ESSENTIAL How It Works Guide - Components & Software V0.3
ESSENTIAL How It Works Guide - Components & Software V0.3
Essential systems
Tools needed Interactive flow schematics in Flash® are available on the WW Service
Support database. They can be used to complete this document and to
understand the different system process and software modes (see Operating
Status).
Trademarks Elix, AFS, Progard, Opticap, BioPak, Q-Gard, Millitrack and Millipak are
registered trademarks of Merck KGaA.
RiOs is trademark of Merck KGaA.
All other trademarks are trademarks of their respective manufacturers.
Table of Contents
Terminology .......................................................................................................................... 5
Reminder ........................................................................................................................ 5
Flow Schematic ..................................................................................................................... 6
Interactive files ............................................................................................................... 6
Monitoring Devices ............................................................................................................... 8
Conductivity and Resistivity Cells .................................................................................. 8
Pressure Sensor ............................................................................................................... 9
Hydraulic Devices ............................................................................................................... 10
Solenoid Valves ............................................................................................................ 10
RO Booster Pump ......................................................................................................... 11
Distribution pump ......................................................................................................... 13
Check Valves ................................................................................................................ 15
Capillary Device ........................................................................................................... 16
Flow Controller ............................................................................................................. 18
Pressure Regulator ........................................................................................................ 19
Electronic Devices ............................................................................................................... 22
Printed Circuit Board .................................................................................................... 22
RFID – Radio Frequency Identification Device ............................................................. 24
Software Package and Web Interface ................................................................................ 26
Software Package.......................................................................................................... 26
Web Interface – Installation Step .................................................................................. 31
Web Interface - Millitrack® Software ........................................................................... 33
Man Machine Interface or MMI ........................................................................................ 36
Display and keypad ....................................................................................................... 36
First installation with MMI - remarks ............................................................................ 43
Table of alarms and alerts ............................................................................................. 44
Terminology
Reminder
Table of terms The table below lists all terms and their equivalent used in this document.
Units The table below lists all units used in this document.
Units Meaning
°C degree Celsius
A Ampere
b bar
h hour
L litre
L/min Litre per minute
L/h Litre per hour
mA Milli ampere
MΩ.cm Mega ohm centimetre
min minute
psi Pound per square inch
V Volt
µS/cm Micro siemens per centimeter
Introduction An Essential system is made of different parts and hydraulic components put
together in such a way that the:
• Elix section purifies tap water to make Elix water which is then stored in a
tank, and
• AFS or distribution Section purifies the stored water (upon demand) to
make Product water to analyzer.
List of flow For each type of system, an animated flow schematic in Flash® format is
schematics available for better understanding the different system process.
Step Action
1 Save the ZIP file on your hard disk drive.
2 Unzip the file .
3 Choose the system type.
Open the folder and double click on ACME.html:
Note: a web browser is needed to run the flow schematic (IE 8).
Symbols The table describes the meaning of each icon used in the flow schematic.
description
Item Icon Description
2 way electro valve Electronic device used to block or to let
go the water flow.
3 way electro valve Electronic device used to block or to let
go the water flow.
Capillary device Thin tube that regulates the amount of
water to reject.
Check valve Mechanical device that controls the
direction of the water flow.
Flow controller Hydraulic device that limits the amount
of water rejected by the RO.
Pressure regulator Hydraulic device that is used to
maintain and control water pressure.
Thermistor The thermistor or temperature sensor is measuring the water temperature. The
resistivity/conductivity measurements can be compensated at 25°C for
purified water quality measurement (recommendation by United States
Pharmacopoeia as a reference temperature).
Looking inside An Elix Resistivity Cell, when opened up, looks like the photo below.
Purpose There are one or two pressure sensors depending on the type of system. The
Pressure Sensor is used to measure the pressure of the
• RO loop, and
• Distribution loop (AFS type).
Principle Water enters in the pressure sensor housing. Its pressure is pushing on a
membrane that measures the voltage which is converted then into a pressure
value in bar, psi or kpa (depending on the unit chosen in the software).
Spare part The same part number is used for both pressure sensors. Only some parts are
used for one or the other.
AND
Distribution • The pressure sensor measures the distribution pressure. And then it
pressure sensor compares these measured values to start and stop set point values in order to
send water to analyzer when required.
• These set point values can be adjusted in Millitrack software depending on
the feed water pressure requirements of the analyzer. It is very important
to adjust the back pressure regulator accordingly.
AFS HF AFS D
Start distribution pressure: 0.7 bar Start distribution pressure: 0.6 bar
Stop distribution pressure: 1.3 bar Stop distribution pressure: 1.0 bar
Back pressure regulator: 2.0 bar ± 0.1 (default) No back pressure regulator
BPR adjustment range: 0.9 - 3.0 bar ± 0.1 No back pressure regulator
Start distribution pressure min: 0.3 bar Start distribution pressure min: 0.0 bar
Stop distribution pressure max: 2.0 bar Stop distribution pressure max: 2.0 bar
Purpose • Solenoid Valves are used to control the water flow in different sections of
the system.
• There can be a maximum of 4 solenoid valves depending on the type of
system.
Valves Purpose
System inlet Controls the flow of the feed water entering the
system
RO Flush • Increases the RO Reject flow rate to drain in
Flush Mode
• Allows the RO pump pressure to build up in Tank
Filling Mode
RO Permeate divert Allows the flow of the
• permeate water to be sent to drain via the RO
reject tube
• permeate water to be sent to EDI module
Recirculation loop Controls the flow of the distribution water to
(AFS® D only) recirculate in the loop
Introduction The RO booster pump increases the flow rate of the water exiting the
Internal Pressure Regulator. Since the RO Reject Solenoid Valve is closed
when the RO Pump is powered, the water flow encounters a resistance. This
builds up the water pressure after the pump. This increases the feed pressure
to the RO Membrane and causes a higher flow across it.
Principle The RO pump voltage is regulated with the feed water temperature in order to
have a constant flow rate to the EDI module.
RO voltage and When voltage is adjusted manually, there is a relationship between the
speed Motor% (X axis) and the applied voltage (Y axis). This relationship is shown
in the graphic below.
RO Pump Output
45
40
35
Output Voltage (V)
30
25
20
15
10
5
0
0 20 40 60 80 100
Output Reference (%)
As an example, if the RO Pump Speed was set to 90%, then the applied
voltage to the RO Pump would be 37 VDC.
Looking inside The illustration below describes the principle of a diaphragm pump.
Principle • The distribution pump is used to send the water to an external device or an
analyzer upon request. This request is detected on pressure variations by the
pressure sensor that starts or stops the distribution pump.
• When distribution is stopped, the pump is still operating through a
recirculation process: this maintains the water quality in the distribution
loop and avoids restarting of the pump, in order to increase its lifetime.
• In idle mode, the distribution pump goes into a 5 min recirculation every
hour to refresh the water in the loop.
• For AFS degasser, the distribution pump has a vacuum side on the pump
head. This creates the vacuum for the degasser device to remove air from
the product water.
Characteristics There are two types of distribution pump and their characteristics are:
AFS HF AFS D
24 Vdc diaphragm pump 24 Vdc brushless pump
I nominal = 1.1A @ 30psi I max = 0.75A
Up to 2.2 L/min Up to 0.6 L/min
8 mm fitting connection ¼” fitting connection
Recirculation There are two types of recirculation: post-recirculation and an hourly time
based recirculation.
Type Description
Post recirculation – 10 • Initiated when analyzer stops requesting
min water.
• Duration adjustable between 0 and 30 min.
Recirculation – 5 min/hr • Initiated 5 min every hour when system is
not in distribution or post-recirculation.
• Frequency adjustable between 0 and 60 min.
Start and stop • The distribution pump is controlled by the distribution pressure sensor and
set points the back pressure regulator.
• The distribution pressure sensor has two set point values that start and stop
the distribution pump upon the analyzer request.
Item Description
Distribution pressure Used for starting and stopping the distribution
sensor pump.
(Adjustable. Default Start • The start (default 0.7 bar) is based on a set
at 0.7 bar and Stop at 1.3 point value and is detected by a drop of
bar) pressure in the distribution loop.
• The stop (default 1.3 bar) is based on a set
point and is detected by an increase of
pressure in the distributing loop.
Back pressure regulator • Used to maintaining and adjusting the
(Adjustable. Default at 2 pressure in the distribution loop. This device
bar) is adjusted 0.7 bar higher than the stop set
point value.
• When analyzer requests water, the
distribution loop delivers water at 2 bar of
pressure.
Part Function
Vacuum pump Membrane pump head creates vacuum when the pump
is operating in distribution or recirculation.
Vacuum The regulator is used to mix some outside air with the
regulator vacuum. This decreases the vacuum to a desired level.
Vacuum gauge The gauge is used to display the applied vacuum level.
Degasser The degasser contains a very large amount of micro
porous hollow fibres. These fibres allow water to flow
through the inside of each fibre. The vacuum is applied
on the outside of the fibre. The dissolved gases inside
the fibres are pulled through tiny holes.
Purpose • A Check Valve prevents water from entering the system in the wrong
location and bypassing various components.
• There are several check valves used in the system range:
Purpose • The Capillary Device looks like a thin tubing and regulates the amount of
RO Reject water sent to the drain when the RO Reject Solenoid Valve is
closed.
• Ions, particles, organic molecules and other impurities rejected by the RO
Cartridge need to be sent to a drain. Otherwise, these impur ities would
accumulate on the feed water surface of the RO Cartridge.
• The water flowing through the Capillary Device contains all the impurities
sent to drain.
Types There are 5 types of Capillary Devices. These are summarized below.
Proper There is a way to determine the proper Capillary Device. This determination
Capillary is based upon the Feed water Hardness, Alkalinity and Pressure.
RO recovery The RO Recovery for each system is shown in the table below. The RO
Recovery can change if the RO Reject flow to the drain changes. Thus, the
flow through the Capillary Device directly changes the RO Recovery.
Example: If an Elix Essential 10 is fed with 5 bar feed water, then the RO
Reject flow to drain would be 31 L/h. The RO Permeate flow would be 16
L/h. Thus the RO System recovery is 16 / (16+31) = 35%.
The same system fed with 1.5 bar feed water would need a 1 mm Capillary
device to keep a similar RO Recovery.
Purpose The Flow Controller limits the amount of RO Reject flow to 60L/h from the
RO Cartridge.
Principle A pressure is applied to the flow controller. The flow controller has a
membrane with a small hole in its middle that becomes larger as the pressure
is higher. That hole controls the amount of water passing through it.
Introduction The Internal Pressure Regulator (‘IPR’) is used to control the water pressure:
• after the Progard Pack,
• before the RO Pump, and
• before the Capillary Device.
Note: because the IPR sets the pressure drop across the Capillary Device, the
IPR setting (output pressure) changes the RO Reject flow to drain.
Dynamic vs. When an IPR is adjusted to a particular outlet pressure, then this pressure is
static pressure only maintained when water is flowing through the IPR.
Back Pressure • The BPR is used to maintain the pressure in the distribution loop and to
Regulator adjust the distribution pressure according to the analyzer feed pressure
requirements.
• It is set at 2 bar ± 0.1 by default but it can be adjusted between 0.9 and 3.0
bar ± 0.1 using Millitrack software.
• It is installed on the return loop between the tank and the system connection
n° 8. It has two ports connection.
Introduction The printed circuit board is called PCB and can be a main PCB or interface
PCB. There are several printed circuit boards like the main PC board, the
TAG reader PC board, etc.
Real Time • The RTC is a high precision clock for an electronic system, used for dating
Clock and initiating events based on hour.
• RTC super capacity autonomy is 7 days when capacitor is fully charged and
system is not powered. After 7 days, the capacitor is discharged and the date
and time lost. It may take several hours for capacitor to be fully charged
again while system is powered.
• Once the capacitor is discharged and the system powered on, it prompts the
user to enter the date and time.
System main The schematic below describes the different process that each chip is taking
PCB care of.
Item Function
Coldfire or It’s the “brain” of the system. Its “memory” SD Ram is
main processor used for data storage. Coldfire is communicating with
Ethernet, RFID and the PIC.
Flash memory • This is the “memory” of the system. The software
package, config.ini, history log file, etc… are stored
on this chip. All the files that can be viewed when
connected via FTP are there.
• The tools delivered in the software package are used to
upgrade or reset the flash memory.
PIC or micro • This µC is controlling the actuators, LCD and keypad,
controller and the sensors circuit.
• It is communicating with the coldfire by CAN bus and
provides the real time clock for the sequence events
for coldfire process tasks.
RTC The super capacitor is providing energy to the RTC
which gives real time to PIC and coldfire process events.
Purpose • RFID is a method for memorizing and collecting data remotely using radio
frequency technology. RFID uses markers called RFID tag or RFID
transponder.
• RFID tag can be a small sticker which can be applied on objects or
products. RFID tag is made of an antenna combined with an electronic chip
that allows receiving and answering to requests from a radio emitter-
receiver (RFID tag PC board in that case).
• These electronic chips contain an identity and eventually further data. The
RFID are 2 tag reader PC boards and tag label sticker on consumable packs.
Function This identification technology is used to identify the type of consumables, its
presence and to optimize their usage. All these data are stored in the
electronic chip for traceability.
RFID tag • These active devices emit radiofrequencies that activate the markers by
reader supplying the necessary energy that they need in a short distance.
• The length of the frequency is variable depending on the type of
application.
• A high frequency has the advantage to exchange data (between reader and
label) at higher rates than lower frequency.
RFID tag label These passive devices don’t require any source of energy except the one
supplied by the reader during a request.
The marker is very thin, small size and negligible weight. The marker is made
of:
• an antenna,
• a silicon chip, and
• a substrate and/or an encapsulation.
Consumables On the tag label, the following consumable data are stored:
data on tag • type of pack,
label • Catalogue, serial and lot numbers
• Installation date,
• Manufacturing date, and
• Volume processed.
Note: when a new pack is installed, the system recognizes the type of pack
(i.e. if a pre-treatment or a polisher) but the installation date is written once
the rinse is initiated by pressing on the user keypad.
Tag diagnostic • The tag diagnostic tool can be used to verify that the tag reader PC board is
tool functioning correctly.
• If there is a “Pack out” while the pack is in place, remove the pack and
place the tag tool in front of the tag reader.
• Connect to Millitrack software, the tag tool should be recognized in the
following menu:
Procedure and All information related to upload and download is found in the Procedure
documents Upload & Download Software/Firmware Guide on the WW Service Support
database.
Software All software information in this document has been verified using an
/firmware Essential System having Software Package 29.
versions This package consists of the following versions of firmware and software.
Note: “NA” not applicable means that the version cannot be upgraded at all.
The replacement of the PC board is required to have the latest software
version.
Item Function
Configurations “blank” config.ini used
when initial config.ini is
corrupted or lost.
System* Folder containing
application, execution
and Millitrack resources
files.
ACME_update.exe Application that is used
to update actual
software package –
content of the “System”
folder precisely.
System_Reset.bat Command file for
erasing system memory
and uploading a
software package.
Upload_date.log Upload event history log
file.
Software files When receiving a system from manufacturing, it has the following items in its
stored in memory (this is viewed using FTP – File Transfer Protocol):
system
Software • Two tools are provided with the software package and used for this
upgrade tools upgrade:
Tool Purpose
ACME_update.exe • This program is used to upgrade the software
package. It replaces the following files in the
[Launch this Flash memory:
application in
Standby mode]
Note: the uploading tools are provided in each version of software package.
During an upload, use the version of the tools that are coming with the
version of software package. The modified versions of the tools are not
notified.
Manual • When the system is powered on, the boot loader is running during 10 sec
software before the application “Acme.exe” is loaded. During these 10 sec, the
upgrade connection to the system with a Telnet* session is possible in order to
establish a safe connection and upgrade the software package.
Config.ini • If for some reason the “config.ini” file is corrupted or has not been saved, a
blank “config.ini” must be used for recovering the system type. Though,
putting a blank “config.ini” from the software package makes the system as
it was new. When powered, the system displays – PC –. This – PC –
connection has to be cancelled by pressing for 3 seconds to go to Standby
mode.
• IMPORTANT! All configuration and calibration factors have to be entered
once again using Millitrack software.
First • When typing the IP address of the system in web browser on a brand new
connection system, Installation Step web page is displayed (when LCD is displaying –
PC -). Installation Step is used for installing the system using a laptop.
• If the – PC – connection is cancelled (for installing the system using the
MMI), it is not possible to display Installation Step web page again.
• Installation Step web page is only displayed once. Canceling or clicking on
makes Installation Step never occur again.
Note: the only way to display Installation Step again, is to upload a blank
“config.ini” from the software package.
Attention! A blank config.ini has no serial number, no calibration factors and
no configuration settings.
Definition • When installing the system for the first time using laptop, INSTALLATION
STEP web page is displayed for helping to simplify installation process by a
mouse click.
• Up to 5 different steps – depending on the type of system – can be started
using this web page.
Step Description
1 SET DATE Check and/or set the system date and time.
2 PROGARD FLUSH • Flush out a new pretreatment pack.
• Fill the system with feed water
3 RO RINSE Initiate 4 hours of RO rinse which can be
cancelled after 1 hour.
4 POLISHER RINSE Flush out a new polisher pack.
5 FINAL RINSE Flush out a new final filter.
• Some configurations can be done during the steps like choosing the type of
tank, changing the set points, activating options, etc.
Details on each • SET DATE: as the RTC battery has a short autonomy, when powering on
step the system for the first time, it may be necessary to set the date and time.
This is very important as the date and time is used for software events,
managing timers on consumables lifetime, history reports, etc.
• PROGARD FLUSH: when clicking on START button, it writes the
Installation Date on the tag label. This flush is lasting 13 minutes when
replacing the pack in a normal maintenance procedure. For the installation,
the user has to cancel after 5 min, the time for the system to be filled with
feed water (that avoids LOW PRESSURE when starting RO rinse).
• RO RINSE: a timer of 240 min decrements and a red button STOP is
displayed when reaching 179 min. Stop RO rinse when STOP button is
displayed.
• POLISHER RINSE: a timer of 4 min is started when the rinse is initiated.
This is done without the final filter.
• FINAL RINSE: a timer of 4 min is started when the rinse is initiated. This
is done for rinsing and air purging the final filter.
Quit • When all the steps are done, the web page displays a button QUIT
Installation INSTALLATION PAGE. The closing of the page has to be confirmed: this
Step resets all the timers related to UV lamp, cleaning and sanitization, reminder
messages for service contracts, etc.
• When clicking this button, the internet browser refreshes the page and
Millitrack software is displayed.
AFS 8D “Low When installing an AFS 8D, it is possible to lower the RO permeate flow rate
Flow” to make an “AFS low flow”. This is called the “Type III Water Production”
parameter.
Analogy Millitrack® is like a small “web site” that can display information for
configuring and controlling the system, using a laptop, a computer connected
to a server or any device having an Ethernet connection.
Standard For accessing and using Millitrack® software, read the following SOP:
Operating • Millitrack® Essential Activation Procedure for Customer
Procedure • Millitrack® Essential Activation Procedure for Service
• Millitrack® Essential Activation Key for Service
Login role There are two types of Role when connecting to Millitrack® software:
Note:
• The activation key for user must be entered once for all and is linked to the
system.
• The activation key for service must be entered each time when connecting
to Millitrack on all Essential and Integral systems.
Trial period A 15 days trial is available for customer when USER role is selected (1) and
license agreement is accepted (2). Click on IDENTIFICATION (3) to access
Millitrack® software.
2
3
Note: this 15 days trial is activated each time Millitrack® Service Activation
Key for Service is entered by a Service Representative.
Save a copy or
printer
friendly? • When clicking that button on Millitrack, a new browser page is displayed
with the content in XML code. This XML code can be used to display data
(i.e. history report data) in a web page or other software that can use this
XML code.
Display and The display is made of segments and icons. Different area can display
icons different kind of information.
Part Function
1 System status or software navigation.
Icon Description
Maintenance menu or Standby mode. Cleanings or
lifetimes reset can be done here.
Configuration parameters: set points value, date and
time, economic mode and ASM configuration can
be changed here.
This icon is displayed when system is in
• Rinsing mode
• Flush A (3 min RO flush)
• Flush B (15 min Progard flush or cleaning
sequence)
• Depressurization sequence (8 sec)
• Maintenance countdown sequence (cleaning, RO
rinse, etc)
Display and
icons (continued) Part Function
2 Maintenance or warning icons.
Icon Description
RO Cl2 cleaning (84 days)
Icon Description
New pretreatment or polisher pack is
or detected. Pack flushing or rinsing is required.
Pretreatment or polisher pack replacement is
or required within 15 days.
Pretreatment or polisher pack replacement is
or required.
Pretreatment or polisher tag reader is
or disabled for 24 hours (below alarm will be
displayed after 24 hours).
Pack out or incorrect pack.
or
RO CL2 cleaning is required.
Display and
icons (continued) Part Function
6 Tank level display.
Icon Description
Tank full display. Fixed icon.
minor major
major
Low feed pressure icon is displayed Error 14 and Call Merck Millipore
with a red color background. icon are displayed with a red color
background.
Note: if two alarm messages are displayed, press on arrow keypad button to
display the error code.
Keypad action The keypad has 4 buttons. They are described below:
Keypad help Keypad help icon is displayed if an action is associated to the corresponding
indicators keypad button.
• A fixed key help icon: an action can be done by pressing the corresponding
key button. 1 to 3 key help icons can be displayed at the same time.
• A blinking key help icon: an action is required by pressing the
corresponding key button. Only one key help icon can be displayed at the
same time. This is prompted when a change in maintenance, in an alarm, in
a system parameter needs attention from user.
• No key help icon: the keypad button is disabled.
Description of The table below describes some menus of the software MMI.
some displays
Menu Description
The laptop can be or is connected to the system. This
is displayed when
• First installation of the system is done, and
• “Enable tests” button on DASHBOARD in
Millitrack software is activated.
Lab closed allows system going in Tank Filling for
30 min every day between 10:00-10:30 AM.
System sanitization is made of 3 different cycles
SAN1, SAN2 and SAN3.This process enables to
sanitize the whole system and the tank.
In this menu, IP address can be viewed depending on
the network configuration:
• System default IP address can be displayed using
point to point connection (i.e. 192.168.1.69).
• Different IP address can be displayed when entered
manually or attributed automatically by the DHCP
server.
If a different IP address has been entered using
Millitrack software (e.g. 192.168.1.72), confirm this
menu to switch back to the system default one
(192.168.1.69).
System • If the Installation Step is not used for installing the system, it is possible to
installation install the system using the Man Machine Interface.
• This – PC – connection has to be cancelled by pressing for 3 seconds to
go to manual installation.
• The table below describes the summary steps for installing the system
without Installation Step web page:
Step Description
1 Set Date • If date and time are lost, system prompts to enter
the new date and time automatically.
• Probably the super capacitor is discharged and RTC
lost data.
2 Progard Flush • System detects a new pack and prompts the user to
start the Progard Flush.
• A keypad action is necessary to start this sequence.
• This sequence has to be cancelled after 5 min or
when key help indicator is displayed. System goes
in Standby mode.
Introduction When powering ON a brand new system for installation, after 10 sec, a – PC –
message is displayed. This – PC – connection has to be cancelled for installing
the system using MMI.
Note: there is no specific “menu” for installing the system with MMI
compared to Installation Step web page.
Date and time Most of the time, the system asks to enter the date and time before initiating
any process. Make sure to check or to configure properly the date and time as
it has an impact on all timers (consumables, UV lamp, cleaning, etc).
Resetting timers Comparing to Installation Step web page, the installation using MMI does not
allow to automatically reset timers on
• UV lamp lifetime,
• final filter lifetime, and
• Cl2 Cleaning.
The alert messages related to the previous list could occur when the date and
time have been configured. In that case, they have to be reset manually by
resetting the lifetime or initiating and cancelling the cleaning.