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CH191447A - Process for the production of a new condensation product. - Google Patents

Process for the production of a new condensation product.

Info

Publication number
CH191447A
CH191447A CH191447DA CH191447A CH 191447 A CH191447 A CH 191447A CH 191447D A CH191447D A CH 191447DA CH 191447 A CH191447 A CH 191447A
Authority
CH
Switzerland
Prior art keywords
condensation product
production
new condensation
yellow
new
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH191447A publication Critical patent/CH191447A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B57/00—Other synthetic dyes of known constitution

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Herstellung eines neuen Kondensationsproduktes.    Es wurde gefunden,     dass    man ein neues  Kondensationsprodukt erhält, wenn man     p-          Chlorphenylsulfonacetonitril    mit     (N-Äthyl-          N-oxäthyl)-p-aminobenzaldehyd    kondensiert.  



  Das neue Kondensationsprodukt ist ein  gelbes Pulver, das in Wasser     unlöslich    ist,  sich dagegen in Essigester leicht mit grün  gelber Farbe löst und, in geeignete feine  Verteilung gebracht,     Acetatkunstseide    in       grünstichig    gelben Tönen färbt.

           Beispiel:       21,5     Gewichtsteile        p-Chlorphenylsulfon-          acetonitril    werden zusammen mit<B>19,3</B> Ge  wichtsteilen     (N-Äthyl-N-oxäthyl)p-amino-          benzaldehyd    in Alkohol gelöst und unter  Zusatz von einigen Tropfen     Piperidin    einige  Zeit unter     Rückfluss    gekocht.     iSchon    nach  kurzem Kochen tritt     intensive    Gelbfärbung  der Flüssigkeit durch     dae    sich bildende Kon  densationsprodukt ein.

   Man kocht solange,    bis die Farbintensität nicht mehr zunimmt,  was den Endpunkt der     Reaktion    anzeigt.  Darauf lädt man unter Rühren erkalten,  wobei sich das     Kondensationsprodukt    als  gelbes Pulver ausscheidet.



  Process for the production of a new condensation product. It has been found that a new condensation product is obtained when p-chlorophenylsulfonacetonitrile is condensed with (N-ethyl-N-oxethyl) -p-aminobenzaldehyde.



  The new condensation product is a yellow powder that is insoluble in water, but easily dissolves in ethyl acetate with a green-yellow color and, when appropriately finely divided, dyes acetate rayon in greenish yellow tones.

           Example: 21.5 parts by weight of p-chlorophenylsulfonic acetonitrile are dissolved in alcohol together with 19.3 parts by weight of (N-ethyl-N-oxethyl) p-aminobenzaldehyde and a few drops of piperidine are added refluxed for some time. Even after a short boil, the liquid turns yellow due to the condensation product that forms.

   The mixture is boiled until the color intensity no longer increases, which indicates the end point of the reaction. The mixture is then cooled while stirring, the condensation product separating out as a yellow powder.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines neuen Kondensationsproduktes, dadurch gekenn- zeichnet,,dass man p-Chlorphenylsulfonaceto- nitril mit (N-Äthyl-N-oxäthyl)-p-aminobenz- aldehyd kondensiert. PATENT CLAIM: Process for the production of a new condensation product, characterized in that p-chlorophenylsulfonacetonitrile is condensed with (N-ethyl-N-oxethyl) -p-aminobenzaldehyde. Das neue Kondensationsprodukt ist ein gelbes Pulver, das in Wasser unlöslich ist, sich dagegen in Essigester leicht mit grün gelber Farbe löst und, in geeignete feine Verteilung gebracht, Acetatkunsbseide in gr'ünstiehig gelben Tönen färbt. The new condensation product is a yellow powder which is insoluble in water, but dissolves easily in ethyl acetate with a greenish-yellow color and, when appropriately finely divided, dyes acetate-artificial silk in greenish yellow tones.
CH191447D 1935-04-05 1935-04-05 Process for the production of a new condensation product. CH191447A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH189874T 1935-04-05
CH191447T 1935-04-05

Publications (1)

Publication Number Publication Date
CH191447A true CH191447A (en) 1937-06-15

Family

ID=25721907

Family Applications (1)

Application Number Title Priority Date Filing Date
CH191447D CH191447A (en) 1935-04-05 1935-04-05 Process for the production of a new condensation product.

Country Status (1)

Country Link
CH (1) CH191447A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3140308A (en) * 1952-09-25 1964-07-07 Du Pont Colored 1: 1 pi complexes of tetracyanoethylene and aromatic compounds

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3140308A (en) * 1952-09-25 1964-07-07 Du Pont Colored 1: 1 pi complexes of tetracyanoethylene and aromatic compounds

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