Salt Analysis o- Bim qualitative anahyslt A x avn soll For acid aml lagie vadinl . Theory: Quali tative analysis yA concerned with. Adection & clemmnts qr ot damants in ® compound, or o mixture. Guahitodivn anolyais A an in erpmic. involves the. datcetion the vasion utin Alt is eomposea. of to and ani. Ax. morgane aolt jong — 0 cation and an anion. The anion te calle. oid radical om the cation 18 cll bosic molteal « Makerial requtved ¢ Tost tube , Test tebe holley, feat tube 4 tan, funnd, FSlter paper » coitel flor , Teogorts. Chyziced observations Colour + odaur ¢ Stats § SalusDry test Lov ociol_sadliols * ® Actm pith olilute H,$% - ee _ Expeviment Obsesrotin - i Ww Fesonce. Salt + dil. Hy$0, |D Hes seer A clues — |g oy be + Hot md odautless 908’ tre qs press smakos fimo wakey milly be pow Her it. © Raddish- room famus elves | 0,7 may Th the cold. oa Colourlesr ay with, ow | authacadng odour A Pousving | 3037 moy be sulphur present - e on ato hang. prreluced. cugeos” a be awell vinegar 1 present = | E | D fetim with cnuondrortel HaS0u Zuperivent | Obsewrin I tnferones « 4 OD Effrves comer A colawless aml Cos” way be | oaueltd ae ate ~ mals | pregent ‘ | fame water rity on poly | Herman it: | ® evlubion Af tron Lumar. Nox Moy Oe, @ Colowitoe gag with pwryart Arall wolves - To the oboe mixture , added | a rekon . | Mag. omd wormed ,A yellowish [ren Colour 943 evol¥2eh . Salt + Cme- H,5%Eapesinat [ aeretin | Snferee. @ A oddich brown solution 1s = Looned . OF waren qive By mop be radolish be yom TUM present. Reditin f Myo, accelerated. the production A tues. @ On ata heeding + produerd - anddish browne Lymngs » Reldition Nos mort be. 4 copper tang produced more preust | -paddish- wroon Furie. @) fe colourless qn evil, | males ime water milky , | 2,00" v4 Agpitin A the mouth Ata ie preset tube produced bins Came QSpecial test fer chlovicle Ch my chloride test Experiment | Observation Inference - Salt + Kit | Denp Yed vopous d Hy 9% | + ene. HS + cherry chloride (C444), | ay preset . eeea © wet tert for ocil_sadlick + ° Sine He salt water poluble . Thar gall Sofiction 1B prepared ky adding galt | | Expestment absewetin a Anverence ~ | cipitete 5 4oluble ir co," preset © sm galt sachin [> White pre dil Wel | + | bed, aolution . ; | b> white pee pied» ingoluble Pr dilute HY | ® srl salt solstin | oy hit ppt , soluble in dihdte HG] COs" present agits aaetin ® whit pet dliscolves wong soe” presot © Cusdy white ppt, inmluble he | ex present | dhlute HNO, bub sdluble fe NH QOH | | 4) Cardy yellow pot xoluble im | ar prose emeerntnded NH, solvdion | lurdy yellow pet Tolle eine x presot. | conunrodecl NH, zation | - 4) Blak ppty Prgduble, in Wviling — S” ptiont ® srl salt solution |oy white ppts soluble in dil. HNe, C927 preset * ord quotstesauttn 2 Whit ppt, soluble in avamonivm a- so, ‘exert acetate gation 3 Pr | 1 Coystellin white ppt, soluble i be err oF Be | tw polling Dates 17 present | © Black ppt, sohuble te ws | <2 prewnt PYellav ppt, soluble in bling water@O- db seevation Inferene « gm salt solution | + Feso, sotction « the maintuye, Jeosled wnoler 0p Jwater ord added (SoH cme H,$% down tHe Aide of He | 4eet tube Oat for nihil am 4alt Zobetion | am) Fesa Adhtion + aml dilute H, 5%, @ tat fe oF tT aomk galt Aol om + | aml ohierrf on + | few obaaps cones H¥Q, | + shake WL Ga) test Fer_atetote Test fer acectorte gin zalt solvtion | + a-3 dips nevrtol Fedly zolvtion @ toot Lor subphide am) galt goledin + Nao Smelt sf ammonia mn be. ammon'un ede He tot} Tube colt continuansly up Block sesiolue Or solte & Ca, Mm, aang hacking ‘ Ni, Fe, > Yellow When hot, edts ff Zn white when cold : BY Yellow whan Vet» aati Ah. Yellow when cold €) Origanel subs toa vat solve, — white ord | Moy be SY Aho, black ™ cosh 1 | saite & fas @ Flame Test : f) No fe colour - ee Bas Mae Al Expovimert galt tg thor. ina watch fot ome. moistened V4 Wit coe, HCL , Touches! “He golt with tip Aa at vod. Now, intwoduced. the plat gfouk od. into the flame . [_ooservatin | tnferomea | o> Boik~ Ted Flame. la- Balt 2D Yellowish— ven flame Ba- salt > Bluish- qreen flame | ta- salt | ay Blee Frame. Pb - alt ae | 1Ra «16 (haoup +esh) Wel test fos basic. golical § Grronp teat) — @s axoction $ 0. ; * ™ Stn te alt 18 water xduble, 20H soludin 6 pre gu, water tov taste. Olosetvedh on. | interme Expeotment 7 ! aon ® som sath soltion a pres pie | pe ~ Ho precipitate Gat obegent dilde Hol ee ~ ® Abore solution [Hanh slack pruipttsle, [ewe promt + (ret ye mrt, Curt od passed HS a” No poecipitede | a bf oo | O pow sohdin [Gitte wat | taro ond expellect digsolved Precipi tote 4 HAS “4 looilirg [Curie 3 may be AND) + (Gran 3 Way be FP Cone. HN G5 (nly ey colo salt) | | i ‘No- prastpiteti on Goh absert - ) NHgek + NH OW fe ® Above sotidin / GAH rode . | “ee | Precipitode, 1 Gsm ® preont | incon White 22?) | | 7 (Glock ~ Co? Nit) | posse H2S gos [No = ppt Gsm ovset. © Abon solution / Horde was dnt, tok aye, dissed, WNC pp tae boil ced aed ft Bo"*, “) Gay preva he alum. of the Adlon to sat almost half by eveporading . “6 Ne ppt Gey absent L_ Neyer +t Qty), ca, 6aidEEL RRB Oo Expeainunt absewedion Inference. Daum sation] tl Trade © Above sain] vdhite ppt Gav prot | Disodium Tlnges Piesphaley Cony Ye ye Salwtion Stake No ppt Gry obsert ax &f no precipita is Ooloingl in the qtorps , Pron Noy” taditels My preset - atest Far NHAe Experiment Docent. [ Lafeyente oe | Salt ( part) + Nazles (3 po) | | | % meg | purgert | Nig present Heat in dry rest ube i % Holebd ov Filter paper | | docked swith. coe. HOL at | Demge shite Funes He | i reset. | the mouth of te test tbe rele “Pyoo nrg Analysis af mp 3 ° Filtered and transfosel te precipitede +o a beaker pode 40 Wh & woltr ig adele amd thon toviled +e dissolve : the paeaipide - Divided He Addin into 4 pads ame perbovrwl phe Bllacig tests b- | Experiment Olaseriction _ _avtoma | +. Poot ove | Codtal ules cumiva | othite ppt AF Poth Pe pret water i | RQ. Parka | Yellow ppt xf Peso, | PL presnd + CH3@.00H | + KA C4 Oy 3 Port 3 Yellas ppt 4 evs, PL” present ¥KI | De fot Y | +dbk H,$0, Bo ts | | vikte ppt 4 pb soy OB praent—| a e_e_ 7. Alga A gO Filtend ard tragferel the precipitate inte a powerlain dich. Added Smal of Yelle ammonium sulphide soluctig one weetil For abot 3-4 minutes with constant Aining Filteveol ane sdvtn ord peofomel the llowig Aerts :— [ Resiclere | Ruiclus + g-to ml Core HNO, + Boll + | Nagow golubion . | Filtered Ye aloe solution. te ppt > mney be ne ) Whi colour ppE YY oe Cut | Residue Filbsoh | | Residus. + Neon 4dludin} Divided inte a parts + Worm | tst_past Divided inte 2 poy Adds UNC00H ome | Sek post KalFeen),] | | Radel Kole 0y Colour ppt > Cul preserd | | Mellow Prhane * pruest| nk gost | Bod_oat ts i faded exon NOH | | i KT solution gavdion “ler ret 7 mi “punt Bluz colour > Cr embiimned (dissotved on vuiling) Filtaate CiVyrede + cone. HEL + as dit. Wh 34 Hate Waren | Aion divided the | | ole solution in R parts | Ast post | Radel game amount | of Nitya om | mw in mixta anes . ve | | White ppk > As” preset | ak yak AddseL ornmonium me dote solution healed, Yellow ppt > As SY presAnalysis of qoorp A: Filtered ama transfer the precipitate fn a beater. pddul 2emt NaCl golution gmc 4 ral of CEH, zeluion. Boiled He advtion ool Fidtered . ° Residue Fillaote Divided te weridue in Q parts. ist port pissolved with dint ail. HNO, . Adda fus alvaps aA Hy92 ond oiled . Cooled amd asldoct pinch A podiwm bis muthate (ta Bi 03) ond prhood - Violet colar > May present a Disolvad with A Her amd divide into 2 parts. thet part + KufFeen),] Se eth Blue ppt > Fe? * present 4% and port 4+ WHyseN ReA colows > Fe presont Filboade + NHyth + bail white ppt > AL°* presentSinalys Added Ana ond Residue Dissolved Ha reside im sm) oqua vegia . Evaporated almest to dsyness a thon added Lom water ad divided into 2 parts. dst part Addecl NHyoH adusin pd del DM Teyprt at | geal ppt > Ni present nk port + 2x onmal alecho) +E Gaid NAY SEN Blue Colour > Coe preserd Resiclve + Fl dil: HNo, Al tere ogein. Fildsote Boiled te above Zo) Residus. | + Foss dveps H0. + Poot! Divided He ovhove. advlion fa a yorts Ast_powt Peddad sodiumn bisyautlet amd AK Zhoed purple talus > We peosont | ad pooh fidded OS 4 Phy gma Arak cont. HN amd sovileal- Boiled AP HS + NaOH exer) + Lint Bele Filbrede + UHconH Gli) Frltend aml transfer the qesiolue in a beakey. HO, vin onl Gltered , Filtvahe_ + possel HS. White ppl a Za” preset purple calout > Ma prod + Reva Tea => mitture A ammeonlyotal HIN ome cone, HEL in 429 gallo .salen ond transfered the ppt mo beaker, Added 5 mk hn dil. acai acid ark divided into Fe) parts, J fost Pout 2 f ‘ [fost 4 + Pasty gael) Ta ami of th aloion, ode! aahurnded ihe nto att present solution a (WH) $0, and 0 crystal A | Aodlium Ahioanlplode (a, $503) | White ppl —> S427 pret . TE s4%4 preset fibterad the solutin,, Reside Burned the ei eo. ino cyveibe wih o | + fitter popes = Added | Wocsm (i drape. ch cone. MeL ite 4 Fillake+ Wy) eo, ond Game | hat erly th an Applied Flame test Coivnson - Yaad flame [with te ret > Cat cand amed Brlekaed flame > 62% catinwwel.Priya es | r émapanhd He filtrate ff en, olp IV. to doynese. Adolad. ool a weber, ativedl amd warmed. Hieron . Residue Resid + % dops dll. Hot, + 2 wb totes Divide TE aloo solwtion irvcto tub povte. Pot 1 ao “EMH + NHQOK + Nas H Poy vite ppt —> mer pret | Pott 2 IO | a fio dies ‘moana eagont Na’ aiotion (| bh po Ww cacti. Fillzate Dividel te Slhode into a pasta. | fast 4 1+ Zine, Udon autede oy Mosnecion weaned awedtate (+ sheKed Nulloo ppt Pe Ne™ present Poot 2. + Sodium cobeMtinitsite. Adusion Nello ft —>K* prerort .