AR083101A1 - Proceso y sistema para la produccion de acido acetico - Google Patents
Proceso y sistema para la produccion de acido aceticoInfo
- Publication number
- AR083101A1 AR083101A1 ARP110103499A ARP110103499A AR083101A1 AR 083101 A1 AR083101 A1 AR 083101A1 AR P110103499 A ARP110103499 A AR P110103499A AR P110103499 A ARP110103499 A AR P110103499A AR 083101 A1 AR083101 A1 AR 083101A1
- Authority
- AR
- Argentina
- Prior art keywords
- acetic acid
- reagent
- reactor
- reaction solution
- reaction medium
- Prior art date
Links
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 title abstract 24
- 238000000034 method Methods 0.000 title abstract 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 6
- 239000003153 chemical reaction reagent Substances 0.000 abstract 5
- 239000012429 reaction media Substances 0.000 abstract 5
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 abstract 4
- TZIHFWKZFHZASV-UHFFFAOYSA-N methyl formate Chemical compound COC=O TZIHFWKZFHZASV-UHFFFAOYSA-N 0.000 abstract 4
- 238000011084 recovery Methods 0.000 abstract 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract 3
- 229910002091 carbon monoxide Inorganic materials 0.000 abstract 3
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 abstract 2
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- INQOMBQAUSQDDS-UHFFFAOYSA-N iodomethane Chemical compound IC INQOMBQAUSQDDS-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
- C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Reivindicación 1: Un proceso para producir ácido acético, que comprende las etapas de: hacer reaccionar monóxido de carbono con al menos un reactivo en un primer reactor que contiene un medio de reacción para producir una solución de reacción que comprende ácido acético, en donde el al menos un reactivo está seleccionado del grupo que consiste en metanol, acetato de metilo, formiato de metilo, éter dimetílico y mezclas de ellos y en donde el medio de reacción comprende agua, ácido acético, yoduro de metilo y un catalizador; introducir al menos una porción de la solución de reacción en un segundo reactor para producir una primera corriente de recuperación de calor; e introducir la primera corriente de recuperación de calor en el primer reactor.Reivindicación 14: Un sistema para producir ácido acético, que comprende: un primer reactor para hacer reaccionar monóxido de carbono, al menos un reactivo y un medio de reacción para producir una primera solución de reacción que comprende ácido acético; un separador para separar la primera solución de reacción en una pluralidad de corrientes de recuperación de calor derivado; y un segundo reactor para hacer reaccionar monóxido de carbono, el al menos un reactivo y el medio de reacción para producir una segunda solución de reacción que comprende ácido acético y para recuperar vapor y/o calor de al menos una de las corrientes de recuperación de calor, en donde el al menos un reactivo esta seleccionado del grupo que consiste en metanol, acetato de metilo, formiato de metilo, éter dimetílico y mezclas de ellos, y en donde el medio de reacción comprende agua, ácido acético, yoduro de metilo y un catalizador.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/890,383 US8530696B2 (en) | 2010-09-24 | 2010-09-24 | Pump around reactor for production of acetic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR083101A1 true AR083101A1 (es) | 2013-01-30 |
Family
ID=44675835
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP110103499A AR083101A1 (es) | 2010-09-24 | 2011-09-23 | Proceso y sistema para la produccion de acido acetico |
Country Status (15)
| Country | Link |
|---|---|
| US (2) | US8530696B2 (es) |
| EP (1) | EP2621880B1 (es) |
| JP (1) | JP5960143B2 (es) |
| CN (1) | CN103201247B (es) |
| AR (1) | AR083101A1 (es) |
| BR (1) | BR112013006963B1 (es) |
| CA (1) | CA2812700C (es) |
| ES (1) | ES2832198T3 (es) |
| HK (1) | HK1187329A1 (es) |
| MX (1) | MX345481B (es) |
| RS (1) | RS61426B1 (es) |
| RU (1) | RU2584422C2 (es) |
| SG (1) | SG189059A1 (es) |
| TW (1) | TWI634103B (es) |
| WO (1) | WO2012039973A1 (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8563773B2 (en) | 2010-12-16 | 2013-10-22 | Celanese International Corporation | Eductor-based reactor and pump around loops for production of acetic acid |
| US9663437B2 (en) * | 2011-09-13 | 2017-05-30 | Celanese International Corporation | Production of acetic acid with high conversion rate |
| WO2016054608A1 (en) | 2014-10-02 | 2016-04-07 | Celanese International Corporation | Process for producing acetic acid |
| US9487464B2 (en) | 2015-01-30 | 2016-11-08 | Celanese International Corporation | Processes for producing acetic acid |
| US9561994B2 (en) | 2015-01-30 | 2017-02-07 | Celanese International Corporation | Processes for producing acetic acid |
| US9505696B2 (en) | 2015-02-04 | 2016-11-29 | Celanese International Corporation | Process to control HI concentration in residuum stream |
| US10807935B2 (en) | 2018-11-02 | 2020-10-20 | Celanese International Corporation | Process for continuous acetic acid production |
| WO2021202270A1 (en) | 2020-04-01 | 2021-10-07 | Celanese International Corporation | Processes for removing and/or reducing permanganate reducing compounds and alkyl iodides |
| KR20230019135A (ko) | 2020-06-03 | 2023-02-07 | 셀라니즈 인터내셔날 코포레이션 | 공정 스트림으로부터 아세탈의 제거 |
| US20230202957A1 (en) | 2020-06-03 | 2023-06-29 | Celanese International Corporation | Production and purification of acetic acid |
| EP4161888A1 (en) | 2020-06-03 | 2023-04-12 | Celanese International Corporation | Process for acetic acid production by removing permanganate reducing compounds |
| US11807597B2 (en) * | 2021-04-02 | 2023-11-07 | Lyondellbasell Acetyls, Llc | Methods and systems for producing acetic acid |
Family Cites Families (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3769329A (en) | 1970-03-12 | 1973-10-30 | Monsanto Co | Production of carboxylic acids and esters |
| US4102922A (en) | 1974-12-30 | 1978-07-25 | Monsanto Company | Purification of carbonylation products |
| US5001259A (en) | 1984-05-03 | 1991-03-19 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US5144068A (en) | 1984-05-03 | 1992-09-01 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US5026908A (en) | 1984-05-03 | 1991-06-25 | Hoechst Celanese Corporation | Methanol carbonylation process |
| CA1299195C (en) | 1986-06-16 | 1992-04-21 | G. Paull Torrence | Addition of hydrogen to carbon monoxide feed gas in producing acetic acid by carbonylation of methanol |
| US5334755A (en) * | 1992-04-24 | 1994-08-02 | Chiyoda Corporation | Process for the production of acetic acid from methanol and carbon monoxide using supported rhodium catalyst |
| DE4239580C2 (de) * | 1992-11-25 | 1996-07-25 | Samson Ag | Stellantrieb mit Sicherheitseinrichtung |
| US5672743A (en) | 1993-09-10 | 1997-09-30 | Bp Chemicals Limited | Process for the production of acetic acid |
| US5364963A (en) | 1993-04-30 | 1994-11-15 | Chiyoda Corporation | Supported rhodium catalyst, method of preparing same and process of producing acetic acid by methanol carbonylation using same |
| JP3308392B2 (ja) | 1994-06-02 | 2002-07-29 | ダイセル化学工業株式会社 | カルボニル化反応方法 |
| US5696284A (en) | 1995-06-21 | 1997-12-09 | Bp Chemicals Limited | Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof |
| GB9517184D0 (en) * | 1995-08-22 | 1995-10-25 | Bp Chem Int Ltd | Process |
| KR100462697B1 (ko) | 1995-10-27 | 2005-02-28 | 씨엔에이 홀딩즈 인코포레이티드 | 부식금속을제거하여카보닐화촉매용액의생산성을증진시키는방법 |
| US6339171B1 (en) | 1996-10-18 | 2002-01-15 | Celanese International Corporation | Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream |
| GB9625335D0 (en) * | 1996-12-05 | 1997-01-22 | Bp Chem Int Ltd | Process |
| GB9626429D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9626317D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9626428D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| US6114576A (en) | 1997-12-18 | 2000-09-05 | Uop Llc | Carbonylation process with integrated heat exchange |
| ATE261426T1 (de) | 1998-08-06 | 2004-03-15 | Haldor Topsoe As | Reaktiv distillierungsverfahren zur herstellung von essigsäure auf der basis von dme/methanol carbonylierung |
| US6232352B1 (en) * | 1999-11-01 | 2001-05-15 | Acetex Limited | Methanol plant retrofit for acetic acid manufacture |
| US6627770B1 (en) | 2000-08-24 | 2003-09-30 | Celanese International Corporation | Method and apparatus for sequesting entrained and volatile catalyst species in a carbonylation process |
| US6657078B2 (en) | 2001-02-07 | 2003-12-02 | Celanese International Corporation | Low energy carbonylation process |
| FR2826960B1 (fr) | 2001-07-03 | 2005-10-21 | Acetex Chimie | Procede de controle d'une production d'acide acetique et/ou d'acetate de methyle en continu |
| GB0211560D0 (en) | 2002-05-20 | 2002-06-26 | Bp Chem Int Ltd | Process |
| US7005541B2 (en) | 2002-12-23 | 2006-02-28 | Celanese International Corporation | Low water methanol carbonylation process for high acetic acid production and for water balance control |
| MY141209A (en) * | 2003-03-13 | 2010-03-31 | Chiyoda Corp | Method of manufacturing acetic acid |
| US7223886B2 (en) | 2004-03-02 | 2007-05-29 | Celanese International Corporation | Removal of permanganate reducing compounds from methanol carbonylation process stream |
| US7465823B2 (en) * | 2004-03-17 | 2008-12-16 | Celanese International Corporation | Utilization of acetic acid reaction heat in other process plants |
| US7767848B2 (en) | 2005-02-08 | 2010-08-03 | Celanese International Corporation | Method of controlling acetic acid process |
| JP5047984B2 (ja) * | 2005-12-21 | 2012-10-10 | ビーピー ケミカルズ リミテッド | カルボニル化方法 |
| US7989659B2 (en) | 2007-05-17 | 2011-08-02 | Celanese International Corporation | Method and apparatus for making acetic acid with improved light ends column productivity |
| US8017802B2 (en) | 2007-05-21 | 2011-09-13 | Celanese International Corporation | Control of impurities in reaction product of rhodium-catalyzed methanol carbonylation |
| US7619113B2 (en) | 2007-09-27 | 2009-11-17 | Celanese International Corporation | Method and apparatus for making acetic acid with improved purification |
| US8062482B2 (en) | 2007-10-30 | 2011-11-22 | Celanese International Corporation | Acetaldehyde removal from methyl acetate by distillation at elevated pressure |
| EP2093209A1 (en) | 2008-02-19 | 2009-08-26 | BP Chemicals Limited | Process for the production of acetic acid |
| RU2469783C2 (ru) | 2008-04-29 | 2012-12-20 | Селаниз Интернэшнл Корпорейшн | Устройство для карбонилирования метанола, имеющее абсорбер с возможностью выбора из нескольких растворителей |
| US9012683B2 (en) * | 2010-11-12 | 2015-04-21 | Eastman Chemical Company | Coproduction of acetic acid and acetic anhydride |
-
2010
- 2010-09-24 US US12/890,383 patent/US8530696B2/en active Active
-
2011
- 2011-09-12 ES ES11760922T patent/ES2832198T3/es active Active
- 2011-09-12 BR BR112013006963-5A patent/BR112013006963B1/pt active IP Right Grant
- 2011-09-12 JP JP2013530178A patent/JP5960143B2/ja active Active
- 2011-09-12 RS RS20210101A patent/RS61426B1/sr unknown
- 2011-09-12 RU RU2013118697/04A patent/RU2584422C2/ru active
- 2011-09-12 CN CN201180054453.7A patent/CN103201247B/zh active Active
- 2011-09-12 EP EP11760922.2A patent/EP2621880B1/en active Active
- 2011-09-12 WO PCT/US2011/051168 patent/WO2012039973A1/en active Application Filing
- 2011-09-12 SG SG2013021522A patent/SG189059A1/en unknown
- 2011-09-12 MX MX2013003395A patent/MX345481B/es active IP Right Grant
- 2011-09-12 CA CA2812700A patent/CA2812700C/en active Active
- 2011-09-15 TW TW100133171A patent/TWI634103B/zh active
- 2011-09-23 AR ARP110103499A patent/AR083101A1/es unknown
-
2013
- 2013-08-14 US US13/966,772 patent/US9550714B2/en active Active
-
2014
- 2014-01-10 HK HK14100293.8A patent/HK1187329A1/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| ES2832198T3 (es) | 2021-06-09 |
| JP5960143B2 (ja) | 2016-08-02 |
| SG189059A1 (en) | 2013-05-31 |
| CN103201247B (zh) | 2015-11-25 |
| BR112013006963A2 (pt) | 2016-07-26 |
| WO2012039973A1 (en) | 2012-03-29 |
| CN103201247A (zh) | 2013-07-10 |
| RU2584422C2 (ru) | 2016-05-20 |
| CA2812700C (en) | 2018-07-10 |
| EP2621880B1 (en) | 2020-11-11 |
| JP2013538826A (ja) | 2013-10-17 |
| MX345481B (es) | 2017-01-31 |
| RS61426B1 (sr) | 2021-03-31 |
| TW201217328A (en) | 2012-05-01 |
| EP2621880A1 (en) | 2013-08-07 |
| MX2013003395A (es) | 2013-09-13 |
| US8530696B2 (en) | 2013-09-10 |
| US20140012040A1 (en) | 2014-01-09 |
| WO2012039973A9 (en) | 2014-04-03 |
| BR112013006963B1 (pt) | 2019-05-28 |
| HK1187329A1 (zh) | 2014-04-04 |
| US9550714B2 (en) | 2017-01-24 |
| CA2812700A1 (en) | 2012-03-29 |
| RU2013118697A (ru) | 2014-10-27 |
| TWI634103B (zh) | 2018-09-01 |
| US20120078011A1 (en) | 2012-03-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FB | Suspension of granting procedure |