CN102381882A - 一种均质微晶化结构氧化锆耐火材料及其制备方法 - Google Patents
一种均质微晶化结构氧化锆耐火材料及其制备方法 Download PDFInfo
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- CN102381882A CN102381882A CN2011102117389A CN201110211738A CN102381882A CN 102381882 A CN102381882 A CN 102381882A CN 2011102117389 A CN2011102117389 A CN 2011102117389A CN 201110211738 A CN201110211738 A CN 201110211738A CN 102381882 A CN102381882 A CN 102381882A
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- zirconium oxide
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- zirconia refractory
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- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 title abstract 7
- 229910001928 zirconium oxide Inorganic materials 0.000 title abstract 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 34
- 239000000843 powder Substances 0.000 claims abstract description 19
- 238000005520 cutting process Methods 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 15
- 238000001035 drying Methods 0.000 claims abstract description 7
- 239000003381 stabilizer Substances 0.000 claims abstract description 6
- 238000001354 calcination Methods 0.000 claims abstract description 3
- 238000012216 screening Methods 0.000 claims abstract description 3
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 73
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 30
- 239000000463 material Substances 0.000 claims description 25
- 238000003723 Smelting Methods 0.000 claims description 23
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 claims description 22
- 238000005469 granulation Methods 0.000 claims description 20
- 230000003179 granulation Effects 0.000 claims description 20
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 17
- 239000011819 refractory material Substances 0.000 claims description 16
- SIWVEOZUMHYXCS-UHFFFAOYSA-N oxo(oxoyttriooxy)yttrium Chemical compound O=[Y]O[Y]=O SIWVEOZUMHYXCS-UHFFFAOYSA-N 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- BXJPTTGFESFXJU-UHFFFAOYSA-N yttrium(3+);trinitrate Chemical compound [Y+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O BXJPTTGFESFXJU-UHFFFAOYSA-N 0.000 claims description 9
- 238000000748 compression moulding Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 5
- 229920002472 Starch Polymers 0.000 claims description 4
- 235000019698 starch Nutrition 0.000 claims description 4
- 239000008107 starch Substances 0.000 claims description 4
- 239000008187 granular material Substances 0.000 claims description 3
- 239000000395 magnesium oxide Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 206010013786 Dry skin Diseases 0.000 claims description 2
- 239000000758 substrate Substances 0.000 claims description 2
- 238000002156 mixing Methods 0.000 abstract description 17
- 239000011148 porous material Substances 0.000 abstract description 12
- 230000035939 shock Effects 0.000 abstract description 10
- 238000005245 sintering Methods 0.000 abstract description 9
- 229910000831 Steel Inorganic materials 0.000 abstract description 7
- 239000010959 steel Substances 0.000 abstract description 7
- 238000009749 continuous casting Methods 0.000 abstract description 5
- 229920001353 Dextrin Polymers 0.000 abstract 1
- 239000004375 Dextrin Substances 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 235000019425 dextrin Nutrition 0.000 abstract 1
- 238000003801 milling Methods 0.000 abstract 1
- 238000003825 pressing Methods 0.000 abstract 1
- 238000009991 scouring Methods 0.000 abstract 1
- 238000004513 sizing Methods 0.000 abstract 1
- 239000002245 particle Substances 0.000 description 22
- 238000000034 method Methods 0.000 description 21
- 239000003595 mist Substances 0.000 description 17
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical group [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 8
- 238000007906 compression Methods 0.000 description 5
- 230000006835 compression Effects 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000011236 particulate material Substances 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 229910052726 zirconium Inorganic materials 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- 239000011575 calcium Substances 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000010304 firing Methods 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 230000003245 working effect Effects 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- RQMIWLMVTCKXAQ-UHFFFAOYSA-N [AlH3].[C] Chemical compound [AlH3].[C] RQMIWLMVTCKXAQ-UHFFFAOYSA-N 0.000 description 1
- DNXNYEBMOSARMM-UHFFFAOYSA-N alumane;zirconium Chemical compound [AlH3].[Zr] DNXNYEBMOSARMM-UHFFFAOYSA-N 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000001192 hot extrusion Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000009766 low-temperature sintering Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
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- Compositions Of Oxide Ceramics (AREA)
Abstract
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CN 201110211738 CN102381882B (zh) | 2011-07-27 | 2011-07-27 | 一种均质微晶化结构氧化锆耐火材料及其制备方法 |
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CN 201110211738 CN102381882B (zh) | 2011-07-27 | 2011-07-27 | 一种均质微晶化结构氧化锆耐火材料及其制备方法 |
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CN102381882A true CN102381882A (zh) | 2012-03-21 |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103936442A (zh) * | 2014-04-02 | 2014-07-23 | 上海宝威陶瓷新材料有限公司 | 一种镁钇钙复合稳定氧化锆水口砖的组成及制备方法 |
CN108164275A (zh) * | 2018-01-14 | 2018-06-15 | 江苏嘉耐高温材料有限公司 | 一种耐侵蚀氧化锆水口砖及其制备方法 |
CN109400191A (zh) * | 2018-12-10 | 2019-03-01 | 中钢集团洛阳耐火材料研究院有限公司 | 一种高纯氧化锆隔热耐火制品 |
CN109516802A (zh) * | 2018-12-10 | 2019-03-26 | 江苏省陶瓷研究所有限公司 | 一种精密铸造用氧化锆坩埚及其热处理方法 |
CN109608193A (zh) * | 2018-12-10 | 2019-04-12 | 中钢集团洛阳耐火材料研究院有限公司 | 一种高纯氧化锆轻质耐火骨料及其制备方法 |
CN111087250A (zh) * | 2019-12-29 | 2020-05-01 | 太仓宏达俊盟新材料有限公司 | 一种基于氧化锆的耐火材料及其制备方法 |
CN111606721A (zh) * | 2020-06-01 | 2020-09-01 | 海城市方宏耐火材料有限公司 | 一种用于耐火材料的环保型结合剂及其制备方法 |
CN116082035A (zh) * | 2023-02-01 | 2023-05-09 | 中钢集团洛阳耐火材料研究院有限公司 | 一种高光洁度、高抗热震性薄壁氧化锆坩埚的制备方法 |
Citations (7)
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CN101209926A (zh) * | 2007-12-22 | 2008-07-02 | 淄博华创精细陶瓷有限公司 | 低成本氧化锆陶瓷磨介的制作方法 |
CN101259347A (zh) * | 2007-12-14 | 2008-09-10 | 济南圣泉集团股份有限公司 | 氧化锆泡沫陶瓷过滤器 |
CN101628733A (zh) * | 2008-07-14 | 2010-01-20 | 东北大学 | 一种常压低温制备氧化镁部分稳定单斜氧化锆粉末的方法 |
JP2010228949A (ja) * | 2009-03-26 | 2010-10-14 | Ngk Insulators Ltd | セラミック多孔体及びその製造方法 |
CN102040382A (zh) * | 2009-10-13 | 2011-05-04 | 江苏晶辉耐火材料有限公司 | 镁锆砂的加工工艺 |
US20110107796A1 (en) * | 2008-04-15 | 2011-05-12 | Saint-Gobain Centre De Recherches Et D'etudes Europeen | Sintered product produced from a zircon-based charge |
WO2011083022A1 (de) * | 2009-12-16 | 2011-07-14 | Ceramtec Gmbh | Keramischer verbundwerkstoff, bestehend aus den hauptbestandteilen aluminiumoxid und zirkonoxid |
-
2011
- 2011-07-27 CN CN 201110211738 patent/CN102381882B/zh not_active Expired - Fee Related
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101259347A (zh) * | 2007-12-14 | 2008-09-10 | 济南圣泉集团股份有限公司 | 氧化锆泡沫陶瓷过滤器 |
CN101209926A (zh) * | 2007-12-22 | 2008-07-02 | 淄博华创精细陶瓷有限公司 | 低成本氧化锆陶瓷磨介的制作方法 |
US20110107796A1 (en) * | 2008-04-15 | 2011-05-12 | Saint-Gobain Centre De Recherches Et D'etudes Europeen | Sintered product produced from a zircon-based charge |
CN101628733A (zh) * | 2008-07-14 | 2010-01-20 | 东北大学 | 一种常压低温制备氧化镁部分稳定单斜氧化锆粉末的方法 |
JP2010228949A (ja) * | 2009-03-26 | 2010-10-14 | Ngk Insulators Ltd | セラミック多孔体及びその製造方法 |
CN102040382A (zh) * | 2009-10-13 | 2011-05-04 | 江苏晶辉耐火材料有限公司 | 镁锆砂的加工工艺 |
WO2011083022A1 (de) * | 2009-12-16 | 2011-07-14 | Ceramtec Gmbh | Keramischer verbundwerkstoff, bestehend aus den hauptbestandteilen aluminiumoxid und zirkonoxid |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103936442A (zh) * | 2014-04-02 | 2014-07-23 | 上海宝威陶瓷新材料有限公司 | 一种镁钇钙复合稳定氧化锆水口砖的组成及制备方法 |
CN108164275A (zh) * | 2018-01-14 | 2018-06-15 | 江苏嘉耐高温材料有限公司 | 一种耐侵蚀氧化锆水口砖及其制备方法 |
CN108164275B (zh) * | 2018-01-14 | 2020-12-18 | 江苏嘉耐高温材料股份有限公司 | 一种耐侵蚀氧化锆水口砖及其制备方法 |
CN109400191A (zh) * | 2018-12-10 | 2019-03-01 | 中钢集团洛阳耐火材料研究院有限公司 | 一种高纯氧化锆隔热耐火制品 |
CN109516802A (zh) * | 2018-12-10 | 2019-03-26 | 江苏省陶瓷研究所有限公司 | 一种精密铸造用氧化锆坩埚及其热处理方法 |
CN109608193A (zh) * | 2018-12-10 | 2019-04-12 | 中钢集团洛阳耐火材料研究院有限公司 | 一种高纯氧化锆轻质耐火骨料及其制备方法 |
CN109608193B (zh) * | 2018-12-10 | 2021-01-22 | 中钢集团洛阳耐火材料研究院有限公司 | 一种高纯氧化锆轻质耐火骨料及其制备方法 |
CN109516802B (zh) * | 2018-12-10 | 2021-09-21 | 江苏省陶瓷研究所有限公司 | 一种精密铸造用氧化锆坩埚及其热处理方法 |
CN111087250A (zh) * | 2019-12-29 | 2020-05-01 | 太仓宏达俊盟新材料有限公司 | 一种基于氧化锆的耐火材料及其制备方法 |
CN111606721A (zh) * | 2020-06-01 | 2020-09-01 | 海城市方宏耐火材料有限公司 | 一种用于耐火材料的环保型结合剂及其制备方法 |
CN116082035A (zh) * | 2023-02-01 | 2023-05-09 | 中钢集团洛阳耐火材料研究院有限公司 | 一种高光洁度、高抗热震性薄壁氧化锆坩埚的制备方法 |
CN116082035B (zh) * | 2023-02-01 | 2023-10-24 | 中钢集团洛阳耐火材料研究院有限公司 | 一种高光洁度、高抗热震性薄壁氧化锆坩埚的制备方法 |
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Address after: 312000 No. 9 Juxian No. 2 Road, East 2 District, Shangyu Economic and Technological Development Zone, Hangzhou Bay, Shaoxing City, Zhejiang Province Patentee after: Zhejiang Zili High Temperature Technology Co.,Ltd. Address before: 310026 Zhejiang Hangzhou Shangyu economic and Technological Development Zone East two district two two Road No. 9 Patentee before: ZHEJIANG ZILI HIGH TEMPERATURE TECHNOLOGY Co.,Ltd. |
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