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CA2925170C - Procedes de preparation d'alumine et de divers autres produits - Google Patents

Procedes de preparation d'alumine et de divers autres produits Download PDF

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Publication number
CA2925170C
CA2925170C CA2925170A CA2925170A CA2925170C CA 2925170 C CA2925170 C CA 2925170C CA 2925170 A CA2925170 A CA 2925170A CA 2925170 A CA2925170 A CA 2925170A CA 2925170 C CA2925170 C CA 2925170C
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CA
Canada
Prior art keywords
hci
aluminum
precipitate
concentration
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CA2925170A
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English (en)
Other versions
CA2925170A1 (fr
Inventor
Richard Boudreault
Joel Fournier
Marie-Maxime LABRECQUE-GILBERT
Hubert Dumont
Jonathan BOUFFARD
Denis ARGUIN
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Aem Technologies Inc
Original Assignee
Aem Technologies Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aem Technologies Inc filed Critical Aem Technologies Inc
Publication of CA2925170A1 publication Critical patent/CA2925170A1/fr
Application granted granted Critical
Publication of CA2925170C publication Critical patent/CA2925170C/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B21/00—Obtaining aluminium
    • C22B21/0015—Obtaining aluminium by wet processes
    • C22B21/0023—Obtaining aluminium by wet processes from waste materials
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00—Halides of sodium, potassium or alkali metals in general
    • C01D3/04—Chlorides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
    • C01D5/02—Preparation of sulfates from alkali metal salts and sulfuric acid or bisulfates; Preparation of bisulfates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/212—Scandium oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/224—Oxides or hydroxides of lanthanides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/224—Oxides or hydroxides of lanthanides
    • C01F17/235—Cerium oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00—Compounds of magnesium
    • C01F5/02—Magnesia
    • C01F5/06—Magnesia by thermal decomposition of magnesium compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00—Compounds of magnesium
    • C01F5/26—Magnesium halides
    • C01F5/30—Chlorides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/028—Beta-aluminas
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/30—Preparation of aluminium oxide or hydroxide by thermal decomposition or by hydrolysis or oxidation of aluminium compounds
    • C01F7/306—Thermal decomposition of hydrated chlorides, e.g. of aluminium trichloride hexahydrate
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/34—Preparation of aluminium hydroxide by precipitation from solutions containing aluminium salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/44—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water
    • C01F7/441—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water by calcination
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/48—Halides, with or without other cations besides aluminium
    • C01F7/56—Chlorides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/68—Aluminium compounds containing sulfur
    • C01F7/70—Sulfides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00—Compounds of iron
    • C01G49/02—Oxides; Hydroxides
    • C01G49/06—Ferric oxide [Fe2O3]
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00—Compounds of iron
    • C01G49/10—Halides
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/34—Simultaneous production of alkali metal hydroxides and chlorine, oxyacids or salts of chlorine, e.g. by chlor-alkali electrolysis
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

L'invention concerne un procédé de préparation d'alumine. Le procédé comprend une étape consistant à lixivier un matériau contenant de l'aluminium (par exemple un déchet industriel choisi parmi la boue rouge, des cendres volantes et leur mélange) avec du HCl afin d'obtenir un lixiviat comprenant des ions aluminium et un solide, et séparer le solide du lixiviat. Le procédé comprend ensuite une étape consistant à faire réagir le lixiviat avec du HCl afin d'obtenir un liquide et un précipité comprenant les ions aluminium en tant que AlCl3, et à séparer le précipité du liquide. On fait ensuite réagir le précipité avec une base. Enfin, le procédé comprend une étape consistant à chauffer le précipité dans des conditions efficaces pour convertir celui-ci en Al2O3.
CA2925170A 2013-09-26 2014-09-26 Procedes de preparation d'alumine et de divers autres produits Active CA2925170C (fr)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201361882864P 2013-09-26 2013-09-26
US61/882,864 2013-09-26
US201461947908P 2014-03-04 2014-03-04
US61/947,908 2014-03-04
PCT/CA2014/000714 WO2015042692A1 (fr) 2013-09-26 2014-09-26 Procédés de préparation d'alumine et de divers autres produits

Publications (2)

Publication Number Publication Date
CA2925170A1 CA2925170A1 (fr) 2015-04-02
CA2925170C true CA2925170C (fr) 2021-12-07

Family

ID=52741670

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2925170A Active CA2925170C (fr) 2013-09-26 2014-09-26 Procedes de preparation d'alumine et de divers autres produits

Country Status (2)

Country Link
CA (1) CA2925170C (fr)
WO (1) WO2015042692A1 (fr)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105039731B (zh) * 2015-09-10 2017-09-29 攀钢集团攀枝花钢铁研究院有限公司 维持钛渣浸出过程体系热平衡的方法
CN105923640A (zh) * 2016-04-20 2016-09-07 航天推进技术研究院 硫酸活化除杂从粉煤灰提取氧化铝的方法
CN105883873B (zh) * 2016-04-20 2017-10-20 中国神华能源股份有限公司 基于硫酸热浸出从粉煤灰提取氧化铝的方法
CN106399693A (zh) * 2016-10-08 2017-02-15 淄博海慧工程设计咨询有限公司 一种铝灰的综合处理利用方法
CN108950212B (zh) * 2018-06-25 2020-11-20 中南大学 一种赤泥中综合回收钠、铝、铁的方法
CN109052402A (zh) * 2018-08-16 2018-12-21 陕西科技大学 一种绿色连续制备纯相碳化铁纳米颗粒的方法
CN112110714A (zh) * 2020-09-18 2020-12-22 神华准能资源综合开发有限公司 一种耐酸砖材料的制备方法及其应用
CN114672818A (zh) * 2022-03-25 2022-06-28 华北理工大学 一种利用赤泥制备铁铝硅-碳化硅复合材料的方法
WO2024250058A1 (fr) * 2023-06-06 2024-12-12 Andromeda Technologies Holdings Pty Ltd Production d'alumine de haute pureté et/ou d'alumine métallurgique
CN118183812B (zh) * 2024-05-15 2024-09-10 江苏晶晶新材料有限公司 一种氧化铝及其加工工艺

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013037054A1 (fr) * 2011-09-16 2013-03-21 Orbite Aluminae Inc. Procédés de préparation d'alumine et de divers autres produits
CN102849767B (zh) * 2012-04-10 2014-07-16 沈阳金博新技术产业有限公司 一种利用电厂粉煤灰制取氧化铝的方法
CN102849765B (zh) * 2012-04-10 2014-05-21 沈阳金博新技术产业有限公司 一种利用低品位铝土矿酸浸制取氧化铝的方法
JP2015535886A (ja) * 2012-09-26 2015-12-17 オーバイト アルミナ インコーポレイテッドＯｒｂｉｔｅ Ａｌｕｍｉｎａｅ Ｉｎｃ． 種々の材料のＨＣｌ浸出によるアルミナおよび塩化マグネシウムを調製するためのプロセス
CA2891427C (fr) * 2012-11-14 2016-09-20 Orbite Aluminae Inc. Procede de purification d'ions aluminium
CN103420405B (zh) * 2013-08-05 2015-07-01 山西大学 一种从含铝废渣中提取氧化铝的方法

Also Published As

Publication number Publication date
WO2015042692A1 (fr) 2015-04-02
CA2925170A1 (fr) 2015-04-02

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Effective date: 20190924