settled 3 hours, got supernatant, 200 mesh filter screen coarse filtrations, 5000 rev/mins centrifugal 10 minutes, get supernatant, supernatant clarification is bright to be light red.
Supernatant places rotary evaporator to concentrate, and removes ethanol, is condensed into rare extractum shape, is peony to dark brown thick liquid, and density is 1.10-1.30; The density calculation method is: Chinese medicine extract density=quality (g)/volume (ml).
Embodiment 4, be the preparation of the shampoo of active component with Chinese medicine extract of the present invention
Raw material components according to table 1 prepares shampoo, and concrete steps are described below:
1), is mixed into the mixture of A, B, C, D phase respectively according to the component of the A in the table 1, B, C, D phase.
2) A being added in the part water 60 ℃ of stirrings of heating makes material dissolution complete;
3) with B be added to the back that stirs in the remainder water add A mutually in, be heated to 80-85 ℃, homogenizing 3min stirs cooling.The cooling back adds the C phase, stirs, and adds the D phase again, and the Chinese medicine extract that obtains respectively behind the mixing with embodiment 1, embodiment 2 or embodiment 3 is the shampoo of active component.
The raw material components of table 1. shampoo
One, Chinese medicine shampoo treatment alopecia 120 routine clinical observations provided by the invention
Experiment purpose: choose seborrheic alopecia crowd (men and women does not limit), respectively (trial edition invention Chinese medicine ingredients shampoo is that the shampoo (method for preparing of shampoo such as embodiment 4 are said) of active component is identical with number of times with matched group (trying out commercially available shampoo) trial method with the Chinese medicine extract of embodiment 1, embodiment 2 or embodiment 3 to the contrived experiment group.Method: hair is drenched, and is placed on rubbing on hand with the shampoo of monobasic coin-size and bubbles, and is put on then to begin to crumple hair on the hair; If feel not have wash clean, the method for reuse front is washed, and consumption is the half the of front; After once with referring to the abdominal massage scalp, rinse with clear water.General two days once.
Observe " alopecia situation ", " scalp fat secretion situation ", " the anti-dandruff situation " of two groups of crowds before and after on probation, analyze the present invention's preparation Chinese medicine ingredients shampoo anticreep and control oily effect.
Experimentation: experimental group crowd age 18-60 one full year of life, the men and women does not limit, and the form of taking to go into group is at random carried out.Case load 120, wherein experimental group is 80 examples, matched group is 40 examples.With the Chinese medicine extract of embodiment 1, embodiment 2 or embodiment 3 is that the shampoo of active component is on probation to above-mentioned experiment crowd successively, all establishes matched group at every turn.
Evaluation criterion: through patient's readme impression, human experimentation and naked eyes visual experiment.Effectively: the amount of losing hair reduces during hair washing, the hair quality hardening, and the scalp fat secretion reduces.It is fine and better effectively being divided into two grades, and fine the scalp greasy feeling alleviates greatly for the alopecia amount significantly reduces before the use, and the dandruff significantly reduces; Be preferably and reduce to some extent before the alopecia amount is used, the scalp greasy feeling alleviates, and the dandruff reduces to some extent.Not obvious: the no significant change of sensation before and after using.Relatively poor: as to use the no any variation in back.
The result is of table 2-table 7, the result show the Chinese medicine extract with embodiment 1, embodiment 2 or embodiment 3 be the shampoo of active component at the effective percentage of anti-alopecia and control oil all more than 80%.
Table 2. is the shampoo trial effect statistical table of active component with the Chinese medicine extract of embodiment 1
| Effect/evaluation (test group) | Fine | Better | Not obvious | Relatively poor | Do not know | Effective percentage |
| The anticreep condition of oestrusing | 32 | 40 | 8 | 0 | 0 | 90% |
| Control oily situation | 39 | 31 | 10 | 0 | 0 | 87.5% |
| Control oily persistency | 36 | 31 | 13 | 0 | 0 | 83.75% |
| Anti-dandruff situation | 29 | 27 | 22 | 2 | 0 | 70% |
Table 3. contrast shampoo trial effect statistical table
| Effect/evaluation (matched group) | Fine | Better | Not obvious | Relatively poor | Do not know | Effective percentage |
| The anticreep condition of oestrusing | 8 | 13 | 16 | 3 | 0 | 52.5% |
| Control oily situation | 6 | 16 | 15 | 3 | 0 | 55% |
| Control oily persistency | 2 | 10 | 19 | 6 | 0 | 30% |
| Anti-dandruff situation | 6 | 18 | 12 | 6 | 0 | 60% |
Table 4. is the shampoo trial effect statistical table of active component with the Chinese medicine extract of embodiment 2
| Effect/evaluation (test group) | Fine | Better | Not obvious | Relatively poor | Do not know | Effective percentage |
| The anticreep condition of |
30 | 39 | 11 | 0 | 0 | 86.25% |
| Control oily situation | 41 | 30 | 9 | 0 | 0 | 88.75% |
| Control |
35 | 30 | 15 | 0 | 0 | 81.25% |
| Anti-dandruff situation | 28 | 30 | 20 | 2 | 0 | 72.5% |
Table 5. contrast shampoo trial effect statistical table
| Effect/evaluation (matched group) | Fine | Better | Not obvious | Relatively poor | Do not know | Effective percentage |
| The anticreep condition of oestrusing | 9 | 15 | 15 | 1 | 0 | 56% |
| Control oily situation | 10 | 16 | 12 | 2 | 0 | 65% |
| Control oily persistency | 3 | 12 | 20 | 5 | 0 | 37.5% |
| Anti-dandruff situation | 8 | 18 | 12 | 2 | 0 | 65% |
Table 6. is the shampoo trial effect statistical table of active component with the Chinese medicine extract of embodiment 3
| Effect/evaluation (test group) | Fine | Better | Not obvious | Relatively poor | Do not know | Effective percentage |
| The anticreep condition of oestrusing | 32 | 39 | 9 | 0 | 0 | 88.75% |
| Control oily situation | 42 | 28 | 10 | 0 | 0 | 87.5% |
| Control oily persistency | 36 | 32 | 12 | 0 | 0 | 85% |
| Anti-dandruff situation | 26 | 31 | 21 | 2 | 0 | 71.25% |
Table 7. contrast shampoo trial effect statistical table
| Effect/evaluation (matched group) | Fine | Better | Not obvious | Relatively poor | Do not know | Effective percentage |
| The anticreep condition of oestrusing | 10 | 16 | 14 | 0 | 0 | 65% |
| Control oily situation | ?8 | 15 | 11 | 2 | 0 | 57.5% |
| Control oily persistency | ?5 | 12 | 13 | 5 | 0 | 42.5% |
| Anti-dandruff situation | ?9 | 16 | 13 | 2 | 0 | 62.5% |
Two, Chinese medicine shampoo provided by the invention suppresses scalp fat secretion effect test
1, experimental principle
Human experimentation is chosen the seborrheic alopecia crowd as the experimenter, and test subject is used the variation of Chinese medicine shampoo front and back leather point haze wax fat content, thereby confirms the oily effect of control.
2, experimental apparatus and sample
Experimental apparatus: skin oil and fat tester
3, experiment crowd
The experimenter amounts to 40 people.Concrete sex composition and age structure are confirmed at random; The result does not find untoward reaction.
4, experimental technique
The form of taking to go into group is at random carried out, and selects experimenter's scalp to receive the examination zone.Each 20 people of sample sets and matched group; Sample component sample 1 and sample 2; Wherein sample 1 is the shampoo (method for preparing is seen embodiment 4) of active component preparation for the Chinese medicine extract with embodiment 1 preparation; Sample 2 is the shampoo (method for preparing is seen embodiment 4) of active component preparation for the Chinese medicine extract with embodiment 2 preparations; Sample 3 is the shampoo (method for preparing is seen embodiment 4) of active component preparation for the Chinese medicine extract with embodiment 3 preparations, and sample 4 is commercially available shampoo.Matched group is not add drug extract still adds other component according to the method for embodiment 4 shampoo.
The technical staff uses skin oil and fat tester
test test position 3-5 time; Average the blank value of data acquisition for the first time.
Test the position the experimenter and use sample, and tried the fat content at position.
The experimenter is using sample after 1,2,4 hours continuously; Use skin oil and fat tester
to measure 3-5 time by the technical staff, average.
The experimenter was using sample the 7th day, the 14th day, the 21st day, the 28th day continuously; Use skin oil and fat tester
to measure 3-5 time by the technical staff, average.
The numerical value that statistics records adopts averaging method, analyzing skin fat secretion Changing Pattern and persistency.
Five, experimental result
The fat content variation is reflected in test period Experimental Area fat content change with time.Its value is big more, and fat content is big more, otherwise fat content is more little.
Each time point oil content (T behind fat content difference (Δ T)=use product
hOil content (T before)-the use product
0).
Table 8. uses the difference between shampoo of the present invention back haze wax fat content and the initial value
From last table 8, can find out; After sample 1, sample 2, sample 3 and sample 4 used, the difference of fat content was lower than blank control group always, with respect to sample 4; Sample 1, sample 2, sample 3 differences are relatively little, show that sample 1, sample 2, sample 3 press down the fat more remarkable effect.
As can be seen from Figure 2, along with the prolongation of time, the effect that Chinese medicine shampoo (sample 1, sample 2 and sample 3) suppresses the scalp fat secretion is obvious more.This is also consistent with the human body test, and the obvious person of control oil feels that obviously scalp is dry among the experimenter crowd, and the secretion oil quantity significantly reduces.
Claims (10)
1. one kind has the compositions that the anticreep hair care is controlled oily effect, and its active component is processed by the former medicine of following portions by weight ratio:
Radix Salviae Miltiorrhizae 10～20 weight portions, Radix Angelicae Sinensis 5～10 weight portions, Radix Sophorae Flavescentis 10～15 weight portions, Rhizoma Chuanxiong 5～8 weight portions, Fructus Lycii 5～8 weight portions, Fructus Zanthoxyli 5～10 weight portions, Fructus Ligustri Lucidi 4～8 weight portions, Radix Scrophulariae 10～15 weight portions, Fructus Aurantii Immaturus 5～8 weight portions, Radix Puerariae 6～10 weight portions.
2. compositions according to claim 1, its active component of said compositions is processed by the former medicine of following portions by weight ratio:
Radix Salviae Miltiorrhizae 20 weight portions, Radix Angelicae Sinensis 10 weight portions, Radix Sophorae Flavescentis 15 weight portions, Rhizoma Chuanxiong 8 weight portions, Fructus Lycii 5 weight portions, Fructus Zanthoxyli 5 weight portions, Fructus Ligustri Lucidi 4 weight portions, Radix Scrophulariae 10 weight portions, Fructus Aurantii Immaturus 8 weight portions, Radix Puerariae 10 weight portions.
3. the method for preparing with Chinese medicine extract of the oily effect of anticreep hair care control comprises the steps:
1) take by weighing each former medicine according to claim 1 or 2 described proportionings, after former medicine was mixed, pulverizer was pulverized;
2) the former medicine of Chinese medicine after pulverizing in the step 1) is joined in the alcoholic solution, soaked 1-2 hour;
3) agitating heating is extracted, and extracting temperature is 65-75 ℃, extracts 2 hours;
4) room temperature staticly settled 2-4 hour, got supernatant, filtered, and is centrifugal, gets supernatant;
5) supernatant that step 4) is obtained places rotary evaporator to concentrate, and removes ethanol, is condensed into rare extractum shape, obtains peony to dark brown thick liquid,, be Chinese medicine extract.
4. method according to claim 3 is characterized in that: in the said step 1), said pulverizing is that said former medicated powder is broken to granular size is 20 orders-60 orders; Said step 2) in, the concentration expressed in percentage by volume of said alcoholic solution is 90-95%, and is preferred 95%, and the ratio of former medicine of said Chinese medicine and alcoholic solution is 1g: (15-25) ml is preferably 1g:20ml.
5. method according to claim 4 is characterized in that: filtering in the said step (4) is that 100～200 mesh filter screens filter; 5000 rev/mins of centrifugal rotational speeds, the time is 10 minutes; In the said step (5), said spissated temperature is 55 ℃～60 ℃, and being preferably is 55 ℃ or 60 ℃.
6. be the hair care formulations of active component with claim 1 or 2 described compositionss with the oily effect of anticreep hair care control.
7. preparation according to claim 6 is characterized in that: said preparation is tincture, shampoo or hair conditioner.
8. preparation according to claim 7 is characterized in that: said shampoo is processed by following component:
Laureth sulfuric ester ammonium 20%; Fatty acid distribution of coconut oil single ethanol amide 1%; Dodecanamide propyl betanin 4%; Guar hydroxypropyltrimonium chloride 0.2%; Disodiumedetate 0.1%; Cetearyl alcohol 0.5%; Dimethyl siloxane 2%; The Chinese medicine extract 1-2% of any preparation among the claim 3-5, methylchloroisothiazandnone or Methylisothiazolinone 0.1%; Ethylene glycol stearate or glycol distearate 2%; Surplus is a water, and said " % " is meant the quality percentage composition; The mass percent concentration of said Chinese medicine extract is preferably 1%.
9. the method for preparing of a shampoo comprises the steps:
1), make material dissolution complete 60 ℃ of stirrings of heating in the laureth sulfuric ester ammonium adding part water according to the described component of claim 8;
2) according to the described component of claim 8; With fatty acid distribution of coconut oil single ethanol amide, dodecanamide propyl betanin, guar hydroxypropyltrimonium chloride, disodiumedetate be added to stir in the remainder water after; Add in the solution of step 1) acquisition; Be heated to 80-85 ℃, homogenizing 3min stirs cooling; The cooling back adds the Chinese medicine extract of any preparation among cetearyl alcohol, dimethyl siloxane and cocamido propyl betaine, the claim 3-5; Stir; After adding methylchloroisothiazandnone or Methylisothiazolinone, ethylene glycol stearate or glycol distearate again, mixing obtains shampoo.
10. claim 1 or the 2 described compositionss application in the hair care formulations with the oily effect of anticreep hair care control of preparation.
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| CN104188847A (en) * | 2014-08-07 | 2014-12-10 | 兰晶 | Non-silicone-oil plant anti-allergic shampoo |
| CN107898703A (en) * | 2017-12-20 | 2018-04-13 | 杨新三 | A kind of Chinese medicine shampoo |
| WO2018171117A1 (en) * | 2017-03-23 | 2018-09-27 | 苏州顶裕节能设备有限公司 | Shampoo prepared with kudzu powder waste water and method therefor |
| CN111956587A (en) * | 2020-09-16 | 2020-11-20 | 陈媛婷 | Black-hair and bright-hair shampoo and preparation method thereof |
| CN114732847A (en) * | 2022-04-19 | 2022-07-12 | 赵鸿斌 | Oil-control anti-alopecia composition, oil-control anti-alopecia product and preparation method thereof |
| CN115531273A (en) * | 2022-11-02 | 2022-12-30 | 广州恒宁生物科技有限公司 | Traditional Chinese medicine composition for removing oil from hair and shampoo thereof |
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| CN103432227A (en) * | 2013-08-23 | 2013-12-11 | 广州市天吻娇颜化妆品有限公司 | Anti-hair loss Chinese herbal medicine compound with antagonism androgen receptor expression and preparation method of anti-hair loss Chinese herbal medicine compound |
| CN103432227B (en) * | 2013-08-23 | 2015-07-29 | 广州市天吻娇颜化妆品有限公司 | Anti-hair loss Chinese herb compound of antagonism expression of androgen receptor and preparation method thereof |
| CN104188847A (en) * | 2014-08-07 | 2014-12-10 | 兰晶 | Non-silicone-oil plant anti-allergic shampoo |
| WO2018171117A1 (en) * | 2017-03-23 | 2018-09-27 | 苏州顶裕节能设备有限公司 | Shampoo prepared with kudzu powder waste water and method therefor |
| CN107898703A (en) * | 2017-12-20 | 2018-04-13 | 杨新三 | A kind of Chinese medicine shampoo |
| CN111956587A (en) * | 2020-09-16 | 2020-11-20 | 陈媛婷 | Black-hair and bright-hair shampoo and preparation method thereof |
| CN111956587B (en) * | 2020-09-16 | 2021-05-04 | 孙开军 | Black-hair and bright-hair shampoo and preparation method thereof |
| CN114732847A (en) * | 2022-04-19 | 2022-07-12 | 赵鸿斌 | Oil-control anti-alopecia composition, oil-control anti-alopecia product and preparation method thereof |
| CN115531273A (en) * | 2022-11-02 | 2022-12-30 | 广州恒宁生物科技有限公司 | Traditional Chinese medicine composition for removing oil from hair and shampoo thereof |
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