This document provides a tutorial on infrared (IR) spectroscopy. It discusses key topics such as the components of IR instruments, sample preparation techniques, and the differences between dispersive and Fourier transform IR spectroscopy. Specifically, it addresses the basic principles of IR spectroscopy, common sample preparation methods for solids and liquids, the purpose of monochromators and their components, and how correlation charts can be used to predict and identify major IR absorptions in unknown compounds.
This document provides a tutorial on infrared (IR) spectroscopy. It discusses key topics such as the components of IR instruments, sample preparation techniques, and the differences between dispersive and Fourier transform IR spectroscopy. Specifically, it addresses the basic principles of IR spectroscopy, common sample preparation methods for solids and liquids, the purpose of monochromators and their components, and how correlation charts can be used to predict and identify major IR absorptions in unknown compounds.
This document provides a tutorial on infrared (IR) spectroscopy. It discusses key topics such as the components of IR instruments, sample preparation techniques, and the differences between dispersive and Fourier transform IR spectroscopy. Specifically, it addresses the basic principles of IR spectroscopy, common sample preparation methods for solids and liquids, the purpose of monochromators and their components, and how correlation charts can be used to predict and identify major IR absorptions in unknown compounds.
This document provides a tutorial on infrared (IR) spectroscopy. It discusses key topics such as the components of IR instruments, sample preparation techniques, and the differences between dispersive and Fourier transform IR spectroscopy. Specifically, it addresses the basic principles of IR spectroscopy, common sample preparation methods for solids and liquids, the purpose of monochromators and their components, and how correlation charts can be used to predict and identify major IR absorptions in unknown compounds.
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TUTORIAL 7 (IR)
1. Define IR Spectroscopy and list two different type of IR instrument.
2. List down all basic component of IR instrument. 3. State the wavelength range of infra red region in unit of wave number. 4. Name and draw the modes of vibrational motion found in the molecule that infra red active with a correct arrow (direction) and label. 5. Draw the vibration mode of the molecules CO2 and SO2 for Symmetric stretching vibration, Asymmetric stretching vibration, Bending vibration with a correct arrow (direction) and label 6. Why potassium bromide is widely used as the sample holder rather than sodium chloride? 7. Name and explain two common for preparation liquid samples in IR measurement? 8. What is the disadvantage of using salt plates when preparing liquid samples? 9. State three common methods of preparing solid samples for IR measurements? 10. Describe each of the solid samples preparation method. 11. Name the typical sources of infra red. 12. What is the purpose of monochromators? 13. Name the components that commonly found in monochromators. 14. What is the purpose of the grooves on the diffraction gratings in the monochromators? 15. Why solution of the analysis of unknown compound must be prepared in high concentration? 16. Name the three types of the detectors used in infra red. 17. Give two advantages of using photon detectors in infra red spectrometer? 18. Define the interferogram. 19. What is the major difference between dispersive infra red and Fourier Transform Infra Red? 20. Draw the schematic diagram of interferometer in FTIR. 21. Name and give wavelength range for two region of IR spectrum. 22. What is the purpose of correlation charts? 23. Predict what is a major IR absorption are present above 1500 cm-1 for following compound; O CH3 CH2 CH2 CH2 CH2 CH3, CH3CH2 C CH2CH3 CH2= CH CH2 CH2 CH2 CH3,
1 CHCCH2CH2CH2CH3, CH3CH2CH2OH CH3COOH
24. Based on correlation charts given, identify major IR absorption for following compound (C2H6O). Predict their homolog series.
25. The following isomer can be deriving from molecular formula C2H6O.They are CH3CH2-OH and CH3 O CH3. Describe how this compound can be distinguished by using IR spectroscopy?
