CN102334607A - Composite of butyrate or butyrin and tannin as well as preparation method and application thereof to feed additive - Google Patents
Composite of butyrate or butyrin and tannin as well as preparation method and application thereof to feed additive Download PDFInfo
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- CN102334607A CN102334607A CN2011102196696A CN201110219669A CN102334607A CN 102334607 A CN102334607 A CN 102334607A CN 2011102196696 A CN2011102196696 A CN 2011102196696A CN 201110219669 A CN201110219669 A CN 201110219669A CN 102334607 A CN102334607 A CN 102334607A
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- Prior art keywords
- butyrate
- tannin
- compound
- glycerol monobutyralte
- monobutyralte
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- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Natural products CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 title claims abstract description 71
- 229920001864 tannin Polymers 0.000 title claims abstract description 57
- 239000001648 tannin Substances 0.000 title claims abstract description 57
- 235000018553 tannin Nutrition 0.000 title claims abstract description 57
- FERIUCNNQQJTOY-UHFFFAOYSA-M Butyrate Chemical compound CCCC([O-])=O FERIUCNNQQJTOY-UHFFFAOYSA-M 0.000 title claims abstract description 55
- UYXTWWCETRIEDR-UHFFFAOYSA-N Tributyrin Chemical compound CCCC(=O)OCC(OC(=O)CCC)COC(=O)CCC UYXTWWCETRIEDR-UHFFFAOYSA-N 0.000 title claims abstract description 14
- 239000002131 composite material Substances 0.000 title abstract description 8
- 239000003674 animal food additive Substances 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- 239000000843 powder Substances 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000001694 spray drying Methods 0.000 claims abstract description 10
- 239000007864 aqueous solution Substances 0.000 claims abstract description 7
- 239000000725 suspension Substances 0.000 claims abstract description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 120
- 150000001875 compounds Chemical class 0.000 claims description 27
- 238000000034 method Methods 0.000 claims description 13
- 238000012546 transfer Methods 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 239000003094 microcapsule Substances 0.000 claims description 5
- 239000000376 reactant Substances 0.000 claims description 5
- 238000013019 agitation Methods 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- 238000010669 acid-base reaction Methods 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 239000007762 w/o emulsion Substances 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 2
- 150000004648 butanoic acid derivatives Chemical class 0.000 claims 1
- 206010012735 Diarrhoea Diseases 0.000 abstract description 10
- 241001465754 Metazoa Species 0.000 abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000003756 stirring Methods 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 210000003608 fece Anatomy 0.000 abstract description 2
- 239000000839 emulsion Substances 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000002474 experimental method Methods 0.000 description 9
- MFBOGIVSZKQAPD-UHFFFAOYSA-M sodium butyrate Chemical compound [Na+].CCCC([O-])=O MFBOGIVSZKQAPD-UHFFFAOYSA-M 0.000 description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 8
- 235000006667 Aleurites moluccana Nutrition 0.000 description 6
- 240000004957 Castanea mollissima Species 0.000 description 6
- 235000018244 Castanea mollissima Nutrition 0.000 description 6
- 235000013601 eggs Nutrition 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 239000012295 chemical reaction liquid Substances 0.000 description 3
- 235000011121 sodium hydroxide Nutrition 0.000 description 3
- 239000002689 soil Substances 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 208000021017 Weight Gain Diseases 0.000 description 2
- 230000037396 body weight Effects 0.000 description 2
- 238000009395 breeding Methods 0.000 description 2
- 230000001488 breeding effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000003203 everyday effect Effects 0.000 description 2
- 235000021050 feed intake Nutrition 0.000 description 2
- 239000010408 film Substances 0.000 description 2
- 230000000968 intestinal effect Effects 0.000 description 2
- 235000013372 meat Nutrition 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 235000019786 weight gain Nutrition 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- 241000124008 Mammalia Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 241000219492 Quercus Species 0.000 description 1
- 235000016976 Quercus macrolepis Nutrition 0.000 description 1
- 240000003152 Rhus chinensis Species 0.000 description 1
- 235000014220 Rhus chinensis Nutrition 0.000 description 1
- 241000282887 Suidae Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 235000019728 animal nutrition Nutrition 0.000 description 1
- 235000019606 astringent taste Nutrition 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 235000013330 chicken meat Nutrition 0.000 description 1
- 229940105051 chinese chestnut extract Drugs 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 230000001079 digestive effect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 210000001842 enterocyte Anatomy 0.000 description 1
- 239000004459 forage Substances 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 210000004347 intestinal mucosa Anatomy 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 235000013594 poultry meat Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Landscapes
- Fodder In General (AREA)
Abstract
The invention discloses a composite of butyrate or butyrin and tannin. The composite comprises the two components by weight percentage: 10-90% of butyrate or butyrin and 5-50% of the tannin. The preparation method comprises the following steps of: mixing a butyrate aqueous solution or butyrin water emulsion with the tannin based on a proportion, stirring until the tannin is dissolved or a suspension is formed; spray drying at the air inlet temperature of 150-260 DEG C and the air outlet temperature of 65-160 DEG C; and collecting dry powder by a cyclone separator or a vibrating fluidized bed so as to obtain the composite of the butyrate and the tannin. The composite can be applied to a feed additive and has the beneficial effects of reducing phenomena such as wet dropping, feed like feces or diarrhea of monogastric animals and improving the production performance of animals.
Description
Technical field
The present invention relates to a kind of mixture that contains butyrate or glycerol monobutyralte, refer in particular to the compound of butyrate or glycerol monobutyralte and tannin, and relevant with the method for making and the application of this mixture in feed addictive of this compound.
Background technology
Butyrate or glycerol monobutyralte have characteristic odor, lure that the mammal feed intake increases, and swashs in vivo digestive ferment into; Improve beneficial microbe flora ratio in the alimentary canal; Promote the absorption of back offseting of intestinal segment content water sodium, most crucial effect is for enterocyte provides energy fast, thereby promotes the intestinal villus growth; Make the whole enlarged areas of digesting and assimilating, improved the digestion power of animal.Yet when animal increased feed intake, content was long more in the enteron aisle holdup time, and the rate that digests and absorbs of feed just can be high more.
Tannin is claimed the tannins material again, and its main body is multivalence phenol C
14H
10O
8, have astringent taste.Occurring in nature, tannin are present in plant xylem, bark, leaf, fruit and the root in a large number, and especially oak, Chinese sumac and Chinese chestnut tree content are abundant.Generally classifying as ANFs to tannin in Animal nutrition circle, is the material that restriction is used.Yet tannin has astriction.The formation thin film covered the intestinal mucosa surface after tannin and ptyalin, alimentary canal endogenous enzymes and forage protein were combined into compound, prevented the reverse inflow enteric cavity of body fluid, had reduced the ight soil water content.
The inventor is according to the characteristics separately of above-mentioned substance; It is composite to get Chinese chestnut tree extract and butyrate or glycerol monobutyralte; Be applied to nonruminant, significantly reduce poultry muck (wet dropping), material excrement (feed like feces) or diarrhea of pigs (Diarrhea).This case produces thus.
Summary of the invention
The object of the present invention is to provide compound and the method for making and the application in feed addictive of a kind of butyrate or glycerol monobutyralte and tannin,, and improve breeding performonce fo animals with reduction nonruminant muck, material excrement or diarrhoea.
To achieve these goals, technical scheme of the present invention is following:
The compound of a kind of butyrate or glycerol monobutyralte and tannin comprises following substances in percentage by weight and combines: butyrate or glycerol monobutyralte 5-95%, tannin 95-5%.
The method for making of the compound of a kind of butyrate or glycerol monobutyralte and tannin; May further comprise the steps: (1) is according to the ratio of percentage by weight butyrate or glycerol monobutyralte 5-95%, tannin 95-5%; With the aqueous solution of butyrate or the water-in-oil emulsion of tributyrin; With tannin carry out miscible, be stirred to the dissolving or suspension; (2), carry out spray-drying under 65 ℃～160 ℃ conditions of leaving air temp 150 ℃～260 ℃ of EATs; (3), get the compound of butyrate or glycerol monobutyralte and tannin through the dry powder of cyclone separator or vibrated fluidized bed collection.
The aqueous solution of the butyrate in the said step (1) can be prepared by following steps: (1-1) acid-base reaction: add entry in retort; Under agitation add hydroxide, be stirred to dissolving, add butyric acid more gradually; The control temperature is not higher than 105 ℃; Generate butyrate, reaction finishes, and cooling butyrate reactant liquor is to 25 ℃～80 ℃ of temperature; (1-2) transfer survey pH value, add the corresponding salt of an amount of butyric acid, hydroxide or hydroxide, transfer and survey butyrate reacting liquid pH value to 8～11, continue to cool off the butyrate reactant liquor to 25 ℃～50 ℃ of temperature; Obtain being used for the aqueous solution of the miscible butyrate of abovementioned steps (1) and tannin.
Further, carry out moisture film, spraying and dedusting to producing vaporized gas in the spray-drying simultaneously in the said step 2, dedusting liquid is recycled.
The method for making of the compound of a kind of butyrate or glycerol monobutyralte and tannin; Can be according to the ratio of percentage by weight butyrate or glycerol monobutyralte 5-95%, tannin 95-5%; Directly with butyrate dry powder or glycerol monobutyralte water soluble microcapsule dry powder; Mix in mixer with tannin, promptly get the compound of butyrate or glycerol monobutyralte and tannin.
The ratio that feed is added in the application of the compound of a kind of butyrate or glycerol monobutyralte and tannin in feed addictive, said compound to is 0.2-3.0 kilogram/ton.
Experiment showed, that the present invention is applied in the feed addictive, can reduce nonruminant muck, material excrement or diarrhoea really, and improve breeding performonce fo animals.
The present invention is further specified technical scheme of the present invention in order further to explain below in conjunction with the specific embodiment.
The specific embodiment
A kind of butyrate that the present invention discloses or the compound of glycerol monobutyralte and tannin comprise following substances in percentage by weight and combine: butyrate or glycerol monobutyralte 5-95%, tannin 95-5%.
Concrete processing and preparing is example with the sodium butyrate.
Production method can choice reaction, miscible, spray drying process:
The first step, at first, acid-base reaction: the water that in three retort (three instances), adds 1000 weight portions respectively; The NaOH that under agitation adds 183,256,329 weight portions respectively stirs fully extremely dissolving, and the butyric acid that adds 402,562,723 weight portions is more gradually gone into retort; The control temperature is not higher than 105 ℃; Generate sodium butyrate, reaction finishes, 25 ℃～80 ℃ of cooling reaction liquid to temperature; The component of above-mentioned NaOH and butyric acid can be according to the amount of chemical equation according to desired butyrate, through calculating.
Secondly, transfer and survey pH value, through adding an amount of butyric acid or containing the basic salt of sodium, transfer measured reaction liquid pH value to 8～11, continuation cooling reaction liquid is to 25 ℃～50 ℃ of temperature.
At last, the tannin that under agitation adds 500,300,100 weight portions in the reactant liquor of three retort respectively carries out miscible, stirring and dissolving or be the suspension of part.
In second step, spray-drying: 150 ℃～260 ℃ of EATs, carry out spray-drying under 65 ℃～160 ℃ conditions of leaving air temp, concrete drying condition is seen table 1.Simultaneously, carry out moisture film, spraying and dedusting to producing vaporized gas in the spray-drying, dedusting liquid is recycled; This technology belongs to existing common technique means, so this place repeats no more.
The 3rd step, the dry powder of collecting through cyclone separator or vibrated fluidized bed, the compound of butyrate and tannin, in three groups of instances in the product sodium butyrate content be respectively 50%, 70% and 90%.(because of butyric acid content more than 99%, sodium hydrate content about 99%, real reaction and dry back sodium butyrate actual amount 500,700 and about 900.）
Table 1
If select tributyrin to replace butyrate; Then directly in the water-in-oil emulsion of tributyrin, adding tannin carries out miscible; Mixed proportion is in pure substance, and glycerol monobutyralte 5-95%, tannin 95-5% are spray-dried more by weight percentage; Through the dry powder of cyclone separator or vibrated fluidized bed collection, get the compound of tributyrin and tannin.Spray-drying and the step of collecting dry powder such as aforementioned.
Production method also can be selected the dry powder blend method:
Ratio according to percentage by weight butyrate or glycerol monobutyralte 5-95%, tannin 95-5%; Directly butyrate dry powder or glycerol monobutyralte water soluble microcapsule dry powder and tannin are mixed in mixer, promptly get the compound of butyrate or glycerol monobutyralte and tannin.
With glycerol monobutyralte water soluble microcapsule dry powder (by containing glycerol monobutyralte 50%) is example:
Table 2
Press table 2 proportioning, glycerol monobutyralte water soluble microcapsule powder and tannin are mixed, promptly get the compound of glycerol monobutyralte and tannin with mixer.In three groups of instances in the product glycerol monobutyralte content be respectively 47.5%, 35% and 25%.
Case study on implementation 1
Former powder of 98% sodium butyrate and Chinese chestnut tree extract (including 75% tannin) are processed product in the 70:30 ratio.This product adds in the 1 age in days meat chick fodder by 0,500 grams, 750 grams and 1000 gram/tons.Four processing are respectively to treatment group, experiment I group, experiment II group, experiment III group.Animal used as test is an AA meat chick, 80 every group, be divided into 4 repetitions, and each repeats 20 chickens.In the repetition (group) of whole 1 Japanese instar chickling random distribution to 16, the wood sawdust bedding and padding that 12cm is thick.Measure body weight gains, feedstuff-meat ratio respectively and contain excrement bedding and padding water content when experiment finished in 21 days.The result is:
| Project | Control group | Experiment I group | Experiment II group | Experiment III group |
| Body weight gains (gram) | 620 | 631 | 637 | 630 |
| Feedstuff-meat ratio | 1.56 | 1.53 | 1.51 | 1.56 |
| Bedding and padding water content (%) | 25 | 21 | 19 | 23 |
The result shows: 1, the aggregate performance of the sodium butyrate of feed interpolation 750 grams per ton and the composite product of Chinese chestnut tree extract is best; 2, compare with control group, experiment II bedding and padding water content is 19%, is starkly lower than control group (25%).
Case study on implementation 2
Former powder of 98% sodium butyrate and Chinese chestnut tree extract (including 75% tannin) are processed product in the 90:10 ratio.This product by 500 gram/ton feeds feed continuously 48 age in week laying hen 60 days; Contrast at two rows, 4 range upon range of posture egg cage production lines; A, B row egg cage are raised 19000 blue commodity eggs in sea respectively; The control group of A for not have to add, B is the experimental group by 500 gram/tons interpolation product, adds up 60 days A, B qualified egg rate in arranging continuously.Qualified egg rate computing formula is:
Statistics is: A=95%, B=98%
The result shows: the experimental group of adding sodium butyrate and Chinese chestnut extract composite product by 500 gram/tons improves 3% qualified egg rate than blank group.
Case study on implementation 3
Former powder of 98% sodium butyrate and Chinese chestnut tree extract (including 75% tannin) are processed product in the 50:50 ratio.This product adds 35 ages in days to by 1000 gram/tons and just transfers to the piglet on the child care hurdle from the delivery room.10 piglets in each child care hurdle, experimental group and control group 20 hurdles of respectively feeding are respectively 200 piglets, observe the grice diarrhoea situation every day.Clean the child care hurdle every day, and detail record grice diarrhoea situation.The criterion of grice diarrhoea is: piglet be pulled on the floor can't moulding ight soil heap number account for the ratio of total ight soil heap number on the same day.Observed 30 days continuously, taking pictures keeps sample and makes detail record.The result shows that the control group diarrhea rate is 17%, and the experimental group diarrhea rate is 9%, has descended 8% than control group.
The foregoing description and non-limiting method for making of the present invention and application, the those of ordinary skill of any affiliated technical field all should be regarded as not breaking away from scope of patent protection of the present invention to its suitable variation or modification of making.
Claims (7)
1. the compound of a butyrate or glycerol monobutyralte and tannin is characterized in that comprising following substances in percentage by weight and combines: butyrate or glycerol monobutyralte 5-95%, tannin 95-5%.
2. the method for making of the compound of a butyrate or glycerol monobutyralte and tannin is characterized in that may further comprise the steps:
(1) according to the ratio of percentage by weight butyrate or glycerol monobutyralte 5-95%, tannin 95-5%, with the aqueous solution of butyrate or the water-in-oil emulsion of tributyrin, carry out misciblely with tannin, be stirred to dissolving or suspension;
(2), carry out spray-drying under 65 ℃～160 ℃ conditions of leaving air temp 150 ℃～260 ℃ of EATs;
(3), get the compound of butyrate or glycerol monobutyralte and tannin through the dry powder of cyclone separator or vibrated fluidized bed collection.
3. the method for making of the compound of a kind of butyrate according to claim 2 or glycerol monobutyralte and tannin is characterized in that the aqueous solution of the butyrate in the said step (1) can be prepared by following steps:
(1-1) acid-base reaction: add entry in retort, under agitation add hydroxide, be stirred to dissolving, add butyric acid more gradually, control temperature≤105 ℃ generate butyrate, and reaction finishes, and cooling butyrate reactant liquor is to 25 ℃～80 ℃ of temperature;
(1-2) transfer survey pH value, add the corresponding salt of butyric acid, hydroxide or hydroxide, transfer and survey butyrate reacting liquid pH value to 8～11, continue to cool off the butyrate reactant liquor to 25 ℃～50 ℃ of temperature; Obtain being used for the aqueous solution of the miscible butyrate of abovementioned steps (1) and tannin.
4. according to the method for making of the compound of claim 2 or 3 described a kind of butyrates or glycerol monobutyralte and tannin, it is characterized in that carrying out moisture film, spraying and dedusting to producing vaporized gas in the spray-drying simultaneously in the said step 2, dedusting liquid is recycled.
5. the method for making of the compound of a butyrate or glycerol monobutyralte and tannin; It is characterized in that may further comprise the steps: according to the ratio of percentage by weight butyrate or glycerol monobutyralte 5-95%, tannin 95-5%; Directly butyrate dry powder or glycerol monobutyralte water soluble microcapsule dry powder and tannin are mixed in mixer, promptly get the compound of butyrate or glycerol monobutyralte and tannin.
6. the application of compound in feed addictive of a kind of butyrate according to claim 1 or glycerol monobutyralte and tannin.
7. the application of compound in feed addictive of a kind of butyrate according to claim 6 or glycerol monobutyralte and tannin is characterized in that: the ratio that said compound adds feed to is 0.2-3.0 kilogram/ton.
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| CN107927348A (en) * | 2017-11-10 | 2018-04-20 | 杭州康德权饲料有限公司 | It is a kind of while produce sodium butyrate original powder and the system and production technology of butyric acid salt particle |
| CN109090349A (en) * | 2018-07-27 | 2018-12-28 | 浙江耀飞生物科技有限公司 | A kind of compound tannin feed granules and preparation method thereof |
| CN112335798A (en) * | 2019-08-08 | 2021-02-09 | 徐州新奥生物科技有限公司 | Composition for feed and preparation method and application thereof |
| CN113261621A (en) * | 2020-05-20 | 2021-08-17 | 江门嘉年华饲料实业有限公司 | Antibiotic-free broiler chicken compound feed |
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| CN107027973A (en) * | 2017-05-25 | 2017-08-11 | 广州汇加生物科技有限公司 | A kind of tannin mixture for reducing or eliminating vegatable tannin astringent taste and preparation method and application |
| CN107027973B (en) * | 2017-05-25 | 2021-03-19 | 广州汇加生物科技有限公司 | Tannin mixture capable of reducing or eliminating astringent taste of plant tannin and preparation method and application thereof |
| CN107927348A (en) * | 2017-11-10 | 2018-04-20 | 杭州康德权饲料有限公司 | It is a kind of while produce sodium butyrate original powder and the system and production technology of butyric acid salt particle |
| CN109090349A (en) * | 2018-07-27 | 2018-12-28 | 浙江耀飞生物科技有限公司 | A kind of compound tannin feed granules and preparation method thereof |
| CN112335798A (en) * | 2019-08-08 | 2021-02-09 | 徐州新奥生物科技有限公司 | Composition for feed and preparation method and application thereof |
| CN113261621A (en) * | 2020-05-20 | 2021-08-17 | 江门嘉年华饲料实业有限公司 | Antibiotic-free broiler chicken compound feed |
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| CN102334607B (en) | 2013-12-18 |
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