CH197196A - Process for the production of an acidic wool dye. - Google Patents
Process for the production of an acidic wool dye.Info
- Publication number
- CH197196A CH197196A CH197196DA CH197196A CH 197196 A CH197196 A CH 197196A CH 197196D A CH197196D A CH 197196DA CH 197196 A CH197196 A CH 197196A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- dye
- acidic
- wool dye
- acidic wool
- Prior art date
Links
Landscapes
- Coloring (AREA)
Description
Verfahren zur Herstellung eines sauren Wollfarbstoffes. Vorliegendes Patent bezieht sich auf ein Verfahren zur Herstellung eines sauren Woll- farbstoffes, dadurch gekennzeichnet, dass man 1-Chlor-2-nitrobenzol-4-äthylsulfon mit 4' Methoxy-4- amino-diphenylamin-2-sulfonsäure kondensiert.
Der so erhaltene Farbstoff färbt Wolle aus saurem Bade in braunen Tönen von sehr guter Egalität und hervorragender Lichtecht heit. <I>Beispiel:</I> 31,6 Teile 4'-methoxy-4-amino-dipheuyl- amin-2-sulfonsaures Natrium werden in der zehnfachen Menge Wasser gelöst. Dann fügt man 25 Teile 1-Chlor-2-nitrobenzol-4-äthyl- sulfon in etwa 160 Teilen Alkohol und 10 Teile Natriumacetat zu und erhitzt das Ganze mehrere Stunden unter Rückfluss zum Sieden.
Hierauf wird der Alkohol abdestilliert und der gebildete Farbstoff aus der wässerigen Lösung durch Eindampfen oder Aussalzen abgeschieden.
Process for the production of an acidic wool dye. The present patent relates to a process for the production of an acidic wool dye, characterized in that 1-chloro-2-nitrobenzene-4-ethyl sulfone is condensed with 4 'methoxy-4-aminodiphenylamine-2-sulfonic acid.
The dye obtained in this way dyes wool from an acid bath in brown shades of very good levelness and excellent lightfastness. <I> Example: </I> 31.6 parts of 4'-methoxy-4-amino-dipheuyl-amine-2-sulfonic acid sodium are dissolved in ten times the amount of water. Then 25 parts of 1-chloro-2-nitrobenzene-4-ethylsulfone in about 160 parts of alcohol and 10 parts of sodium acetate are added and the whole is refluxed for several hours.
The alcohol is then distilled off and the dye formed is deposited from the aqueous solution by evaporation or salting out.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE197196X | 1935-08-13 | ||
DE193627X | 1935-08-13 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH197196A true CH197196A (en) | 1938-04-15 |
Family
ID=25757660
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH197196D CH197196A (en) | 1935-08-13 | 1936-08-10 | Process for the production of an acidic wool dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH197196A (en) |
-
1936
- 1936-08-10 CH CH197196D patent/CH197196A/en unknown
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