BG102504A - Method for the preparation of pure melamine - Google Patents
Method for the preparation of pure melamineInfo
- Publication number
- BG102504A BG102504A BG102504A BG10250498A BG102504A BG 102504 A BG102504 A BG 102504A BG 102504 A BG102504 A BG 102504A BG 10250498 A BG10250498 A BG 10250498A BG 102504 A BG102504 A BG 102504A
- Authority
- BG
- Bulgaria
- Prior art keywords
- melamine
- ammonia
- pressure
- decompressed
- pure
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/54—Three nitrogen atoms
- C07D251/56—Preparation of melamine
- C07D251/60—Preparation of melamine from urea or from carbon dioxide and ammonia
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/54—Three nitrogen atoms
- C07D251/62—Purification of melamine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Phenolic Resins Or Amino Resins (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Sorption Type Refrigeration Machines (AREA)
Abstract
According to the method liquid ammonia-containing melamine isquickly decompressed from partial pressure of ammonia P1 from 400to 50 bar to partial pressue of ammonia P2 between 200 bar andatmospheric pressure at temperature range from 0 to 60oC above thespecified point of the solidification of the melamine, dependingon the prevailing partial pressure of the ammonia. The higherpressure allows a greater distance in the temperature from themelamine solidification point then the lower one, and P1 is alwaysbigger than P2. As a result of this the pure melamine is producedin solid form after which the melamine is decompressed toatmospheric pressure, and if necessary, is cooled to roomtemperature and the pure melamine is isolated.20 claims
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT0199495A AT403579B (en) | 1995-12-07 | 1995-12-07 | METHOD FOR PRODUCING HIGH PURITY MELAMINE |
PCT/EP1996/005389 WO1997020826A1 (en) | 1995-12-07 | 1996-12-04 | Process for producing pure melamine |
Publications (1)
Publication Number | Publication Date |
---|---|
BG102504A true BG102504A (en) | 1999-04-30 |
Family
ID=3525542
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BG102504A BG102504A (en) | 1995-12-07 | 1998-06-02 | Method for the preparation of pure melamine |
Country Status (29)
Country | Link |
---|---|
EP (1) | EP0874832B1 (en) |
JP (1) | JP2000501404A (en) |
KR (1) | KR100462920B1 (en) |
CN (1) | CN1067995C (en) |
AR (1) | AR004873A1 (en) |
AT (2) | AT403579B (en) |
AU (1) | AU709030B2 (en) |
BG (1) | BG102504A (en) |
BR (1) | BR9611892A (en) |
CA (1) | CA2239542A1 (en) |
CO (1) | CO4770995A1 (en) |
DE (1) | DE59609075D1 (en) |
DZ (1) | DZ2135A1 (en) |
EA (1) | EA000931B1 (en) |
EG (1) | EG20917A (en) |
HR (1) | HRP960575A2 (en) |
HU (1) | HUP9904406A3 (en) |
IL (1) | IL124630A0 (en) |
MX (1) | MX9804435A (en) |
MY (1) | MY112761A (en) |
NO (1) | NO309982B1 (en) |
NZ (1) | NZ324297A (en) |
PL (1) | PL189811B1 (en) |
SK (1) | SK74998A3 (en) |
TR (1) | TR199801029T2 (en) |
TW (1) | TW341567B (en) |
UA (1) | UA46072C2 (en) |
WO (1) | WO1997020826A1 (en) |
ZA (1) | ZA9610295B (en) |
Families Citing this family (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE69813545T2 (en) | 1997-05-21 | 2004-04-08 | Dsm N.V. | METHOD FOR PRODUCING MELAMINE |
NL1006095C2 (en) * | 1997-05-21 | 1998-11-25 | Dsm Nv | Preparation of melamine from urea via a high pressure process |
AU729323B2 (en) | 1997-05-28 | 2001-02-01 | Dsm Ip Assets B.V. | Method for preparing melamine |
NL1006147C2 (en) * | 1997-05-28 | 1998-12-01 | Dsm Nv | Pure melamine is formed from urea by spray cooling the melamine melt |
ID24348A (en) * | 1997-06-02 | 2000-07-13 | Dsm Nv | METHODS FOR MELAMIN PREPARATION |
EP0986546B1 (en) * | 1997-06-02 | 2007-03-28 | DSM IP Assets B.V. | Crystalline melamine |
NL1006191C2 (en) * | 1997-06-02 | 1998-12-03 | Dsm Nv | Multi-crystalline melamine powder is prepared from urea |
NL1006192C2 (en) * | 1997-06-02 | 1998-12-03 | Dsm Nv | Melamine is prepared from urea in a high pressure process |
NL1008571C2 (en) * | 1998-03-12 | 1999-07-28 | Dsm Nv | Crystalline melamine. |
SK6192001A3 (en) | 1998-11-13 | 2001-12-03 | Agrolinz Melamin Gmbh | Method for producing pure melamine |
BR9916562A (en) | 1998-12-23 | 2001-10-09 | Agrolinz Melamin Gmbh | Melamine purification process |
EP1035117A1 (en) * | 1999-03-08 | 2000-09-13 | Dsm N.V. | Method for preparing melamine from urea |
US6603001B1 (en) | 1999-03-15 | 2003-08-05 | Agrolinz Melamin Gmbh | Process for preparing solid melamine |
WO2001007420A2 (en) * | 1999-07-27 | 2001-02-01 | Agrolinz Melamin Gmbh | Method for producing solid melamine |
NL1013217C2 (en) * | 1999-10-05 | 2001-04-06 | Dsm Nv | Process for the preparation of melamine. |
EP1138676A1 (en) * | 2000-03-27 | 2001-10-04 | Casale Chemicals SA | Process for producing melamine at high pureness |
AT410210B (en) | 2000-08-07 | 2003-03-25 | Agrolinz Melamin Gmbh | METHOD FOR PRODUCING MELAMINE |
AT500297B8 (en) | 2000-11-08 | 2007-02-15 | Agrolinz Melamin Gmbh | PROCESS FOR CLEANING MELAMINE AMMONIA |
AT410793B (en) * | 2000-12-27 | 2003-07-25 | Agrolinz Melamin Gmbh | METHOD FOR PRODUCING MELAMINE |
CN1315812C (en) | 2001-11-16 | 2007-05-16 | Ami-阿格罗林茨三聚氰胺有限公司 | Method for producing melem-free melamine and quenching device |
FR2843964B1 (en) * | 2002-08-29 | 2004-10-01 | Sanofi Synthelabo | DIOXANE-2-ALKYLCARBAMATES DERIVATIVES, THEIR PREPARATION AND THEIR THERAPEUTIC APPLICATION |
RU2417992C2 (en) * | 2009-07-20 | 2011-05-10 | Открытое акционерное общество "Научно-исследовательский и проектный институт карбамида и продуктов органического синтеза" (ОАО "НИИК") | Method of producing melamine and method of removing dissolved gases from aqueous solution of crude melamine |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3116294A (en) * | 1963-12-31 | Process- for preparing high-purity melamine from urea | ||
US3637686A (en) * | 1969-02-10 | 1972-01-25 | Nissan Chemical Ind Ltd | Process for recovering purified melamine |
DE3500188C2 (en) * | 1984-01-05 | 1994-08-18 | Melamine Chemicals Inc | Anhydrous high-pressure melamine synthesis |
US4565867A (en) * | 1984-01-05 | 1986-01-21 | Melamine Chemicals, Inc. | Anhydrous high-pressure melamine synthesis |
DE3546893C3 (en) * | 1984-01-05 | 1998-01-29 | Melamine Chemicals Inc | Anhydrous high-pressure melamine synthesis |
AT402294B (en) * | 1994-12-23 | 1997-03-25 | Agrolinz Melamin Gmbh | METHOD FOR PRODUCING HIGH PURITY MELAMINE |
AT402296B (en) * | 1995-02-03 | 1997-03-25 | Agrolinz Melamin Gmbh | METHOD FOR PURIFYING MELAMINE |
US5514797A (en) * | 1995-06-07 | 1996-05-07 | Melamine Chemicals, Inc. | Method for increasing purity of melamine |
US5514796A (en) * | 1995-06-07 | 1996-05-07 | Melamine Chemicals, Inc. | Melamine of improved purity produced by high-pressure, non-catalytic process |
-
1995
- 1995-12-07 AT AT0199495A patent/AT403579B/en active
-
1996
- 1996-12-02 TW TW085114862A patent/TW341567B/en active
- 1996-12-03 EG EG106896A patent/EG20917A/en active
- 1996-12-04 HU HU9904406A patent/HUP9904406A3/en unknown
- 1996-12-04 MY MYPI96005088A patent/MY112761A/en unknown
- 1996-12-04 AT AT96942322T patent/ATE215936T1/en not_active IP Right Cessation
- 1996-12-04 AU AU11755/97A patent/AU709030B2/en not_active Ceased
- 1996-12-04 UA UA98063040A patent/UA46072C2/en unknown
- 1996-12-04 TR TR1998/01029T patent/TR199801029T2/en unknown
- 1996-12-04 PL PL96327067A patent/PL189811B1/en not_active IP Right Cessation
- 1996-12-04 EP EP96942322A patent/EP0874832B1/en not_active Expired - Lifetime
- 1996-12-04 DE DE59609075T patent/DE59609075D1/en not_active Expired - Lifetime
- 1996-12-04 NZ NZ324297A patent/NZ324297A/en unknown
- 1996-12-04 CN CN96198818A patent/CN1067995C/en not_active Expired - Fee Related
- 1996-12-04 BR BR9611892A patent/BR9611892A/en active Search and Examination
- 1996-12-04 IL IL12463096A patent/IL124630A0/en unknown
- 1996-12-04 EA EA199800532A patent/EA000931B1/en not_active IP Right Cessation
- 1996-12-04 SK SK749-98A patent/SK74998A3/en unknown
- 1996-12-04 JP JP9520981A patent/JP2000501404A/en active Pending
- 1996-12-04 KR KR10-1998-0704219A patent/KR100462920B1/en not_active IP Right Cessation
- 1996-12-04 DZ DZ960180A patent/DZ2135A1/en active
- 1996-12-04 CA CA002239542A patent/CA2239542A1/en not_active Abandoned
- 1996-12-04 WO PCT/EP1996/005389 patent/WO1997020826A1/en active IP Right Grant
- 1996-12-05 CO CO96063884A patent/CO4770995A1/en unknown
- 1996-12-05 HR HRA1994/95A patent/HRP960575A2/en not_active Application Discontinuation
- 1996-12-06 ZA ZA9610295A patent/ZA9610295B/en unknown
- 1996-12-06 AR ARP960105520A patent/AR004873A1/en active IP Right Grant
-
1998
- 1998-05-15 NO NO982251A patent/NO309982B1/en not_active IP Right Cessation
- 1998-06-02 BG BG102504A patent/BG102504A/en unknown
- 1998-06-04 MX MX9804435A patent/MX9804435A/en unknown
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