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CN100584507C - Composite control method of heat cycle for electron beam welding of TiAl intermetallic compounds - Google Patents

Composite control method of heat cycle for electron beam welding of TiAl intermetallic compounds Download PDF

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CN100584507C
CN100584507C CN200710072370A CN200710072370A CN100584507C CN 100584507 C CN100584507 C CN 100584507C CN 200710072370 A CN200710072370 A CN 200710072370A CN 200710072370 A CN200710072370 A CN 200710072370A CN 100584507 C CN100584507 C CN 100584507C
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welding
intermetallic compound
tial intermetallic
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CN101073849A (en
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冯吉才
陈国庆
张秉刚
何景山
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Harbin Institute of Technology Shenzhen
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Abstract

TiAl intermetallic compound electron beam welding thermal cycle composite control method belongs to intermetallic compound jointing field.The invention solves the electron beam welding of TiAl intermetallic compound and be easy to generate macroscopical cold crack problem, can obtain the flawless joint.Method of the present invention is between welding object and welding machine anchor clamps thermal insulation board to be housed; Apply clamping force in two tabular welding object directions parallel then and fix, perhaps fix in the clamping force that axially applies of two tubulose welding objects with weld seam; Divide the thermal cycle of three phases programming continuous control whole welding process under vacuum condition, employing defocuses butt welded seam and carries out shuttle-scanning, preheating step by step; Weld immediately after the preheating; Adopt immediately after the welding and defocus butt welded seam and carry out shuttle-scanning after heat step by step.Welding control method process of the present invention is easy, need not increase equipment or fill transition material, is applicable to multiple joint type of attachment.

Description

TiAl金属间化合物电子束焊接热循环复合控制方法 Composite control method of heat cycle for electron beam welding of TiAl intermetallic compounds

技术领域 technical field

本发明涉及TiAl金属间化合物电子束焊接方法,属于金属间化合物焊接领域。The invention relates to a TiAl intermetallic compound electron beam welding method, belonging to the field of intermetallic compound welding.

背景技术 Background technique

目前在发动机研究方面的一个重点是采用新型材料替代传统的Ti合金和Ni基高温合金,以增加发动机的推重比并提高高温使用性能。TiAl金属间化合物密度低,弹性模量高,并且具有良好的高温强度、抗蠕变和抗氧化能力,相比于传统的高温合金来说TiAl金属间化合物使用温度可提高到750℃~950℃,而密度仅为Ni基高温合金的一半,是一种很有应用前景的高温结构材料,可应用于汽车或航空发动机的高温部件,如叶片、涡轮盘、尾喷管和气门阀等。对于在工程实际中应用TiAl金属间化合物,必须成功地开发出其连接技术,国内外研究结果表明,固态连接如钎焊、扩散焊、摩擦焊等被认为是较为有效的连接技术,但往往受连接形式和使用温度的限制,并且较多地采用搭接接头使焊接结构复杂,难以实现轻量化。因此有必要对TiAl金属间化合物的熔焊进行深入研究,尤其是真空条件下高能电子束焊接技术的开发。但是,TiAl金属间化合物最突出的问题是γ-TiAl本身滑移系较少,位错运动和增殖困难,室温塑性低及变形能力差。虽然通过合金化或采用不同的热处理工艺可改善这种材料的组织和塑韧性,但电子束焊接时的快速热循环使接头形成的组织不同于母材,并且容易造成较大的热致应力,导致了接头极易形成冷裂纹,制约了该合金在工程实际中的应用,目前国内外解决这一问题的合理方法尚未见报道。At present, a focus in engine research is to use new materials to replace traditional Ti alloys and Ni-based superalloys to increase the thrust-to-weight ratio of the engine and improve high-temperature performance. TiAl intermetallic compound has low density, high elastic modulus, and has good high-temperature strength, creep resistance and oxidation resistance. Compared with traditional superalloys, the service temperature of TiAl intermetallic compound can be increased to 750 ° C ~ 950 ° C , and the density is only half of that of Ni-based superalloys, it is a promising high-temperature structural material, which can be applied to high-temperature components of automobiles or aero-engines, such as blades, turbine discs, exhaust pipes and valves. For the application of TiAl intermetallic compounds in engineering practice, its connection technology must be successfully developed. Research results at home and abroad show that solid-state connections such as brazing, diffusion welding, friction welding, etc. are considered to be more effective connection technologies, but are often subject to The connection form and the use temperature are limited, and more lap joints are used to make the welding structure complicated and it is difficult to achieve light weight. Therefore, it is necessary to conduct in-depth research on the fusion welding of TiAl intermetallic compounds, especially the development of high-energy electron beam welding technology under vacuum conditions. However, the most prominent problems of TiAl intermetallic compounds are that γ-TiAl itself has few slip systems, difficulty in dislocation movement and proliferation, low room temperature plasticity and poor deformability. Although the microstructure and plasticity of this material can be improved by alloying or using different heat treatment processes, the rapid thermal cycle during electron beam welding makes the microstructure of the joint different from that of the base metal, and it is easy to cause large thermally induced stress. It leads to the easy formation of cold cracks in the joints, which restricts the application of the alloy in engineering practice. At present, there are no reports on the reasonable methods to solve this problem at home and abroad.

发明内容 Contents of the invention

本发明的目的在于解决TiAl金属间化合物电子束焊接容易产生宏观冷裂纹问题。The purpose of the invention is to solve the problem that the electron beam welding of TiAl intermetallic compound is easy to produce macroscopic cold cracks.

TiAl金属间化合物电子束焊接热循环复合控制方法,它的焊接对象是两块厚度为0.8mm~5.0mm的板状物,具体步骤为:TiAl intermetallic compound electron beam welding heat cycle composite control method, its welding object is two plates with a thickness of 0.8mm ~ 5.0mm, the specific steps are:

步骤一、将已经去除内部应力、待焊面平整清洁的两块TiAl金属间化合物的板材用夹具固定之前,在焊机夹具底座和每个焊接对象之间分别固定一块隔热板;Step 1. Before fixing the two TiAl intermetallic compound plates whose internal stress has been removed and whose welding surface is smooth and clean, fix a heat shield between the welding fixture base and each welding object;

步骤二、对焊接对象实施夹紧,所述夹具仅在焊接对象的与焊缝平行的方向施加夹紧力;Step 2, clamping the welding object, the clamp only applies a clamping force in the direction parallel to the welding seam of the welding object;

步骤三、在5×10-2Pa至5×10-4Pa的大气压下,采用散焦对待焊处进行往复扫描、分级预热,每一级分别采用2mA~12mA中从小到大依次递增的束流从焊缝的一端扫描到另一端,加速电压为50kV~55kV,聚焦电流3370mA,扫描速度为2mm/s~10mm/s;Step 3. Under the atmospheric pressure of 5×10 -2 Pa to 5×10 -4 Pa, use defocus to scan back and forth on the part to be welded, and preheat in stages. The beam scans from one end of the weld to the other end, the accelerating voltage is 50kV~55kV, the focusing current is 3370mA, and the scanning speed is 2mm/s~10mm/s;

步骤四、步骤三完成之后,立即进行焊接,加速电压与步骤三相同,聚焦电流为2590mA,束流为3mA~50mA,焊接速度为2mm/s~15mm/s;After step 4 and step 3 are completed, weld immediately, the acceleration voltage is the same as step 3, the focusing current is 2590mA, the beam current is 3mA-50mA, and the welding speed is 2mm/s-15mm/s;

步骤五、步骤四完成之后,立即采用散焦对焊缝进行分级后热,每一级分别采用12mA~1mA中从大到小依次递减的束流从焊缝的一端扫描到另一端,加速电压与步骤三相同,聚焦电流为3370mA,扫描速度为2mm/s~20mm/s。After step 5 and step 4 are completed, defocusing is used to classify the weld immediately after heating, and each level uses 12mA ~ 1mA beam current in descending order to scan from one end of the weld to the other end, and the acceleration voltage Same as Step 3, the focusing current is 3370mA, and the scanning speed is 2mm/s-20mm/s.

TiAl金属间化合物电子束焊接热循环复合控制方法,它的焊接对象为两根壁厚为0.8mm~3.5mm的TiAl金属间化合物的管材,焊接的焊缝为环形焊缝,具体步骤为:TiAl intermetallic compound electron beam welding heat cycle compound control method, its welding object is two pipes of TiAl intermetallic compound with a wall thickness of 0.8mm to 3.5mm, and the welded seam is a circular weld seam. The specific steps are:

步骤一、将已经去除内部应力、待焊面平整清洁的两个焊接对象用夹具固定之前,在夹具与焊接对象之间固定隔热板;Step 1. Fix the heat shield between the fixture and the welding object before fixing the two welding objects whose internal stress has been removed and whose welding surface is to be smooth and clean;

步骤二、对焊接对象实施夹紧,所述夹具对焊接对象采用轴向夹紧的方式;Step 2, clamping the welding object, and the clamp adopts an axial clamping method for the welding object;

步骤三、在5×10-2Pa至5×10-4Pa的大气压下,采用散焦对待焊处进行重复扫描、分级预热,每一级分别采用2mA~10mA中从小到大依次递增的束流绕环形焊缝扫描一周;加速电压为50kV~55kV,聚焦电流3350mA,扫描速度为2mm/s~8mm/s;Step 3. Under the atmospheric pressure of 5×10 -2 Pa to 5×10 -4 Pa, use defocus to scan repeatedly and preheat the area to be welded in stages. The beam scans around the circular weld seam for one week; the accelerating voltage is 50kV~55kV, the focusing current is 3350mA, and the scanning speed is 2mm/s~8mm/s;

步骤四、步骤三完成之后立即进行焊接,加速电压与步骤三相同,聚焦电流为2590mA,束流为2mA~32mA,焊接速度为2mm/s~10mm/s;Step 4. Immediately weld after step 3 is completed. The acceleration voltage is the same as step 3. The focusing current is 2590mA, the beam current is 2mA~32mA, and the welding speed is 2mm/s~10mm/s;

步骤五、步骤四完成之后,立即对焊接完成的焊缝采用散焦进行分级后热,每一级分别采用10mA~2mA中从大到小依次递减的束流绕环形焊缝扫描一周,加速电压与步骤三相同,聚焦电流为3350mA,扫描速度为2mm/s~12mm/s。After step 5 and step 4 are completed, immediately defocus the welded seam and heat it after classification. Each level uses 10mA-2mA beam currents that decrease in order from large to small to scan around the circular weld seam for a week, and the acceleration voltage Same as Step 3, the focusing current is 3350mA, and the scanning speed is 2mm/s~12mm/s.

当焊接对象是两块厚度为0.8mm~2.0mm的板状物时,具体步骤为:When the welding objects are two plates with a thickness of 0.8mm to 2.0mm, the specific steps are:

步骤一、将已经去除内部应力、待焊面平整清洁的两块TiAl金属间化合物的板材用夹具固定之前,在焊机夹具底座和每个焊接对象之间分别固定一块隔热板;Step 1. Before fixing the two TiAl intermetallic compound plates whose internal stress has been removed and whose welding surface is smooth and clean, fix a heat shield between the welding fixture base and each welding object;

步骤二、对焊接对象实施夹紧,所述夹具仅在焊接对象与焊缝平行的方向施加夹紧力;Step 2, clamping the welding object, the clamp only applies a clamping force in the direction parallel to the welding object and the weld seam;

步骤三、在5×10-2Pa至5×10-4Pa的大气压下,采用散焦对待焊处进行往复扫描、两级预热,每一级分别采用2mA的束流从焊缝的一端扫描到另一端,加速电压为50kV~55kV,聚焦电流3370mA,扫描速度为2mm/s~10mm/s;Step 3. Under the atmospheric pressure of 5×10 -2 Pa to 5×10 -4 Pa, use defocusing to scan the part to be welded back and forth, and preheat in two stages. Each stage uses 2mA beam current from one end of the weld Scanning to the other end, the accelerating voltage is 50kV~55kV, the focusing current is 3370mA, and the scanning speed is 2mm/s~10mm/s;

步骤四、步骤三完成之后,立即进行焊接,加速电压与步骤三相同,聚焦电流为2590mA,束流为2mA~8mA,焊接速度为5mm/s~15mm/s;After step 4 and step 3 are completed, weld immediately, the acceleration voltage is the same as step 3, the focusing current is 2590mA, the beam current is 2mA~8mA, and the welding speed is 5mm/s~15mm/s;

步骤五、步骤四完成之后,立即采用散焦对焊缝进行四级后热,每一级分别采用4mA、4mA、2mA、2mA的束流从焊缝的一端扫描到另一端,加速电压与步骤三相同,聚焦电流为3370mA,扫描速度为2mm/s~20mm/s。After Step 5 and Step 4 are completed, immediately use defocusing to perform four-stage afterheating on the weld seam. Each stage uses 4mA, 4mA, 2mA, and 2mA beam current to scan from one end of the weld seam to the other end to accelerate the voltage and step. The three are the same, the focusing current is 3370mA, and the scanning speed is 2mm/s~20mm/s.

当焊接对象为两根管壁厚度为0.8mm~1.5mm的TiAl金属间化合物的管材时,焊接的焊缝为环形焊缝,具体步骤为:When the welding object is two TiAl intermetallic compound pipes with a wall thickness of 0.8mm to 1.5mm, the welded seam is a circular weld seam, and the specific steps are:

步骤一、将已经去除内部应力、待焊面平整清洁的两个焊接对象用夹具固定之前,在夹具与焊接对象之间固定隔热板;Step 1. Fix the heat shield between the fixture and the welding object before fixing the two welding objects whose internal stress has been removed and whose welding surface is to be smooth and clean;

步骤二、对焊接对象实施夹紧,所述夹具对焊接对象采用轴向夹紧的方式;Step 2, clamping the welding object, and the clamp adopts an axial clamping method for the welding object;

步骤三、在5×10-2Pa至5×10-4Pa的大气压下,采用散焦对待焊处进行重复扫描、二级预热,每一级分别采用2mA的束流绕环形焊缝扫描一周;加速电压为50kV~55kV,聚焦电流3350mA,扫描速度为2mm/s~8mm/s;Step 3. Under the atmospheric pressure of 5×10 -2 Pa to 5×10 -4 Pa, use defocus to scan repeatedly and preheat the area to be welded, and use 2mA beam current to scan around the circular weld seam at each stage One week; the accelerating voltage is 50kV~55kV, the focusing current is 3350mA, and the scanning speed is 2mm/s~8mm/s;

步骤四、步骤三完成之后立即进行焊接,加速电压与步骤三相同,聚焦电流为2590mA,束流为2mA~8mA,焊接速度为2mm/s~10mm/s;Step 4. Immediately weld after step 3 is completed. The acceleration voltage is the same as step 3. The focusing current is 2590mA, the beam current is 2mA~8mA, and the welding speed is 2mm/s~10mm/s;

步骤五、步骤四完成之后,立即对焊接完成的焊缝采用散焦进行四级后热,每一级分别采用4mA、2mA、2mA、2mA的束流绕环形焊缝扫描一周,加速电压与步骤三相同,聚焦电流为3350mA,扫描速度为2mm/s~12mm/s。After step 5 and step 4 are completed, immediately defocus the welded seam for four-stage post-heating. Each stage uses 4mA, 2mA, 2mA, and 2mA beams to scan around the circular weld seam to accelerate the voltage and step. The three are the same, the focusing current is 3350mA, and the scanning speed is 2mm/s~12mm/s.

当焊接对象为两根管壁厚度为2.0mm~3.5mm的TiAl金属间化合物的管材时,焊接的焊缝为环形焊缝,具体步骤为:When the welding object is two TiAl intermetallic compound pipes with a wall thickness of 2.0mm to 3.5mm, the welded seam is a circular weld, and the specific steps are:

步骤一、将已经去除内部应力、待焊面平整清洁的两个焊接对象用夹具固定之前,在夹具与焊接对象之间固定隔热板;Step 1. Fix the heat shield between the fixture and the welding object before fixing the two welding objects whose internal stress has been removed and whose welding surface is to be smooth and clean;

步骤二、对焊接对象实施夹紧,所述夹具对焊接对象采用轴向夹紧的方式;Step 2, clamping the welding object, and the clamp adopts an axial clamping method for the welding object;

步骤三、在5×10-2Pa至5×10-4Pa的大气压下,采用散焦对待焊处进行重复扫描、四级预热,每一级分别采用2mA、2mA、4mA、6mA的束流绕环形焊缝扫描一周;加速电压为50kV~55kV,聚焦电流3350mA,扫描速度为2mm/s~8mm/s;Step 3. Under the atmospheric pressure of 5×10 -2 Pa to 5×10 -4 Pa, use defocus to scan repeatedly the area to be welded, and preheat in four stages. Each stage uses 2mA, 2mA, 4mA, 6mA beams respectively. Flow around the annular weld and scan for one cycle; the acceleration voltage is 50kV~55kV, the focusing current is 3350mA, and the scanning speed is 2mm/s~8mm/s;

步骤四、步骤三完成之后立即进行焊接,加速电压与步骤三相同,聚焦电流为2590mA,束流为10mA~32mA,焊接速度为2mm/s~10mm/s;Step 4. Immediately weld after step 3 is completed. The acceleration voltage is the same as step 3. The focusing current is 2590mA, the beam current is 10mA~32mA, and the welding speed is 2mm/s~10mm/s;

步骤五、步骤四完成之后,立即对焊接完成的焊缝采用散焦进行六级后热,每一级分别采用6mA、5mA、4mA、3mA、2mA、2mA的束流绕环形焊缝扫描一周,加速电压与步骤三相同,聚焦电流为3350mA,扫描速度为2mm/s~12mm/s。After step 5 and step 4 are completed, immediately defocus the welded seam for six levels of afterheating. Each level uses 6mA, 5mA, 4mA, 3mA, 2mA, and 2mA beams to scan around the circular weld seam. The accelerating voltage is the same as step three, the focusing current is 3350mA, and the scanning speed is 2mm/s~12mm/s.

所述焊接对象TiAl金属间化合物的成分包含:Ti:48~65at.%、Al:35~51at.%,还包含V:1.0~9.0at.%或Cr:1.5~2.5at.%或Nb:1.5~5.0at.%,所述TiAl金属间化合物的各种成分的百分比之和为100%。The composition of the TiAl intermetallic compound to be welded includes: Ti: 48-65 at.%, Al: 35-51 at.%, and V: 1.0-9.0 at.% or Cr: 1.5-2.5 at.% or Nb: 1.5-5.0 at.%, the sum of the percentages of various components of the TiAl intermetallic compound is 100%.

本发明的TiAl金属间化合物电子束焊接热循环复合控制方法,不需要增加特殊设备或添加过渡层金属,就可以完全避免焊缝产生宏观裂纹,达到无裂纹焊接的目的,适用于TiAl金属间化合物各种接头形式的焊接。The thermal cycle compound control method for electron beam welding of TiAl intermetallic compounds of the present invention can completely avoid macroscopic cracks in the weld seam without adding special equipment or adding transition layer metal, and achieve the purpose of crack-free welding, which is suitable for TiAl intermetallic compounds Welding of various joint forms.

具体实施方式 Detailed ways

具体实施方式一:TiAl金属间化合物电子束焊接热循环复合控制方法,它的焊接对象是两块厚度为0.8mm~5.0mm的板状物,具体步骤为:Specific implementation mode 1: TiAl intermetallic compound electron beam welding thermal cycle compound control method, its welding object is two plates with a thickness of 0.8 mm to 5.0 mm, and the specific steps are:

步骤一、将已经去除内部应力、待焊面平整清洁的两块TiAl金属间化合物的板材用夹具固定之前,在焊机夹具底座和每个焊接对象之间分别固定一块隔热板;Step 1. Before fixing the two TiAl intermetallic compound plates whose internal stress has been removed and whose welding surface is smooth and clean, fix a heat shield between the welding fixture base and each welding object;

步骤二、对焊接对象实施夹紧,所述夹具仅在焊接对象与焊缝平行的方向施加夹紧力;Step 2, clamping the welding object, the clamp only applies a clamping force in the direction parallel to the welding object and the weld seam;

步骤三、在5×10-2Pa至5×10-4Pa的大气压下,采用散焦对待焊处进行往复扫描、分级预热,每一级分别采用2mA~12mA中从小到大依次递增的束流从焊缝的一端扫描到另一端,加速电压为50kV~55kV,聚焦电流3370mA,扫描速度为2mm/s~10mm/s;Step 3. Under the atmospheric pressure of 5×10 -2 Pa to 5×10 -4 Pa, use defocus to scan back and forth on the part to be welded, and preheat in stages. The beam scans from one end of the weld to the other end, the accelerating voltage is 50kV~55kV, the focusing current is 3370mA, and the scanning speed is 2mm/s~10mm/s;

步骤四、步骤三完成之后,立即进行焊接,加速电压与步骤三相同,聚焦电流为2590mA,束流为3mA~50mA,焊接速度为2mm/s~15mm/s;After step 4 and step 3 are completed, weld immediately, the acceleration voltage is the same as step 3, the focusing current is 2590mA, the beam current is 3mA-50mA, and the welding speed is 2mm/s-15mm/s;

步骤五、步骤四完成之后,立即采用散焦对焊缝进行分级后热,每一级分别采用12mA~1mA中从大到小依次递减的束流从焊缝的一端扫描到另一端,加速电压与步骤三相同,聚焦电流为3370mA,扫描速度为2mm/s~20mm/s。After step 5 and step 4 are completed, defocusing is used to classify the weld immediately after heating, and each level uses 12mA ~ 1mA beam current in descending order to scan from one end of the weld to the other end, and the acceleration voltage Same as Step 3, the focusing current is 3370mA, and the scanning speed is 2mm/s-20mm/s.

本实施方式所述的TiAl金属间化合物的成分包含:Ti:48~65at.%、Al:35~51at.%,还可以包含V:1.0~9.0at.%或Cr:1.5~2.5at.%或Nb:1.5~5.0at.%。The composition of the TiAl intermetallic compound described in this embodiment includes: Ti: 48-65 at.%, Al: 35-51 at.%, and may also include V: 1.0-9.0 at.% or Cr: 1.5-2.5 at.%. Or Nb: 1.5 to 5.0 at.%.

本实施方式的步骤一中,在焊接对象与夹具底座之间增加了隔热板,用以限制焊接对象与夹具之间的热传导,能够有效的降低焊后接头的冷却速度。In step 1 of this embodiment, a heat shield is added between the welding object and the fixture base to limit the heat conduction between the welding object and the fixture, which can effectively reduce the cooling speed of the welded joint.

本实施方式的步骤二中,采用对焊接对象仅施加与焊缝平行方向的夹紧力进行夹紧,用以约束热循环加热阶段焊接对象沿焊缝方向的热膨胀,降低焊接对象在热循环冷却阶段产生的热致应力,而在其他方向不施加拘束,有效地避免热循环冷却阶段产生较大的拘束应力,对防止宏观裂纹的产生有一定的作用。In step 2 of this embodiment, the welding object is clamped only by applying a clamping force in the direction parallel to the weld seam, so as to restrain the thermal expansion of the welding object along the direction of the weld seam during the thermal cycle heating stage, and reduce the temperature of the welding object during thermal cycle cooling. The thermally induced stress generated in the thermal cycle stage, while no restraint is applied in other directions, effectively avoids the large restraint stress generated in the cooling stage of the thermal cycle, and has a certain effect on preventing the generation of macroscopic cracks.

本实施方式从步骤三至五,分三个阶段编程连续控制整个焊接过程的热循环,其中步骤三的预热过程中采用分级预热,逐级增加束流,可以使焊缝周围部位的温度逐渐上升,在焊接之后的步骤五后热过程中,采用分级后热,逐级递减束流,可以使焊接后的焊缝及其周围的温度逐渐下降。采取这些方法能够改善接头组织结构,延长应力释放时间,可获得无宏观冷裂纹的电子束焊接头。In this embodiment, from steps 3 to 5, the thermal cycle of the entire welding process is continuously controlled by programming in three stages. In the preheating process of step 3, graded preheating is adopted, and the beam current is increased step by step, so that the temperature of the surrounding parts of the weld can be increased. Gradually increase, in step five post-heating process after welding, adopt graded post-heating, gradually reduce the beam current, can make the temperature of the weld seam after welding and its surroundings drop gradually. Taking these methods can improve the structure of the joint, prolong the stress release time, and obtain an electron beam welded joint without macroscopic cold cracks.

具体实施方式二:本实施方式的焊接对象的厚度为2.0mm~3.0mm,焊接方法与具体实施方式一的区别在于,Specific embodiment 2: The thickness of the welding object in this embodiment is 2.0 mm to 3.0 mm. The difference between the welding method and specific embodiment 1 is that

在步骤三的预热过程中,采用四级预热,每级分别采用2mA、4mA、6mA和8mA的束流从焊缝的一端扫描到另一端;In the preheating process of step 3, four stages of preheating are used, and each stage uses beam currents of 2mA, 4mA, 6mA and 8mA to scan from one end of the weld to the other end;

在步骤四中,采用16mA~32mA的束流、5mm/s~10mm/s的焊接速度进行焊接;In step 4, welding is performed with a beam current of 16mA-32mA and a welding speed of 5mm/s-10mm/s;

在步骤五的后热过程中,采用四级后热,每级分别采用8mA、6mA、4mA、2mA的束流从焊缝的一端扫描到另一端。In the post-heating process of step five, four stages of post-heating are used, and each stage adopts beam currents of 8mA, 6mA, 4mA, and 2mA to scan from one end of the weld to the other end.

具体实施方式三:本实施方式与具体实施方式一的区别在于,所焊接对象的厚度为0.8mm~2.0mm,焊接方法与具体实施方式一的区别在于,Embodiment 3: The difference between this embodiment and Embodiment 1 is that the thickness of the object to be welded is 0.8 mm to 2.0 mm. The difference between the welding method and Embodiment 1 is that

在步骤三的预热过程中,采用两级预热,每级分别采用2mA的束流从焊缝的一端扫描到另一端;In the preheating process of step 3, two stages of preheating are used, and each stage uses a 2mA beam current to scan from one end of the weld to the other end;

在步骤四中,采用2mA~8mA的束流、5mm/s~15mm/s的焊接速度对焊接部位进行焊接;In step 4, the welding part is welded with a beam current of 2mA-8mA and a welding speed of 5mm/s-15mm/s;

在步骤五的后热过程中,采用四级后热,每级分别采用4mA、4mA、2mA、2mA的束流从焊缝的一端扫描到另一端。In the post-heating process of step five, four stages of post-heating are used, and each stage adopts beam currents of 4mA, 4mA, 2mA, and 2mA to scan from one end of the weld to the other end.

具体实施方式四:本实施方式与具体实施方式一的区别在于,所焊接对象的厚度为3.0mm~5.0mm,焊接方法与具体实施方式一的区别在于,Embodiment 4: The difference between this embodiment and Embodiment 1 is that the thickness of the object to be welded is 3.0 mm to 5.0 mm. The difference between the welding method and Embodiment 1 is that

在步骤三的预热过程中,采用六级预热,每级分别采用2mA、4mA、6mA、8mA、9mA、10mA的束流从焊缝的一端扫描到另一端;In the preheating process of step 3, six levels of preheating are used, and each level uses beam currents of 2mA, 4mA, 6mA, 8mA, 9mA, and 10mA to scan from one end of the weld to the other end;

在步骤四中,采用24mA~50mA的束流对焊接部位进行焊接,焊接速度为2mm/s~10mm/s;In step 4, the welding part is welded with a beam current of 24mA-50mA, and the welding speed is 2mm/s-10mm/s;

在步骤五的后热过程中,采用六级后热,每级分别采用10mA、9mA、8mA、6mA、4mA、2mA的束流从焊缝的一端扫描到另一端。In the post-heating process of step five, six levels of post-heating are used, and each level uses beam currents of 10mA, 9mA, 8mA, 6mA, 4mA, and 2mA to scan from one end of the weld to the other end.

具体实施方式五:具体实施方式一所述的步骤一中所述的隔热板的材料成分为二氧化硅和硅酸盐。Embodiment 5: The material composition of the insulation board described in Step 1 of Embodiment 1 is silicon dioxide and silicate.

本实施方式的隔热板的隔热效果好,能够有效地防止被焊接物体上由于焊接产生的热量传导到焊机夹具底座上,一方面降低了能量的损失,另一方面也防止由于焊机夹具底座的热传导导致接头冷却速度增大。The heat insulation board of this embodiment has a good heat insulation effect, and can effectively prevent the heat generated by welding on the object to be welded from being transferred to the base of the welding fixture. On the one hand, it reduces energy loss, and on the other hand, it also prevents the Heat conduction from the base of the fixture results in an increased joint cooling rate.

具体实施方式六:本实施方式与具体实施方式一至五的区别在于,在步骤五完成之后,进行步骤六、去应力退火的工艺,将焊接对象加热到900℃,保温10h,然后随炉冷却。Embodiment 6: The difference between this embodiment and Embodiments 1 to 5 is that after step 5 is completed, step 6, the process of stress relief annealing is carried out, and the welding object is heated to 900 ° C, kept for 10 hours, and then cooled with the furnace.

具体实施方式七:TiAl金属间化合物电子束焊接热循环复合控制方法,它的焊接对象为两根壁厚为0.8mm~3.5mm的TiAl金属间化合物的管材,焊接的焊缝为环形焊缝,具体步骤为:Embodiment 7: TiAl intermetallic compound electron beam welding thermal cycle composite control method, its welding object is two pipes of TiAl intermetallic compound with a wall thickness of 0.8 mm to 3.5 mm, and the welded seam is a circular weld seam. The specific steps are:

步骤一、将已经去除内部应力、待焊面平整清洁的两个焊接对象用夹具固定之前,在夹具与焊接对象之间固定隔热板;Step 1. Fix the heat shield between the fixture and the welding object before fixing the two welding objects whose internal stress has been removed and whose welding surface is to be smooth and clean;

步骤二、对焊接对象实施夹紧,所述夹具对焊接对象采用轴向夹紧的方式;Step 2, clamping the welding object, and the clamp adopts an axial clamping method for the welding object;

步骤三、在5×10-2Pa至5×10-4Pa的大气压下,采用散焦对待焊处进行重复扫描、分级预热,每一级分别采用2mA~10mA中从小到大依次递增的束流绕环形焊缝扫描一周;加速电压为50kV~55kV,聚焦电流3350mA,扫描速度为2mm/s~8mm/s;Step 3. Under the atmospheric pressure of 5×10 -2 Pa to 5×10 -4 Pa, use defocus to scan repeatedly and preheat the area to be welded in stages. The beam scans around the circular weld seam for one week; the accelerating voltage is 50kV~55kV, the focusing current is 3350mA, and the scanning speed is 2mm/s~8mm/s;

步骤四、步骤三完成之后立即进行焊接,加速电压与步骤三相同,聚焦电流为2590mA,束流为2mA~32mA,焊接速度为2mm/s~10mm/s;Step 4. Immediately weld after step 3 is completed. The acceleration voltage is the same as step 3. The focusing current is 2590mA, the beam current is 2mA~32mA, and the welding speed is 2mm/s~10mm/s;

步骤五、步骤四完成之后,立即对焊接完成的焊缝采用散焦进行分级后热,每一级分别采用10mA~2mA中从大到小依次递减的束流绕环形焊缝扫描一周,加速电压与步骤三相同,聚焦电流为3350mA,扫描速度为2mm/s~12mm/s。After step 5 and step 4 are completed, immediately defocus the welded seam and heat it after classification. Each level uses 10mA-2mA beam currents that decrease in order from large to small to scan around the circular weld seam for a week, and the acceleration voltage Same as Step 3, the focusing current is 3350mA, and the scanning speed is 2mm/s~12mm/s.

本实施方式所述的TiAl金属间化合物的成分包含:Ti:48~65at.%、Al:35~51at.%,还可以包含V:1.0~9.0at.%或Cr:1.5~2.5at.%或Nb:1.5~5.0at.%。The composition of the TiAl intermetallic compound described in this embodiment includes: Ti: 48-65 at.%, Al: 35-51 at.%, and may also include V: 1.0-9.0 at.% or Cr: 1.5-2.5 at.%. Or Nb: 1.5 to 5.0 at.%.

本实施方式的步骤一中,在夹具与焊接对象之间固定隔热板,用以限制焊接对象与夹具之间的热传导,降低焊后接头的冷却速度。In step 1 of this embodiment, a heat shield is fixed between the fixture and the welding object to limit the heat conduction between the welding object and the fixture, and reduce the cooling speed of the welded joint.

本实施方式的步骤二中,仅在焊接对象的轴向施加加紧力,避免了热循环冷却阶段产生较大的拘束应力。In the second step of this embodiment, the tightening force is only applied in the axial direction of the welding object, so as to avoid the large restraint stress generated in the thermal cycle cooling stage.

本实施方式从步骤三至五分三个阶段编程连续控制整个焊接过程的热循环,使焊缝及其周围的温度始终保持缓慢过渡的状态,有效地防止了由于温度突变而导致焊缝周围产生宏观裂纹的情况。In this embodiment, the thermal cycle of the entire welding process is continuously controlled by programming in three stages from steps 3 to 5, so that the temperature of the weld seam and its surroundings is always in a slow transition state, effectively preventing the occurrence of thermal shocks around the weld seam due to sudden temperature changes. The case of macro-cracks.

具体实施方式八:本实施方式的焊接对象的管壁厚度为0.8mm~1.5mm,与具体实施方式七所述的方法的区别在于,Embodiment 8: The pipe wall thickness of the welding object in this embodiment is 0.8 mm to 1.5 mm. The difference from the method described in Embodiment 7 is that

在步骤三的预热过程中,采用二级预热,每级均采用2mA的束流绕环形焊缝扫描一周;In the preheating process of step 3, two stages of preheating are used, and each stage uses a 2mA beam to scan around the circular weld seam for one week;

在步骤四中,采用2mA~8mA的束流进行焊接;In step 4, welding is performed with a beam current of 2mA-8mA;

在步骤五的后热过程中,采用四级后热,每级分别采用4mA、2mA、2mA、2mA的束流绕环形焊缝扫描一周。In the post-heating process of Step 5, four stages of post-heating are used, and beam currents of 4mA, 2mA, 2mA, and 2mA are respectively used in each stage to scan around the circular weld seam for one circle.

具体实施方式九:本实施方式的焊接对象的管壁厚度为2.0mm~3.5mm,与具体实施方式七所述的方法的区别在于,Specific embodiment nine: the thickness of the pipe wall of the welding object in this embodiment is 2.0 mm to 3.5 mm, and the difference from the method described in specific embodiment seven is that,

在步骤三的预热过程中,采用四级预热,每级均采用2mA、2mA、4mA、6mA的束流绕环形焊缝扫描一周;In the preheating process of step 3, four stages of preheating are used, and each stage uses 2mA, 2mA, 4mA, and 6mA beams to scan around the circular weld for one week;

在步骤四中,采用10mA~32mA的束流进行焊接;In step 4, welding is performed with a beam current of 10mA-32mA;

在步骤五的后热过程中,采用六级后热,每级分别采用6mA、5mA、4mA、3mA、2mA、2mA的束流绕环形焊缝扫描一周。In the post-heating process of step five, six levels of post-heating are used, and beam currents of 6mA, 5mA, 4mA, 3mA, 2mA, and 2mA are used for each level to scan around the annular weld seam for one circle.

具体实施方式十:在具体实施方式七至九中,在步骤五之后,增加步骤六、去应力退火工艺,将焊接对象加热到900℃,保温10h,然后随炉冷却。Embodiment 10: In Embodiments 7 to 9, after step 5, add step 6, stress relief annealing process, heating the welding object to 900°C, keeping it warm for 10 hours, and then cooling with the furnace.

Claims (8)

1, TiAl intermetallic compound electron beam welding thermal cycle composite control method, its welding object is two plate objects that thickness is 0.8mm~5.0mm, it is characterized in that concrete steps are:
Step 1, will remove internal stress, the smooth cleaning of surface to be welded the sheet material of two TiAl intermetallic compounds with anchor clamps fixing before, between welding machine clamp base and each welding object, fix a thermal insulation board respectively;
Step 2, welding object implement is clamped, described anchor clamps only apply clamping force in the welding object direction parallel with weld seam;
Step 3,5 * 10 -2Pa to 5 * 10 -4Under the atmospheric pressure of Pa, employing defocuses carries out shuttle-scanning, classification preheating to place to be welded, each grade adopts the line that increases progressively successively from small to large among 2mA~12mA to scan the other end from an end of weld seam respectively, accelerating potential is 50kV~55kV, focus current 3370mA, sweep speed is 2mm/s~10mm/s;
Step 4, step 3 are welded after finishing immediately, and accelerating potential is identical with step 3, and focus current is 2590mA, and line is 3mA~50mA, and speed of welding is 2mm/s~15mm/s;
After step 5, step 4 are finished, employing immediately defocuses butt welded seam and carries out the classification after heat, each grade adopts the line that successively decreases successively from big to small among 12mA~1mA to scan the other end from an end of weld seam respectively, accelerating potential is identical with step 3, focus current is 3370mA, and sweep speed is 2mm/s~20mm/s;
The composition of described TiAl intermetallic compound comprises: Ti:48~65at.%, Al:35~51at.%, also comprise V:1.0~9.0at.% or Cr:1.5~2.5at.% or Nb:1.5~5.0at.%, the percentage sum of the various compositions of described TiAl intermetallic compound is 100%.
2, TiAl intermetallic compound electron beam welding thermal cycle composite control method according to claim 1, the material composition that it is characterized in that described thermal insulation board is silica and silicate.
3, TiAl intermetallic compound electron beam welding thermal cycle composite control method according to claim 1, the thickness that it is characterized in that welding object is 2.0mm~3.0mm, welding method is:
In the warm of step 3, adopt the level Four preheating, every grade of line that adopts 2mA, 4mA, 6mA and 8mA respectively scans the other end from an end of weld seam;
In step 4, adopt the line of 16mA~32mA, the speed of welding of 5mm/s~10mm/s to weld;
In the back thermal process of step 5, adopt the level Four after heat, every grade of line that adopts 8mA, 6mA, 4mA, 2mA respectively scans the other end from an end of weld seam.
4, TiAl intermetallic compound electron beam welding thermal cycle composite control method according to claim 1, the thickness that it is characterized in that institute's welding object is 3.0mm~5.0mm, welding method is:
In the warm of step 3, adopt six grades of preheatings, every grade of line that adopts 2mA, 4mA, 6mA, 8mA, 9mA, 10mA respectively scans the other end from an end of weld seam;
In step 4, adopt the line of 24mA~50mA that the welding position is welded, speed of welding is 2mm/s~10mm/s;
In the back thermal process of step 5, adopt six grades of after heat, every grade of line that adopts 10mA, 9mA, 8mA, 6mA, 4mA, 2mA respectively scans the other end from an end of weld seam.
5, TiAl intermetallic compound electron beam welding thermal cycle composite control method, its welding object is two plate objects that thickness is 0.8mm~2.0mm, it is characterized in that concrete steps are:
Step 1, will remove internal stress, the smooth cleaning of surface to be welded the sheet material of two TiAl intermetallic compounds with anchor clamps fixing before, between welding machine clamp base and each welding object, fix a thermal insulation board respectively;
Step 2, welding object implement is clamped, described anchor clamps only apply clamping force in the welding object direction parallel with weld seam;
Step 3,5 * 10 -2Pa to 5 * 10 -4Under the atmospheric pressure of Pa, employing defocuses carries out shuttle-scanning, two-stage preheating to place to be welded, and the line that each grade adopts 2mA respectively scans the other end from an end of weld seam, and accelerating potential is 50kV~55kV, focus current 3370mA, sweep speed is 2mm/s~10mm/s;
Step 4, step 3 are welded after finishing immediately, and accelerating potential is identical with step 3, and focus current is 2590mA, and line is 2mA~8mA, and speed of welding is 5mm/s~15mm/s;
After step 5, step 4 are finished, employing immediately defocuses butt welded seam and carries out the level Four after heat, the line that each grade adopts 4mA, 4mA, 2mA, 2mA respectively scans the other end from an end of weld seam, accelerating potential is identical with step 3, focus current is 3370mA, and sweep speed is 2mm/s~20mm/s;
The composition of described TiAl intermetallic compound comprises: Ti:48~65at.%, Al:35~51at.%, also comprise V:1.0~9.0at.% or Cr:1.5~2.5at.% or Nb:1.5~5.0at.%, the percentage sum of the various compositions of described TiAl intermetallic compound is 100%.
6, TiAl intermetallic compound electron beam welding thermal cycle composite control method, its welding object are that two root canal wall thickness are the tubing of the TiAl intermetallic compound of 0.8mm~3.5mm, and the weld seam of welding is a circular weld, it is characterized in that concrete steps are:
Step 1, will remove internal stress, the smooth cleaning of surface to be welded two welding objects with anchor clamps fixing before, fixing thermal insulation board between anchor clamps and welding object;
Step 2, welding object implement is clamped, described anchor clamps adopt the mode that axially clamps to welding object;
Step 3,5 * 10 -2Pa to 5 * 10 -4Under the atmospheric pressure of Pa, adopt to defocus place to be welded is carried out multiple scanning, classification preheating, each grade adopts the line that increases progressively successively from small to large among 2mA~10mA around the circular weld run-down respectively; Accelerating potential is 50kV~55kV, focus current 3350mA, and sweep speed is 2mm/s~8mm/s;
Step 4, step 3 are welded after finishing immediately, and accelerating potential is identical with step 3, and focus current is 2590mA, and line is 2mA~32mA, and speed of welding is 2mm/s~10mm/s;
After step 5, step 4 are finished, the weld seam that welding is finished adopts to defocus and carries out the classification after heat immediately, each grade adopts the line that successively decreases successively from big to small among 10mA~2mA around the circular weld run-down respectively, accelerating potential is identical with step 3, focus current is 3350mA, sweep speed is 2mm/s~12mm/s
The composition of described TiAl intermetallic compound comprises: Ti:48~65at.%, Al:35~51at.%, also comprise V:1.0~9.0at.% or Cr:1.5~2.5at.% or Nb:1.5~5.0at.%, the percentage sum of the various compositions of described TiAl intermetallic compound is 100%.
7, TiAl intermetallic compound electron beam welding thermal cycle composite control method, its welding object are that two root canal wall thickness are the tubing of the TiAl intermetallic compound of 0.8mm~1.5mm, and the weld seam of welding is a circular weld, it is characterized in that concrete steps are:
Step 1, will remove internal stress, the smooth cleaning of surface to be welded two welding objects with anchor clamps fixing before, fixing thermal insulation board between anchor clamps and welding object;
Step 2, welding object implement is clamped, described anchor clamps adopt the mode that axially clamps to welding object;
Step 3,5 * 10 -2Pa to 5 * 10 -4Under the atmospheric pressure of Pa, adopt to defocus place to be welded is carried out multiple scanning, secondary preheating, each grade adopts the line of 2mA around the circular weld run-down respectively; Accelerating potential is 50kV~55kV, focus current 3350mA, and sweep speed is 2mm/s~8mm/s;
Step 4, step 3 are welded after finishing immediately, and accelerating potential is identical with step 3, and focus current is 2590mA, and line is 2mA~8mA, and speed of welding is 2mm/s~10mm/s;
After step 5, step 4 are finished, the weld seam that welding is finished adopts to defocus and carries out the level Four after heat immediately, each grade adopts the line of 4mA, 2mA, 2mA, 2mA around the circular weld run-down respectively, accelerating potential is identical with step 3, focus current is 3350mA, sweep speed is 2mm/s~12mm/s
The composition of described TiAl intermetallic compound comprises: Ti:48~65at.%, Al:35~51at.%, also comprise V:1.0~9.0at.% or Cr:1.5~2.5at.% or Nb:1.5~5.0at.%, the percentage sum of the various compositions of described TiAl intermetallic compound is 100%.
8, TiAl intermetallic compound electron beam welding thermal cycle composite control method, its welding object are that two root canal wall thickness are the tubing of the TiAl intermetallic compound of 2.0mm~3.5mm, and the weld seam of welding is a circular weld, it is characterized in that concrete steps are:
Step 1, will remove internal stress, the smooth cleaning of surface to be welded two welding objects with anchor clamps fixing before, fixing thermal insulation board between anchor clamps and welding object;
Step 2, welding object implement is clamped, described anchor clamps adopt the mode that axially clamps to welding object;
Step 3,5 * 10 -2Pa to 5 * 10 -4Under the atmospheric pressure of Pa, adopt to defocus place to be welded is carried out multiple scanning, level Four preheating, each grade adopts the line of 2mA, 2mA, 4mA, 6mA around the circular weld run-down respectively; Accelerating potential is 50kV~55kV, focus current 3350mA, and sweep speed is 2mm/s~8mm/s;
Step 4, step 3 are welded after finishing immediately, and accelerating potential is identical with step 3, and focus current is 2590mA, and line is 10mA~32mA, and speed of welding is 2mm/s~10mm/s;
After step 5, step 4 are finished, the weld seam that welding is finished adopts to defocus and carries out six grades of after heat immediately, each grade adopts the line of 6mA, 5mA, 4mA, 3mA, 2mA, 2mA around the circular weld run-down respectively, accelerating potential is identical with step 3, focus current is 3350mA, sweep speed is 2mm/s~12mm/s
The composition of described TiAl intermetallic compound comprises: Ti:48~65at.%, Al:35~51at.%, also comprise V:1.0~9.0at.% or Cr:1.5~2.5at.% or Nb:1.5~5.0at.%, the percentage sum of the various compositions of described TiAl intermetallic compound is 100%.
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