CN101007055B - Preparation method of eucommia pollen soft capsule rich in α-linolenic acid - Google Patents
Preparation method of eucommia pollen soft capsule rich in α-linolenic acid Download PDFInfo
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- CN101007055B CN101007055B CN200710017223A CN200710017223A CN101007055B CN 101007055 B CN101007055 B CN 101007055B CN 200710017223 A CN200710017223 A CN 200710017223A CN 200710017223 A CN200710017223 A CN 200710017223A CN 101007055 B CN101007055 B CN 101007055B
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Abstract
本发明公开了一种杜仲花粉软胶囊产品的制备方法，原料选择杜仲花粉和紫苏籽油或杜仲籽油。制备方法包括清揀、消毒、烘炒、破壁、配料、装软胶囊等工艺制备成杜仲花粉软胶囊。本发明所制备的杜仲花粉软胶囊营养成分含量高(营养成分不损失)、富含α-亚麻酸，杜仲总黄酮含量高、并能较易保存。产品具有降血压、降血脂、预防脑血栓和心肌梗塞、预防老年痴呆症，抗肿瘤等作用，有良好的市场前景。The invention discloses a preparation method of eucommia pollen soft capsule product. The raw materials are eucommia pollen and perilla seed oil or eucommia seed oil. The preparation method comprises the processes of cleaning, sterilizing, roasting, breaking walls, batching ingredients, filling soft capsules and the like to prepare the eucommia pollen soft capsules. The eucommia pollen soft capsule prepared by the invention has high nutrient content (no loss of nutrient content), is rich in alpha-linolenic acid, has high eucommia total flavonoid content, and is easy to preserve. The product has the effects of lowering blood pressure, lowering blood fat, preventing cerebral thrombosis and myocardial infarction, preventing senile dementia, anti-tumor, etc., and has a good market prospect.
Description
Technical field
The invention belongs to food (health food) manufacture method, be specifically related to a kind of preparation method that is rich in the eucommia pollen soft capsule product of alpha-linolenic acid nutritional labeling.
Background technology
Pollen has the characteristics of low fat high protein, contains several amino acids, the rope of supporting one's family, enzyme, trace element, bioactive substance, and people claim that pollen is the condensation product of nutrition, nutrient source completely, has the good reputation of " miniature nutrition library ".Modern science studies confirm that pollen has functions such as raise immunity, resisting fatigue, physical strength reinforcing, nourishing the brain and improving intelligence, anti-hypoxia, sexual function improving, defying age and skin maintenance.Also have functions such as the prostatic hyperplasia of inhibition, angiocardiopathy preventing, blood sugar regulation, promotion hemopoietic, control agent intracellular metabolite and endocrine simultaneously.Therefore in the nourishing healthy of back to nature was modish, pollen more and more was subjected to people's favor.
Since the seventies in 20th century, many countries are constantly goed deep into and comprehensively research the development and use pay attention to day by day of pollen.China starts from 20th century the mid-80 for the research of pollens nutrition composition, effect.Many experts study the nutritional labeling of China's 60 various plants pollen, for the development and use of China's pollen contribute.
The Cortex Eucommiae (Eucommia ulmoides Oliv.) all has distribution for the Eucommiaceae Cortex Eucommiae belongs to deciduous tree in more than 20 province of China (city, autonomous region), about 360,000 hm of planting area
2Its skin, leaf, really, spend and all be rich in multiple natural active matter, be important medicinal plants, Cortex Eucommiae, leaf, seed and male flower have been developed as medicine or health food.Have effects such as blood pressure regulation, blood fat reducing, blood sugar lowering, reducing weight and beautifying features, defying age, enhancing immunity.The Cortex Eucommiae is a dioecian plant, the male Cortex Eucommiae that large tracts of land is planted, and annual spring, first leaf was opened to a large amount of pollen.But the someone researches and develops so far, does not see relevant report both at home and abroad.
Study recently according to the applicant, the protein content of eucommia pollen reaches 28.27% (according to Wang Kaifa and Wu Wenshan etc. to 60 kinds of nectariferous plant pollen analysis results, the protein content average out to about 20% of nectariferous plant pollen, protein content only accounts for 10% in the pollen kind more than 25%), its content is profuse.Crude fat content low (2.50%), it is close with nectariferous plant pollen that (as Flos Camelliae Japonicae powder is 2.34%, Caulis fici pumilae (Fructus Fici Pumilae) pollen is 2.46%), reducing sugar (6.70%) and sucrose (1.90%) content are than general nectariferous plant pollen low (as the Flos Camelliae Japonicae powder reducing sugar is 27.72%, and sucrose is 8.57%).Eucommia pollen just in time meets diabetes patient's high protein, low sugar, low-fat dietary requirements.Contain 17 seed amino acids in the eucommia pollen, comprise 7 kinds of essential amino acids such as threonine, valine, methionine, isoleucine, leucine, phenylalanine, lysine.Total amino acid content is 18.01g/100g, must aminoacid be 6.097g/100g wherein, accounts for 33.85% of total amino acid content.The essential amino acids proportioning is almost approaching or exceed the mode standard value that FAO/WHO recommends, and proves that its protein quality is higher.In addition, also containing the semi-dispensable amino acid that lacks in egg, the milk in the eucommia pollen---the necessary histidine of tyrosine and infants growth and development proves absolutely that eucommia pollen is a kind of good proteinaceous nutrient source.Content of vitamin E is 2.246mg/100g in the eucommia pollen.According to interrelated data, Caulis fici pumilae (Fructus Fici Pumilae) pollen is 1.13mg/100g, and Malay oil palm pollen is 1.22mg/100g.As seen, content of vitamin E is higher in the eucommia pollen.Vitamin E can be caught human body waste (free radical), and can make radical reduction rapidly, and causes free radical chain reactions to stop, and has protected cell membrane, thereby has helped prolonging the life-span of cell, has very strong anti-aging effects.Be rich in 11 kinds of mineral elements such as potassium, sodium, phosphorus, calcium, magnesium, ferrum and zinc in the eucommia pollen, can fully satisfy the human body needs.What is particularly worth mentioning is that to contain selenium element (0.0096mg/100g) in the eucommia pollen that selenium energy antagonism noxious substance has antitumaous effect to the harm of human body.Selenium destroys the lipid peroxide that has formed in human body, vitamin E stops the generation of lipid peroxide in human body, both collaborative mutually performance antioxidations.And just in time contain this two classes material in the eucommia pollen, thereby the nutritional labeling of further understanding eucommia pollen is abundant and comprehensive.
Study recently according to the applicant, the eucommia pollen general flavone content reaches 3.36%.To 16 kinds of nectariferous plant pollen count analysis results, the general flavone content of nectariferous plant pollen on average is about 2.65% according to Li quintessence etc., and the eucommia pollen general flavone content is 1.27 times of meansigma methods; The general flavone content of eucommia pollen is Cortex Eucommiae (0.46%), leaf (1.61%) 7.3 times and 2.1 times.As seen, the general flavone content in the eucommia pollen is higher.Total flavones is a kind of natural active matter, has the prevention cardiovascular and cerebrovascular disease, defying age, effect such as anticancer.
Fructus Perillae be the first batch of promulgation of Ministry of Public Health be food be again one of 60 kinds of article of medicine, Oleum Perillae alpha-linolenic acid content very high (alpha-linolenic acid content 〉=50%) is than the numb acid content height of α-industry in the oleum lini.The blood fat reducing prevention of brain thrombosis that it had, keep the necessary factor of brain and function of nervous system, prevention canceration and suppress physiological functions such as tumor cell transferance, cause countries in the world expert's extensive concern, now be developed as food, health food and the cosmetics of super quality.After biochemistry proof alpha-linolenic acid enters human body, under the effect of enzyme, generate EPA, DHA successively.Because above-mentioned biochemical process is irreversible, so bathypelagic fish oil not only all has the function alpha-linolenic acid of human body, and abundanter, more comprehensively.Because the non-oxidizability of alpha-linolenic acid is better than EPA, DHA, and fat do not contain cholesterol, and the delicate fragrance of vegetable oil has remedied the shortcoming of fish oil fishy smell again, so medical circle thinks that Oleum Perillae is the renewal product of bathypelagic fish oil.At present, countries such as Japan, Germany, the U.S. all pay much attention to exploitation Oleum Perillae product, and China has also formed Oleum Perillae exploitation heat, at present, Oleum Perillae soft capsule product is arranged on the market.The fatty acid of eucommia ulmoides seed oil (alpha-linolenic acid content 〉=50%) and Oleum Perillae is formed and not only surprising similar of content, and quality index such as outward appearance, abnormal smells from the patient, index of refraction is very close again, has shown that the size of molecular structure, fatty acid molecule amount of both inside and proportion etc. are basic identical.So eucommia ulmoides seed oil also has same exploitation and is worth.But the existing market product is that Oleum Perillae (or eucommia ulmoides seed oil) is the soft capsule product of raw material, but because raw material is single, its efficacy effect still awaits improving.
Relevant in the market pollen product is that the water extract of pollen or ethanol extraction are the oral liquid made of raw material, soft capsule, tablet, beverage etc. mostly, but because of some nutritional labeling in leaching process has lost, so the pollen utilization rate is lower; Also have pollen (plastics package or bottling) directly edible product behind sterilization, breaking cellular wall,,, be difficult for longer-term and preserve in case open plastics package or bottle though its pollen utilization rate is high.
The present situation that problem that exists based on the existing market pollen product and eucommia pollen product are not seen research and development so far.Therefore, seek a kind of preparation method and become the industry problem demanding prompt solution with nutrient composition content height, pollen utilization rate height, health-care effect eucommia pollen product strong, that also can more easily preserve.
Summary of the invention
Problem that exists at the existing market pollen product and eucommia pollen product be the blank of research and development not so far, the object of the invention is, a kind of that be rich in alpha-linolenic acid and nutrient composition content height, pollen utilization rate height, and the preparation method of the eucommia pollen product that can preserve easily are provided.
The technical solution that realizes above-mentioned purpose is, a kind of alpha-linolenic acid, nutrient composition content height, pollen utilization rate height, and preparation method of the eucommia pollen product that can more easily preserve of being rich in, it is characterized in that, raw material is eucommia pollen and Oleum Perillae or eucommia ulmoides seed oil, adopts the following step to be prepared into the eucommia pollen soft capsule:
QINGJIAN step: eucommia pollen is carried out QINGJIAN, remove impurity;
Sterilisation step: the eucommia pollen after the QINGJIAN adopts 75% alcohol disinfecting;
The bake and parch step: the eucommia pollen after will sterilizing carries out bake and parch, and bake and parch elder generation bake and parch under 100 ℃ of temperature reduced the temperature to 60 ℃ after 3 minutes, continued bake and parch again, till bake and parch is done;
The breaking cellular wall step: the eucommia pollen that bake and parch is done adopts conventional method to carry out breaking cellular wall, promptly gets Cortex Eucommiae pollen (processed by breaking wall);
Batching step: Cortex Eucommiae pollen (processed by breaking wall) and Oleum Perillae or eucommia ulmoides seed oil (are adopted traditional squeezing or Co
2That supercritical extraction method extracts, and purify after added the crude oil of 0.1%VE antioxidant) mixes mutually by 1: 1～1: 3 (weight ratio), usefulness homogenizer (colloid mill) mix homogeneously must mix extractum;
Dress soft capsule step: pilular extract is packed into soft capsule according to a conventional method gets final product.
The eucommia pollen soft capsule of method preparation of the present invention is in blood pressure lowering, blood fat reducing, prevention of brain thrombosis and myocardial infarction, prevention senile dementia, aspects such as antitumor, the effect direction of Oleum Perillae (or eucommia ulmoides seed oil) is consistent with eucommia pollen (general flavone content height), both effect stacks, have extremely strong potentiation, can improve the health-care effect of eucommia pollen and Oleum Perillae (or eucommia ulmoides seed oil) greatly.
The specific embodiment
Below in conjunction with the embodiment that the inventor provides, the present invention is described in further detail.
Eucommia pollen soft capsule preparation method of the present invention, it comprises 6 technical processs such as QINGJIAN, sterilization, bake and parch, breaking cellular wall, batching, dress soft capsule, concrete steps are:
1. QINGJIAN step: eucommia pollen is carried out QINGJIAN, remove impurity;
2. sterilisation step: the eucommia pollen after the QINGJIAN adopts 75% alcohol disinfecting;
3. bake and parch step: the eucommia pollen after will sterilizing carries out bake and parch, bake and parch earlier under 100 ℃ of temperature bake and parch reduce the temperature to 60 ℃ after 3 minutes, continue bake and parch again, till bake and parch is done;
4. breaking cellular wall step: the eucommia pollen that bake and parch is done adopts conventional method to carry out breaking cellular wall, promptly gets Cortex Eucommiae pollen (processed by breaking wall).
5. batching step: (wherein Oleum Perillae or eucommia ulmoides seed oil adopt traditional squeezing or Co with Cortex Eucommiae pollen (processed by breaking wall) and Oleum Perillae or eucommia ulmoides seed oil
2That supercritical extraction method extracts, and purify after added the crude oil of 0.1%VE antioxidant) mixes mutually by 1: 1～1: 3 (weight ratio), usefulness homogenizer (colloid mill) mix homogeneously must mix extractum.
6. dress soft capsule step: will mix pilular extract and be packed into soft capsule according to a conventional method and get final product.
Below be the specific embodiment that the inventor provides:
Eucommia pollen soft capsule embodiment 1:
Get the 20kg eucommia pollen, Pick removes foreign material such as stone, sprig, and earlier bake and parch 3 minutes under 100 ℃ of temperature forwards bake and parch under 60 ℃ of temperature to, oven dry back breaking cellular wall again.With Cortex Eucommiae pollen (processed by breaking wall) and Oleum Perillae (wherein traditional the squeezing or Co of Oleum Perillae or eucommia ulmoides seed oil employing
2Supercritical extraction method extracts, through purifying after and added the crude oil of 0.1%VE antioxidant) 20kg mixes mutually, usefulness homogenizer (colloid mill) mix homogeneously must mix extractum, will mix pilular extract and be packed into soft capsule according to a conventional method.
Eucommia pollen capsule embodiment 2:
Get the 10kg eucommia pollen, Pick removes foreign material such as stone, sprig, and earlier bake and parch 3 minutes under 100 ℃ of temperature forwards bake and parch under 60 ℃ of temperature to, oven dry back breaking cellular wall again.Cortex Eucommiae pollen (processed by breaking wall) and Oleum Perillae (are adopted traditional squeezing or Co
2That supercritical extraction method extracts, through purifying after and added the crude oil of 0.1%VE antioxidant) 20kg mixes mutually, usefulness homogenizer (colloid mill) mix homogeneously must mix extractum, will mix pilular extract and be packed into soft capsule according to a conventional method and get final product.
Eucommia pollen soft capsule embodiment 3:
Get the 10kg eucommia pollen, Pick removes foreign material such as stone, sprig, and earlier bake and parch 3 minutes under 100 ℃ of temperature forwards bake and parch under 60 ℃ of temperature to, oven dry back breaking cellular wall again.Cortex Eucommiae pollen (processed by breaking wall) and Oleum Perillae (are adopted traditional squeezing or Co
2That supercritical extraction method extracts and after purifying, added the crude oil of 0.1%VE antioxidant) mix mutually by 30kg, with homogenizer (colloid mill) mix homogeneously, must mix extractum, will mix pilular extract and be packed into soft capsule according to a conventional method.
Eucommia pollen soft capsule embodiment 4:
Get the 20kg eucommia pollen, Pick removes foreign material such as stone, sprig, and earlier bake and parch 3 minutes under 100 ℃ of temperature forwards bake and parch under 60 ℃ of temperature to, oven dry back breaking cellular wall again.Cortex Eucommiae pollen (processed by breaking wall) and eucommia ulmoides seed oil (are adopted traditional squeezing or Co
2That supercritical extraction method extracts and after purifying, added the crude oil of 0.1%VE antioxidant) 20kg mixes mutually, with homogenizer (colloid mill) mix homogeneously, must mix extractum, and will mix pilular extract and be packed into soft capsule according to a conventional method and get final product.
Eucommia pollen capsule embodiment 5:
Get the 10kg eucommia pollen, Pick removes foreign material such as stone, sprig, and earlier bake and parch 3 minutes under 100 ℃ of temperature forwards bake and parch under 60 ℃ of temperature to, oven dry back breaking cellular wall again.Cortex Eucommiae pollen (processed by breaking wall) and eucommia ulmoides seed oil (are adopted traditional squeezing or Co
2That supercritical extraction method extracts and after purifying, added the crude oil of 0.1%VE antioxidant) mix mutually by 20kg, with homogenizer (colloid mill) mix homogeneously, must mix extractum, will mix pilular extract and be packed into soft capsule according to a conventional method and get final product.
Eucommia pollen soft capsule embodiment 6:
Get the 10kg eucommia pollen, Pick removes foreign material such as stone, sprig, and earlier bake and parch 3 minutes under 100 ℃ of temperature forwards bake and parch under 60 ℃ of temperature to, oven dry back breaking cellular wall again.Cortex Eucommiae pollen (processed by breaking wall) and eucommia ulmoides seed oil (are adopted traditional squeezing or Co
2That supercritical extraction method extracts, and purify after added the crude oil of 0.1%VE antioxidant) 30kg mixes mutually, with homogenizer (colloid mill) mix homogeneously, must mix extractum, will mix pilular extract and be packed into soft capsule according to a conventional method and get final product.
Method of the present invention can be amplified on the basis of the application's technical scheme and produced, and all can reach purpose of the present invention.
Need to prove that raw material of the present invention is selected natural eucommia pollen, Oleum Perillae or eucommia ulmoides seed oil for use,, do not need to do toxicology test, can think that it is safe, nontoxic according to the regulation of FAO/WHO food additive Professional Committee.
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| CN104068403A (en) * | 2014-07-04 | 2014-10-01 | 张海龙 | Capsule containing staminate flower power of eucommia ulmoides |
| CN106036818A (en) * | 2016-05-10 | 2016-10-26 | 王斌 | Capsules containing eucommia ulmoides male flowers and pollen |
| CN107951921A (en) * | 2018-01-12 | 2018-04-24 | 郑州中科新兴产业技术研究院 | A kind of method that flavones is extracted in the powder from eucommia Bark male flower |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1686309A (en) * | 2005-03-28 | 2005-10-26 | 王庆才 | Compound rose essential oil soft capsule and its preparation method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1686309A (en) * | 2005-03-28 | 2005-10-26 | 王庆才 | Compound rose essential oil soft capsule and its preparation method |
Non-Patent Citations (2)
| Title |
|---|
| 赵德义,徐爱遐,张博勇,张鞍灵,张康健.杜仲籽油与紫苏籽油脂肪酸组成的比较研究.西北植物学报25 1.2005,25(1),191-193. |
| 赵德义,徐爱遐,张博勇,张鞍灵,张康健.杜仲籽油与紫苏籽油脂肪酸组成的比较研究.西北植物学报25 1.2005,25(1),191-193. * |
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