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CN101044850B - Special sticky shellac for tea garden and preparation method thereof - Google Patents

Special sticky shellac for tea garden and preparation method thereof Download PDF

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Publication number
CN101044850B
CN101044850B CN200710008942A CN200710008942A CN101044850B CN 101044850 B CN101044850 B CN 101044850B CN 200710008942 A CN200710008942 A CN 200710008942A CN 200710008942 A CN200710008942 A CN 200710008942A CN 101044850 B CN101044850 B CN 101044850B
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sticky
shellac
attractant
tea
polyisobutylene
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CN101044850A (en
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胡宏友
李雄
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Xiamen University
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Xiamen University
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Abstract

茶园专用粘虫胶及其制备方法,涉及一种粘虫胶。提供一种粘捕能力较好的主要用于茶园的粘虫胶及其制备方法。其原料组成及其按质量百分比的含量为:聚异丁烯为60%~80%,填充剂为10%~30%,增粘剂为0.5%~5%,引诱剂为1%~6%。制备时,先将引诱剂按比例加入聚异丁烯搅拌;加入填充剂和增粘剂,再搅拌均匀即可。由于采用无污染的高分子粘结剂聚异丁烯为主,添加优选的增粘剂、填充剂和引诱剂等,其粘虫效果及其性价比好,尤其是对茶园体型较大的害虫粘捕能力更好,因此是一种适用于有机茶园生产的无污染粘虫胶,若与其它产品例如市场上俗称的黄纸板等配合使用,可获得极好的引诱粘结茶园害虫的效果。The special sticky shellac for tea gardens and a preparation method thereof relate to a sticky shellac. The invention provides a sticky shellac mainly used in tea gardens with good sticking and catching ability and a preparation method thereof. The raw material composition and its mass percentage content are as follows: 60%-80% of polyisobutylene, 10%-30% of filler, 0.5%-5% of tackifier, and 1%-6% of attractant. During preparation, the attractant is firstly added in proportion to the polyisobutylene and stirred; the filler and the viscosifier are added, and then stirred evenly. Due to the use of non-polluting polymer binder polyisobutylene as the main agent, adding preferred tackifiers, fillers and attractants, etc., the sticky insect effect and cost-effectiveness are good, especially for large-scale pests in tea gardens. Even better, it is a kind of non-polluting sticky insect glue suitable for the production of organic tea gardens. If it is used in conjunction with other products such as yellow cardboard commonly known in the market, it can obtain an excellent effect of attracting and bonding tea garden pests.

Description

茶园专用粘虫胶及其制备方法 Special sticky shellac for tea garden and preparation method thereof

技术领域technical field

本发明涉及一种粘虫胶,尤其是涉及一种主要用于有机茶园的粘虫胶及其制备方法。The invention relates to a sticky shellac, in particular to a sticky shellac mainly used in organic tea gardens and a preparation method thereof.

背景技术Background technique

由于茶叶适宜生长在水热资源较为丰富的地区,因此病毒虫害较为严重,对茶叶生产造成严重的影响,特别是体型较大的害虫,例如小绿叶蟑、刺粉虱、蓟马及蚜虫等。由于现有市售的粘虫板的粘捕能力较差,特别是对体型较大的害虫的粘捕能力更差,普遍存在不易涂覆、易老化、遇水易失效、价格高等缺点。因此造成茶农大量使用禁用农药,而茶叶又是一种直接泡饮的食品,茶叶农残已严重影响了人们的健康。为此必须大力开展茶树病虫采用无公害防治技术,以确保茶叶的卫生品质。Since tea is suitable for growing in areas with rich water and heat resources, virus and insect pests are more serious, which have a serious impact on tea production, especially large-scale pests, such as small green leaf cockroaches, whiteflies, thrips and aphids. Due to the poor sticky catch ability of the existing commercially available insect sticky boards, especially for larger pests, there are generally disadvantages such as difficult coating, easy aging, easy failure when exposed to water, and high price. Therefore cause tea farmers to use banned pesticides in large quantities, and tealeaves is a kind of food that directly soaks and drinks, and tealeaves pesticide residues have had a strong impact on people's health. For this reason must vigorously carry out tea tree pests adopting pollution-free control technology, to ensure the hygienic quality of tea.

公开号为CN1847354的发明专利申请提供一种特别适用于防治害虫的粘虫胶。它由以下重量份比的原料制成的:聚丙烯20-35份,植物油15-25份,松香25-35份,动物胶或动物蜡20-35份。Publication number is that the invention patent application of CN1847354 provides a kind of sticky shellac that is especially suitable for controlling pests. It is made of the following raw materials by weight: 20-35 parts of polypropylene, 15-25 parts of vegetable oil, 25-35 parts of rosin, and 20-35 parts of animal gum or animal wax.

公开号为CN1911012的发明专利申请提供一种粘虫胶及其制备方法,将松香、蓖麻油和石蜡按一定的重量比例混合而成,制作工艺简便易行,粘性强且持续时间长,克服了同类产品由于粘稠度太高而难于实施操作的缺陷,可用于农林业部分植物害虫的防治,特别用于粘滞草履蚧上树、制作性诱捕器粘板用胶。The invention patent application with the publication number CN1911012 provides a kind of sticky shellac and its preparation method, which is formed by mixing rosin, castor oil and paraffin in a certain weight ratio. Similar products are difficult to operate due to the high viscosity, which can be used for the prevention and control of some plant pests in agriculture and forestry, especially for sticky paramecium climbing trees and making traps for sticking boards.

公开号为CN1067255的发明专利申请提供一种粘虫胶粘剂,其主要特点是,将天然橡胶与添加剂混合而制成,天然橡胶为凝固的胶或乳胶,添加剂为柴油等,所制成的胶粘剂具有粘住害虫的能力。适用于农业灭害虫、家庭灭蚊蝇、防盗等。The invention patent application with publication number CN1067255 provides a kind of sticky insect adhesive. Its main feature is that it is made by mixing natural rubber with additives. The natural rubber is solidified glue or latex, and the additives are diesel oil. The prepared adhesive has Ability to stick to pests. It is suitable for agricultural pest control, household mosquito control, anti-theft and so on.

有关用于茶园的粘虫胶鲜有报道。There are few reports about the sticky shellac used in tea gardens.

发明内容Contents of the invention

本发明的目的在于提供一种粘捕能力较好的主要用于茶园的粘虫胶及其制备方法。The object of the present invention is to provide a kind of sticky shellac mainly used in tea gardens with good sticking and catching ability and its preparation method.

本发明所述的茶园粘虫胶的原料组成及其按质量百分比的含量为:The raw material composition of tea garden sticky shellac and its content by mass percentage are:

聚异丁烯为60%~80%,填充剂为10%~30%,增粘剂为0.5%~5%,引诱剂为1%~6%。The polyisobutylene is 60%-80%, the filler is 10%-30%, the tackifier is 0.5%-5%, and the attractant is 1%-6%.

所述的聚异丁烯的分子量最好<180万,填充剂选自二氧化硅或氧化钙,增粘剂选自羧甲基纤维素(CMC)、橡胶或卡拉胶等,引诱剂选自糖、脂溶性香、乙酸乙酯或果蔬提取液等。The molecular weight of described polyisobutylene is preferably<1,800,000, filler is selected from silicon dioxide or calcium oxide, tackifier is selected from carboxymethyl cellulose (CMC), rubber or carrageenan etc., attractant is selected from sugar, Fat-soluble incense, ethyl acetate or fruit and vegetable extracts, etc.

本发明所述的茶园粘虫胶的制备方法包括以下步骤:The preparation method of tea garden sticky shellac of the present invention comprises the following steps:

1)先将引诱剂按比例加入聚异丁烯,搅拌均匀;1) Add the attractant to polyisobutylene in proportion, and stir evenly;

2)加入填充剂和增粘剂,再次搅拌均匀即可。2) Add filler and tackifier, and stir evenly again.

由于本发明所述的茶园粘虫胶采用无污染的高分子粘结剂聚异丁烯为主,添加优选的增粘剂、填充剂和引诱剂等,通过大田施用证明,其粘虫效果及其性价比等要优于市售的类似产品(例如中国台湾产的黄板纸等),尤其是对茶园体型较大的害虫粘捕能力要显著优于市售类似产品,而价格仅约为市售相同产品的1/4。因此本发明所述的茶园粘虫胶是一种适用于有机茶园生产的无污染粘虫胶,若与其它产品例如市场上俗称的黄纸板等配合使用,可获得极好的引诱粘结茶园害虫的效果。Because the tea garden sticky insect glue of the present invention mainly adopts the non-polluting polymer binder polyisobutylene, and adds preferred tackifiers, fillers and attractants, etc., it has been proved by field application that its armyworm effect and cost performance etc. are better than similar products on the market (such as yellow cardboard produced in Taiwan, China, etc.), especially the ability to stick and catch larger pests in tea gardens is significantly better than similar products on the market, and the price is only about the same as that on the market. 1/4 of the product. Therefore the tea garden sticky shellac described in the present invention is a kind of non-polluting sticky shellac suitable for the production of organic tea gardens. If it is used in conjunction with other products such as yellow cardboard commonly known as the market, it can obtain excellent lure and bonding tea garden pests. Effect.

具体实施方式Detailed ways

以下实施例将对本发明作进一步的说明。The following examples will further illustrate the present invention.

先将引诱剂白砂糖按比例加入聚异丁烯,搅拌均匀,再加入填充剂二氧化硅和增粘剂CMC,再次搅拌均匀,得茶园粘虫胶。按质量百分比,各原料的含量为聚异丁烯60%,填充剂二氧化硅30%,增粘剂CMC 5%,引诱剂白砂糖5%,聚异丁烯的分子量<180万。Add the attractant white granulated sugar into the polyisobutylene in proportion, stir evenly, then add the filler silicon dioxide and the tackifier CMC, stir again evenly, and get the tea garden sticky shellac. According to mass percentage, the content of each raw material is 60% of polyisobutylene, 30% of filler silicon dioxide, 5% of tackifier CMC, 5% of attractant white granulated sugar, and the molecular weight of polyisobutylene is less than 1.8 million.

在上述实施例中,可将引诱剂改用葡萄糖,加入的填充剂改用氧化钙,增粘剂改用橡胶。按质量百分比,各原料的含量为聚异丁烯69.5%,填充剂氧化钙26%,增粘剂橡胶0.5%,引诱剂葡萄糖4%,聚异丁烯的分子量<180万。In the above embodiment, the attractant can be replaced by glucose, the added filler can be replaced by calcium oxide, and the tackifier can be replaced by rubber. According to mass percentage, the content of each raw material is polyisobutylene 69.5%, filler calcium oxide 26%, tackifier rubber 0.5%, attractant glucose 4%, and the molecular weight of polyisobutylene is less than 1.8 million.

在上述实施例中,可将引诱剂改用脂溶性香,加入的填充剂仍为氧化钙,增粘剂改用卡拉胶。按质量百分比,各原料的含量为聚异丁烯72.5%,填充剂氧化钙22%,增粘剂卡拉胶2.5%,引诱剂脂溶性香3%,聚异丁烯的分子量<180万。In the above embodiment, the attractant can be changed to fat-soluble incense, the added filler is still calcium oxide, and the tackifier is changed to carrageenan. According to mass percentage, the content of each raw material is polyisobutylene 72.5%, filler calcium oxide 22%, tackifier carrageenan 2.5%, attractant fat-soluble fragrance 3%, and the molecular weight of polyisobutylene is less than 1.8 million.

在上述实施例中,可将引诱剂改用乙酸乙酯,加入的填充剂改用二氧化硅,增粘剂改用CMC。按质量百分比,各原料的含量为聚异丁烯78%,填充剂二氧化硅18%,增粘剂CMC3%,引诱剂乙酸乙酯1%,聚异丁烯的分子量<180万。In the above examples, the attractant can be changed to ethyl acetate, the added filler can be changed to silicon dioxide, and the tackifier can be changed to CMC. According to mass percentage, the content of each raw material is 78% of polyisobutylene, 18% of filler silicon dioxide, 3% of tackifier CMC, 1% of attractant ethyl acetate, and the molecular weight of polyisobutylene is less than 1.8 million.

在上述实施例中,可将引诱剂改用果蔬提取液,加入的填充剂仍为二氧化硅,增粘剂改用橡胶。按质量百分比,各原料的含量为聚异丁烯80%,填充剂二氧化硅10%,增粘剂橡胶4%,引诱剂果蔬提取液6%,聚异丁烯的分子量<180万。In the above embodiments, the attractant can be replaced by fruit and vegetable extracts, the added filler is still silicon dioxide, and the tackifier can be replaced by rubber. According to mass percentage, the content of each raw material is 80% of polyisobutylene, 10% of filler silicon dioxide, 4% of tackifier rubber, 6% of attractant fruit and vegetable extract, and the molecular weight of polyisobutylene is less than 1.8 million.

Claims (2)

1. insects adherbing glue used specially for tea-tree garden is characterized in that its raw material is formed and content by mass percentage is that polyisobutene is 60%~80%, and filler is 10%~30%, and tackifier are 0.5%~5%, and attractant is 1%~6%;
The molecular weight of polyisobutene<1,800,000;
Filler is selected from silica or calcium oxide;
Tackifier are selected from carboxymethyl cellulose, rubber or carragheen;
Attractant is selected from sugar, fat-soluble perfume (or spice), ethyl acetate or fruits and vegetables extract.
2. the preparation method of insects adherbing glue used specially for tea-tree garden as claimed in claim 1 is characterized in that may further comprise the steps:
1) earlier attractant is added polyisobutene in proportion, stir;
2) add filler and tackifier, stirring once more gets final product.
CN200710008942A 2007-04-30 2007-04-30 Special sticky shellac for tea garden and preparation method thereof Expired - Fee Related CN101044850B (en)

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CN102161874A (en) * 2010-02-24 2011-08-24 江苏动感控虫科技有限公司 Dynamic noctilucent insect glue
CN102161463A (en) * 2010-02-24 2011-08-24 江苏动感控虫科技有限公司 Dynamic noctilucent armyworm glue filling technology
CN102850965B (en) * 2012-08-13 2014-07-23 北京绿叶世纪日化用品有限公司 Binder, preparation method of the binder and insect bonding plate coated with the binder
CN106922665A (en) * 2015-12-30 2017-07-07 江苏龙灯化学有限公司 A kind of method lured the jelly composition and spray and adhesive tape of insect and reduce insect infestations
CN105918352A (en) * 2016-05-17 2016-09-07 梁文荣 Hyphantria cunea attractant
CN105961437A (en) * 2016-05-17 2016-09-28 梁文荣 Geometrid moth attractant
CN105794882A (en) * 2016-05-17 2016-07-27 梁文荣 Psilgramma menephorn attractant
CN106070288A (en) * 2016-06-03 2016-11-09 华南农业大学 A kind of pine tumor is as attractant
CN106350002A (en) * 2016-08-28 2017-01-25 仇颖超 Preparation method of persistently-adhesive weather-proof insecticidal shellac
CN109181589A (en) * 2018-08-31 2019-01-11 黄旭东 A kind of environmental protection mythimna separata offset plate and preparation method thereof
CN109280538B (en) * 2018-09-21 2020-12-18 刘伟萍 Insect sticking glue for tree trunk

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