BR112019008816A2 - processo para a recuperação de furfural - Google Patents
processo para a recuperação de furfuralInfo
- Publication number
- BR112019008816A2 BR112019008816A2 BR112019008816A BR112019008816A BR112019008816A2 BR 112019008816 A2 BR112019008816 A2 BR 112019008816A2 BR 112019008816 A BR112019008816 A BR 112019008816A BR 112019008816 A BR112019008816 A BR 112019008816A BR 112019008816 A2 BR112019008816 A2 BR 112019008816A2
- Authority
- BR
- Brazil
- Prior art keywords
- furfural
- subjecting
- top stream
- stream
- water
- Prior art date
Links
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 title abstract 14
- 238000000034 method Methods 0.000 title abstract 2
- 238000011084 recovery Methods 0.000 title 1
- 238000004821 distillation Methods 0.000 abstract 2
- 150000007524 organic acids Chemical class 0.000 abstract 2
- 239000012074 organic phase Substances 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 239000003849 aromatic solvent Substances 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 150000007522 mineralic acids Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000011877 solvent mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
- C07D307/50—Preparation from natural products
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/36—Azeotropic distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Furan Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
trata-se de um processo para a extração de furfural incluindo: (a) submeter uma composição que compreende furfural, água, pelo menos um ácido inorgânico, pelo menos um ácido orgânico e uma mistura de solventes que compreende um solvente aromático e um solvente oxigenado, a uma primeira etapa de separação que proporciona: (i) uma primeira fase orgânica; (b) submeter a primeira fase orgânica a uma primeira etapa de destilação que proporciona: (i) uma primeira corrente de topo que compreende furfural e uma porção de pelo menos um ácido orgânico; (c) submeter a primeira corrente de topo da etapa (b) a um segunda etapa de separação que proporciona: (i) uma segunda corrente de topo enriquecida com furfural; (d) submeter a segunda corrente de topo da etapa (c) a uma segunda etapa de destilação que proporciona: (i) uma terceira corrente de topo que compreende um azeótropo de água e furfural e (ii) uma terceira corrente de fundo que compreende furfural.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201662415533P | 2016-11-01 | 2016-11-01 | |
US62/415,533 | 2016-11-01 | ||
PCT/US2017/058951 WO2018085182A1 (en) | 2016-11-01 | 2017-10-30 | Process for the recovery of furfural |
Publications (2)
Publication Number | Publication Date |
---|---|
BR112019008816A2 true BR112019008816A2 (pt) | 2019-07-16 |
BR112019008816B1 BR112019008816B1 (pt) | 2023-01-10 |
Family
ID=60302484
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112019008816-4A BR112019008816B1 (pt) | 2016-11-01 | 2017-10-30 | Processo para a recuperação de furfural |
Country Status (6)
Country | Link |
---|---|
US (1) | US10501430B2 (pt) |
EP (1) | EP3535247B1 (pt) |
CN (1) | CN109890800B (pt) |
BR (1) | BR112019008816B1 (pt) |
CA (1) | CA3039794A1 (pt) |
WO (1) | WO2018085182A1 (pt) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BR112019008839B1 (pt) * | 2016-11-01 | 2022-12-27 | Shell Internationale Research Maatschappij B.V | Processo para a extração de furfural |
Family Cites Families (45)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2078241A (en) | 1935-12-14 | 1937-04-27 | Chemical Foundation Inc | Production of furfural |
US2536732A (en) | 1947-03-20 | 1951-01-02 | Quaker Oats Co | Production of furfural |
US3549319A (en) | 1968-05-06 | 1970-12-22 | Fraser Co Ltd | Production of alkali metal sulfites or bisulfites |
CA1100266A (en) | 1977-08-31 | 1981-05-05 | Laszlo Paszner | Organosolv delignification and saccharification process for lignocellulosic plant materials |
US5366558A (en) | 1979-03-23 | 1994-11-22 | Brink David L | Method of treating biomass material |
US4461648A (en) | 1980-07-11 | 1984-07-24 | Patrick Foody | Method for increasing the accessibility of cellulose in lignocellulosic materials, particularly hardwoods agricultural residues and the like |
US4533743A (en) | 1983-12-16 | 1985-08-06 | Atlantic Richfield Company | Furfural process |
SU1365674A1 (ru) | 1984-01-10 | 1996-07-27 | Институт химии древесины АН ЛатвССР | Способ совместного получения фурфурола и сахаров |
US5562777A (en) | 1993-03-26 | 1996-10-08 | Arkenol, Inc. | Method of producing sugars using strong acid hydrolysis of cellulosic and hemicellulosic materials |
US5789210A (en) | 1993-11-08 | 1998-08-04 | Purdue Research Foundation | Recombinant yeasts for effective fermentation of glucose and xylose |
IN191596B (pt) | 1996-05-06 | 2003-12-06 | Purdue Research Foundation | |
SE9901298D0 (sv) | 1999-04-09 | 1999-04-09 | Forskarpatent I Syd Ab | Xylose isomerase with improved kinetic properties |
US7223575B2 (en) | 2000-05-01 | 2007-05-29 | Midwest Research Institute | Zymomonas pentose-sugar fermenting strains and uses thereof |
SE0400816D0 (sv) | 2004-03-26 | 2004-03-26 | Forskarpatent I Syd Ab | Mutated xylose reductase in xylose-fermentation by S. Cerevisiae |
WO2006096130A1 (en) | 2005-03-11 | 2006-09-14 | Forskarpatent I Syd Ab | Arabinose- and xylose-fermenting saccharomyces cerevisiae strains |
US7781191B2 (en) | 2005-04-12 | 2010-08-24 | E. I. Du Pont De Nemours And Company | Treatment of biomass to obtain a target chemical |
EP2172568A1 (en) | 2005-07-19 | 2010-04-07 | Inbicon A/S | Method and apparatus for conversion of cellulosic material to enthanol |
EP1922408A1 (en) | 2005-09-06 | 2008-05-21 | Cargill, Incorporated | Thermostable xylose isomerase enzyme |
ES2529176T3 (es) | 2006-05-19 | 2015-02-17 | Ls9, Inc. | Producción de ácidos grasos y derivados de los mismos |
WO2008119082A2 (en) | 2007-03-28 | 2008-10-02 | Ls9, Inc. | Enhanced production of fatty acid derivatives |
US7741084B2 (en) | 2006-09-28 | 2010-06-22 | E. I. Du Pont De Nemours And Company | Ethanol production using xylitol synthesis mutant of xylose-utilizing zymomonas |
US7741119B2 (en) | 2006-09-28 | 2010-06-22 | E. I. Du Pont De Nemours And Company | Xylitol synthesis mutant of xylose-utilizing zymomonas for ethanol production |
CN101583583A (zh) | 2006-12-15 | 2009-11-18 | 巴斯夫欧洲公司 | 通过非均相催化氢解多元醇生产1,2-乙二醇和1,2-丙二醇的方法 |
DE502008001144D1 (de) | 2007-07-02 | 2010-09-30 | Basf Se | Verfahren zur einstufigen herstellung von 2-methyltetrahydrofuran aus furfural an zwei katalysatoren in strukturierter schüttung |
AU2008291588A1 (en) | 2007-08-27 | 2009-03-05 | Iogen Energy Corporation | Method for the production of a fermentation product from a pretreated lignocellulosic feedstock |
WO2009109631A1 (en) | 2008-03-07 | 2009-09-11 | Dsm Ip Assets B.V. | A pentose sugar fermenting cell |
FI121541B (fi) | 2008-04-21 | 2010-12-31 | Kemira Oyj | Menetelmä muurahaishapon talteenottamiseksi |
EP2438144A4 (en) | 2009-06-05 | 2013-02-20 | Energy & Environ Res Ct Found | BIOVERFINDING OF SEVERAL PRODUCTS FOR SYNTHETIZING FUEL COMPONENTS AND CHEMICALS FROM LIGNOCELLULOSE MATERIALS USING LEVULINATE CAPACITORS |
PL2585184T3 (pl) | 2010-06-22 | 2017-11-30 | Shell Internationale Research Maatschappij B.V. | Proces oddzielania furfuralu od ciekłej fazy wodnej zawierającej furfural i jeden lub większą liczbę kwasów organicznych |
CN103189118B (zh) | 2010-08-23 | 2015-05-13 | 加州大学评议会 | 用于由水性混合物中提取有机化合物的方法 |
US20120083611A1 (en) | 2010-09-30 | 2012-04-05 | Shell Oil Company | Process for producing furfural |
WO2012047832A2 (en) | 2010-10-07 | 2012-04-12 | Shell Oil Company | Process for the production of alcohols from biomass |
CN103189526B (zh) | 2010-11-05 | 2015-07-08 | 国际壳牌研究有限公司 | 处理生物质以产生可用于生物燃料的材料 |
US8524924B2 (en) | 2010-12-21 | 2013-09-03 | E I Du Pont De Nemours And Company | Process for furfural production from biomass |
PH12013501775B1 (en) | 2011-02-28 | 2020-02-28 | Dsm Nutritional Products Llc | Polymeric acid catalysts and uses thereof |
US8389749B2 (en) | 2011-05-25 | 2013-03-05 | Wisconsin Alumni Research Foundation | Method to produce, recover and convert furan derivatives from aqueous solutions using alkylphenol extraction |
FI126351B (en) * | 2011-11-04 | 2016-10-14 | Taminco Finland Oy | Method and apparatus for separating at least one carboxylic acid and furfural from a dilute aqueous solution |
WO2013102007A1 (en) * | 2011-12-28 | 2013-07-04 | E. I. Du Pont De Nemours And Company | Process for the production of furfural |
AU2013259739B2 (en) | 2012-05-07 | 2015-08-20 | Shell Internationale Research Maatschappij B.V. | Continuous or semi-continuous process for treating biomass to produce materials useful for biofuels |
CN104379570A (zh) | 2012-07-13 | 2015-02-25 | 帝斯曼知识产权资产管理有限公司 | 从木质纤维素生物质生产糠醛和乙酰丙酸的工艺 |
US8772515B2 (en) | 2012-10-11 | 2014-07-08 | Wisconsin Alumni Research Foundation | Method to convert biomass to 5-(hydroxymethyl)-furfural (HMF) and furfural using lactones, furans, and pyrans as solvents |
US20140186903A1 (en) | 2012-12-28 | 2014-07-03 | Api Intellectual Property Holdings, Llc | Processes and apparatus for producing furfural, levulinic acid, and other sugar-derived products from biomass |
CN203469537U (zh) * | 2013-09-09 | 2014-03-12 | 中糠有限公司 | 用于多塔连续精馏制取糠醛工艺中的萃取塔 |
BR112016030661B8 (pt) | 2014-08-14 | 2022-03-29 | Shell Int Research | Processo de circuito fechado para converter biomassa em furfural |
BR112016030664B1 (pt) | 2014-08-14 | 2021-06-29 | Shell Internationale Research Maatschappij B.V. | Método para produzir furfural a partir de material de biomassa contendo pentosano |
-
2017
- 2017-10-30 BR BR112019008816-4A patent/BR112019008816B1/pt active IP Right Grant
- 2017-10-30 CN CN201780066178.8A patent/CN109890800B/zh active Active
- 2017-10-30 EP EP17797506.7A patent/EP3535247B1/en active Active
- 2017-10-30 WO PCT/US2017/058951 patent/WO2018085182A1/en unknown
- 2017-10-30 US US16/346,317 patent/US10501430B2/en active Active
- 2017-10-30 CA CA3039794A patent/CA3039794A1/en active Pending
Also Published As
Publication number | Publication date |
---|---|
BR112019008816B1 (pt) | 2023-01-10 |
EP3535247B1 (en) | 2020-11-25 |
CA3039794A1 (en) | 2018-05-11 |
US20190276422A1 (en) | 2019-09-12 |
WO2018085182A1 (en) | 2018-05-11 |
CN109890800B (zh) | 2023-05-23 |
CN109890800A (zh) | 2019-06-14 |
US10501430B2 (en) | 2019-12-10 |
EP3535247A1 (en) | 2019-09-11 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B350 | Update of information on the portal [chapter 15.35 patent gazette] | ||
B06W | Patent application suspended after preliminary examination (for patents with searches from other patent authorities) chapter 6.23 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 30/10/2017, OBSERVADAS AS CONDICOES LEGAIS |