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CN100334968C - Preparation method of hairgvein agrimony poly saccharide gum - Google Patents

Preparation method of hairgvein agrimony poly saccharide gum Download PDF

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CN100334968C
CN100334968C CNB2004100935284A CN200410093528A CN100334968C CN 100334968 C CN100334968 C CN 100334968C CN B2004100935284 A CNB2004100935284 A CN B2004100935284A CN 200410093528 A CN200410093528 A CN 200410093528A CN 100334968 C CN100334968 C CN 100334968C
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polysaccharide gum
jelly
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CN1650737A (en
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杨敏
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Zhejiang University ZJU
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Abstract

The present invention discloses a preparation method for lucid ganoderma polysaccharide glue. The method mainly comprises the processes of pressurization, boiling and extraction for preparing the lucid ganoderma polysaccharide glue, and obtained products are lucid ganoderma polysaccharide glue powder and lucid ganoderma polysaccharide glue granules which have a favorable instant property. According to the needs of product applications, color elements can be reserved or completely removed through the control of the operation processes. Operation steps do not have chemical pollution to the environment, effectively active components are not destroyed, and the product mouth feel is favorable.

Description

仙草多糖胶的制备方法Preparation method of celestial grass polysaccharide gum

技术领域technical field

本发明属于食品加工技术领域,涉及一种具有保健功效的纯天然食品凝固剂的加工技术,即一种仙草多糖胶的制备方法。The invention belongs to the technical field of food processing, and relates to a processing technology of a pure natural food coagulant with health care function, namely a preparation method of jelly grass polysaccharide gum.

背景技术Background technique

仙草(Mesona Blume),又名仙人草、凉粉草、薪草等,系唇形科仙草属一年生草本植物,是我国传统的药食两用的植物资源,富含多糖、色素(花青素)、降血压因子熊果酸、齐墩果酸、香树精和谷甾醇、谷甾烯醇、谷甾醇葡萄糖及多种对人体有益的微量元素,具有提高人体免疫能力、降血压、降血糖和抑制肿瘤等保健功效。Mesona Blume (Mesona Blume), also known as fairy grass, jelly grass, firewood, etc., is an annual herb of the Labiatae family, and is a traditional medicinal and edible plant resource in my country. It is rich in polysaccharides, pigments (anthocyanidins) ursolic acid), hypotensive factor ursolic acid, oleanolic acid, aroma tree essence and sitosterol, sitosterol, sitosterol glucose and a variety of trace elements beneficial to the human body, which have the functions of improving human immunity, lowering blood pressure, lowering Health benefits such as blood sugar and tumor suppression.

从仙草中提取的仙草多糖胶与淀粉糊化后,可形成非常牢固的键,通过网络状结构将物料紧裹其中而形成凝胶。此种凝胶弹性和韧性俱佳,口感、品质远远超过目前常用的“海藻酸钠”、“明胶”、“卡拉胶”、“魔芋胶”等胶凝剂,具有良好的市场前景。After gelatinization, the jelly jelly polysaccharide gum and starch can form a very strong bond, and the material is tightly wrapped in the network structure to form a gel. This kind of gel has excellent elasticity and toughness, and its taste and quality are far superior to the currently commonly used gelling agents such as "sodium alginate", "gelatin", "carrageenan" and "konjac gum", and has a good market prospect.

目前从仙草中制备仙草多糖胶主要采取碱法提取。但是碱液提取不完全,易破坏其有效活性成分,并产生一种不良的碱味,增加后续工序,从而提高成本。At present, the preparation of jelly jelly polysaccharide gum mainly adopts alkaline extraction. But the lye extraction is not complete, it is easy to destroy its effective active ingredients, and produce a bad alkaline taste, increase the follow-up process, thereby increasing the cost.

本发明的目的在于改进对仙草多糖胶的制备工艺,不用碱液提取,简化工艺,降低生产成本,有利于保护环境,所得产品口感好,弹性好,质感佳,制成的颗粒制剂速溶性良好。The purpose of the present invention is to improve the preparation process of celestiaceae polysaccharide gum, without lye extraction, simplify the process, reduce production costs, and help protect the environment. The resulting product has good taste, good elasticity, and good texture. good.

发明内容Contents of the invention

本发明公开的是一种加压煮提制备仙草多糖胶的方法。The invention discloses a method for preparing jelly jelly polysaccharide gum by decocting under pressure.

本发明仙草多糖胶的制备方法包括以下步骤:The preparation method of grass jelly polysaccharide gum of the present invention comprises the following steps:

(1)将原料仙草叶洗净后,用胶体磨粉碎成超细颗粒状的预处理物料;(1) After washing the raw material jelly grass leaves, use a colloid mill to pulverize them into superfine granular pretreatment materials;

(2)按重量计算,在预处理物料中加入10~20倍量的清水,在多功能提取罐中加热至沸,在1~2Kpa蒸汽压力下连续煮提0.5~3.5小时;(2) Calculated by weight, add 10 to 20 times the amount of clear water to the pretreated material, heat it to boiling in a multi-functional extraction tank, and boil it continuously for 0.5 to 3.5 hours under a steam pressure of 1 to 2Kpa;

(3)将煮提后的物料离心去渣,然后板框过滤,滤液导入沉淀罐;(3) centrifuging the boiled and extracted material to remove slag, then plate and frame filtration, and the filtrate is imported into a settling tank;

(4)在滤液中加入糖用活性炭,加入量占滤液总重量的0.5~1.5%,80~100℃温度下搅拌30~60分钟,使之混合均匀,混合液在沉降式离心机中分离脱色,在分离因素大于9000的条件下,去除活性炭及其附着物;(4) Add activated carbon for sugar to the filtrate, the amount added accounts for 0.5-1.5% of the total weight of the filtrate, stir at a temperature of 80-100°C for 30-60 minutes to make it evenly mixed, and the mixed solution is separated and decolorized in a decanter centrifuge , under the condition that the separation factor is greater than 9000, remove activated carbon and its attachments;

(5)在脱色后的滤液中按常规加入乳化剂、稳定剂,配料调浆,然后用喷雾干燥机喷雾干燥,喷雾干燥的温度控制为:进口150~200℃,出口60~80℃,制成仙草多糖胶粉。再将仙草多糖胶粉造粒成颗粒径为2~10毫米左右的仙草多糖胶颗粒。(5) Add emulsifier and stabilizer to the filtrate after decolorization as usual, mix the ingredients, and then spray dry with a spray dryer. Become grass jelly polysaccharide gum powder. Then the grass jelly polysaccharide gum powder is granulated into jelly grass polysaccharide gum particles with a particle diameter of about 2-10 mm.

按本方法得到的仙草多糖胶粉和仙草多糖胶颗粒是本发明方法所得到的两种产品。The grass jelly polysaccharide gum powder and the grass jelly polysaccharide gum particles obtained by the method are two kinds of products obtained by the method of the present invention.

根据对仙草多糖胶产品颜色的要求,选择对步骤(4)不操作或多次操作。如不操作步骤(4),即得到含咖啡色素的仙草多糖胶产品;如反复操作步骤(4),直至滤液无色透明,即得到不含色素的仙草多糖胶产品;可根据产品的用途所需要的色泽选择对步骤(4)的操作次数。According to the requirements for the color of the grass jelly polysaccharide gum product, choose not to operate or perform multiple operations on step (4). If step (4) is not performed, the celestial grass polysaccharide gum product containing coffee pigment can be obtained; if step (4) is repeated until the filtrate is colorless and transparent, the celestial grass polysaccharide gum product without pigment can be obtained; according to the product The color and luster required by the application is selected for the number of operations of step (4).

具体实施方式Detailed ways

原料选择:仙草最好选用一年只收割一茬的,一年收割二至三茬的仙草含糖量较低。仙草必须在花蕊全部形成后,刚开花时收割为宜,此时多糖的含量较高。从收割后的仙草中挑选无腐烂、无病害的仙草叶晒干,妥善收藏,以防霉变。Selection of raw materials: It is best to use grass jelly that is only harvested once a year, and grass jelly that is harvested two to three crops a year has a lower sugar content. Grass jelly must be harvested after the pistils are all formed, and when they have just bloomed, the content of polysaccharides is higher at this time. From the harvested grass jelly, select non-rotten and disease-free jelly grass leaves and dry them in the sun, and store them properly to prevent mildew.

实施例一:Embodiment one:

1、挑选无腐烂、无病害的仙草干叶用清水冲洗干净,除去泥砂和杂质。1. Select dry grass jelly leaves that are free from rot and disease, and rinse them with clean water to remove mud, sand and impurities.

2、将洗净的仙草叶用胶体磨粉碎成超细颗粒。2. Use a colloid mill to pulverize the washed grass jelly leaves into ultra-fine particles.

3、将经过以上预处理的物料投至多功能提取罐,按1∶15的重量比例加入清水,逐渐加温至沸,在1.5Kpa的蒸汽压力下连续煮提1小时。3. Put the above pretreated materials into a multi-functional extraction tank, add water in a weight ratio of 1:15, gradually heat to boiling, and continuously cook and extract for 1 hour under a steam pressure of 1.5Kpa.

4、将提取的原液通过离心去渣,然后板框过滤,滤液导入沉淀罐。4. Centrifuge the extracted stock solution to remove slag, then filter the plate and frame, and import the filtrate into the sedimentation tank.

5、滤液中加入重量比为1%的糖用活性炭,在90℃下搅拌45分钟,使之混合均匀。将混合液放入沉降式离心机中分离脱色,在分离因素大于9000的条件下,去除活性炭及其附着物。反复此过程,直至汁液澄清透明为止。5. Add 1% activated carbon for sugar in the filtrate, and stir at 90°C for 45 minutes to make it evenly mixed. Put the mixed solution into a decanter centrifuge for separation and decolorization, and remove activated carbon and its attachments under the condition that the separation factor is greater than 9000. Repeat this process until the juice is clear and transparent.

6、在滤液中加入乳化剂、稳定剂等配料调浆,然后送入喷雾干燥机中喷雾干燥。喷雾干燥进口温度控制在180℃,出口温度控制在70℃。6. Add emulsifier, stabilizer and other ingredients to the filtrate to make slurry, and then send it to the spray dryer for spray drying. The spray drying inlet temperature is controlled at 180°C, and the outlet temperature is controlled at 70°C.

7、喷雾干燥后的仙草多糖胶粉装入沸腾造粒机中进行造粒,至颗粒直径2~10mm左右。得到仙草多糖胶颗粒产品。7. Put the spray-dried grass jelly polysaccharide gum powder into a boiling granulator for granulation until the particle diameter is about 2-10mm. Obtain the celestial grass polysaccharide gum granule product.

实施例二:Embodiment two:

将洗净的仙草叶按1∶10的比例加入清水,胶体磨粉碎,在1Kpa的蒸汽压力下连续煮提0.5小时,过滤弃渣。滤液中加入重量比为0.5%的糖用活性炭,在80℃下搅拌30分钟,使之混合均匀。混合液在离心机中分离脱色一次,除去活性炭及其附着物。滤液进行喷雾干燥,喷雾干燥器进口温度控制在150℃,出口温度控制在60℃。所得仙草多糖胶粉产品呈浅黄色,造粒后为浅黄色颗粒。Add the washed jelly grass leaves to water at a ratio of 1:10, pulverize them in a colloid mill, boil and extract them continuously for 0.5 hours under a steam pressure of 1Kpa, and filter out the residue. Adding 0.5% activated carbon for sugar in the filtrate was stirred at 80° C. for 30 minutes to make it evenly mixed. The mixture is separated and decolorized once in a centrifuge to remove activated carbon and its attachments. The filtrate was spray-dried, the inlet temperature of the spray dryer was controlled at 150°C, and the outlet temperature was controlled at 60°C. The obtained grass jelly polysaccharide gum powder product is light yellow, and becomes light yellow granules after granulation.

实例三:Example three:

将洗净的仙草叶按1∶20的比例加入清水,胶体磨粉碎,在2Kpa的蒸汽压力下连续煮提1.5小时,过滤弃渣,滤液进行喷雾干燥,喷雾干燥器进口温度控制在200℃,出口温度控制在80℃。得到的仙草多糖胶粉产品呈咖啡色,造粒后为咖啡色颗粒。Add clean water to the washed jelly grass leaves at a ratio of 1:20, pulverize them in a colloid mill, boil and extract them continuously for 1.5 hours under a steam pressure of 2Kpa, filter and discard the residue, and spray-dry the filtrate. The inlet temperature of the spray dryer is controlled at 200°C , the outlet temperature is controlled at 80°C. The obtained grass jelly polysaccharide gum powder product is brown, and after granulation, it is brown granules.

将以上实例制得的不同颜色仙草多糖胶颗粒加入到100~300倍量的料液(果汁、牛奶、布丁等)中,与3~5倍量的食用淀粉混合,搅拌均匀并加热至100℃后,自然冷却,形成透明的或含色素的胶冻或凝胶。Add the jelly grass polysaccharide gum particles of different colors prepared in the above example into 100 to 300 times the amount of feed liquid (fruit juice, milk, pudding, etc.), mix with 3 to 5 times the amount of edible starch, stir evenly and heat to 100 After ℃, cool naturally to form transparent or pigmented jelly or gel.

本发明制备的仙草多糖胶弹性好、质感佳、耐咀嚼,在食品工业上可用作果酱、果冻、布丁、甜食等的胶凝剂,也可用作酸奶饮料、浓缩果汁等的增稠剂,以提高产品的稳定性,改善口感,具有良好的市场前景。此外用仙草多糖制成的天然凝胶食品,清凉爽口,味道醇美,含有较多的水溶性膳食纤维,具有提高人体免疫能力、降血压、降血糖和抑制肿瘤等保健功效,是一种纯天然的保健食品胶。The jelly polysaccharide gum prepared by the invention has good elasticity, good texture, and chewability, and can be used as a gelling agent for jams, jellies, puddings, desserts, etc. in the food industry, and can also be used as a thickener for yogurt drinks, concentrated fruit juices, etc. agent, in order to improve the stability of the product, improve the taste, and has a good market prospect. In addition, the natural gel food made of grass jelly polysaccharide is cool and refreshing, tastes mellow, contains more water-soluble dietary fiber, and has health effects such as improving human immunity, lowering blood pressure, lowering blood sugar and inhibiting tumors. Natural health food glue.

采用加压煮提法制备仙草多糖胶,可提高产品得率,保护植物中的活性成分不受破坏;用此种方法提取的仙草原液色泽较浅,可减少脱色过程中活性炭的使用量,有利于降低成本;非碱法提取,简化了脱碱工序,有利于环境保护、降低成本和提高产品适口性。The preparation of celestial grass polysaccharide gum by pressure cooking can increase the yield of the product and protect the active ingredients in the plant from damage; the color of the celestial grass liquid extracted by this method is lighter, which can reduce the amount of activated carbon used in the decolorization process , which is beneficial to reduce costs; non-alkali extraction simplifies the dealkalization process, which is beneficial to environmental protection, reduces costs and improves product palatability.

喷雾干燥制备的仙草多糖胶比重轻,一次性集中投入水中时,表面颗粒由于水溶胀而形成胶质层,延缓并阻碍水分子向胶内部渗透,形成表面是初期胶冻而内部却是干芯的大团块。通过二次造粒技术,将许多细小的微粒附聚成较大颗粒,构成体积大、比表面积大,内部空穴多的膨松结构,有利于产品在水中的溶解,从而有效地解决了产品的速溶性问题。The jelly polysaccharide gel prepared by spray drying has a light specific gravity. When it is put into water at one time, the surface particles will form a gel layer due to water swelling, delaying and hindering the penetration of water molecules into the gel, forming an initial gel on the surface but dry inside. Large lumps of core. Through the secondary granulation technology, many fine particles are agglomerated into larger particles to form a bulky structure with large volume, large specific surface area, and many internal cavities, which is conducive to the dissolution of the product in water, thus effectively solving the problem of the product. instant solubility problem.

Claims (2)

1、仙草多糖胶的制备方法,其特征在于以下步骤:1, the preparation method of grass jelly polysaccharide gum, is characterized in that following steps: (1)将原料仙草叶洗净后,用胶体磨粉碎成超细颗粒状的预处理物料;(1) After washing the raw material jelly grass leaves, use a colloid mill to pulverize them into superfine granular pretreatment materials; (2)按重量计算,在预处理物料中加入10~20倍量的清水,在多功能提取罐中加热至沸,在1~2Kpa蒸汽压力下连续煮提0.5~3.5小时;(2) Calculated by weight, add 10 to 20 times the amount of clear water to the pretreated material, heat it to boiling in a multi-functional extraction tank, and boil it continuously for 0.5 to 3.5 hours under a steam pressure of 1 to 2Kpa; (3)将煮提后的物料离心去渣,然后板框过滤,滤液导入沉淀罐;(3) centrifuging the boiled and extracted material to remove slag, then plate and frame filtration, and the filtrate is imported into a settling tank; (4)在滤液中加入糖用活性炭,加入量占滤液总重量的0.5~1.5%,80~100℃温度下搅拌30~60分钟,使之混合均匀,混合液在沉降式离心机中分离脱色,在分离因素大于9000的条件下,去除活性炭及其附着物;(4) Add activated carbon for sugar to the filtrate, the amount added accounts for 0.5-1.5% of the total weight of the filtrate, stir at a temperature of 80-100°C for 30-60 minutes to make it evenly mixed, and the mixed solution is separated and decolorized in a decanter centrifuge , under the condition that the separation factor is greater than 9000, remove activated carbon and its attachments; (5)在脱色后的滤液中按常规加入乳化剂、稳定剂,配料调浆,然后用喷雾干燥机喷雾干燥,喷雾干燥的温度控制为:进口150~200℃,出口60~80℃,制成仙草多糖胶粉;(5) Add emulsifier and stabilizer to the filtrate after decolorization as usual, mix the ingredients, and then spray dry with a spray dryer. Chengxiancao polysaccharide gum powder; (6)将仙草多糖胶粉造粒成颗粒径为2~10毫米左右的仙草多糖胶颗粒。(6) Granulating the jellybean polysaccharide gum powder into jellybean polysaccharide gum granules with a particle diameter of about 2-10 mm. 2、按权利要求1所述仙草多糖胶的制备方法,其特征在于:根据对仙草多糖胶产品颜色的要求,选择对步骤(4)不操作或多次操作。2. The preparation method of the grass jelly polysaccharide gum according to claim 1, characterized in that: according to the requirements for the color of the grass jelly polysaccharide gum product, step (4) is selected not to be operated or to be operated multiple times.
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中国凉粉草资源的研究与利用 谌国莲等,农牧产品开发,第5期 2000 *

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