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CN102189706B - High-pressure shearing deformation method and device for tubular materials - Google Patents

High-pressure shearing deformation method and device for tubular materials Download PDF

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CN102189706B
CN102189706B CN201110030903.0A CN201110030903A CN102189706B CN 102189706 B CN102189706 B CN 102189706B CN 201110030903 A CN201110030903 A CN 201110030903A CN 102189706 B CN102189706 B CN 102189706B
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workpiece
anvil
rigid
pressure
tubular
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CN102189706A (en
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王经涛
李政
王进
刘金强
尹德良
刘冉
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Nanjing University of Science and Technology
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C23/00Extruding metal; Impact extrusion
    • B21C23/001Extruding metal; Impact extrusion to improve the material properties, e.g. lateral extrusion
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J1/00Preparing metal stock or similar ancillary operations prior, during or post forging, e.g. heating or cooling
    • B21J1/02Preliminary treatment of metal stock without particular shaping, e.g. salvaging segregated zones, forging or pressing in the rough
    • B21J1/025Preliminary treatment of metal stock without particular shaping, e.g. salvaging segregated zones, forging or pressing in the rough affecting grain orientation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • B21J5/008Incremental forging
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21KMAKING FORGED OR PRESSED METAL PRODUCTS, e.g. HORSE-SHOES, RIVETS, BOLTS OR WHEELS
    • B21K1/00Making machine elements
    • B21K1/76Making machine elements elements not mentioned in one of the preceding groups
    • B21K1/761Making machine elements elements not mentioned in one of the preceding groups rings

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Forging (AREA)

Abstract

本发明公开了一种管状材料高压剪切变形方法及其装置,首先选择加工的工件,工件为管状,采用约束体分别约束工件的内壁和外壁;然后直接对工件端部施加轴向压力,使得工件发生弹性变形或微小塑性变形,在工件内累加高达1~15GPa的静水压力;随后对与工件内壁或外壁接触的一个约束体提供扭矩,使其绕工件的中心轴转动,同时固定另一个约束体,在约束体与工件内外壁环向摩擦力的作用下,工件内部沿径向不同厚度处的材料以不同的角速度转动,从而实现工件的环向剪切变形。本发明技术可行性高,操作无特殊要求,所需设备简单易得。同时,由于本发明是依托传统挤压设备实现的新的塑性加工方法,因此扩展了传统挤压设备的功用。

The invention discloses a method and device for high-pressure shear deformation of tubular materials. Firstly, the workpiece to be processed is selected, and the workpiece is tubular, and the inner wall and the outer wall of the workpiece are respectively restrained by constraining bodies; then axial pressure is directly applied to the end of the workpiece, so that The workpiece undergoes elastic deformation or slight plastic deformation, and accumulates a hydrostatic pressure of up to 1 to 15GPa in the workpiece; then, a torque is provided to a constraint body in contact with the inner or outer wall of the workpiece to make it rotate around the central axis of the workpiece and fix another constraint at the same time Under the action of the circumferential friction between the restraining body and the inner and outer walls of the workpiece, the materials at different thicknesses in the radial direction inside the workpiece rotate at different angular velocities, thereby realizing the circumferential shear deformation of the workpiece. The invention has high technical feasibility, no special requirements for operation, and the required equipment is simple and easy to obtain. At the same time, because the present invention is a new plastic processing method realized by relying on traditional extrusion equipment, it expands the functions of traditional extrusion equipment.

Description

管状材料高压剪切变形方法及其装置High-pressure shear deformation method and device for tubular material

技术领域 technical field

本发明涉及材料加工工程领域,特别是一种实现管状材料环向剪切塑性变形的方法及其装置,主要应用于各种金属及合金材料、无机非金属材料及高分子材料等,以实现这些材料在高静水压力的塑性变形,从而控制和优化其组织结构,提高其性能。The invention relates to the field of material processing engineering, in particular to a method and device for realizing circumferential shear plastic deformation of tubular materials, which are mainly applied to various metals and alloy materials, inorganic non-metallic materials and polymer materials, etc., to realize these The plastic deformation of the material under high hydrostatic pressure can control and optimize its structure and improve its performance.

背景技术 Background technique

剧烈塑性变形(severe plastic deformation,简称SPD)方法是一系列具有大变形量的塑性加工技术的总称。SPD方法细化晶粒效果明显,可以将材料内部组织细化到亚微米级、纳米级甚至非晶态[R.Z.Valiev.Nature materials.2004(3):511-516.;R.Z.Valiev,A.K.Mukherjee.Scripta mater.2001(44):1747-1750.]。近年来,采用SPD方法制备块体纳米结构材料的技术受到了材料科学领域专家、学者们的普遍关注。与此同时,大量的研究推动SPD技术在制备块体超细晶、纳米晶材料方面的不断发展。俄罗斯Ufa航空技术大学的R.Z.Valiev领导的研究小组认为,采用SPD方法制备超细晶材料应满足多项条件[R.Z.Valiev,R.K.Islamgaliev,I V.Alexandrov.Progress in Materials Science.2000(45):103-189.],主要包括:大塑性变形量、相对低的变形温度和变形材料内部高的静水压力。在这一原则指导下,人们提出并开发了各种SPD工艺和方法。The severe plastic deformation (SPD) method is a general term for a series of plastic processing techniques with large deformation. The effect of the SPD method on grain refinement is obvious, and the internal structure of the material can be refined to submicron level, nanometer level or even amorphous state [R.Z.Valiev.Nature materials.2004(3):511-516.; R.Z.Valiev, A.K.Mukherjee. Scripta mater. 2001(44): 1747-1750.]. In recent years, the technology of preparing bulk nanostructure materials by SPD method has attracted widespread attention from experts and scholars in the field of materials science. At the same time, a large number of researches have promoted the continuous development of SPD technology in the preparation of bulk ultrafine crystal and nanocrystalline materials. The research team led by R.Z.Valiev of Ufa Aeronautical Technology University in Russia believes that the preparation of ultrafine-grained materials by SPD method should meet a number of conditions [R.Z.Valiev, R.K.Islamgaliev, I V.Alexandrov.Progress in Materials Science.2000(45): 103 -189.], mainly including: large plastic deformation, relatively low deformation temperature and high hydrostatic pressure inside the deformed material. Under the guidance of this principle, various SPD processes and methods have been proposed and developed.

目前最受关注的SPD方法主要是,累积轧制(accumulative roll-bonding,简称ARB)技术,等径角变形(equal-channel angular pressing,简称ECAP)技术,以及高压扭转(high-pressure torsion,简称HPT)技术等。其中ARB技术如图1所示,可连续制备薄板类超细晶结构材料,且易于在传统轧机上实现,设备简单,实际应用意义重大。但是,在ARB技术加工过程中,为了实现良好的轧制复合,往往不能使用润滑剂,这对轧辊的服役寿命不利。同时,由于材料在轧制过程中受到变形条件限制所能达到的静水压力不够高,在加工过程中的累积一定的变形量后会出现开裂问题[N.Tsuji,Y.Saito,S.H.Lee,et al.Advanced Engineering Materials.2003(5):338-344.]。ECAP技术如图2所示,采用该技术进行超细晶金属加工处理具有巨大潜力。但是,对于一些难加工合金(如镁合金等),进行ECAP经常发生开裂,如果提高变形温度,一方面会影响模具寿命,另一方面又会影响晶粒细化效果。再加上由于模具材料的限制,变形温度不可能无限制地提高。而且ECAP为实现大的累积塑性变形,需要多道次加工,操作复杂。背压ECAP(back pressure equal-channel angular pressing,简称BP-ECAP)即在模具出口通道施加背压的ECAP技术,如图3所示,可以在一定程度上解决难变形金属ECAP的开裂问题,从而改善材料的微观组织和机械性能;所施加的背压有限,静水压力一般维持在几百兆帕[R.YE.Lapovok.Journal of materials science.2005(40):341-346.]。施加的背压太高则由于摩擦力和模具强度等因素而无法实现ECAP。HPT技术最符合前文中提到的SPD方法制备超细晶材料应满足的多项条件。在现有的SPD技术之中,HPT技术晶粒细化能力最强。然而,HPT所能加工的试样厚度方向尺寸很小[A.P.Zhilyaev,T.G.Langdon.Progress in Materials Science.2008(53):893-979.],所加工的盘状试样,沿径向存在较大的应变梯度,变形不均匀,晶粒细化程度也不均匀。At present, the most concerned SPD methods are mainly accumulative roll-bonding (ARB for short) technology, equal-channel angular pressing (ECAP for short) technology, and high-pressure torsion (high-pressure torsion for short) technology. HPT) technology, etc. Among them, the ARB technology, as shown in Figure 1, can continuously prepare thin-plate ultrafine-grained materials, and is easy to implement on a traditional rolling mill. The equipment is simple and the practical application is of great significance. However, in the process of ARB technology, in order to achieve good rolling compounding, lubricants are often not used, which is detrimental to the service life of the rolls. At the same time, because the hydrostatic pressure that the material can achieve due to the limitation of deformation conditions during the rolling process is not high enough, cracking will occur after a certain amount of deformation is accumulated during the processing [N.Tsuji, Y.Saito, S.H.Lee, et al. al. Advanced Engineering Materials. 2003(5): 338-344.]. ECAP technology is shown in Figure 2, and the use of this technology for ultra-fine-grained metal processing has great potential. However, for some difficult-to-process alloys (such as magnesium alloys, etc.), cracking often occurs during ECAP. If the deformation temperature is increased, it will affect the life of the mold on the one hand, and affect the grain refinement effect on the other hand. In addition, due to the limitation of the mold material, the deformation temperature cannot be increased without limit. Moreover, in order to achieve large cumulative plastic deformation, ECAP requires multi-pass processing, and the operation is complicated. Back pressure ECAP (back pressure equal-channel angular pressing, BP-ECAP for short) is an ECAP technology that applies back pressure to the outlet channel of the mold. Improve the microstructure and mechanical properties of the material; the applied back pressure is limited, and the hydrostatic pressure is generally maintained at several hundred MPa [R.YE.Lapovok.Journal of materials science.2005(40):341-346.]. If the applied back pressure is too high, ECAP cannot be achieved due to factors such as friction and die strength. HPT technology is the most in line with the multiple conditions that should be met in the preparation of ultrafine-grained materials by the SPD method mentioned above. Among the existing SPD technologies, the HPT technology has the strongest grain refinement ability. However, the size of the thickness direction of the sample that can be processed by HPT is very small [A.P.Zhilyaev, T.G.Langdon. Progress in Materials Science. Large strain gradient, uneven deformation, and uneven grain refinement.

Tóth等人[L.S.Tóth,M.Arzaghi,J.J.Fundenberger,B.Beausir:Scr.Mater.Vol.60(2009),p.175]提出了一种管状材料高压扭转方法(high-pressure tube twisting,HPTT),如图5所示,在管状试样内部安放弹性芯轴,外侧套置刚性圆盘(rigid disk),试样两端用挡板固定。对芯轴加压时,芯轴径向膨胀对管状试样内壁产生径向压力,同时刚性圆盘对管状试样外壁产生一个相反方向的径向压力,从而在管状试样中产生静水压力。此时转动环套,管状试样在表面环向摩擦力作用下实现环向剪切变形。这种方法思路很好,其最主要的问题是该方法对试样的加载方式是径向加载方式,也就是说,该方法直接对芯棒施加轴向压力,芯棒在对试样产生径向压力。在这种加载方式下,压力并没有直接加载在管状材料的轴向,试样所承受的静水压力来自芯棒受压后的弹性变形,由于材料弹性变形不可能很大,很难产生高的静水压力,因而能提供的环向摩擦力有限,仅适用于强度较低的纯金属等。对于强度较高的材料,由于所能产生的摩擦力达不到材料的屈服强度,容易出现打滑等现象,无法实现所需要的变形。Tóth et al [L.S.Tóth, M.Arzaghi, J.J.Fundenberger, B.Beausir: Scr.Mater.Vol.60 (2009), p.175] proposed a high-pressure torsion method for tubular materials (high-pressure tube twisting, HPTT ), as shown in Figure 5, an elastic mandrel is placed inside the tubular sample, a rigid disk is placed outside, and both ends of the sample are fixed with baffles. When the mandrel is pressurized, the radial expansion of the mandrel produces radial pressure on the inner wall of the tubular sample, while the rigid disk produces a radial pressure in the opposite direction on the outer wall of the tubular sample, thereby generating hydrostatic pressure in the tubular sample. At this time, the ring sleeve is rotated, and the tubular sample realizes hoop shear deformation under the action of hoop friction on the surface. The idea of this method is very good, but the main problem is that the method of loading the sample is a radial loading method, that is to say, this method directly applies axial pressure to the mandrel, and the mandrel exerts radial pressure on the sample. to pressure. In this loading mode, the pressure is not directly loaded on the axial direction of the tubular material, and the hydrostatic pressure on the sample comes from the elastic deformation of the mandrel after compression. Since the elastic deformation of the material cannot be very large, it is difficult to produce high Hydrostatic pressure, so the hoop friction that can be provided is limited, and it is only suitable for pure metals with low strength. For materials with higher strength, since the friction force that can be generated cannot reach the yield strength of the material, it is prone to slipping and other phenomena, and the required deformation cannot be achieved.

该方法另一方面问题是位于管状试样两端的档板是一悬臂梁式结构,对试样轴向变形的约束不够,试样承受的静水压力较高时,材料很容易从缝隙中挤出,影响加工过程。Another problem with this method is that the baffles located at both ends of the tubular sample are a cantilever beam structure, which does not constrain the axial deformation of the sample enough. When the hydrostatic pressure on the sample is high, the material is easily squeezed out from the gap. , affecting the processing process.

发明内容 Contents of the invention

本发明的目的在于提供一种新的剧烈塑性变形方法及其装置:管状材料高压剪切(tube-High Pressure Shearing,简称t-HPS)技术。该技术很好地满足了采用SPD方法制备超细晶材料应满足多项条件,如大塑性变形量、相对低的变形温度和变形材料内部高的静水压力。该方法避免了ARB、ECAP以及背压ECAP等技术需要多道次操作的繁琐工艺过程,同时,由于加载方式本质上的不同,该方法也克服了Tóth等人HPTT法静水压力不足等问题,在加工材料时能提供类似HPT技术的高静水压力条件,从而适用于对难变形金属及合金的加工,达到控制和优化材料的组织结构、提高其性能的效果。The object of the present invention is to provide a new severe plastic deformation method and its device: tube-High Pressure Shearing (t-HPS for short) technology. This technology satisfies many requirements for the preparation of ultrafine-grained materials by SPD method, such as large plastic deformation, relatively low deformation temperature and high hydrostatic pressure inside the deformed material. This method avoids the cumbersome process of ARB, ECAP and back pressure ECAP technologies that require multiple operations. At the same time, due to the essential difference in loading methods, this method also overcomes the problem of insufficient hydrostatic pressure in the HPTT method of Tóth et al. When processing materials, it can provide high hydrostatic pressure conditions similar to HPT technology, so it is suitable for processing difficult-to-deform metals and alloys, so as to control and optimize the structure of materials and improve their performance.

实现本发明目的的技术解决方案为:一种管状材料高压剪切变形方法,首先选择加工的工件,工件为管状,采用约束体分别约束工件的内壁和外壁;然后直接对工件端部施加轴向压力,使得工件发生弹性变形或微小塑性变形,在工件内累加高静水压力;随后对与工件内壁或外壁接触的一个约束体提供扭矩,使其绕工件的中心轴转动,同时固定另一个约束体,在约束体与工件内外壁环向摩擦力的作用下,工件内部沿径向不同厚度处的材料以不同的角速度转动,从而实现工件的环向剪切变形。The technical solution to realize the object of the present invention is: a method for high-pressure shear deformation of tubular materials. First, select the workpiece to be processed. The pressure causes the workpiece to undergo elastic deformation or slight plastic deformation, and accumulates high hydrostatic pressure in the workpiece; then, a torque is provided to a constraint body in contact with the inner or outer wall of the workpiece to make it rotate around the central axis of the workpiece while fixing the other constraint body , under the action of the circumferential friction between the restraining body and the inner and outer walls of the workpiece, the materials at different thicknesses in the radial direction inside the workpiece rotate at different angular velocities, thereby realizing the circumferential shear deformation of the workpiece.

一种管状材料高压剪切变形装置,包括具有恒压功能的压力机和具有传递压力、约束形变以及实现部分旋转功能的模具;所述模具包括:上砧头、下砧头、固定或者可转动的刚性芯轴以及可转动或者固定的刚性环套;上砧头、下砧头分别安装在压力机的上压头和底座上,工件放置于上砧头和下砧头之间,上砧头下端与下砧头上端通过设置的凸台与工件的上、下端面接触,凸台的截面是与工件的上、下端面完全吻合的环形;工件的内部同心设有刚性芯轴,刚性芯轴外表面与工件的内壁接触,工件的外部同心设有刚性环套,刚性环套内表面与工件的外壁接触。A high-pressure shear deformation device for tubular materials, including a press with constant pressure function and a mold with the functions of transmitting pressure, restraining deformation and realizing partial rotation; the mold includes: an upper anvil, a lower anvil, fixed or rotatable The rigid mandrel and the rotatable or fixed rigid ring; the upper anvil and the lower anvil are respectively installed on the upper pressure head and the base of the press, the workpiece is placed between the upper anvil and the lower anvil, and the upper anvil The lower end and the upper end of the lower anvil come into contact with the upper and lower end surfaces of the workpiece through the set bosses. The outer surface is in contact with the inner wall of the workpiece, the outer surface of the workpiece is concentrically provided with a rigid ring, and the inner surface of the rigid ring is in contact with the outer wall of the workpiece.

本发明与现有技术相比,其显著优点:(1)加工工序简单。本发明提出的t-HPS方法是一种在传统的具有恒压功能的挤压机上单一道次即可实现的剧烈塑性变形方法。反观诸如累积轧制(ARB)方法、多向锻造、等径角挤压(ECAP)方法以及背压ECAP等方法,往往需要很多重复的工艺道次才能实现高应变量的塑性变形,人力消耗大。而本方法利用刚性环套、管状工件以及芯轴、管状工件之间摩擦力,转动刚性环套并固定芯轴,使得管状工件与刚性环套接触的外层区域相对于与芯轴接触的内层区域发生环向剪切,从而实现单一工艺道次下的剧烈塑性变形。真应变为1~10,甚至更高。如前文技术方案所述,本发明提出的t-HPS方法原理简单,设备易得,在一般的塑性成形实验室即可实现。Compared with the prior art, the present invention has significant advantages: (1) the processing procedure is simple. The t-HPS method proposed by the invention is a severe plastic deformation method that can be realized in a single pass on a traditional extruder with a constant pressure function. In contrast, methods such as the cumulative rolling (ARB) method, multi-directional forging, equal-diameter angular extrusion (ECAP) method, and back pressure ECAP often require many repeated process passes to achieve high-strain plastic deformation, which consumes a lot of manpower. . However, this method utilizes the frictional force between the rigid collar, the tubular workpiece, the mandrel, and the tubular workpiece to rotate the rigid collar and fix the mandrel so that the outer area of the tubular workpiece in contact with the rigid collar is relative to the inner area in contact with the mandrel. Circumferential shear occurs in the layer area, thereby achieving severe plastic deformation under a single process pass. The true value should be 1-10, or even higher. As described in the above technical solution, the t-HPS method proposed by the present invention has a simple principle and easy-to-obtain equipment, and can be realized in a general plastic forming laboratory.

(2)能够提供的静水压力高,因此可加工材料种类广,加工能力强。本发明提出的t-HPS方法直接对管状材料轴向加压,同时约束其径向变形,因而可在材料内部产生静水压力高达15~GPa。这是目前包括HPTT在内其它工艺无法达到的。而且,随着模具材料的发展,设计的改进,所能提供的静水压力会更高。在这种高静水压力条件进行塑性变形,材料表面和内部裂纹的产生和发展被有效抑制,从而使得很多难加工材料(如塑性较差的镁合金等)的可加工性提高。众所周知,镁合金等材料由于晶体结构为密排六方,滑移系数量有限,往往塑性差。对镁合金等难变形材料进行ARB或者ECAP加工时,试样经常有开裂现象。为避免开裂,往往需要提高加工温度,势必增加加工成本,更重要的是,随着加工温度的升高,材料的晶粒细化效果变差,晶粒变得粗大,这与我们提高材料性能的初衷相左。相比之下,本方法在室温条件或者较低的加热温度下即可实现对铝、铜、镍、镁、钛、钨及其合金以及低碳钢等众多材料的塑性加工,从而控制和改善其组织结构,提高其性能。(2) The hydrostatic pressure that can be provided is high, so the types of materials that can be processed are wide and the processing capacity is strong. The t-HPS method proposed by the present invention directly pressurizes the tubular material in the axial direction while constraining its radial deformation, so that the hydrostatic pressure inside the material can be as high as 15-GPa. This is currently unattainable by other processes including HPTT. Moreover, with the development of mold materials and design improvements, the hydrostatic pressure that can be provided will be higher. Plastic deformation under such high hydrostatic pressure conditions effectively inhibits the generation and development of surface and internal cracks, thus improving the machinability of many difficult-to-machine materials (such as magnesium alloys with poor plasticity, etc.). As we all know, materials such as magnesium alloys often have poor plasticity due to the hexagonal close-packed crystal structure and limited slip coefficients. When performing ARB or ECAP processing on hard-to-deform materials such as magnesium alloys, the samples often crack. In order to avoid cracking, it is often necessary to increase the processing temperature, which will inevitably increase the processing cost. More importantly, as the processing temperature increases, the grain refinement effect of the material will become worse, and the grains will become coarser. This has nothing to do with our improvement of material properties. Contrary to the original intention. In contrast, this method can realize plastic processing of many materials such as aluminum, copper, nickel, magnesium, titanium, tungsten and their alloys, and low-carbon steel at room temperature or at a lower heating temperature, thereby controlling and improving Its organizational structure improves its performance.

(3)能够获得的管状成品尺寸大。本发明提出的t-HPS方法选取的加工工件呈管状,其尺寸仅受设备规模限制。即便是在实验室,也可通过该方法制得~100mm高的管状材料,具有良好的性能,稍做后续处理即可在很多领域得到应用,此外获得的管状材料沿轴向剖开,经过轧制即可获得高性能板材。(3) The tubular finished product that can be obtained has a large size. The processing workpiece selected by the t-HPS method proposed by the present invention is in the shape of a tube, and its size is only limited by the scale of the equipment. Even in the laboratory, a tubular material with a height of ~100mm can be obtained by this method, which has good performance and can be applied in many fields with a little follow-up treatment. In addition, the obtained tubular material is cut along the axial direction and rolled. High-performance panels can be obtained by manufacturing.

附图说明 Description of drawings

图1是累积复合轧制(ARB)技术原理示意图。Figure 1 is a schematic diagram of the principle of cumulative composite rolling (ARB).

图2是等径角挤压(ECAP)技术原理示意图。Figure 2 is a schematic diagram of the principle of the equal radial angular extrusion (ECAP) technology.

图3是背压ECAP(BP-ECAP)技术原理示意图。Fig. 3 is a schematic diagram of the principle of back pressure ECAP (BP-ECAP) technology.

图4是高压扭转(HPT)技术原理示意图。Fig. 4 is a schematic diagram of the principle of high pressure torsion (HPT) technology.

图5是高压管扭转(high-pressure tube twisting-HPTT)技术原理示意图。Fig. 5 is a schematic diagram of the technical principle of high-pressure tube twisting (HPTT).

图6是本发明t-HPS技术原理示意图,其中,61-上砧头,62-刚性环套,63-管状工件,64-下砧头,65-刚性芯轴;h为管状工件高度;r为管状工件内半径;R管状工件外半径;P为压力;T为扭矩。Fig. 6 is a schematic diagram of the technical principle of t-HPS of the present invention, wherein, 61-upper anvil, 62-rigid ring sleeve, 63-tubular workpiece, 64-lower anvil, 65-rigid mandrel; h is the height of tubular workpiece; r R is the inner radius of the tubular workpiece; R is the outer radius of the tubular workpiece; P is the pressure; T is the torque.

图7是有限元模拟尺寸为r=10mm,R=11mm的2219T62铝合金管状工件经过90°环向剪切变形后的应变分布情况:沿径向最大应变10.79,最小应变8.41,统计平均值9.45。Figure 7 shows the strain distribution of the 2219T62 aluminum alloy tubular workpiece with finite element simulation size r=10mm and R=11mm after 90° circumferential shear deformation: the maximum strain along the radial direction is 10.79, the minimum strain is 8.41, and the statistical average value is 9.45 .

图8是t-HPS剧烈塑性变形方法实施方案的装置示意图,其中,(a)为爆炸视图:1-支撑柱,2-上砧头连接套筒,3-上砧头连接螺栓,4-连接套筒方形插销,5-连接套筒圆柱插销,6-下砧头,7-管状工件,8-刚性环套,9-下环形垫圈,10-上环形垫圈,11-一体化的上砧头与芯轴,12-芯轴套板,13-下砧头连接螺栓,14-伺服电机,15-空心轴减速器齿轮箱,16-皮带,17-推力轴承,18-刚性环套套筒,19-套筒连接螺栓;(b)为主视图。Fig. 8 is the device schematic diagram of t-HPS severe plastic deformation method embodiment, and wherein, (a) is exploded view: 1-support column, 2-up anvil head connection sleeve, 3-up anvil head connection bolt, 4-connection Sleeve square pin, 5-connecting sleeve cylindrical pin, 6-lower anvil, 7-tubular workpiece, 8-rigid collar, 9-lower ring washer, 10-upper ring washer, 11-integrated upper anvil With mandrel, 12-mandrel sleeve plate, 13-lower anvil connecting bolt, 14-servo motor, 15-hollow shaft reducer gearbox, 16-belt, 17-thrust bearing, 18-rigid ring sleeve, 19-sleeve connecting bolt; (b) main view.

具体实施方式 Detailed ways

本发明的材料加工目的在传统的具有恒压功能的挤压机上即可实现:管状工件被放置在下砧头上,工件外侧套有可转动的刚性环套,刚性芯轴从管状工件的中心穿过,上砧头直接将轴向压力传递给工件,管状工件在巨大轴向压力的作用下产生沿径向膨胀的趋势,刚性圆盘、芯轴对管状工件径向变形起到约束作用,这种对管状工件端部施加高压的同时限制其形变的设计使得在工件内部累加了高静水压力(1GPa~15GPa)。高静水压力条件下,将会在管状工件的内外壁都产生很大的摩擦力。虽然管状工件形状改变被限制,但其有沿轴向旋转的自由度,而上下砧头分别安装在挤压机的上下底板上,使与工件内壁或者外壁接触的约束体(分别为芯轴和刚性环套)中的一个绕管状工件的中心轴转动而另外一个固定,由于管状工件的内外壁与设备约束体之间摩擦力存在,工件内、外壁附近的材料有随约束体一起转动或者固定不动的趋势。高静水压力条件下,为了保持材料的连续性,管状工件沿径向不同厚度层的材料将以不同的角速度转动,即发生相对转动,材料在摩擦力的驱动下实现环向剪切(circumferential shearing)变形,很重要的一点是该变形是工件内部材料的切变,并未改变管状工件的宏观尺寸形状。The material processing purpose of the present invention can be realized on the traditional extruder with constant pressure function: the tubular workpiece is placed on the lower anvil, the outer side of the workpiece is covered with a rotatable rigid ring, and the rigid mandrel passes through the center of the tubular workpiece. However, the upper anvil directly transmits the axial pressure to the workpiece, and the tubular workpiece tends to expand in the radial direction under the action of the huge axial pressure. The rigid disk and the mandrel play a role in restraining the radial deformation of the tubular workpiece. This design of applying high pressure to the end of the tubular workpiece while limiting its deformation results in the accumulation of high hydrostatic pressure (1GPa-15GPa) inside the workpiece. Under high hydrostatic pressure conditions, great friction will be generated on both the inner and outer walls of the tubular workpiece. Although the shape change of the tubular workpiece is limited, it has the freedom of axial rotation, and the upper and lower anvils are respectively installed on the upper and lower bottom plates of the extruder, so that the constraints (respectively mandrel and One of the rigid rings rotates around the central axis of the tubular workpiece while the other is fixed. Due to the friction between the inner and outer walls of the tubular workpiece and the equipment constraints, the material near the inner and outer walls of the workpiece rotates or is fixed with the constraints. immobile trend. Under the condition of high hydrostatic pressure, in order to maintain the continuity of the material, the materials of different thickness layers along the radial direction of the tubular workpiece will rotate at different angular velocities, that is, relative rotation will occur, and the material will realize circumferential shearing (circumferential shearing) driven by friction. ) deformation, it is very important that the deformation is the shear of the internal material of the workpiece, and does not change the macroscopic size and shape of the tubular workpiece.

本发明能使管状材料真正在高静水压力(可达15~GPa)条件下,发生环向剪切塑性变形(真应可达10~)。从而通过塑性变形,控制和优化材料的组织结构、提高其性能。The invention can make the tubular material undergo circumferential shear plastic deformation (up to 10-GPa) under the condition of high hydrostatic pressure (up to 15-GPa). In this way, through plastic deformation, the structure of the material can be controlled and optimized, and its performance can be improved.

同时,本发明只需要在传统的具有恒压功能的挤压设备上安装一个由上砧头、芯轴、下砧头以及刚性圆盘等关键要素构成的组合模具,即可在较低的温度(如室温或者较低的加热温度)实现一种全新的剧烈塑性变形(SPD)加工方法——管状工件高压剪切(t-HPS)技术。t-HPS技术可行性高,操作无特殊要求,所需设备简单易得。同时,由于本发明是依托传统挤压设备实现的新的塑性加工方法,因此扩展了传统挤压设备的功用。本发明适用于剧烈塑性变形制备块体超细晶、纳米晶材料的实验研究和工业生产。利用本发明,可以制备高性能金属、合金、无机非金属材料及高分子材料。t-HPS方法制得的样品形状为管状,具有很高的实际应用潜力和价值。At the same time, the present invention only needs to install a combination mold consisting of key elements such as an upper anvil, a mandrel, a lower anvil, and a rigid disk on the traditional extrusion equipment with constant pressure function, so that it can be processed at a lower temperature. (such as room temperature or lower heating temperature) to achieve a new severe plastic deformation (SPD) processing method - tubular workpiece high pressure shearing (t-HPS) technology. t-HPS has high technical feasibility, no special requirements for operation, and the required equipment is simple and easy to obtain. At the same time, because the present invention is a new plastic processing method realized by relying on traditional extrusion equipment, it expands the functions of traditional extrusion equipment. The invention is suitable for experimental research and industrial production of bulk ultrafine crystal and nano crystal materials prepared by severe plastic deformation. Utilizing the invention, high-performance metals, alloys, inorganic non-metallic materials and polymer materials can be prepared. The shape of the sample prepared by the t-HPS method is tubular, which has high potential and value for practical application.

下面结合附图对本发明作进一步详细描述。The present invention will be described in further detail below in conjunction with the accompanying drawings.

结合图6,本发明管状材料高压剪切变形方法,首先选择加工的工件,工件为管状,采用约束体分别约束工件的内壁和外壁;然后直接对工件端部施加轴向压力,使得工件发生弹性变形或微小塑性变形,在工件内累加高达1~15GPa的静水压力;随后对与工件内壁或外壁接触的一个约束体提供扭矩,使其绕工件的中心轴转动,同时固定另一个约束体,在约束体与工件内外壁环向摩擦力的作用下,工件内部沿径向不同厚度处的材料以不同的角速度转动,从而实现工件的环向剪切变形。Referring to Fig. 6, the method for high-pressure shear deformation of tubular materials in the present invention first selects the workpiece to be processed. The workpiece is tubular, and the inner wall and outer wall of the workpiece are respectively restrained by constraining bodies; then axial pressure is directly applied to the end of the workpiece to make the workpiece elastic. Deformation or micro-plastic deformation, accumulating hydrostatic pressure up to 1-15GPa in the workpiece; then providing torque to a constraint body in contact with the inner or outer wall of the workpiece to make it rotate around the central axis of the workpiece, while fixing the other constraint body, in Under the action of the circumferential friction between the restraining body and the inner and outer walls of the workpiece, the materials at different thicknesses in the radial direction inside the workpiece rotate at different angular velocities, thereby realizing the circumferential shear deformation of the workpiece.

本发明管状材料高压剪切变形装置,包括具有恒压功能的压力机和具有传递压力、约束形变以及实现部分旋转功能的模具;所述模具包括:上砧头61、下砧头64、固定或者可转动的刚性芯轴65以及可转动或者固定的刚性环套62;上砧头61、下砧头64分别安装在压力机的上压头和底座上,工件63放置于上砧头61和下砧头64之间,上砧头61下端与下砧头64上端通过设置的凸台与工件63的上、下端面接触,凸台的截面是与工件63的上、下端面完全吻合的环形;工件63的内部同心设有刚性芯轴65,刚性芯轴65外表面与工件63的内壁接触,工件63的外部同心设有刚性环套,刚性环套62内表面与工件63的外壁接触。刚性环套62内表面与刚性芯轴65外表面经过毛化处理以增大与工件63之间的摩擦。上砧头61与刚性环套62之间采用间隙配合;刚性芯轴65与下砧头64之间采用间隙配合。The high-pressure shear deformation device for tubular materials of the present invention includes a press with constant pressure function and a mold with the functions of transmitting pressure, constraining deformation and realizing partial rotation; the mold includes: an upper anvil 61, a lower anvil 64, a fixed or A rotatable rigid mandrel 65 and a rotatable or fixed rigid ring 62; the upper anvil 61 and the lower anvil 64 are respectively installed on the upper ram and the base of the press, and the workpiece 63 is placed on the upper anvil 61 and the lower anvil. Between the anvil heads 64, the lower end of the upper anvil head 61 and the upper end of the lower anvil head 64 are in contact with the upper and lower end surfaces of the workpiece 63 through the provided bosses, and the cross-section of the bosses is a ring that completely matches the upper and lower end surfaces of the workpiece 63; The inside of the workpiece 63 is concentrically provided with a rigid mandrel 65 , the outer surface of the rigid mandrel 65 is in contact with the inner wall of the workpiece 63 , and the outer surface of the workpiece 63 is concentrically provided with a rigid collar, and the inner surface of the rigid collar 62 is in contact with the outer wall of the workpiece 63 . The inner surface of the rigid ring 62 and the outer surface of the rigid mandrel 65 are roughened to increase friction with the workpiece 63 . A clearance fit is adopted between the upper anvil 61 and the rigid ring sleeve 62 ; a clearance fit is adopted between the rigid mandrel 65 and the lower anvil 64 .

本发明管状材料高压剪切变形装置,所述刚性芯轴65或者刚性环套62之中有一个可转动,另一个则为固定,转动的角度无限制。In the high-pressure shear deformation device for tubular materials of the present invention, one of the rigid mandrel 65 or the rigid ring 62 is rotatable, and the other is fixed, and the angle of rotation is unlimited.

本发明管状材料高压剪切变形装置,所述刚性环套62可采用单层模具设计、预应力缠绕模具设计或预应力多层模具设计。所述上砧头61、刚性芯轴65为独立的两部分或者采用一体化设计使其成为一部分;所述上砧头61为整体设计或者组合设计,采用整体设计时,上砧头61、下砧头64端部分别有与工件63的上、下端面形状吻合的环形凸台,采用组合设计时,砧头包括砧头主体和环形垫圈两部分,环形垫圈截面与工63端面形状吻合。In the high-pressure shear deformation device for tubular materials of the present invention, the rigid ring sleeve 62 can adopt a single-layer mold design, a prestressed winding mold design or a prestressed multi-layer mold design. The upper anvil 61 and the rigid mandrel 65 are two independent parts or adopt an integrated design to make it a part; the upper anvil 61 is an integral design or a combined design. Anvil head 64 ends have the annular boss that matches with the upper and lower end face shape of workpiece 63 respectively, when adopting combined design, anvil head comprises two parts of anvil head main body and ring gasket, and ring gasket cross section matches with tool 63 end face shapes.

下面结合图6说明依据本发明提出的剧烈塑性变形新方法具体实施细节及设备工作情况。The specific implementation details and equipment working conditions of the new method for severe plastic deformation proposed by the present invention will be described below in conjunction with FIG. 6 .

如图6所示,t-HPS方法由一个包括61-上砧头,62-刚性环套,64-下砧头和65-刚性芯轴等四部分构成的模具,结合具有保压功能的压力机,在63-管状工件上实现。As shown in Figure 6, the t-HPS method consists of a mold consisting of four parts including 61-upper anvil, 62-rigid ring, 64-lower anvil and 65-rigid mandrel, combined with a pressure holding function machine, realized on a 63-tubular workpiece.

首先,将61-上砧头、64-下砧头分别安装在压力机的上底板和下底板(或工作台)上,63-管状工件放置于61-上砧头和64-下砧头之间,61-上砧头下端与64-下砧头上端通过设置的凸台与63-管状工件的上、下端面接触,凸台的截面是与63-管状工件的上、下端面完全吻合的环形;63-管状工件的内部同心设有65-刚性芯轴,65-刚性芯轴外表面与63-管状工件的内壁接触,63-管状工件的外部同心设有62-刚性环套,62-刚性环套内表面与63-管状工件的外壁接触。First, install 61-upper anvil and 64-lower anvil on the upper and lower bases (or workbenches) of the press respectively, and place 63-tubular workpiece between 61-upper anvil and 64-lower anvil Between, the lower end of 61-upper anvil head and the upper end of 64-lower anvil head are in contact with the upper and lower end surfaces of 63-tubular workpiece through the set boss, and the section of the boss is completely consistent with the upper and lower end faces of 63-tubular workpiece Ring; 63- the inner concentricity of tubular workpiece is provided with 65- rigid mandrel, the outer surface of 65- rigid mandrel is in contact with the inner wall of 63- tubular workpiece, the outer concentricity of 63- tubular workpiece is provided with 62- rigid ring sleeve, 62- The inner surface of the rigid collar is in contact with the outer wall of the 63-tubular workpiece.

此时,63-管状工件处在由61-上砧头、62-刚性环套、64-下砧头和65-刚性芯轴构成的密闭空腔中。然后,压力机对61-上砧头进行下压,并维持压力恒定于某一数值。61-上砧头向下位移的过程中,61-上砧头同样会对3-管状工件产生向下的压力,由于63-管状工件受到由61-上砧头、62-刚性环套、64-下砧头和65-刚性芯轴构成的密闭空腔的约束,因此其内部产生高的静水压力(可高达~15GPa)。对62-刚性环套施加环向推力,在扭矩的作用下使之环向旋转,与此同时,61-上砧头、64-下砧头和65-刚性芯轴不发生旋转,在62-刚性环套与63-管状工件以及65-芯轴与63-管状工件之间摩擦力的作用下,63-管状工件将发生环向剪切变形。随着旋转角度的增大,剪切变形量变得很大,从而有效地控制和优化材料的组织结构,提高其性能。At this time, 63-tubular workpiece is in the airtight cavity formed by 61-upper anvil, 62-rigid collar, 64-lower anvil and 65-rigid mandrel. Then, the press presses down on the 61-upper anvil, and keeps the pressure constant at a certain value. During the downward displacement of the 61-upper anvil, the 61-upper anvil will also produce downward pressure on the 3-tubular workpiece, because the 63-tubular workpiece is subjected to the 61-upper anvil, 62-rigid ring sleeve, 64 -Constraint of the closed cavity formed by the lower anvil and the 65-rigid mandrel, thus generating high hydrostatic pressure (up to ~15GPa) inside. Apply a hoop thrust to the 62-rigid ring sleeve, and make it hoop-rotate under the action of torque. At the same time, 61-upper anvil, 64-lower anvil and 65-rigid mandrel do not rotate. At 62- Under the action of friction between the rigid ring and the 63-tubular workpiece and the 65-mandrel and the 63-tubular workpiece, the 63-tubular workpiece will undergo circumferential shear deformation. As the rotation angle increases, the amount of shear deformation becomes large, which effectively controls and optimizes the structure of the material and improves its performance.

此外,其它条件不变的情况下,环向旋转65-刚性芯轴而固定62-刚性环套可以使管状材料产生类似的环向剪切塑性变形效果。这种情况的t-HPS技术原理示意图从略。In addition, under the condition that other conditions remain unchanged, the circular rotation 65-rigid mandrel and fixed 62-rigid collar can produce a similar circumferential shear plastic deformation effect on the tubular material. The schematic diagram of the t-HPS technology principle in this case is omitted.

为了考察t-HPS工艺过程中管状工件的力学行为,特别是应变的分布情况,而对该方法进行了二维和三维的有限元模拟分析。有限元模拟时,选用了2219T62铝合金工件,该铝合金的材料性能参数如表1所示,该材料的流变规律可以用Crussard-Jaoul应变硬化模型加以描述。其中为流变应力,σ0=290MPa为屈服强度,K=248MPa为强度系数,εp为塑性应变,n=0.36为应变硬化指数。In order to investigate the mechanical behavior of the tubular workpiece during the t-HPS process, especially the strain distribution, two-dimensional and three-dimensional finite element simulations were carried out on the method. In the finite element simulation, the 2219T62 aluminum alloy workpiece was selected. The material performance parameters of the aluminum alloy are shown in Table 1. The rheological law of the material can be calculated using the Crussard-Jaoul strain hardening model be described. where is flow stress, σ 0 =290MPa is yield strength, K=248MPa is strength coefficient, ε p is plastic strain, n=0.36 is strain hardening exponent.

简便起见,模拟温度为室温,并且不考虑变形过程中材料的温升和应变速率敏感性。结果表明t-HPS方法能够在尺寸较大的工件中累加非常高的应变量,如图7所示,内径20mm,外径22mm的管状工件仅仅经过90度的环向剪切,其平均应变即可达到9.45。For simplicity, the simulation temperature is room temperature, and the temperature rise and strain rate sensitivity of the material during deformation are not considered. The results show that the t-HPS method can accumulate very high strain in larger workpieces. As shown in Figure 7, the tubular workpiece with an inner diameter of 20mm and an outer diameter of 22mm only undergoes a 90-degree circumferential shear, and its average strain is Can reach 9.45.

表1.t-HPS工艺有限元模拟选材2219T62铝合金力学常数和物理性质Table 1. Mechanical constants and physical properties of 2219T62 aluminum alloy material selected by t-HPS process finite element simulation

下面结合实施例对本发明做进一步详细说明。The present invention will be described in further detail below in conjunction with the examples.

如图8所示装置由t-HPS剧烈塑性变形法原理实现部、动力装置和连接部等三部分组成。图8(a)为装置的爆炸视图,详细给出了装置的组成细节。As shown in Figure 8, the device consists of three parts: the realization part of the t-HPS severe plastic deformation method principle, the power device and the connection part. Figure 8(a) is an exploded view of the device, detailing the composition of the device.

6-下砧头、7-管状工件、8-刚性环套、9-下环形垫圈、10-上环形垫圈、11-一体化的上砧头与芯轴和12-芯轴套板组成了整个装置的原理实现部。7-管状工件穿过11-一体化的上砧头与芯轴,其上下端面各放置一个环形垫圈(9-、10-),工件被8-刚性环套包围,上、下砧头(11-、6-)通过上、下垫圈(9-、10-)对7-管状工件轴向施压时,11-芯轴和8-刚性环套约束了其径向膨胀,在工件内部累积的高静水压力。11-芯轴末端为六棱柱,与12-芯轴套板中孔形状尺寸相同。芯轴插入套板中孔后,其转动将受到约束。对8-刚性环套施加环向推力,在扭矩的作用下使之旋转,转动速度1~5rpm,与此同时,11-一体化的上砧头和芯轴受约束而不发生旋转,在8-刚性环套与7-管状工件以及11-芯轴与7-管状工件之间摩擦力的作用下,7-管状工件将发生环向剪切变形。6-lower anvil head, 7-tubular workpiece, 8-rigid ring sleeve, 9-lower ring washer, 10-upper ring washer, 11-integrated upper anvil head and mandrel and 12-mandrel sleeve plate constitute the whole The principle realization part of the device. 7-The tubular workpiece passes through the 11-integrated upper anvil and the mandrel, and an annular gasket (9-, 10-) is placed on the upper and lower end faces, the workpiece is surrounded by 8-rigid rings, and the upper and lower anvils (11 -, 6-) When the 7-tubular workpiece is axially pressed through the upper and lower gaskets (9-, 10-), the 11-mandrel and the 8-rigid ring restrict its radial expansion, and the accumulation inside the workpiece High hydrostatic pressure. The end of the 11-mandrel is a hexagonal prism, which has the same shape and size as the hole in the 12-mandrel sleeve plate. After the mandrel is inserted into the hole in the cover plate, its rotation will be constrained. Apply a hoop thrust to the 8-rigid ring sleeve, and make it rotate under the action of torque at a rotation speed of 1-5rpm. -Under the action of friction between the rigid collar and the 7-tubular workpiece and the 11-mandrel and the 7-tubular workpiece, the 7-tubular workpiece will undergo circumferential shear deformation.

该实施方案中,上砧头与芯轴采用一体化设计,一方面使得芯轴易于固定,另一方面,对管状工件脱模有利。此外上、下砧头(11-、6-)并不直接接触7-管状工件,压力是通过上、下环形垫圈(9-、10-)传递给工件。这样设计是因为与工件断面直接接触的部位受力情况非常恶劣,增设由硬质合金制成的环形垫圈,可提高砧头的使用寿命,降低模具更换成本。考虑到8-刚性环套与11-芯轴之间既需要沿轴向自有移动又需要沿周向自由转动,而6-下砧头与11-芯轴之间只要求沿轴向自有移动,因此在选取孔与轴之间的配合时,11-一体化的上砧头、芯轴与8-刚性环套之间采用F7/h6基轴制间隙配合;11-一体化的上砧头、芯轴与6-下砧头采用H7/g6基孔制间隙配合。这种间隙配合的选择,从脱模的角度考虑,也是有利的。In this embodiment, the upper anvil and the mandrel adopt an integrated design, which on the one hand makes the mandrel easy to fix and on the other hand facilitates the demoulding of the tubular workpiece. In addition, the upper and lower anvils (11-, 6-) do not directly contact the 7-tubular workpiece, and the pressure is transmitted to the workpiece through the upper and lower annular gaskets (9-, 10-). This design is because the stress on the part directly in contact with the workpiece section is very bad. Adding an annular gasket made of hard alloy can improve the service life of the anvil and reduce the cost of mold replacement. Considering that the 8-rigid ring sleeve and the 11-mandrel need to move freely in the axial direction and freely rotate in the circumferential direction, while the relationship between the 6-lower anvil and the 11-mandrel only requires free movement in the axial direction. Therefore, when selecting the fit between the hole and the shaft, 11-integrated upper anvil head, mandrel and 8-rigid ring sleeve adopt F7/h6 base shaft clearance fit; 11-integrated upper anvil The head, mandrel and 6-lower anvil adopt H7/g6 base hole clearance fit. This choice of clearance fit is also advantageous from the standpoint of demoulding.

刚性环套旋转并在摩擦力作用下使管状工件发生环向剪切,该动作所需扭矩依靠动力装置实现。该动力装置通过一个14-伺服电机通过16-皮带轮带动15-空心轴减速器输出扭矩。The rigid ring rotates and shears the tubular workpiece in a circumferential direction under the action of friction, and the torque required for this action is realized by the power device. The power unit drives the 15-hollow shaft reducer to output torque through a 14-servo motor through a 16-belt pulley.

由2-上砧头连接套筒、3-上砧头连接螺栓、4-连接套筒方形插销和5-连接套筒圆柱插销组成的连接部将11-一体化的上砧头和芯轴与压力机的上压板相连。由1-支撑柱、13-下砧头连接螺栓、17-推力轴承、18-刚性环套套筒和19-套筒连接螺栓组成的连接部将The connecting part composed of 2-upper anvil head connection sleeve, 3-upper anvil head connection bolt, 4-connection sleeve square pin and 5-connection sleeve cylindrical pin connects 11-integrated upper anvil head and mandrel with The upper platen of the press is connected. The connecting part consisting of 1-support column, 13-lower anvil connecting bolt, 17-thrust bearing, 18-rigid ring sleeve and 19-sleeve connecting bolt will

6-下砧头通过1-支撑柱与压力机的下底板相连,同时18-刚性环套套筒和19-套筒连接螺栓连接15-空心轴减速器和8-刚性环套,实现扭矩的传递。17-推力轴承降低了轴向摩擦力对8-刚性环套旋转的阻碍。6-The lower anvil head is connected to the lower base plate of the press through 1-support column, while 18-rigid ring sleeve and 19-sleeve connecting bolt are connected to 15-hollow shaft reducer and 8-rigid ring sleeve to realize torque transfer. The 17-thrust bearing reduces the resistance of axial friction to the rotation of the 8-rigid collar.

18-刚性环套采用预应力缠绕模具设计时,内层选择硬度和韧性都较高的材质,如模具钢;缠绕层采用韧性较高的材质,如弹簧钢丝或者弹簧钢带;外层采用韧性较高的材质,如中碳钢。18-刚性环套采用预应力多层环套设计时,内层选择硬度和韧性都较高的材质,如模具钢;其它层选择韧性较高的材质,如中碳合金钢或者模具钢。11-一体化的上砧头与芯轴、下砧头在工作部位镶嵌硬质合金,其余部位选择材质为模具钢。9-下环形垫圈、10-上环形垫圈选用硬质合金或者钢结硬质合金。18- When the rigid ring is designed with a prestressed winding mold, the inner layer should be made of a material with high hardness and toughness, such as die steel; the winding layer should be made of a material with high toughness, such as spring steel wire or spring steel belt; the outer layer should be made of toughness Higher materials, such as medium carbon steel. 18-When the rigid ring is designed with prestressed multi-layer rings, the inner layer should be made of a material with high hardness and toughness, such as die steel; the other layers should be made of a material with high toughness, such as medium carbon alloy steel or die steel. 11- The integrated upper anvil head and mandrel, and the lower anvil head are inlaid with hard alloy in the working part, and the material of the rest parts is mold steel. 9-the lower ring washer, 10-the upper ring washer are selected hard alloy or steel-bonded hard alloy.

具体选材如下:模具钢为Cr5Mo1V钢;弹簧钢为65Mn钢;中碳钢为45号钢;中碳合金钢为45Mn钢;硬质合金为YG6A。The specific materials are as follows: die steel is Cr5Mo1V steel; spring steel is 65Mn steel; medium carbon steel is No. 45 steel; medium carbon alloy steel is 45Mn steel; hard alloy is YG6A.

该实施方案中,装配好的t-HPS装置的主视图如图8(b)所示。A front view of the assembled t-HPS device in this embodiment is shown in Figure 8(b).

通过该方案对工业纯铝、6063铝合金以及AZ31镁合金管状工件进行了初步实验研究。管状工件的内径40mm,外径46mm,高40mm。变形前后,工件的宏观尺寸、形状保持不变。Through this scheme, a preliminary experimental study was carried out on industrial pure aluminum, 6063 aluminum alloy and AZ31 magnesium alloy tubular workpieces. The inner diameter of the tubular workpiece is 40 mm, the outer diameter is 46 mm, and the height is 40 mm. Before and after deformation, the macroscopic size and shape of the workpiece remain unchanged.

工业纯铝未进行t-HPS前的平均晶粒尺寸为24μm,压缩试验屈服强度73.7MPa;在1.5GPa静水压力下以1rpm的转动速度经过30°的t-HPS变形,平均应变达到4,平均晶粒尺寸达到633nm,压缩试验屈服强度增至261.3MPa。The average grain size of industrial pure aluminum before t-HPS is 24μm, and the yield strength of compression test is 73.7MPa; under 1.5GPa hydrostatic pressure and 1rpm rotation speed, after 30° t-HPS deformation, the average strain reaches 4, the average The grain size reaches 633nm, and the compression test yield strength increases to 261.3MPa.

6063铝合金未进行t-HPS前的平均晶粒尺寸为80μm,压缩试验屈服强度156.8MPa;在2.5GPa静水压力以1rpm的转动速度经过60°的t-HPS变形,平均应变达到8,平均晶粒尺寸达到561nm,压缩试验屈服强度增至447.6MPa。The average grain size of 6063 aluminum alloy before t-HPS is 80 μm, and the yield strength of compression test is 156.8 MPa; under the hydrostatic pressure of 2.5 GPa and the rotation speed of 1 rpm, after t-HPS deformation of 60°, the average strain reaches 8, and the average grain size The particle size reaches 561nm, and the yield strength of compression test increases to 447.6MPa.

AZ31镁合金塑性较差,我们对模具进行了100℃的加热。未进行t-HPS前的平均晶粒尺寸为27μm,压缩试验屈服强度276.4MPa;在3GPa静水压力下以1rpm的转动速度经过90°的t-HPS变形,平均应变达到9,平均晶粒尺寸达到335nm,压缩试验屈服强度增至590.2MPa。AZ31 magnesium alloy has poor plasticity, and we heated the mold at 100°C. The average grain size before t-HPS was 27 μm, and the yield strength of the compression test was 276.4 MPa; under the hydrostatic pressure of 3 GPa and the rotation speed of 1 rpm, after 90° t-HPS deformation, the average strain reached 9, and the average grain size reached 335nm, the compression test yield strength increased to 590.2MPa.

Claims (6)

1.一种管状材料高压剪切变形装置,其特征在于:包括具有恒压功能的压力机和具有传递压力、约束形变以及实现部分旋转功能的模具;所述模具包括:上砧头(61)、下砧头(64)、固定或者可转动的刚性芯轴(65)以及可转动或者固定的刚性环套(62);上砧头(61)、下砧头(64)分别安装在压力机的上压头和底座上,工件(63)放置于上砧头(61)和下砧头(64)之间,上砧头(61)下端与下砧头(64)上端通过设置的凸台与工件(63)的上、下端面接触,凸台的截面是与工件(63)的上、下端面完全吻合的环形;工件(63)的内部同心设有刚性芯轴(65),刚性芯轴(65)外表面与工件(63)的内壁接触,工件(63)的外部同心设有刚性环套(62),刚性环套(62)内表面与工件(63)的外壁接触。1. A tubular material high-pressure shear deformation device is characterized in that: it comprises a press with constant pressure function and a mold with transmission pressure, constraint deformation and partial rotation functions; said mold includes: anvil (61) , the lower anvil (64), the fixed or rotatable rigid mandrel (65) and the rotatable or fixed rigid ring (62); the upper anvil (61) and the lower anvil (64) are respectively installed in the press On the upper indenter and the base, the workpiece (63) is placed between the upper anvil (61) and the lower anvil (64), and the lower end of the upper anvil (61) and the upper end of the lower anvil (64) pass through the set boss In contact with the upper and lower end surfaces of the workpiece (63), the cross section of the boss is a ring that completely matches the upper and lower end surfaces of the workpiece (63); the inner part of the workpiece (63) is concentrically provided with a rigid mandrel (65), and the rigid core The outer surface of the shaft (65) contacts with the inner wall of the workpiece (63), and the outer concentricity of the workpiece (63) is provided with a rigid collar (62), and the inner surface of the rigid collar (62) contacts with the outer wall of the workpiece (63). 2.根据权利要求1所述的管状材料高压剪切变形装置,其特征在于:刚性环套(62)内表面与刚性芯轴(65)外表面经过毛化处理以增大与工件(63)之间的摩擦。2. The high-pressure shear deformation device for tubular materials according to claim 1, characterized in that: the inner surface of the rigid ring (62) and the outer surface of the rigid mandrel (65) are roughened to increase the contact with the workpiece (63) friction between. 3.根据权利要求1所述的管状材料高压剪切变形装置,其特征在于:上砧头(61)与刚性环套(62)之间采用间隙配合;刚性芯轴(65)与下砧头(64)之间采用间隙配合。3. The high-pressure shear deformation device for tubular materials according to claim 1, characterized in that: clearance fit is used between the upper anvil (61) and the rigid ring (62); the rigid mandrel (65) and the lower anvil (64) adopt clearance fit between. 4.根据权利要求1所述的管状材料高压剪切变形装置,其特征在于:所述刚性芯轴(65)或者刚性环套(62)之中有一个可转动,另一个则为固定,转动的角度无限制。4. The high-pressure shear deformation device for tubular materials according to claim 1, characterized in that: one of the rigid mandrel (65) or the rigid collar (62) is rotatable, while the other is fixed and rotates angle is unlimited. 5.根据权利要求1所述的管状材料高压剪切变形装置,其特征在于:所述刚性环套(62)可采用单层模具设计、预应力缠绕模具设计或预应力多层模具设计。5. The high-pressure shear deformation device for tubular materials according to claim 1, characterized in that: the rigid ring (62) can be designed with a single-layer mold, a prestressed winding mold or a prestressed multi-layer mold. 6.根据权利要求1所述的管状材料高压剪切变形装置,其特征在于:所述上砧头(61)、刚性芯轴(65)为独立的两部分或者采用一体化设计使其成为一部分;所述上砧头(61)为整体设计或者组合设计,采用整体设计时,上砧头(61)、下砧头(64)端部分别有与工件(63)的上、下端面形状吻合的环形凸台,采用组合设计时,砧头包括砧头主体和环形垫圈两部分,环形垫圈截面与工件(63)端面形状吻合。6. The high-pressure shear deformation device for tubular materials according to claim 1, characterized in that: the upper anvil (61) and the rigid mandrel (65) are two independent parts or are integrated into one part ; The upper anvil (61) is an integral design or a combined design. When the overall design is adopted, the ends of the upper anvil (61) and the lower anvil (64) are respectively matched with the upper and lower end surfaces of the workpiece (63) The annular boss, when adopting combined design, anvil head comprises two parts of anvil head main body and ring washer, and ring washer cross-section matches with workpiece (63) end face shape.
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