CH171368A - Process for the preparation of a disazo dye. - Google Patents
Process for the preparation of a disazo dye.Info
- Publication number
- CH171368A CH171368A CH171368DA CH171368A CH 171368 A CH171368 A CH 171368A CH 171368D A CH171368D A CH 171368DA CH 171368 A CH171368 A CH 171368A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- disazo dye
- dye
- disazo
- pyrazolone
- Prior art date
Links
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Description
Verfahren zur Herstellung eines Disazofarbstoffes. <B>EI</B> s wurde gefunden, dass man einen wert vollen Disazofarbstoff erhalten kann, wenn man tetra.zotiertes o-Dianisidin mit 1-(4'-11Ie- thylphenyl)-3-methyl-5-pyrazolon kuppelt.
Der erhaltene leuchtend gelbrote Farb stoff ist in organischen Lösungsmitteln, z. B. Benzol, Alkohol, unlöslich und vulkanisier eeht.
Beispiel: Man tetrazotiert 2,5 Gewichtsteile o-Di- anisidin in der üblichen Weise und. gibt die erhaltene Lösung der Tetrazoverbindung zu einer wässerig alkalischen Suspension von 40 Gewichtsteilen 1-(4'-Methylphenyl)-3-me- thyl-5-pyrazolon, die überschüssiges Na triumbikarbonat enthält. Nach beendeter Kupplung wird aufgekocht, dann abfiltriert und salzfrei gewaschen.
Process for the preparation of a disazo dye. It has been found that a valuable disazo dye can be obtained if tetra-doped o-dianisidine is coupled with 1- (4'-11Iethylphenyl) -3-methyl-5-pyrazolone.
The bright yellow-red dye obtained is in organic solvents such. B. benzene, alcohol, insoluble and vulcanizing.
Example: 2.5 parts by weight of o-di anisidine are tetrazotized in the usual manner and. gives the resulting solution of the tetrazo compound to an aqueous alkaline suspension of 40 parts by weight of 1- (4'-methylphenyl) -3-methyl-5-pyrazolone, which contains excess sodium bicarbonate. After the coupling has ended, the mixture is boiled, then filtered off and washed free of salt.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE171368X | 1932-11-22 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH171368A true CH171368A (en) | 1934-08-31 |
Family
ID=5689396
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH171368D CH171368A (en) | 1932-11-22 | 1933-10-17 | Process for the preparation of a disazo dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH171368A (en) |
-
1933
- 1933-10-17 CH CH171368D patent/CH171368A/en unknown
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