ANNEX II

BUREAU OF INDIAN STANDARDS

(SELF EVALUATION CUM VERIFICATION REPORT)

1. GENERAL INFORMATION

a) Applicant’s Name : M/s THIRUMALA INDUSTRIES

b) Person(s) to be contacted during Inspection : Mr. SUBBAREDDY /9440527015

c) BIS licenses, if any, held by the applicant : nil

2. RAW MATERIALS

a) Raw materials used

Sl.No Raw Name of With or without Test How received

material supplier BIS Certification certificate of batches/ lots
mark the supplier nature of
package
1. Bore well Own source Not applicable TR is
enclosed as
Enclosure – I
A
2. 20 Liter Praveen With out BIS Enclosed as Lots
Transparent polymers, Certification Enclosure I B
PET chennai.
Container

b) Arrangement for testing as received : NIL

c) Methods of disposal of sub-standard raw materials : Returned to the Supplier.

d) Record of tests with proforma of records : NIL

3 MANUFACTURE
3.1 Machinery & Equipment
S.No Machinery Make Capacity Number

1. Bore well Pump UNNATHL 5 HP 1

2. Raw water tank CIVIL 5000 LTS 1
3. Raw Water Pump CRI 3 HP 1
4. Sand Filter WAVE CYBER 1000 LPH 1
5. Activated Carbon Filter WAVE CYBER 1000 LPH 1
6. Micron Filter (5) GOPANZ 1000 LPH 1
7. High pressure pump AQUA NOMEX 4 HP 1
8. R.O System TORAX 1000 LPH 1
9. S.S Water Tank 1000 LTS 2
10. S.S Pump AROMA 1HP 1
S.S. Micron filter (1
11. micron)
GOPANZ 1000 LPH 1
S.S. Micron filter (0.5
12. micron)
GOPANZ 1000 LPH 1
S.S. Micron filter (0.2
13. micron)
GOPANZ 1000 LPH 1
14. U.V Sterilizer PHILIPS 1000 LPH 1
15. Ozonater DELTA 1000 LPH 1
1 TON
16. Air Condition (A/C) O general 2
COOLING 2
17. AIR Curtain CONTROL
Electric Instant Water
18. heater BAJAJ 3 KV 1
19. Door closer HARDWYN 10
20. SS Pipeline 304, 316 GRADE
21. Electrical power supply AP TRANSCO 30 HP
22. Refrigerator VEDIOCON 165 LTS 1
SELF
23. Inspection screen FABRICATED
1
24. Pest Killing lamp Kill Pest 2

I hereby declare that the machinery of which details are given above is owned by me and
are actually installed in the premises

I also declare that incase of grant of license, I will send prior intimation to BIS whenever
any equipment is taken out of the premises of the firm due to any reason.
3.2 Process and Production

a) Process Description

1. PRE – TREATMENT:

Raw water is drawn from bore well situated within the factory and stored in the raw
water storage Sump. Chlorination is carried at to the required level. Then it passes
through the sand filter to remove the suspended solids followed by Activated Carbon
Filter for De-chlorination then its passes through the micron filter (5).

2. R.O.SYSTEM:

The pre-treated water passes through R.O. membranes by high-pressure pump and then
taken to the S.S. Product water tank. The permeate water from the R.O. will be blended
with filtered water to obtain the desired TDS and pH.

3. POST – TREATMENT:

The RO water passes through Micron Filter (1, 0.5 & 0.2) and through UV Sterilizer.
Then water is stored in S.S. Final water tank in which Ozonation is carried out and then
the water is pumped to filling points using an SS pump. The filling room is Air
Conditioned and air curtains are provided at entry and exit of cans. S.S. pipeline is used
from outlet of Carbon filter Outlet to filling points.

Process Flow Chart : Please See Enclosure II A

b) Intermediate manufacturing steps where control

Is exercised with records maintained : Please See Enclosure II B

c) Method(s) of disposal of sub-standard products

(Intermediate or finished) : Disposed in waste water line and
used
for gardening.

d) Units of production : 1000 LPH

e) Production per day or per shift : 8000 Liters

f) Enclose hand drawn layout plan of the factory : Please See Enclosure III
4. PACKING AND MARKING

a) Nature of packing : Transparent PET Jar.

b) Quantity per package : 20 liters.

c) Marking on article : Will be done after License is obtained

d) Method of marking
(Printing, stenciling, embossing etc) : PVC labels (Proposed)

e) Form of label(s), if any (enclose one set) : Will be done after License is obtained

f) Batch or code numbering for identification: Will be done after License is obtained.

g) In what manner marking differs from the

provisions in the Indian standard
specification : The Marking is done as per IS 14543: 2004

5. LABORATORY AND INSPECTION

a) Equipment, chemicals and other facilities

for complete specification testing : please see Enclosure IV
 5. LABORATORY AND INSPECTION

a) Equipment, chemicals and other facilities for complete specification testing

TEST EQUIPMENT DECLARATION

Sl. Test Equipment / Least Count & Valid Tests used in Remark
No. Chemicals & Glasswares Make & Serial nos Range (Where calibration with clause (indicate
(where applicable) Applicable) (Where Reference number of
Required) Eqpt.)
Yes/No
Least Range
Count E.coli
1. Autoclave Aravind Scientific 0.05/1 0-2.1kg/cm2 (IS: 15185) 1
/0 – 30 Psi
Hot air oven Digital Aravind Scientific 1ºC Upto 300ºC 1
Incubator Digital - 1 Aravind Scientific 0.1ºC upto 110ºC 1
Refrigerator Whirlpool(165 ltr) 1
Analytical Balance K- Roy 0.1Mg 0.1Mg-200g Calibrated 1
PH Meter SANSEL 0.01 0-14 1
Colony counter SANSEL 1No 0-9999 1
Laminar Air Flow Euro tech UV lamp 1
Vacuum Pump with 1
LPG Gas 360wave
Bunsen burner Length +/-
Petri dishes 20mm
Pipettes
Petri dishes container
Pipettes container
S.S filter assembly
Membrane filter 0.45μm
Dilution Bottles
Media making utensils
Inoculation loop
Lactose TTC Agar
Sodium Heptadecyl sulfate
solution
Triphenyltetrazolium
chloride (TTC)
Tryptophan Broth
Tryptone Soya Agar
Indole Reagent (Kovac’s
Reagent)
Oxidase Reagent
2. Autoclave Aravind Scientific 0.05/1 0-2.1kg/cm2 1Nos
/0 – 30 Psi Coliform
Hot air Digital Aravind Scientific 1ºC Upto 300ºC (IS: 15185) 1
Incubator Digital - 1 Aravind Scientific 0.1ºC upto 110ºC 1
Refrigerator Whirlpool(165 ltr) 1
Analytical Balance K- Roy 0.1Mg 0.1Mg-200g 1
PH Meter SANSEL 0.01 0-14 1
Colony counter SANSEL 1No 0-9999 Calibrated 1
Laminar Air Flow Euro tech UV lamp 1
Vacuum Pump with 1
LPG Gas 360wave
Bunsen burner Length +/-
Petri dishes 20mm
Pipettes
Petri dishes container
Pipettes container
S.S filter assembly
Membrane filter 0.45μm
Dilution Bottles
Media making utensils
Inoculation loop
Lactose TTC Agar
Sodium Heptadecyl sulfate
solution
Triphenyltetrazolium
chloride (TTC)
Tryptophan Broth
Tryptone Soya Agar
Indole Reagent (Kovac’s
Reagent)
Oxidase Reagent
3. Autoclave Aravind Scientific 0.05/1 0-2.1kg/cm2 Sulphite 1
/0 – 30 Psi Reducing
Hot air Over – Digital Aravind Scientific 1ºC Upto 300ºC Anaerobes 1
Incubator Digital – 2 Aravind Scientific 0. 1ºC upto 110ºC (Annex – c 1
Refrigerator Whirlpool(165 ltr) IS:13428) 1
Analytical Balance K- Roy 0.1Mg 0.1Mg-200g 1
PH Meter SANSEL 0.01 0-14 1
Water Bath Aravind Scientific 5ºC upto 110ºC 1
Thermometer for water 1ºC 0ºC- 110ºC 1
bath Euro tech UV lamp
Laminar Air Flow with
LPG Gas 360wave
Bunsen burner Length +/-
Pipette container 20mm
Pipettes
Screw-cap bottles
Volumetric pipettes
Test Tubes
Dilution Bottles
Media making Utensils
Iron wire
Differential reinforced
clostridial Medium
Sodium sulphite
Iron Citrate
4. Autoclave Aravind Scientific 0.05/1 0-2.1kg/cm2 Pseudomonas 1
/0 – 30 Psi Aeruginosa
Hot air Oven Digital Aravind Scientific 1ºC Upto 300ºC (Annex – D 1
Incubator Digital – 2 Aravind Scientific 0.1ºC upto 110ºC IS 13428) 1
Refrigerator Whirlpool(165 ltr) 1
PH Meter SANSEL 0.01 0-14 1
Analytical Balance K- Roy 0.1Mg 0.1Mg-200g 1
Laminar Air Flow Euro tech UV lamp 1
LPG Gas with
 Bunsen burner 360wave
Dark chamber with UV Length +/-
lamp 20mm
Vacuum Pump
S.S filter assembly
Membrane filter 0.2μm
Pipette Container
Pretridish Container
Pipettes
Petridishes
Inoculation loop
Media making utensils
Asperagine Proline Broth
Ethanol
Milk Agar with Cetrimide
5. Autoclave Aravind Scientific 0.05/1 0-4.2kg/cm2 Aerobic 1
/0 – 30 Psi Microbial Count
Hot air Oven Digital Aravind Scientific 1ºC Upto 300ºC IS 5402 1
Incubator Digital – 1 Aravind Scientific 0.1ºC upto 110ºC 1
Incubator BOD – 1 Aravind Scientific 0.1ºC 5ºC to 50ºC 1
Refrigerator Whirlpool(165 ltr) 1
Analytical Balance K - Roy 0.1 Mg 0.1Mg-200g 1
Water bath Aravind Scientific 5ºC upto 110ºC 1
Thermometer for water 1ºC 0ºC - 110ºC 1
bath SANSEL 0.01 0-14 1
PH Meter Euro tech UV lamp
Laminar Air Flow with
LPG Gas 360wave
Bunsen Burner Length +/-
Pipette Container 20mm
Pretridish Container
Pipettes
Petridishes
Media making utensils
Plate count Agar
Water Agar
6. Autoclave Aravind Scientific 0.05/1 0-4.2kg/cm2 Yeast and Mould 1
/0 – 30 Psi IS 5403
Hot air oven – Digital Aravind Scientific 1ºC Upto 300ºC 1
Water bath Aravind Scientific 5ºC upto 110ºC 1
Thermometer for water 1ºC 0ºC - 110ºC 1
bath Vision 10x45x100x 1
Microscope Aravind Scientific 0.1ºC 5ºC to 50ºC 1
Incubator – BOD – 2 Whirlpool(165 ltr) 1
Refrigerator K - Roy 0.1Mg 0.1Mg-200g 1
Analytical Balance SANSEL 0.01 0-14 1
PH Meter SANSEL 1No 0-9999Nos 1
Colony Counter Euro tech UV lamp 1
Laminar Air Flow with
LPG Gas 360wave
Bunsen Burner Length +/-
S.S filter assembly 20mm
Membrane filter 0.45μm
Pipette Container
Petridish Container
Petridishes
Pipettes
Dilution bottles
Media Making utensils
Chloramphenicol Yeast
Extract agar
7. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Calibrated Colour 1
Spectrophotometer DEEPVISION 1nm 340-960nm (Platinum 1
Filter Assembly Cobalt Method)
Vacuum Pump Crompton 1
 Nessler Cylinder
Membrane Filter – 0.45 u
Potassium Choloroplatinate
Cobaltous Chloride
Conc. Hydrochloric Acid
Centrifuge Table Model 1
8. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Odour 1
Water bath Aravind Scientific 5ºC upto 110ºC 1
Thermometer for water 1ºC 0ºC - 110ºC
bath
Wide-mouth glass
Stopper Bottles
Hydrochloric Acid
Activated Carbon
9. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Taste 1
Water Bath Aravind Scientific 5ºC upto 110ºC 1
Thermometer for water 1ºC 0ºC - 110ºC
bath Whirlpool(165 ltr) 1
Refrigerator
Sodium Chloride
10. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Calibrated Turbidity 1
Turbidity meter DEEPVISION 0.1 0 to 200 NTU Nephlometer 1
Filter Assembly NTU method 1
Vacum Pump Crompton 1
Refrigerator Whirlpool(165 ltr) 1
Membrane Filter -0.45
Hexamethylene Teramine
Hydrazine Sulphate
11. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Calibrated Total Dissolved 1
Vaccum Pump Crompton Solids 1
Hot Air Oven Digital Aravind Scientific 1ºC upto 300ºC 1
Water bath Aravind Scientific 5ºC upto 110ºC 1
Refrigerator Whirlpool(165 ltr) 1
Thermometer
Filter Assembly
Desiccators
Evaporating dish
Membrane Filter – 0.45
12. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g pH 1
PH Meter SANSEL 0.01 0-14 1
Magnetic Stirrer vision 1
Thermometer 0.5ºC (-10)- 50ºC
pH Buffer – 4,7,9.2
13. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Barium 1
Hotplate Aravind Scientific 1ºC Upto 100ºC 1
Hot plate with Stirrer vision 1ºC Upto 80ºC 1
Ammonium di chromate
Ammonium acetate
Ammonium hydroxide
Potassium iodide
Sodium thio sulphate
Hydrochloric acid
Ammonium chloride
Starch Indicator
Whatman - 40 filter paper
14. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Copper 1
Spectrophotometer DEEPVISION 1nm 340-960nm (Neocuproine 1
Hotplate Aravind Scientific 1ºC upto 100ºC method) 1
Fume hood 1
Separating Funnel
Ammonium Hydroxide
Hydroxylamine
Hydrochloride
Isopropyl Alcohol
Neocuproine
 Hydrochloride acid
Nitric Acid
Sulphuric Acid
tri Sodium Citrate
Copper metal Power
Hydrogen Peroxide
Chloroform
15. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Iron 1
Spectrophotometer DEEPVISION 1nm 340-960nm (1,10 1
Hot Plate Aravind Scientific 1ºC upto 100ºC Pehnathroline 1
Hydrochloric Acid Method)
Hydroxylamine
Hydrochloride
Ammonium Acetate
Sodium Acetate
1,10 Pehnathroline
Sulphuric Acid
Ferrous Ammonium
sulphate
Di Iso propyl Ether
Potassium permanganate
16 Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Manganese 1
Hot Plate Aravind Scientific 1ºC Upto 100ºC 1
Distillation Apparatus
Kibbs Apparatus
Nessler Cylinder
Fume Hood
Sulphuric Acid
potassium periodiate
Sulphur di oxide
Hydrogen peroxide,
Nitric acid
Potassium permanganate,
ortho Phosphoric acid
17. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Nitrate 1
Spectrophotometer DEEPVISION 1nm 340-960nm Devarda’s alloy 1
Kjeldhal flask apparatus reduction
Ph Meter SANSEL 0.01 0-14 method 1
Heating Mantle Aravind Scientific 1ºC 100ºC 1
Devardas alloy
Boric Acid
Sulphruric Acid
Sodium Hydroxide
Sodium Tetraborate
Methylene Blue
Ethanol/ isopropyl Alcohol
Methyl red indicator
Mercuric Iodide
Potassium Iodide
Ammonium Chloride
18. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Nitrite 1
Spectrophotometer DEEPVISION 1nm 340-960nm 1
Heating Mantle Aravind Scientific 1ºC 100ºC 1
Distillation Apparatus
Sulphanilamide
Potassium permanganate
Calcium hydroxide
Hydrochloric acid,
Chloroform,
NED di hydrochloride
Sodium oxalate
Ferrous ammonium
sulphate
Sodium nitrite
Nesslertube 50 ml
 Sulphuric acid
19. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Zinc 1
Spectrophotometer DEEPVISION 1nm 340-960nm (Zincon method) 1
Fume hood
Pipette Bulb
Sodium Hydroxide
Potassium Cyanide
Cyclohexanone
Zincon
Methanol
Potassium Chloride
Boric Acid
Hydrochloric Acid
Zinc sulphate
Sodium Ascorbate
20. Analytical Balance K- Roy 0.1Mg 0.1Mg -200g Aluminium 1
Spectrophotometer DEEPVISION (Eriochrome 1
pH Meter SANSEL 1nm 340-960nm Cyanine R Dye 1
Sulphuric Acid 0.01 0-14 Method)
Ascorbic Acid
Sodium Acetate
Acetic Acid
Sodium Hydroxide
Eriochrome Cyanine R Dye
Aluminimum Potassium
Sulphate
Methyl Orange
Di-Sodium EDTA
dehydrate
21. Analytical Balance K- Roy 0.1Mg 0.1Mg -200g Chloride 1
Potassium Chromate
Silver Nitrate
Sodium Chloride
Phenophthalein Indicator
Burette
Conical flask
Sulphuric acid
Sodium Hydroxide
Hydrogen peroxide
22. Analytical Balance K-roy 0.1Mg 0.1Mg -200g Sulphate 1
Spectrophotometer DEEPVISION 1nm 340-960nm (Turbidity 1
Refrigerator Whirlpool(165 ltr) Method) 1
Hot Plate Aravind Scientific 1ºC upto 100ºC 1
Volumetric Flask
Barium Chloride
Glycerol
Hydrochloric Acid
Isopropyl Alcohol
Sodium Chloride
Sodium Sulphate(anhydrous)
Membrane filter 0.45
23. Ph Meter SANSEL 0.01 0-14 Alkalinity 1
Analytical Balance K-Roy 0.1Mg, 0.1Mg -200g 1
Magnetic Stirrer vision 1
Sulphuric Acid
Sodium Carbonate
Phenolphthalein Indicator
Methyl red
Ethanol
Bromocresol Indicator
Burette
Conical Flask
24. Analytical Balance K-Roy 0.1Mg, 0.1Mg -200g Calcium 1
Hot Plate Aravind Scientific 1ºC Upto 100ºC (EDTA 1
Hot air oven digital Aravind Scientific 1ºC upto 300ºC Method) 1
 pH meter SANSEL 0.01 0-14 1
Patton & Reeder’s Reagent
Sodium Chloride
Erichrome Black T
Hydroxylamine
Hydrochloride
Methanol
Calcium Carbonate
Zinc Metal
Hydrochloric acid
Nitric Acid
Sodium Hydroxide
Disodium EDTA dihydrate.
Potassium Sulphate
Hydrochloric acid
25. Analytical Balance K-Roy 0.1Mg, 0.1Mg -200g Magnesium 1
Hot plate Aravind Scientific 1ºC Upto 100ºC (Volumetric 1
Hot air oven digital Aravind Scientific 1ºC upto 300ºC method) 1
pH meter SANSEL 0.01 0-14 1
Sodium Chloride
Erichrome black T
Hydroxylamine Hydrochloride
Methanol
Ammonium Chloride
Ammonium hydroxide
Sodium Hydroxide
Triethanol amine
Disodium EDTA didyhrate
Potassium Cyanide
Potassium Sulphate
Patton & Reeder’s Reagent
Zinc Metal
Hydrochloric acid
1M pH meter SANSEL 0.01 0-14 Residual Free 1
ine Analytical Balance K-Roy 0.1Mg, 0.1Mg - Chlorine 1
ral Potassium Iodide 200g
Oil Sodium thiosulphate
0.1 Glacial Acetic Acid
Mg Potassium dichromate
- Starch Indicator
200 Salicylic acid
g0. Conical flask,
1M Burette
g,K
-
Ro
y11
28
An
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.

1
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)

upt
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110
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0-
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o
100
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5ºC
1ºC
1ºC

Ar
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Ar
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29. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Anionic Surface 1
An Spectro photometer DEEPVISION 1nm 340-960nm active agents 1
alyt PH meter SANSEL 0.01 0-14 1
ical Water bath Aravind Scientific 5ºC upto 110ºC 1
Bal Thermometer for water 1ºC 0 - 110ºC 1
anc bath Aravind Scientific 1ºC Upto 100ºC 1
e Heating mantle
Spe Distillation Apparatus
ctr Gas stripping apparatus 1
oph Fume hood
oto Separating Funnel
met Refluxing Apparatus
er Dodecyl benzene
152 sulphonic sodium salt
7 sodium chloride
Wa Ethyl acetate
ter Chloroform
Bat Ethanol
h Air Unit
Th Methanol
er Sulphuric acid
mo Methylene blue
met Sodium hydrogen
er Carbonate
for Sodium hydroxide
wat Sodium carbonate
erb anhydrous
ath Phenolphthalein indicator
pH Evaporating dish
Me
ter
He
ati
ng
ma
ntle
Va
ccu
m
Pu
mp
Filt
er
ass
em
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Dis
till
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.
30. Analytical Balance K-Roy 0.1Mg 0.1Mg -200g Sulphide 1
Spectrophotometer DEEPVISION 1nm 340-960nm (Methylene 1
NN dimethyl P.Phenylene Blue Method)
Diamine oxalate
Sulphuric acid
Ferric chloride
Methyl blue
Diammonium hydrogen
ortho phosphate
Sodium Sulphite
Droppers
Matches Test tube
31. Spectrophotometer DEEPVISION 1nm 340-960nm Borate 1
Analytical Balance K-Roy 0.1Mg, 0.1Mg -200g 1
Refrigerator Whirlpool(165 ltr) 1
Water Bath Aravind Scientific 5ºC upto 110ºC 1
Thermometer for water 1ºC 0- 110ºC 1
bath Aravind Scientific 1ºC upto 100ºC 1
Hot plate Aravind Scientific 0.1ºC 5ºC to 50ºC
B.O.D Incubator
AzomethineHsodium salt
Ammonium Acetate
Sulphuric Acid
Phosphoric Acid
Boric Acid
Citric Acid
Calcium Hydroxide
L Ascorbic acid
Di- Sodiun EDTA
Dihydrate
Polyethylene ware
32. Analytical Balance K-Roy 0.1Mg, 0.1Mg -200g Antimony 1
Spectrophotometer DEEPVISION 1nm 340-960nm 1
Hotplate Aravind Scientific 1ºC upto 100ºC 1
Refrigerator Whirlpool(165 ltr) 1
Fumehood
Separating funnel
Erlenmeyer flask
Antimony metal Powder
Hydrochloric Acid
Phosphoric acid
Sulphuric acid
Perchloric acid
Benzene
Rhoda mine – B
All the Glassware and Chemical necessary for the testing as per IS 14543: 2004

I hereby declare that the test equipments of which details are given above are owned by
me and are actually installed in the premises.

I also declare that in case of grant of license, I will send the intimation to BIS whenever
any equipment is taken out of the premises of the firm due to any reason.

b) Details of quality control staff: Please refer Enclosure V

Sl.No Name of the person Designation Qualification Experience

1. O.MALLESWARAMMA Microbiologist BSc 6 months
2. P.CHINNARAMASUBBAIH Chemist BSc 6 months

c) Records maintained in laboratory for routine tests: Will be maintained after obtaining
the BIS license

Sl.No Requirement/ Specific Observed Value

Characteristic Value

d) Stage of processing where laboratory

reports are made available : Will be maintained after obtaining
the BIS license

e) Sampling and testing of end products : Will be maintained after grand of license
6. OTHER INFORMATION

a) List of dealers and main Byers shall be provided after grant of license and any change
shall be intimated to BIS

b) Storage facilities : 1200 Sq.Ft of Storage capacity is available. It is good and

hygienic for final product storage

c) Hygienic conditions : Please refer Enclosure VI A, VI B, VI C