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BG102504A - Method for the preparation of pure melamine - Google Patents

Method for the preparation of pure melamine

Info

Publication number
BG102504A
BG102504A BG102504A BG10250498A BG102504A BG 102504 A BG102504 A BG 102504A BG 102504 A BG102504 A BG 102504A BG 10250498 A BG10250498 A BG 10250498A BG 102504 A BG102504 A BG 102504A
Authority
BG
Bulgaria
Prior art keywords
melamine
ammonia
pressure
decompressed
pure
Prior art date
Application number
BG102504A
Other languages
Bulgarian (bg)
Inventor
Lorenzo Canzi
Gerhard Coufal
Martin Muellner
Original Assignee
Agrolinz Melamin Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Agrolinz Melamin Gmbh filed Critical Agrolinz Melamin Gmbh
Publication of BG102504A publication Critical patent/BG102504A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D251/00Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40Nitrogen atoms
    • C07D251/54Three nitrogen atoms
    • C07D251/56Preparation of melamine
    • C07D251/60Preparation of melamine from urea or from carbon dioxide and ammonia
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D251/00Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40Nitrogen atoms
    • C07D251/54Three nitrogen atoms
    • C07D251/62Purification of melamine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Phenolic Resins Or Amino Resins (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Sorption Type Refrigeration Machines (AREA)

Abstract

According to the method liquid ammonia-containing melamine isquickly decompressed from partial pressure of ammonia P1 from 400to 50 bar to partial pressue of ammonia P2 between 200 bar andatmospheric pressure at temperature range from 0 to 60oC above thespecified point of the solidification of the melamine, dependingon the prevailing partial pressure of the ammonia. The higherpressure allows a greater distance in the temperature from themelamine solidification point then the lower one, and P1 is alwaysbigger than P2. As a result of this the pure melamine is producedin solid form after which the melamine is decompressed toatmospheric pressure, and if necessary, is cooled to roomtemperature and the pure melamine is isolated.20 claims
BG102504A 1995-12-07 1998-06-02 Method for the preparation of pure melamine BG102504A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AT0199495A AT403579B (en) 1995-12-07 1995-12-07 METHOD FOR PRODUCING HIGH PURITY MELAMINE
PCT/EP1996/005389 WO1997020826A1 (en) 1995-12-07 1996-12-04 Process for producing pure melamine

Publications (1)

Publication Number Publication Date
BG102504A true BG102504A (en) 1999-04-30

Family

ID=3525542

Family Applications (1)

Application Number Title Priority Date Filing Date
BG102504A BG102504A (en) 1995-12-07 1998-06-02 Method for the preparation of pure melamine

Country Status (29)

Country Link
EP (1) EP0874832B1 (en)
JP (1) JP2000501404A (en)
KR (1) KR100462920B1 (en)
CN (1) CN1067995C (en)
AR (1) AR004873A1 (en)
AT (2) AT403579B (en)
AU (1) AU709030B2 (en)
BG (1) BG102504A (en)
BR (1) BR9611892A (en)
CA (1) CA2239542A1 (en)
CO (1) CO4770995A1 (en)
DE (1) DE59609075D1 (en)
DZ (1) DZ2135A1 (en)
EA (1) EA000931B1 (en)
EG (1) EG20917A (en)
HR (1) HRP960575A2 (en)
HU (1) HUP9904406A3 (en)
IL (1) IL124630A0 (en)
MX (1) MX9804435A (en)
MY (1) MY112761A (en)
NO (1) NO309982B1 (en)
NZ (1) NZ324297A (en)
PL (1) PL189811B1 (en)
SK (1) SK74998A3 (en)
TR (1) TR199801029T2 (en)
TW (1) TW341567B (en)
UA (1) UA46072C2 (en)
WO (1) WO1997020826A1 (en)
ZA (1) ZA9610295B (en)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE69813545T2 (en) 1997-05-21 2004-04-08 Dsm N.V. METHOD FOR PRODUCING MELAMINE
NL1006095C2 (en) * 1997-05-21 1998-11-25 Dsm Nv Preparation of melamine from urea via a high pressure process
AU729323B2 (en) 1997-05-28 2001-02-01 Dsm Ip Assets B.V. Method for preparing melamine
NL1006147C2 (en) * 1997-05-28 1998-12-01 Dsm Nv Pure melamine is formed from urea by spray cooling the melamine melt
ID24348A (en) * 1997-06-02 2000-07-13 Dsm Nv METHODS FOR MELAMIN PREPARATION
EP0986546B1 (en) * 1997-06-02 2007-03-28 DSM IP Assets B.V. Crystalline melamine
NL1006191C2 (en) * 1997-06-02 1998-12-03 Dsm Nv Multi-crystalline melamine powder is prepared from urea
NL1006192C2 (en) * 1997-06-02 1998-12-03 Dsm Nv Melamine is prepared from urea in a high pressure process
NL1008571C2 (en) * 1998-03-12 1999-07-28 Dsm Nv Crystalline melamine.
SK6192001A3 (en) 1998-11-13 2001-12-03 Agrolinz Melamin Gmbh Method for producing pure melamine
BR9916562A (en) 1998-12-23 2001-10-09 Agrolinz Melamin Gmbh Melamine purification process
EP1035117A1 (en) * 1999-03-08 2000-09-13 Dsm N.V. Method for preparing melamine from urea
US6603001B1 (en) 1999-03-15 2003-08-05 Agrolinz Melamin Gmbh Process for preparing solid melamine
WO2001007420A2 (en) * 1999-07-27 2001-02-01 Agrolinz Melamin Gmbh Method for producing solid melamine
NL1013217C2 (en) * 1999-10-05 2001-04-06 Dsm Nv Process for the preparation of melamine.
EP1138676A1 (en) * 2000-03-27 2001-10-04 Casale Chemicals SA Process for producing melamine at high pureness
AT410210B (en) 2000-08-07 2003-03-25 Agrolinz Melamin Gmbh METHOD FOR PRODUCING MELAMINE
AT500297B8 (en) 2000-11-08 2007-02-15 Agrolinz Melamin Gmbh PROCESS FOR CLEANING MELAMINE AMMONIA
AT410793B (en) * 2000-12-27 2003-07-25 Agrolinz Melamin Gmbh METHOD FOR PRODUCING MELAMINE
CN1315812C (en) 2001-11-16 2007-05-16 Ami-阿格罗林茨三聚氰胺有限公司 Method for producing melem-free melamine and quenching device
FR2843964B1 (en) * 2002-08-29 2004-10-01 Sanofi Synthelabo DIOXANE-2-ALKYLCARBAMATES DERIVATIVES, THEIR PREPARATION AND THEIR THERAPEUTIC APPLICATION
RU2417992C2 (en) * 2009-07-20 2011-05-10 Открытое акционерное общество "Научно-исследовательский и проектный институт карбамида и продуктов органического синтеза" (ОАО "НИИК") Method of producing melamine and method of removing dissolved gases from aqueous solution of crude melamine

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3116294A (en) * 1963-12-31 Process- for preparing high-purity melamine from urea
US3637686A (en) * 1969-02-10 1972-01-25 Nissan Chemical Ind Ltd Process for recovering purified melamine
DE3500188C2 (en) * 1984-01-05 1994-08-18 Melamine Chemicals Inc Anhydrous high-pressure melamine synthesis
US4565867A (en) * 1984-01-05 1986-01-21 Melamine Chemicals, Inc. Anhydrous high-pressure melamine synthesis
DE3546893C3 (en) * 1984-01-05 1998-01-29 Melamine Chemicals Inc Anhydrous high-pressure melamine synthesis
AT402294B (en) * 1994-12-23 1997-03-25 Agrolinz Melamin Gmbh METHOD FOR PRODUCING HIGH PURITY MELAMINE
AT402296B (en) * 1995-02-03 1997-03-25 Agrolinz Melamin Gmbh METHOD FOR PURIFYING MELAMINE
US5514797A (en) * 1995-06-07 1996-05-07 Melamine Chemicals, Inc. Method for increasing purity of melamine
US5514796A (en) * 1995-06-07 1996-05-07 Melamine Chemicals, Inc. Melamine of improved purity produced by high-pressure, non-catalytic process

Also Published As

Publication number Publication date
AT403579B (en) 1998-03-25
JP2000501404A (en) 2000-02-08
TW341567B (en) 1998-10-01
AU1175597A (en) 1997-06-27
EG20917A (en) 2000-06-28
TR199801029T2 (en) 1999-05-21
CN1067995C (en) 2001-07-04
ATE215936T1 (en) 2002-04-15
HUP9904406A2 (en) 2000-05-28
IL124630A0 (en) 1998-12-06
HUP9904406A3 (en) 2000-07-28
KR19990071932A (en) 1999-09-27
MY112761A (en) 2001-08-30
DE59609075D1 (en) 2002-05-16
EA000931B1 (en) 2000-06-26
CN1203592A (en) 1998-12-30
WO1997020826A1 (en) 1997-06-12
EP0874832A1 (en) 1998-11-04
NO309982B1 (en) 2001-04-30
PL189811B1 (en) 2005-09-30
NZ324297A (en) 1999-07-29
UA46072C2 (en) 2002-05-15
NO982251L (en) 1998-05-15
CA2239542A1 (en) 1997-06-12
AU709030B2 (en) 1999-08-19
CO4770995A1 (en) 1999-04-30
BR9611892A (en) 1999-02-17
SK74998A3 (en) 1998-11-04
AR004873A1 (en) 1999-03-10
EP0874832B1 (en) 2002-04-10
NO982251D0 (en) 1998-05-15
DZ2135A1 (en) 2002-07-23
ZA9610295B (en) 1997-06-17
ATA199495A (en) 1997-08-15
MX9804435A (en) 1998-09-30
HRP960575A2 (en) 1997-12-31
KR100462920B1 (en) 2005-04-08
PL327067A1 (en) 1998-11-23
EA199800532A1 (en) 1998-12-24

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