CH183458A - Process for the preparation of an azo dye. - Google Patents
Process for the preparation of an azo dye.Info
- Publication number
- CH183458A CH183458A CH183458DA CH183458A CH 183458 A CH183458 A CH 183458A CH 183458D A CH183458D A CH 183458DA CH 183458 A CH183458 A CH 183458A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- azo dye
- dye
- sulfophenyl
- pyrazolone
- Prior art date
Links
Landscapes
- Coloring (AREA)
Description
Verfahren zur Herstellung eines Azofarbstof%s. Es wurde gefunden, dass man einen neuen Azofarbstoff von vorzüglichen Echtheits eigenschaften erhält, wenn man die Diazo- verbindung von 1-Amino-4-rhodanbenzol mit 1-(2-Oxy-3-carboxy-5-sulfophenyl)-3-methyl- 5-pyrazolon vereinigt.
Der so erhältliche Farbstoff färbt Wolle in klaren gelben Tönen und zeichnet sich insbesondere durch aussergewöhnlich gute Wasch- und Walkechtheit aus. Auch seine übrigen Eigenschaften, wie Lichtechtheit und Gleichmässigkeit, sind vorzüglich.
<I>Beispiel:</I> Man diazotiert bei 0 C eine wässerige, salzsaure Lösung von 15 Teilen 1-Amino-4- rhodanbenzol und lässt nach wenigen Minuten die Diazolösung in eine abgekühlte soda- alkalische Lösung von 3? Teilen 1-(2-Oxy-3- oarboxy-5-sulfophenyl)- 3 -methyl-5-pyrazolon einlaufen. Die Kupplung ist nach kurzer Zeit beendet.
Der Farbstoff wird dann aus gesalzen, nach einigen Stunden abgepresst und bei etwa <B>50'C</B> getrocknet.
Der Farbstoff oder die mit ihm erhält lichen Färbungen liefern bei der Behandlung mit metallabgebenden Mitteln ebenfalls echte Färbungen.
Process for the preparation of an azo dye% s. It has been found that a new azo dye with excellent fastness properties is obtained if the diazo compound of 1-amino-4-rhodanobenzene with 1- (2-oxy-3-carboxy-5-sulfophenyl) -3-methyl- 5-pyrazolone combined.
The dye obtainable in this way dyes wool in clear yellow shades and is particularly notable for its exceptionally good fastness to washing and boiling. Its other properties, such as lightfastness and evenness, are also excellent.
<I> Example: </I> An aqueous, hydrochloric acid solution of 15 parts of 1-amino-4-rhodanobenzene is diazotized at 0 C and, after a few minutes, the diazo solution is immersed in a cooled soda-alkaline solution of 3? Part 1- (2-oxy-3-oarboxy-5-sulfophenyl) -3-methyl-5-pyrazolone run in. The coupling ends after a short time.
The dye is then salted out, pressed out after a few hours and dried at about <B> 50'C </B>.
The dye or the dyeings obtainable with it likewise produce true dyeings when treated with metal donating agents.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE183458X | 1934-06-27 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH183458A true CH183458A (en) | 1936-04-15 |
Family
ID=5718575
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH183458D CH183458A (en) | 1934-06-27 | 1935-05-10 | Process for the preparation of an azo dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH183458A (en) |
-
1935
- 1935-05-10 CH CH183458D patent/CH183458A/en unknown
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