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WO2025186949A1 - Heated tobacco and electrically-heated tobacco inhalation system - Google Patents

Heated tobacco and electrically-heated tobacco inhalation system

Info

Publication number
WO2025186949A1
WO2025186949A1 PCT/JP2024/008559 JP2024008559W WO2025186949A1 WO 2025186949 A1 WO2025186949 A1 WO 2025186949A1 JP 2024008559 W JP2024008559 W JP 2024008559W WO 2025186949 A1 WO2025186949 A1 WO 2025186949A1
Authority
WO
WIPO (PCT)
Prior art keywords
tobacco
heated
granules
flavor
heated tobacco
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
PCT/JP2024/008559
Other languages
French (fr)
Japanese (ja)
Other versions
WO2025186949A8 (en
Inventor
文貴 寺尾
正浩 千田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Japan Tobacco Inc
Original Assignee
Japan Tobacco Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Japan Tobacco Inc filed Critical Japan Tobacco Inc
Priority to PCT/JP2024/008559 priority Critical patent/WO2025186949A1/en
Publication of WO2025186949A1 publication Critical patent/WO2025186949A1/en
Publication of WO2025186949A8 publication Critical patent/WO2025186949A8/en
Pending legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00Cigars; Cigarettes
    • A24D1/20Cigarettes specially adapted for simulated smoking devices
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/20Devices using solid inhalable precursors

Definitions

  • the present invention relates to heated tobacco products and electrically heated tobacco smoking systems.
  • Heated tobacco products have a tobacco rod formed by filling the inside of a cigarette paper with a tobacco filler material containing tobacco raw materials (e.g., tobacco shreds, tobacco granules, molded tobacco sheets, etc.) and an aerosol-generating base material (glycerin, propylene glycol, etc.) (see, for example, Patent Document 1).
  • tobacco raw materials e.g., tobacco shreds, tobacco granules, molded tobacco sheets, etc.
  • an aerosol-generating base material glycerin, propylene glycol, etc.
  • An electrically heated tobacco smoking system comprising the heated tobacco product according to any one of [1] to [11] and an electrically heated device that heats the heated tobacco product.
  • the present invention makes it possible to adjust the delivery amount and improve delivery efficiency in heated tobacco and electrically heated tobacco smoking systems.
  • FIG. 1 is a schematic diagram of a heated tobacco product according to an embodiment of the present invention.
  • 1 is a cross-sectional view of a heated tobacco product according to an embodiment of the present invention.
  • 1 is a schematic diagram of an electrically heated tobacco smoking system according to an embodiment of the present invention;
  • FIG. 2 is a diagram for explaining the configuration of the periphery of a heating region in an electrically heated device.
  • FIG. 2 is a diagram illustrating the configuration of a control unit.
  • 1 is a cross-sectional schematic diagram of a flavor generation segment of a heated tobacco product according to an embodiment of the present invention.
  • FIG. 1 is a diagram showing the results of an example and a comparative example.
  • FIG. 1 is a diagram showing the results of an example and a comparative example.
  • the left-right direction of the heated tobacco product or the electrically heated device into which the heated tobacco product is inserted is shown as the X direction, the up-down direction as the Y direction, and the depth direction as the Z direction.
  • These directions are merely examples for the sake of convenience and do not limit the elements in the drawings.
  • the elements of the electrically heated tobacco product system are not limited to being arranged in the directions shown in the drawings.
  • a heated tobacco according to one embodiment of the present invention is a heated tobacco comprising a flavor generation segment, the flavor generation segment including a tobacco sheet and granules, the granules being disposed between the tobacco sheets.
  • the heated tobacco may be a non-combustible heated tobacco.
  • the heated tobacco product 100 is in the form of a substantially cylindrical rod.
  • the heated tobacco product 100 includes a flavor generation segment 110, a cooling section 120, a filter section 130, and tipping paper 140 that connects these together.
  • the cooling section 120 and the filter section 130 are connected coaxially to the flavor generation segment 110 by being wrapped around them by the tipping paper 140.
  • Reference numeral 101 denotes the mouth end of the heated tobacco product 100 (filter portion 130).
  • Reference numeral 102 denotes the tip of the heated tobacco product 100 opposite the mouth end 101.
  • the flavor generation segment 110 is located on the tip 102 side of the heated tobacco product 100.
  • the heated tobacco product 100 has a substantially constant diameter over its entire length in the longitudinal direction (hereinafter also referred to as the axial direction or Z direction) from the mouth end 101 along the tip 102.
  • the configuration of the heated tobacco product 100 is not particularly limited and can be any general configuration.
  • the flavor generation segment 110, cooling section 120, and filter section 130 are each illustrated as a single segment, but each section may be composed of a single segment or multiple segments.
  • the flavor generating segment 110 is not particularly limited as long as it includes a tobacco sheet and granules, and the granules are disposed between the tobacco sheets.
  • a tobacco filler 111 consisting of tobacco sheets, granules, etc. (hereinafter, the filler including tobacco sheets and granules filled in the flavor generation segment 110 may be collectively referred to simply as "tobacco filler”) may be used, which is filled into the flavor generation segment 110 and wrapped in cigarette paper 112.
  • the flavor generation segment 110 may also have a fitting portion for fitting with a heater member or the like for heating the heated tobacco product 100 . It is preferable that the flavor generation segment 110 has a columnar shape, and in this case, it is preferable that the aspect ratio, which is represented by the height of the flavor generation segment 110 in the long axis direction relative to the width of the base of the flavor generation segment 110, is 1 or more.
  • the shape of the bottom of the flavor generation segment 110 is not limited and may be polygonal, rounded polygonal, circular, elliptical, or the like, and the width is the diameter when the bottom is circular, the major axis when the bottom is elliptical, and the diameter of the circumscribed circle or the major axis of the circumscribed ellipse when the bottom is polygonal or rounded polygonal.
  • the height of the flavor generation segment 110 is preferably about 10 to 70 mm, and the width is preferably about 4 to 9 mm.
  • the length of the flavor generating segment 110 in the longitudinal direction can be adjusted appropriately to suit the size of the product, but is typically 10 mm or more, preferably 12 mm or more, more preferably 15 mm or more, and even more preferably 18 mm or more. It is typically 70 mm or less, preferably 50 mm or less, more preferably 30 mm or less, and even more preferably 25 mm or less. Furthermore, from the viewpoint of the balance between the amount of flavor delivered and the aerosol temperature, the ratio of the length of the flavor generating segment 110 to its longitudinal length h is typically 10% or more, preferably 20% or more, more preferably 25% or more, and even more preferably 30% or more. It is typically 60% or less, preferably 50% or less, more preferably 45% or less, and even more preferably 40% or less.
  • the tobacco sheet may be a reconstituted tobacco sheet, or a sheet (hereinafter simply referred to as a homogenized sheet) made by grinding dried tobacco leaves to an average particle size of 20 ⁇ m or more and 200 ⁇ m or less to obtain tobacco pulverized material, which is then homogenized and processed into a sheet.
  • the homogenized sheet may be a strand type, in which a homogenized sheet having a length approximately the same as the longitudinal direction of the flavor generation segment 110 is shredded approximately parallel to the longitudinal direction of the flavor generation segment 110 and filled into the flavor generation segment 110.
  • the content of dried tobacco leaves contained in the flavor generation segment 110 is not particularly limited, but may be 200 mg or more and 800 mg or less, with 250 mg or more and 600 mg or less being preferred. This range is particularly suitable for a flavor generation segment 110 having a circumference of 22 mm and a length of 20 mm.
  • the method for filling the flavor generation segment 110 with tobacco sheets is not particularly limited.
  • the tobacco sheets may be wrapped in cigarette paper 112, or the tobacco sheets may be filled into a cylindrical cigarette paper 112.
  • the flavor generation segments 110 may be filled so that their longitudinal directions are in an unspecified direction within the cigarette paper 112, or they may be filled aligned along the axial direction of the flavor generation segment 110 or perpendicular to the axial direction.
  • tobacco sheets cut into widths of 0.5 mm to 2.0 mm may be filled in a random orientation
  • tobacco sheets cut into widths of 1.0 mm to 3.0 mm may be filled aligned parallel to the air passage direction, or the tobacco sheets may be crimped (processed to create vertical grain) and then gathered.
  • the tobacco components contained in the flavor generation segment 110 vaporize, and these are transferred to the cooling section 120 and filter section 130 by suction.
  • gather filling a mode in which multiple channels for vertical air flow are provided
  • This mode makes it easier to arrange the granules described below between the tobacco sheets.
  • flavor components can be efficiently delivered to the user.
  • the tobacco sheet may also be packed in a spiral shape.
  • the amount of tobacco sheet filled into the flavor generation segment 110 depends on the size and shape of the flavor generation segment 110, but as an example, if the flavor generation segment 110 is rod-shaped with a major axis length of 12 mm and a diameter of 7 mm, it is typically 150 mg to 350 mg, preferably 200 mg to 250 mg.
  • the packing density of the tobacco sheet in the flavor generation segment 110 is preferably 0.33 g/cm 3 to 0.76 g/cm 3 , and more preferably 0.43 g/cm 3 to 0.54 g/cm 3. When the packing density of the tobacco sheet is within the above range, sufficient delivery can be ensured while suppressing the total packing amount of tobacco components, resulting in excellent delivery efficiency.
  • the granules according to this embodiment are disposed between the tobacco sheets and filled into the flavor generating segment 110 together with the tobacco sheets.
  • the granules are sandwiched between the tobacco sheets that have been gathered and filled after crimping. This is preferable because it makes it difficult for the granules to fall out from between the sheets. It also makes it easier to ensure the surface area of the tobacco filler and the air flow path in the ventilation direction.
  • the granules may be evenly or unevenly sandwiched between the sheets, but from the viewpoint of delivery, it is preferable that they be disposed as evenly as possible.
  • the granules be distributed so that there are as many contact points between the granules and the tobacco sheet as possible.
  • the granules may be filled between the tobacco sheets after the tobacco sheets have been filled into the flavor generation segment 110.
  • the granules may be adhered to the sheet.
  • the granules may be held in place to prevent spillage when the flavor generating segment 110 is molded into a rod shape.
  • the adhesive for adhering the sheet and the granules may be at least one adhesive selected from the group consisting of a vinyl acetate glue or components commonly used in tobacco sheets, such as binders guar gum, xanthan gum, CMC (carboxymethylcellulose), and CMC-Na (sodium salt of carboxymethylcellulose).
  • the retention agent may be an aerosol source, such as at least one retention agent selected from the group consisting of glycerin, propylene glycol, triacetin, 1,3-butanediol, and mixtures thereof.
  • FIG. 6 is a schematic cross-sectional view perpendicular to the longitudinal direction of a flavor generating segment according to one embodiment of the present invention.
  • a flavor generating segment wrapped in cigarette paper 61 is filled with a folded tobacco sheet 62, and granules 63 are filled between the tobacco sheets 62.
  • the granules 63 may also be filled in a manner that they are sandwiched between the tobacco sheets 62.
  • the base material of the granules is not particularly limited, but from the perspective of thermal conductivity, it is preferable that it contains at least one selected from the group consisting of calcium carbonate, activated carbon, and crystalline cellulose. These base materials can be molded into a granular shape using known methods.
  • the thermal conductivity of the granules is preferably 0.10 W/mK to 250 W/mK, and more preferably 1.0 W/mK to 5.0 W/mK. It is preferable for the thermal conductivity of the granules to be within the above range, as this allows for efficient heating of the entire flavor generation segment 110.
  • the granules can be given various functions by containing other components in addition to the base material.
  • the other components include at least one selected from the group consisting of flavorings, tobacco flavoring components, and nicotine. It is preferable to fill the flavor generating segment 110 with these ingredients supported on granules from the viewpoint of ingredient retention.
  • a method for incorporating other components into the granules a method in which the base material and other components are mixed and then molded into a granular shape can be mentioned.
  • the type of the flavoring is not particularly limited, and from the viewpoint of imparting a good flavor, the following may be used: acetanisole, acetophenone, acetylpyrazine, 2-acetylthiazole, alfalfa extract, amyl alcohol, amyl butyrate, trans-anethole, star anise oil, apple juice, Peru balsam oil, beeswax absolute, benzaldehyde, benzoin resinoid, benzyl alcohol, benzyl benzoate, benzyl phenylacetate, benzyl propionate, 2,3-butanedione, 2-butanol, butyl butyrate, butyric acid, caramel, cardamom oil, carob absolute, ⁇ -Carotene, carrot juice, L-carvone, ⁇ -caryophyllene, cassia bark oil, cedarwood oil, celery seed oil, chamomile oil, cinnamaldeh
  • tobacco flavor components include components derived from tobacco leaves such as tobacco shreds, etc.
  • the material of the tobacco shreds is not particularly limited, and known materials such as lamina and ribs can be used.
  • the delivery of the tobacco flavor components can be controlled.
  • the second is a method in which an appropriate solvent such as water is mixed with ground tobacco leaves to homogenize them, and then a thin layer of the homogenized material is cast onto a metal plate or metal plate belt and dried to produce a cast sheet.
  • the third is a method in which an appropriate solvent such as water is mixed with ground tobacco leaves to homogenize them, and then the homogenized material is extruded into a sheet to produce a rolled sheet. Details of the types of homogenizing sheets are disclosed in "Encyclopedia of Tobacco," Tobacco Research Center, March 31, 2009.
  • the amount of granules filled into the flavor generating segment 110 depends on the size and shape of the flavor generating segment 110, but as an example, if the flavor generating segment 110 is rod-shaped with a major axis length of 12 mm and a diameter of 7 mm, it is typically 20 mg to 100 mg, preferably 50 mg to 80 mg.
  • the packing density of the granules in the flavor generating segment 110 is preferably 0.04 g/cm 3 to 0.22 g/cm 3 , more preferably 0.11 g/cm 3 to 0.17 g/cm 3. If the packing density of the granules is within the above range, it is preferable from the viewpoint of delivery efficiency.
  • the mass ratio of the tobacco sheet to the granules filled in the flavor generation segment 110 is preferably 60/40 to 95/5, and more preferably 70/30 to 80/20.
  • the average particle size of the granules is preferably 250 ⁇ m to 1000 ⁇ m, and more preferably 500 ⁇ m to 800 ⁇ m. When the average particle size of the granules is 250 ⁇ m or more, the effect of improving delivery efficiency can be sufficiently obtained. Furthermore, when the average particle size of the granules is 1000 ⁇ m or less, the production of the granules is easy.
  • the average particle size of the granules can be adjusted appropriately by adjusting the amount of the base material, etc. contained in the granules.
  • the average particle size is measured using a laser diffraction particle sizer such as Mastersizer (manufactured by Malvern).
  • composition and manufacturing method of the granules are not limited to the above examples, and may be, for example, the following composition and manufacturing method.
  • Granule Composition The components contained in the granules include (A) 15-50% by weight of tobacco extract, (B) non-wood fiber, (C) binder, and (D) 10-60% by weight of aerosol base material, and the total of (B) and (C) may be 23-50% by weight. Unless otherwise specified, weights and weight percentages are dry weights and dry weight percentages. Dry weight is the weight excluding the weight of water.
  • Tobacco Extract is a substance or mixture that exhibits a flavor extracted from tobacco.
  • Tobacco extract can be prepared by known methods. Examples include the following: 1) a method in which tobacco raw material is subjected to extraction using an extraction medium to obtain a tobacco extract; 2) a method in which an extraction medium is added to the tobacco raw material and heated, and the generated vapor is collected; and 3) a method in which the extraction medium is vaporized by heating and passed through the tobacco raw material, and the vapor is collected after passing.
  • extraction media include water or hydrophilic organic solvents such as alcohol. In method 1), water is preferably used as the extraction medium from the perspective of workability.
  • alcohols such as propylene glycol, glycerin, or ethanol are preferably used as the extraction medium from the perspective of work efficiency. Acids or alkalis can also be used for extraction as needed.
  • the liquid obtained by extraction, containing the tobacco extract and extraction medium, is called a tobacco extract.
  • Tobacco raw materials can be those of the Nicotiana genus, such as Nicotiana tabacum and Nicotiana rustica.
  • Nicotiana tabacum can be of varieties such as burley or flue-cured varieties. Alternatively, varieties such as the Orient or native burley varieties of the Nicotiana genus can also be used.
  • the tobacco raw material may be shredded or powdered tobacco material (hereinafter also referred to as "raw material pieces").
  • the particle size of the raw material pieces is preferably 0.5 to 1.18 mm.
  • Such raw material pieces can be obtained, for example, by sieving in accordance with JIS Z 8815 using a stainless steel sieve conforming to JIS Z 8801. For example, 1) using a stainless steel sieve with 1.18 mm openings, the raw material pieces are sieved by a dry mechanical shaking method for 20 minutes to obtain raw material pieces that pass through the stainless steel sieve with 1.18 mm openings.
  • raw material pieces are sieved by a dry mechanical shaking method for 20 minutes to remove the raw material pieces that pass through the stainless steel sieve with 0.50 mm openings.
  • tobacco raw materials are treated with alkali. Flavor components are generated through this treatment, and these may be collected to prepare a tobacco extract liquid containing tobacco extract and water. In this case, it is preferable to extract the flavor components as a gas from the alkali-treated tobacco raw material, and then introduce the gas into water to convert the flavor components into a liquid.
  • the alkaline substance is preferably an alkaline liquid such as an aqueous potassium carbonate solution.
  • the alkaline substance is supplied until the pH of the tobacco raw material falls within a specific range. This pH is preferably 8.0 or higher, more preferably 8.9 to 9.7.
  • the pH of the tobacco raw material is the pH of the water when the tobacco raw material is mixed with 10 times the amount of water.
  • the moisture content of tobacco raw materials is not limited, but from the perspective of efficiently extracting flavor components, it is preferable that the moisture content be approximately 5 to 30% by weight.
  • the moisture content of tobacco raw materials is measured by known methods; for example, a 1g sample is taken, heated at 105°C, and the moisture content is determined by the weight loss when heated until the weight change rate is 1mg/min or less. This measurement can be performed using, for example, a halogen heating moisture meter (such as the MB45 manufactured by Ohaus).
  • the tobacco extract content in the tobacco flavor component is preferably 15 to 50% by weight. This amount can be adjusted appropriately, for example, to 20 to 40% by weight.
  • Non-wood fiber is a fiber not derived from wood, preferably a fiber other than tobacco fiber. Dietary fiber is preferred as a non-wood fiber. Dietary fiber is a food component that is not digested by human digestive enzymes, and is more preferably insoluble dietary fiber that does not dissolve in water. Dietary fiber may be porous, i.e., spongy. Porous fiber can increase the surface area of granules and improve thermal conductivity. From the standpoint of availability, the fiber is preferably citrus fiber. Citrus fiber is a fiber derived primarily from the albedo of citrus fruits. Dietary fiber may also be short fibers or columnar particles with a small aspect ratio.
  • Citrus fiber is particularly preferred because it can impart strength to the sheet with a small amount.
  • the moisture content of the non-wood fiber is measured, and the amount of non-wood fiber blended is determined to satisfy the moisture content relationship described below.
  • the moisture content of the non-wood fiber is measured by a known method, for example, the same method as the moisture content of tobacco raw materials.
  • the content of component (B) in the granules is 10 to 30% by weight.
  • wood fiber is a well-known fiber material, the use of non-wood fiber has the advantage of being superior in liquid-carrying capacity compared to wood fiber, and therefore the amount of non-wood fiber added can be reduced, allowing for more components that contribute to flavor and taste.
  • binder examples include carboxyalkyl cellulose and guar gum.
  • the moisture content of the binder is measured by a known method, for example, the same method as that for the moisture content of the tobacco raw material.
  • the total amount of component (B) and component (C) in the sheet is preferably 23 to 50% by weight.
  • this amount is equal to or greater than the lower limit, the granules are easy to handle and tend to have sufficient strength. Furthermore, when this amount is equal to or less than the upper limit, the flavor is sufficient or unpleasant flavors are suppressed.
  • the lower limit of this total amount is preferably 24% by weight or more, and the upper limit is preferably 40% by weight or less, more preferably 30% by weight or less.
  • component (B) and component (C) are determined so as to satisfy the above total amount, and in one embodiment, the amount of component (B) is 10 to 30% by weight or 13 to 25% by weight, and the amount of component (C) is 13 to 20% by weight or 10 to 25% by weight.
  • Aerosol Base examples include polyhydric alcohols such as glycerin or polyethylene glycol.
  • the moisture content in the aerosol base is measured by a known method, for example, the same method as that for the moisture content in tobacco raw materials.
  • the amount of aerosol base in the granules is 10 to 60% by weight. When this amount is equal to or greater than the lower limit, the amount of smoke produced during smoking is sufficient. When this amount is equal to or less than the upper limit, the handleability of the granules is improved. From this perspective, the amount is preferably 15 to 50% by weight, more preferably 20 to 40% by weight.
  • the granules may contain wood fibers.
  • wood fibers include softwood pulp, Vitacel FL400, and Vitacel L600/30 (all manufactured by J. Rettenmaier & Söhne GmbH).
  • the mixture for producing the granules preferably contains water, and the weight ratio of water to components other than water in the mixture is preferably (0.2 to 1:1). It is preferable to measure the moisture content of the wood fibers and determine the amount of wood fibers to satisfy this relationship.
  • the moisture content of the wood fibers is measured by a known method, for example, the same method as that for the moisture content of tobacco raw materials.
  • the wood fiber content in the granules is 1 to 10% by weight.
  • the granules of this embodiment are preferably manufactured by a method comprising step 1A of preparing a mixture of tobacco extract containing component (A), component (B), component (C), and component (D), and step 2A of granulating the mixture.
  • Process 1A Preparation of Tobacco Extract
  • the tobacco raw material described above is subjected to extraction to prepare a tobacco extract containing the tobacco extract as an active ingredient and an extraction medium.
  • Water is preferably used as the extraction medium.
  • the extraction temperature is not limited, but is preferably 60 to 100°C, and more preferably 70 to 90°C from the perspective of smoking taste.
  • the extraction time is preferably 20 to 40 minutes.
  • (1-2) Mixing Mixing can be carried out by known methods; for example, a mixture can be prepared by mixing the components in a mixer or the like.
  • the mixture preferably contains water, and the weight ratio of water to components other than water is preferably (0.2 to 1:1).
  • the water may be water contained in the tobacco extract, or may be water added separately. In particular, when the content of non-wood fibers is increased, it is preferable to also increase the content of water.
  • step 2A the same method as in step 2 described above can be used. Specifically, in step 2A, the mixture obtained in step 1A is granulated (into long columns) in a wet extrusion granulator, and then sized into short columns or spheres. The extrusion pressure during extrusion granulation can be set as desired depending on the viscosity of the mixture, etc.
  • the granules obtained by extrusion granulation may be further dried, if necessary, to adjust the moisture content.
  • the loss on drying of the granules obtained by extrusion granulation may be measured, and if it is higher than the desired loss on drying (for example, 5% by weight or more and 17% by weight or less), the granules may be further dried to obtain the desired loss on drying.
  • the drying conditions (temperature and time) required to obtain the desired loss on drying can be determined in advance and set based on the drying conditions (temperature and time) required to reduce the loss on drying by a predetermined value.
  • the moisture content of the tobacco filler can be 10% by weight or more and 15% by weight or less, and preferably 11% by weight or more and 13% by weight or less, based on the total amount of the tobacco filler. This moisture content suppresses the occurrence of stains on the roll and improves the suitability for rolling during the production of the flavor generating segment 110.
  • dried tobacco leaves may be ground to an average particle size of approximately 20 ⁇ m to 200 ⁇ m, homogenized, and then processed into a sheet, which may then be shredded to a width of 0.5 mm or more and 2.0 mm or less.
  • the tobacco filler may also contain an aerosol base, which is a base that generates an aerosol when heated, and examples of such a base include glycerin, propylene glycol, triacetin, 1,3-butanediol, and mixtures thereof.
  • the content of the aerosol base material in the tobacco filler is not particularly limited, but from the viewpoint of generating sufficient aerosol and imparting a good flavor, it is usually 5% by weight or more, preferably 10% by weight or more, and usually 50% by weight or less, preferably 15% by weight or more and 25% by weight or less, relative to the total amount of the tobacco filler.
  • the tobacco filler may contain a flavoring agent in addition to that contained in the granules.
  • the content of the flavoring in the tobacco filler is not particularly limited, but from the viewpoint of imparting a good flavor, it is usually 10,000 ppm or more, preferably 20,000 ppm or more, more preferably 25,000 ppm or more, and is usually 70,000 ppm or less, preferably 50,000 ppm or less, more preferably 40,000 ppm or less, and even more preferably 33,000 ppm or less.
  • the method for producing a heated tobacco product according to this embodiment is not particularly limited, and a combination of known methods can be applied.
  • a tobacco sheet is extruded from a roller and crimped, and then granules are added to the tobacco sheet, which is then rolled up in cigarette paper to produce a rod-shaped flavor generation segment 110.
  • an aerosol source such as glycerin may be added as needed.
  • the flavor generation segment 110, cooling section 120, and filter section 130 are then rolled up in tipping paper 140 to produce the flavor generation segment 110.
  • an electrically heated tobacco suction system according to another embodiment of the present invention is an electrically heated tobacco suction system that includes the above-described heated tobacco product and an electric heating device that heats the heated tobacco product.
  • the configuration of the electrically heated tobacco suction system is not particularly limited, and may be, for example, as shown in Figures 3 and 4.
  • Figure 3 is a diagram illustrating the internal structure of the electrically heated tobacco suction system 200. Note that the heated tobacco article 100 in Figure 3 is a schematic representation of the heated tobacco article 100 in Figure 1.
  • the electrically heated tobacco suction system 200 comprises a heated tobacco product 100 and an electrically heated device 30 that heats the flavor generation segment 110 of the heated tobacco product 100.
  • the heated tobacco product 100 is inserted into and removed from the storage cavity 313 of the storage unit 310 through the insertion port 3A of the electrically heated device 30.
  • the heated tobacco product 100 is inserted into the storage cavity 313, and in this state, the heater provided in the storage section 310 is made to generate heat, which heats the flavor source within the heated tobacco product 100, thereby generating an aerosol containing components such as tobacco components, which the user can inhale.
  • the heater may directly heat the flavor generation segment 110, or alternatively, it may heat an aerosol generation source within the heated tobacco product 100, supply the heated aerosol to the flavor generation segment 110, and the heated aerosol may further heat tobacco components, etc. within the flavor generation segment 110, thereby allowing the user to inhale it.
  • the electric heating device 30 has a housing 31, which is a case for accommodating various components.
  • the housing 31 contains a heater 32, a temperature sensor 35, a suction sensor 36, a control unit 37, a power supply 38, etc.
  • the housing 31 has a storage section 310 that stores the heated tobacco product 100 in an insertable and removable manner from the front end to the rear end.
  • the storage section 310 extends in the insertion/removal direction of the heated tobacco product 100 and includes a cylindrical peripheral wall 312 that defines the outer periphery of the space into which the heated tobacco product 100 is inserted, and a disk-shaped rear wall 311 that closes the rear end of the peripheral wall 312 so as to define the rear end of the space.
  • the peripheral wall 312 and rear wall 311 of the storage section 310 may be formed integrally with the housing 31, or may be formed separately from the housing 31 and then assembled to the housing 31.
  • the open end of the peripheral wall 312 of the storage section 310 is open toward the outside of the housing 31, and serves as an insertion port 3A for inserting the heated tobacco product 100.
  • the internal space of the peripheral wall 312 serves as a cylindrical storage cavity 313 into which the tip portion of the heated tobacco product 100 can be inserted and removed via the insertion port 3A.
  • the symbol CL indicates the central axis of the storage cavity 313 in the insertion and removal direction of the heated tobacco product 100.
  • the direction along this central axis CL will also be referred to as the axial direction.
  • the outer diameter of the storage cavity 313, i.e., the inner diameter of the peripheral wall 312, may be equal to, slightly larger than, or slightly smaller than the outer diameter of the heated tobacco product 100.
  • a heater 32 is provided around the peripheral wall 312 of the storage section 310.
  • the peripheral wall 312 and rear wall 311 of the storage section 310 are formed from a material that can withstand the heat of the heater 32 and transfer the heat of the heater 32 to the heated tobacco product 100.
  • Materials used for such a storage section 310 include, for example, metals such as stainless steel and heat-resistant resins.
  • the heater 32 may be located within the peripheral wall 312.
  • the heater 32 generates heat upon receiving power from the control unit 37, and heats the heated tobacco product 100 accommodated in the accommodation unit 310.
  • the heater 32 is one form of a heating unit that heats the heated tobacco product 100.
  • the type of heater 32 is not particularly limited, but examples include a steel material with a heating wire (e.g., a wire material with high electrical resistance, such as nichrome, iron chromium, or iron nickel) strung throughout, a ceramic heater, a sheathed heater, etc.
  • a sheathed heater is a heater in which a heating wire is covered with a metal pipe together with a filler.
  • FIG. 4 shows the heated tobacco product 100 inserted into the storage cavity 313.
  • the heater 32 receives power from the control unit 37, as described below, and heats the flavor generation segment 110 to a predetermined temperature.
  • the space in the storage cavity 313 that is heated to a predetermined temperature by the heat of the heater 32 is designated as the heated area A1, and the space adjacent to the insertion opening of the heated area A1 in the axial direction (insertion/removal direction) is designated as the non-heated area A2.
  • the non-heated area A2 is formed on the insertion opening side of the storage cavity 313, and the heated area A1 is formed on the rear side of the storage cavity 313.
  • the heater 32 is disposed around or inside the peripheral wall 312 in the heated area A1, and heats the heated area A1 from the outside.
  • the heater 32 not only heats the area in contact with the heater 32, but also heats areas distant from the heater 32 by radiation and heat transfer.
  • the heater 32 heats at a predetermined temperature from the front end of the heater 32 to position 317 on the insertion opening side in the axial direction. Therefore, the heated region A1 is the region from position 317 to the rear wall 311 in the axial direction of the accommodating portion 310. That is, position 317 is the boundary between the heated region A1 and the non-heated region A2, and the non-heated region A2 is the region from this boundary 317 to the front end of the accommodating cavity 313 in the axial direction.
  • this boundary 317 may be determined as the boundary between the region where the temperature reaches a predetermined temperature and the region where the temperature falls below the predetermined temperature when actually heated by the heater 32, or may be determined as the estimated boundary between the region where the temperature reaches a predetermined temperature and the region where the temperature falls below the predetermined temperature when the heater 32 is operated under predetermined conditions.
  • the boundary position between the region where the temperature reaches a predetermined temperature and the region where the temperature falls below the predetermined temperature of the peripheral wall 312 is estimated, and the plane that passes through this boundary position and is perpendicular to the central axis CL is determined as the boundary 317, as shown by the two-dot chain line in FIG. 4 .
  • the flavor generation segment 110 When the heated tobacco product 100 is inserted into the storage cavity 313, the flavor generation segment 110 is located in the heated region A1, and at least a portion of the cooling unit 120 is located in the non-heated region A2.
  • the portion of the storage cavity 313 where the flavor generation segment 110 is located may be the heated region A1, and the portion where the cooling unit 120 is located may be the non-heated region A2.
  • Control unit] 5 is a diagram showing the configuration of the control unit 37.
  • the control unit 37 controls the operating state of the electric heating device 30, such as controlling heating by the heater 32.
  • the control unit 37 is a computer including a processor 71 such as a CPU (Central Processing Unit), DSP (Digital Signal Processor), or FPGA (Field-Programmable Gate Array), a memory 72 such as RAM (Random Access Memory) or ROM (Read Only Memory), and an input/output unit 73.
  • the control unit 37 also includes a drive circuit 74 for the heater 32.
  • Memory 72 may include a memory that functions as a main memory unit 721 and a memory that functions as an auxiliary memory unit 722. Memory 72 may be formed integrally with processor 71 (on one chip). Examples of memory 72 include storage media such as volatile memory such as RAM, non-volatile memory such as ROM, EPROM (Erasable Programmable ROM), SSD, or removable media.
  • volatile memory such as RAM
  • non-volatile memory such as ROM, EPROM (Erasable Programmable ROM), SSD, or removable media.
  • the memory 72 can store an operating system (OS), various programs (firmware), various data tables, various databases, setting data, user data, and the like, which are used to execute the operations of the electric heating device 30.
  • OS operating system
  • programs firmware
  • data tables various databases, setting data, user data, and the like, which are used to execute the operations of the electric heating device 30.
  • the input/output unit 73 is a means for inputting information such as power on/off by the user (smoker) to the processor 71, or for outputting information to the user.
  • the input/output unit 73 is, for example, an interface that operates the temperature sensor 35 and suction sensor 36 at predetermined times and acquires the detected values of each sensor 35, 36.
  • the input/output unit 73 may also include input means such as operation buttons and a touch panel, as well as output means such as a display, vibrator, and speaker.
  • the input/output unit 73 may also include a communications unit for communicating with an external device via a communications line.
  • the communications unit may connect to another computer via a communications cable, receive programs and data for controlling the electric heating device 30, and store them in the memory 72, thereby updating the firmware, heating profile, etc.
  • the display is a means for displaying information, and may be, for example, an indicator such as an LED, a liquid crystal display, or an organic EL display.
  • the drive circuit 74 supplies power from the power supply 38 to the heater 32 in accordance with instructions from the processor 71, causing the heater 32 to operate.
  • the drive circuit 74 is, for example, a converter that adjusts the amount of current flowing to the heater 32.
  • the control unit 37 functions as predetermined functional units, such as a determination unit 711, a heating control unit 712, and an output control unit 713, when the processor 71 reads and executes a program stored in the memory 72 into the working area of the main storage unit.
  • these functional units are not limited to those realized based on programs (software), and some or all of them may be configured using hardware circuits such as processors, integrated circuits, and logic circuits.
  • the determination unit 711 determines information such as the user's operation, the state of the heated tobacco product 100, and the heating status of the heater 32 based on the detection results of the sensors 35, 36 and input information from the input means. For example, the determination unit 711 measures the number of puffs from the detection value of the suction sensor 36 and determines whether the number of puffs has reached a predetermined number.
  • the heating control unit 712 controls the drive circuit 74 based on the determination result of the determination unit 711, thereby controlling the power supplied from the power source 38 to the heater 32 via the drive circuit 74. For example, the heating control unit 712 terminates heating when the determination unit 711 determines that the number of suctions has reached a predetermined number. Furthermore, when the determination unit 711 determines that the amount of moisture or flavor source in the flavor generation segment 110 has decreased to a predetermined amount, the heating control unit 712 changes the power supplied to the heater 32 to change the heating temperature. Furthermore, when the determination unit 711 determines that the amount of moisture or flavor source in the flavor generation segment 110 has decreased to the point where heating should be terminated, the heating control unit 712 stops the power supply to the heater 32 and terminates heating.
  • the output control unit 713 outputs notifications, warnings, etc. to the user based on the determination result of the determination unit 711. For example, the output control unit 713 outputs a signal when the remaining number of possible suctions reaches a predetermined number or less. As an output to the user, the output control unit 713 may, for example, display on a display unit, output sound from a speaker, or vibrate using a vibrator.
  • the length of the heater 32 in the longitudinal direction can be within the range of L ⁇ 5.0 mm, where L mm is the length of the flavor generation segment 110 in the longitudinal direction. From the perspective of aerosol delivery, i.e., to sufficiently transfer heat to the flavor generation segment 110 and sufficiently volatilize the aerosol base material and flavor components contained in the flavor source, the length of the heater 32 in the longitudinal direction is preferably L mm or more.
  • the length is preferably L + 0.5 mm or less, L + 1.0 mm or less, L + 1.5 mm or less, L + 2.0 mm or less, L + 2.5 mm or less, L + 3.0 mm or less, L + 3.5 mm or less, L + 4.0 mm or less, L + 4.5 mm or less, or L + 5.0 mm or less.
  • the heating intensity such as the heating time and heating temperature of the heated tobacco product 100 by the heater 32, can be preset for each electrically heated tobacco suction system 200. For example, by preheating the heated tobacco product 100 for a certain period of time after it is inserted into the electrically heated device 30, the heated tobacco product 100 can be heated until the temperature of the outer surface of the portion of the heated tobacco product 100 that is inserted into the electrically heated device 30 reaches X (°C), and the temperature can then be set in advance to maintain a constant temperature of X (°C) or less. From the viewpoint of the delivery amount of components generated by heating, the above X (°C) is preferably 80°C or higher and 400°C or lower.
  • the X (°C) may be 80°C, 90°C, 100°C, 110°C, 120°C, 130°C, 140°C, 150°C, 160°C, 170°C, 180°C, 190°C, 200°C, 210°C, 220°C, 230°C, 240°C, 250°C, 260°C, 270°C, 280°C, 290°C, 300°C, 310°C, 320°C, 330°C, 340°C, 350°C, 360°C, 370°C, 380°C, 390°C, or 400°C.
  • the opening 103 that may be provided in the cooling section 120 is preferably located closer to the mouth end than the mouth end of the area of the cooling section 120 that comes into contact with the electrically heated device 30, from the standpoint of promoting the inflow of air from the outside and preventing components and air generated by heating from accumulating within the cooling section 120. Furthermore, the insertion port 3A of the electrically heated device 30 for the heated tobacco 100 may be tapered to make it easier to insert the heated tobacco 100.
  • a heater as a means for heating the heated tobacco product 100
  • the means for heating the heated tobacco product 100 is not limited to this.
  • a rod-shaped or spindle-shaped heater may be used, and when the heated tobacco product 100 is inserted into an electrically heated device, the heater may be inserted into the flavor generation segment 110 of the heated tobacco product 100, thereby heating the heated tobacco product 100 from the inside.
  • an inductor is provided as the heater, and a susceptor for heating a flavor source, etc. is introduced into the flavor generation segment 110 of the heated tobacco product 100. In this embodiment, the flavor source, etc.
  • the output control unit 713 can be heated by supplying power to the inductor via the output control unit 713 and heating the susceptor by induction heating. It is also possible to adopt an embodiment in which a microwave generator is provided as the heater. In this embodiment, the output control unit 713 supplies power to the microwave generator, and the flavor source and the like in the flavor generation segment 110 can be heated by microwave heating.
  • Tobacco sheet A composition of ground tobacco with glycerin added as an aerosol-generating base material at a ratio of 12% by mass to the total, processed into a rolled sheet with a thickness of 248 ⁇ m and a basis weight of 200 gm/ m2.
  • Granules A mixture of calcium carbonate and carboxymethyl cellulose (binder) in a weight ratio of 95:5.
  • Thermal conductivity 2.70 W/mK.
  • Average particle size 500 ⁇ m.
  • Example 1 The tobacco sheet was crimped while being extruded from the roller, and then granules were added onto the tobacco sheet, followed by gathering and wrapping the tobacco sheet together with the granules in cigarette paper to prepare a cylindrical flavor generating segment.
  • the flavor generating segment had a circumference of 22 mm and a length of 12 mm, the tobacco sheet had a width of 85 mm, and the filling amounts were 204 mg of tobacco sheet and 80 mg of granules.
  • the tip segment, flavor generation segment, cooling section, and filter section were arranged in a line in that order from farthest from the mouth end, and these were connected coaxially by wrapping with tipping paper to obtain a heated tobacco product.
  • the tip segment was an 8 mm long paper filter
  • the cooling section was a 20 mm long hollow tube
  • the filter section was a filter from a heated tobacco product (Mevius Deep Regular, exclusive for Ploom X) used in Ploom X (trade name, manufactured by Japan Tobacco Inc.).
  • the obtained heated tobacco product was subjected to the above-mentioned smoking test, and the delivery amount was evaluated. The results are shown in Table 1.
  • Example 1 A heat-not-burn tobacco product was produced and evaluated in the same manner as in Example 1, except that the tobacco sheet had a width of 95 mm and a filling amount of 228 mg, and no granules were filled in the flavor generating segment. The results are shown in Table 1.
  • Figures 7 and 8 are graphs showing the results of Table 1.
  • the results of Table 1, Figures 7 and 8 show that the heated tobacco product of Example 1 has a smaller tobacco sheet filling amount than Comparative Example 1, yet achieves the same level of delivery. That is, a heated tobacco product containing the granules according to this embodiment has improved delivery efficiency and a more satisfying smoking experience.

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Abstract

A heated tobacco comprising a flavor generation segment, wherein the flavor generation segment includes tobacco sheets and granules, and the granules are disposed between the tobacco sheets.

Description

加熱式たばこ及び電気加熱型たばこ吸引システムHeated tobacco and electrically heated tobacco smoking systems

 本発明は、加熱式たばこ及び電気加熱型たばこ吸引システムに関する。 The present invention relates to heated tobacco products and electrically heated tobacco smoking systems.

 たばこ原料(例えば、たばこ刻み、たばこ顆粒、たばこシートの成形体等)及びエアロゾル生成基材(グリセリン、プロピレングリコール等)を含むたばこ充填材を巻紙の内側に充填して形成されたたばこロッドを有する加熱式たばこが知られている(例えば、特許文献1を参照)。この種の加熱式たばこは、加熱装置における電気ヒーターによってたばこ充填材を燃焼させることなく加熱し、たばこ充填材において生成されたエアロゾルを使用者にデリバリーするタイプのたばこ物品である。 Heated tobacco products are known that have a tobacco rod formed by filling the inside of a cigarette paper with a tobacco filler material containing tobacco raw materials (e.g., tobacco shreds, tobacco granules, molded tobacco sheets, etc.) and an aerosol-generating base material (glycerin, propylene glycol, etc.) (see, for example, Patent Document 1). This type of heated tobacco product is a type of tobacco product that heats the tobacco filler material without burning it using an electric heater in a heating device, and delivers the aerosol generated in the tobacco filler material to the user.

 また、特許文献2には、非燃焼加熱式香味吸引物品の性能を向上させることを目的として、香味生成セグメントにたばこ葉、たばこシート、たばこ顆粒等が充填された製品が記載されている。 Furthermore, Patent Document 2 describes a product in which tobacco leaves, tobacco sheets, tobacco granules, etc. are filled into the flavor generating segment with the aim of improving the performance of non-combustion heating-type flavor inhalation articles.

特表2015-503335号公報Special Publication No. 2015-503335 国際公開第2022/210885号International Publication No. 2022/210885

 特許文献2に開示されているように、加熱式たばこ及び電気加熱型たばこ吸引システムにおいて、使用者の吸い応えをより向上させるため、従来香味生成セグメント中の充填物に関する検討がなされてきた。
 しかしながら、従来技術では、使用者が吸引するエアロゾル、香味成分、たばこ成分などのデリバリー量(以下、単に「デリバリー量」とも言う)を増加させるためにたばこ成分の充填量を増加させると、吸い始め初期のデリバリー量(初期パフ)がかえって減少するなど、最適なデリバリー調整は容易ではなかった。
As disclosed in Patent Document 2, in heated tobacco products and electrically heated tobacco smoking systems, studies have been conducted on the filler in the flavor generating segment in order to further improve the smoking experience for users.
However, in conventional technology, if the amount of tobacco components filled in was increased to increase the delivery amount (hereinafter simply referred to as the "delivery amount") of aerosol, flavor components, tobacco components, etc. inhaled by the user, the delivery amount at the beginning of smoking (initial puff) would actually decrease, making it difficult to adjust the delivery optimally.

 本発明者らは、上記課題を解決するために鋭意検討した結果、加熱式たばこの香味生成セグメント中のたばこシートのシート間に顆粒を配置することで、デリバリー量の調整や、デリバリー効率の向上が可能な事を見出した。 As a result of extensive research into solving the above problems, the inventors discovered that by placing granules between the tobacco sheets in the flavor generation segment of a heated tobacco product, it is possible to adjust the delivery amount and improve delivery efficiency.

 すなわち、本発明の要旨は以下の通りである。
[1]香味生成セグメントを備える加熱式たばこであって、
 前記香味生成セグメントが、たばこシート及び顆粒を含み、
 前記顆粒が、前記たばこシートのシート間に配置されている、
 加熱式たばこ。
[2]前記たばこシートが、クリンプ加工した後にギャザー充填させたものであり、前記顆粒がギャザー充填されたたばこシート間に挟持される、[1]に記載の加熱式たばこ。
[3]前記顆粒の熱伝導率が、0.10W/mK~250W/mKである、[1]又は[2]に記載の加熱式たばこ。
[4]前記顆粒が、香料を含有する、[1]~[3]のいずれかに記載の加熱式たばこ。
[5]前記顆粒が、たばこ香味成分を含有する、[1]~[4]のいずれかに記載の加熱式たばこ。
[6]前記顆粒が、ニコチンを含有する、[1]~[5]のいずれかに記載の加熱式たばこ。
[7]前記香味生成セグメント中の前記たばこシートの充填密度が、0.33g/cm~0.76g/cmである、[1]~[6]のいずれかに記載の加熱式たばこ。
[8]前記香味生成セグメント中の前記顆粒の充填密度が、0.04g/cm~0.22g/cmである、[1]~[7]のいずれかに記載の加熱式たばこ。
[9]前記香味生成セグメント中の前記たばこシートと前記顆粒との質量比が、60/40~95/5である、[1]~[8]のいずれかに記載の加熱式たばこ。
[10]前記顆粒の平均粒子径が、250μm~1000μmである、[1]~[9]のいずれかに記載の加熱式たばこ。
[11]前記加熱式たばこが、非燃焼加熱式たばこである、[1]~「10」のいずれかに記載の加熱式たばこ。
[12][1]~[11]のいずれかに記載の加熱式たばこと、前記加熱式たばこを加熱する電気加熱型デバイスと、を備える電気加熱型たばこ吸引システム
That is, the gist of the present invention is as follows.
[1] A heated tobacco product comprising a flavor generating segment,
the flavor-generating segment comprises tobacco sheets and granules;
The granules are disposed between the sheets of the tobacco sheet.
Heated tobacco.
[2] The heated tobacco product according to [1], wherein the tobacco sheets are gathered and filled after being crimped, and the granules are sandwiched between the gathered and filled tobacco sheets.
[3] The heated tobacco product according to [1] or [2], wherein the thermal conductivity of the granules is 0.10 W/mK to 250 W/mK.
[4] The heated tobacco product according to any one of [1] to [3], wherein the granules contain a flavoring.
[5] The heated tobacco product according to any one of [1] to [4], wherein the granules contain a tobacco flavor component.
[6] The heated tobacco product according to any one of [1] to [5], wherein the granules contain nicotine.
[7] The heat-not-burn tobacco according to any one of [1] to [6], wherein the packing density of the tobacco sheet in the flavor generation segment is 0.33 g/cm 3 to 0.76 g/cm 3 .
[8] The heated tobacco product according to any one of [1] to [7], wherein the packing density of the granules in the flavor generating segment is 0.04 g/cm 3 to 0.22 g/cm 3 .
[9] The heated tobacco product according to any one of [1] to [8], wherein the mass ratio of the tobacco sheet to the granules in the flavor generating segment is 60/40 to 95/5.
[10] The heated tobacco product according to any one of [1] to [9], wherein the average particle size of the granules is 250 μm to 1000 μm.
[11] The heated tobacco product according to any one of [1] to [10], wherein the heated tobacco product is a non-combustion heated tobacco product.
[12] An electrically heated tobacco smoking system comprising the heated tobacco product according to any one of [1] to [11] and an electrically heated device that heats the heated tobacco product.

 本発明によれば、加熱式たばこ及び電気加熱型たばこ吸引システムにおけるデリバリー量の調整や、デリバリー効率の向上が可能となる。 The present invention makes it possible to adjust the delivery amount and improve delivery efficiency in heated tobacco and electrically heated tobacco smoking systems.

本発明の実施形態に係る加熱式たばこの概略図である。1 is a schematic diagram of a heated tobacco product according to an embodiment of the present invention. 本発明の実施形態に係る加熱式たばこの断面模式図である。1 is a cross-sectional view of a heated tobacco product according to an embodiment of the present invention. 本発明の実施形態に係る電気加熱型たばこ吸引システムの概略図である。1 is a schematic diagram of an electrically heated tobacco smoking system according to an embodiment of the present invention; 電気加熱型デバイスにおける加熱領域周辺の構成を説明するための図である。FIG. 2 is a diagram for explaining the configuration of the periphery of a heating region in an electrically heated device. 制御部の構成を説明するための図である。FIG. 2 is a diagram illustrating the configuration of a control unit. 本発明の実施形態に係る加熱式たばこの香味生成セグメントの断面模式図である。1 is a cross-sectional schematic diagram of a flavor generation segment of a heated tobacco product according to an embodiment of the present invention. 実施例及び比較例の結果を示す図である。FIG. 1 is a diagram showing the results of an example and a comparative example. 実施例及び比較例の結果を示す図である。FIG. 1 is a diagram showing the results of an example and a comparative example.

 以下に本発明の実施の形態を詳細に説明するが、これらの説明は本発明の実施形態の一例(代表例)であり、本発明はその要旨を超えない限りこれらの内容に限定されない。
 本明細書において、「~」を用いて表される数値範囲は、「~」の前後に記載された数値を下限値及び上限値として含む範囲を意味し、「A~B」は、A以上B以下であることを意味する。
 また、本明細書において「A又はB」の表現は、「A及びBからなる群から選択される少なくとも1つ」と読み替えてもよい。
 また、本明細書では複数の実施形態を説明するが、適用できる範囲で各実施形態における種々の条件を互いに適用し得る。
 また、図面における各図について、X方向、Y方向、及びZ方向が示されているものがあるが、加熱式たばこ又は加熱式たばこが挿入される電気加熱型デバイスの左右方向をX方向、上下方向をY方向、奥行き方向をZ方向として示している。これらの方向は、説明の便宜上、例示したものに過ぎず、図中の各要素を限定するものではない。例えば、電気加熱型たばこ吸引システムの各要素は、図に示す方向に配置されることに限定されるものではない。
The following describes in detail the embodiments of the present invention, but these descriptions are merely examples (typical examples) of the embodiments of the present invention, and the present invention is not limited to these contents as long as it does not deviate from the gist of the invention.
In this specification, a numerical range expressed using "to" means a range that includes the numerical values written before and after "to" as the lower and upper limits, and "A to B" means A or more and B or less.
In addition, in this specification, the expression "A or B" may be read as "at least one selected from the group consisting of A and B."
Furthermore, although a number of embodiments are described in this specification, various conditions in each embodiment may be applied to each other to the extent that they are applicable.
Furthermore, while the X, Y, and Z directions are shown in the drawings, the left-right direction of the heated tobacco product or the electrically heated device into which the heated tobacco product is inserted is shown as the X direction, the up-down direction as the Y direction, and the depth direction as the Z direction. These directions are merely examples for the sake of convenience and do not limit the elements in the drawings. For example, the elements of the electrically heated tobacco product system are not limited to being arranged in the directions shown in the drawings.

 以下、図を参照しながら本実施形態に係る加熱式たばこを説明するが、本実施形態はこの態様に限定されない。
 なお、本明細書では図を用いて各実施形態等を説明することがあるが、各実施形態の説明や図に記載される構成要素の寸法、材質、形状、及びその相対位置等は一例である。
The heated tobacco product according to this embodiment will be described below with reference to the drawings, but this embodiment is not limited to this form.
Although this specification may use drawings to explain each embodiment, the dimensions, materials, shapes, and relative positions of the components described in the drawings and explanations of each embodiment are merely examples.

<加熱式たばこ>
 本発明の一実施形態に係る加熱式たばこは、香味生成セグメントを備える加熱式たばこであって、前記香味生成セグメントが、たばこシート及び顆粒を含み、前記顆粒が、前記たばこシートのシート間に配置されている、加熱式たばこである。加熱式たばこは、非燃焼加熱式たばこであってもよい。
<Heated tobacco>
A heated tobacco according to one embodiment of the present invention is a heated tobacco comprising a flavor generation segment, the flavor generation segment including a tobacco sheet and granules, the granules being disposed between the tobacco sheets. The heated tobacco may be a non-combustible heated tobacco.

 本実施形態に係る加熱式たばこ100の一例は、略円筒形のロッド形態である。図1及び図2に示す例において、加熱式たばこ100は、香味生成セグメント110と、冷却部120と、フィルター部130と、これらを一体に連結するチップペーパー140を含む。冷却部120とフィルター部130は、香味生成セグメント110と共にチップペーパー140によって巻装されることによって香味生成セグメント110と同軸に連結されている。 An example of the heated tobacco product 100 according to this embodiment is in the form of a substantially cylindrical rod. In the example shown in Figures 1 and 2, the heated tobacco product 100 includes a flavor generation segment 110, a cooling section 120, a filter section 130, and tipping paper 140 that connects these together. The cooling section 120 and the filter section 130 are connected coaxially to the flavor generation segment 110 by being wrapped around them by the tipping paper 140.

 符号101は、加熱式たばこ100(フィルター部130)の吸い口端である。符号102は、加熱式たばこ100における吸い口端101とは反対側の先端である。香味生成セグメント110は、加熱式たばこ100における先端102側に配置されている。図1及び図2に示す例では、加熱式たばこ100は吸い口端101から先端102に沿った長手方向(以下、軸方向又はZ方向とも称す)の全長に亘って略一定の直径を有している。 Reference numeral 101 denotes the mouth end of the heated tobacco product 100 (filter portion 130). Reference numeral 102 denotes the tip of the heated tobacco product 100 opposite the mouth end 101. The flavor generation segment 110 is located on the tip 102 side of the heated tobacco product 100. In the example shown in Figures 1 and 2, the heated tobacco product 100 has a substantially constant diameter over its entire length in the longitudinal direction (hereinafter also referred to as the axial direction or Z direction) from the mouth end 101 along the tip 102.

 加熱式たばこ100の構成は、特段制限されず、一般的な態様とすることができる。図1に示す態様では、香味生成セグメント110と、冷却部120と、フィルター部130がそれぞれ単一のセグメントとして図示されているが、各部はそれぞれ単一又は複数のセグメントで構成されていてもよい。 The configuration of the heated tobacco product 100 is not particularly limited and can be any general configuration. In the configuration shown in Figure 1, the flavor generation segment 110, cooling section 120, and filter section 130 are each illustrated as a single segment, but each section may be composed of a single segment or multiple segments.

<香味生成セグメント>
 本発明の一実施形態に係る香味生成セグメント110は、たばこシート及び顆粒を含み、前記顆粒が、前記たばこシートのシート間に配置されている限り特段制限されない。
 一例としては、香味生成セグメント110に充填された、たばこシートや顆粒等からなるたばこ充填物111(以下、香味生成セグメント110に充填される、たばこシート及び顆粒を含む充填物を総称して単に「たばこ充填物」と呼称することがある。)が、巻紙112により巻装されたものを用いることができる。
<Flavor generation segment>
The flavor generating segment 110 according to one embodiment of the present invention is not particularly limited as long as it includes a tobacco sheet and granules, and the granules are disposed between the tobacco sheets.
As an example, a tobacco filler 111 consisting of tobacco sheets, granules, etc. (hereinafter, the filler including tobacco sheets and granules filled in the flavor generation segment 110 may be collectively referred to simply as "tobacco filler") may be used, which is filled into the flavor generation segment 110 and wrapped in cigarette paper 112.

 また、香味生成セグメント110は、加熱式たばこ100を加熱するためのヒーター部材等との嵌合部を有していてもよい。
 香味生成セグメント110は、柱状形状を有していることが好ましく、この場合には、香味生成セグメント110の底面の幅に対する香味生成セグメント110の長軸方向の高さで表されるアスペクト比が1以上であることが好ましい。
 香味生成セグメント110の底面の形状は限定されず、多角、角丸多角、円、又は楕円等であってよく、幅は当該底面が円形の場合は直径、楕円形である場合は長径、多角形又は角丸多角である場合は外接円の直径又は外接楕円の長径である。香味生成セグメント110の高さは10~70mm程度、幅は4~9mm程度であることが好ましい。
The flavor generation segment 110 may also have a fitting portion for fitting with a heater member or the like for heating the heated tobacco product 100 .
It is preferable that the flavor generation segment 110 has a columnar shape, and in this case, it is preferable that the aspect ratio, which is represented by the height of the flavor generation segment 110 in the long axis direction relative to the width of the base of the flavor generation segment 110, is 1 or more.
The shape of the bottom of the flavor generation segment 110 is not limited and may be polygonal, rounded polygonal, circular, elliptical, or the like, and the width is the diameter when the bottom is circular, the major axis when the bottom is elliptical, and the diameter of the circumscribed circle or the major axis of the circumscribed ellipse when the bottom is polygonal or rounded polygonal. The height of the flavor generation segment 110 is preferably about 10 to 70 mm, and the width is preferably about 4 to 9 mm.

 香味生成セグメント110の長軸方向の長さは、製品のサイズに合わせて適宜変更し得るが、通常10mm以上であり、12mm以上であることが好ましく、15mm以上であることがより好ましく、18mm以上であることがさらに好ましく、また、通常70mm以下であり、50mm以下であることが好ましく、30mm以下であることがより好ましく、25mm以下であることがさらに好ましい。また、香味生成セグメント110の長軸方向の長さhに対する香味生成セグメント110の長さの割合は、香味のデリバリー量とエアロゾル温度のバランスの観点から、通常10%以上であり、20%以上であることが好ましく、25%以上であることがより好ましく、30%以上であることがさらに好ましく、また、通常60%以下であり、50%以下であることが好ましく、45%以下であることがより好ましく、40%以下であることがさらに好ましい。 The length of the flavor generating segment 110 in the longitudinal direction can be adjusted appropriately to suit the size of the product, but is typically 10 mm or more, preferably 12 mm or more, more preferably 15 mm or more, and even more preferably 18 mm or more. It is typically 70 mm or less, preferably 50 mm or less, more preferably 30 mm or less, and even more preferably 25 mm or less. Furthermore, from the viewpoint of the balance between the amount of flavor delivered and the aerosol temperature, the ratio of the length of the flavor generating segment 110 to its longitudinal length h is typically 10% or more, preferably 20% or more, more preferably 25% or more, and even more preferably 30% or more. It is typically 60% or less, preferably 50% or less, more preferably 45% or less, and even more preferably 40% or less.

<たばこシート>
 たばこシートは、再構成たばこシートや、乾燥したたばこ葉を平均粒径が20μm以上、200μm以下になるように粉砕してたばこ粉砕物とし、これを均一化したものをシート加工したもの(以下、単に均一化シートともいう)を刻んだものであってもよい。さらに、香味生成セグメント110の長手方向と同程度の長さを有する均一化シートを、香味生成セグメント110の長手方向と略水平に刻んだものを香味生成セグメント110に充填する、いわゆるストランドタイプであってもよい。また、香味生成セグメント110に含まれる乾燥たばこ葉の含有量は、特段制限されないが、200mg以上、800mg以下を挙げることができ、250mg以上、600mg以下が好ましい。この範囲は、特に、円周22mm、長さ20mmの香味生成セグメント110において好適である。
<Tobacco Sheet>
The tobacco sheet may be a reconstituted tobacco sheet, or a sheet (hereinafter simply referred to as a homogenized sheet) made by grinding dried tobacco leaves to an average particle size of 20 μm or more and 200 μm or less to obtain tobacco pulverized material, which is then homogenized and processed into a sheet. Furthermore, the homogenized sheet may be a strand type, in which a homogenized sheet having a length approximately the same as the longitudinal direction of the flavor generation segment 110 is shredded approximately parallel to the longitudinal direction of the flavor generation segment 110 and filled into the flavor generation segment 110. The content of dried tobacco leaves contained in the flavor generation segment 110 is not particularly limited, but may be 200 mg or more and 800 mg or less, with 250 mg or more and 600 mg or less being preferred. This range is particularly suitable for a flavor generation segment 110 having a circumference of 22 mm and a length of 20 mm.

 たばこシートを香味生成セグメント110内に充填する方法は特に限定されないが、例えばたばこシートを巻紙112で包んでもよく、筒状に形成された巻紙112にたばこシートを充填してもよい。香味生成セグメント110の形状が長手方向を有する略直方体状である場合、香味生成セグメント110は長手方向が巻紙112内でそれぞれ不特定の方向となるように充填されていてもよく、香味生成セグメント110の軸方向又は該軸方向に対して垂直な方向となるように整列させて充填されていてもよい。また、例えば、たばこシートを0.5mm以上、2.0mm以下の幅に刻んだもの(長さは、例えば5mm以上、40mm以下)をランダム配向で充填させてもよく、また、たばこシートを1.0mm以上、3.0mm以下の幅に刻んだもの(長さは、例えば5mm以上、40mm以下)を通気方向に並行に整列して充填させてもよく、また、たばこシートをクリンプ加工(縦目にスジを付ける加工)した後でギャザー充填させてもよい。香味生成セグメント110が加熱されることにより、香味生成セグメント110に含まれるたばこ成分が気化し、吸引によりこれらは冷却部120、フィルター部130へと移行する。 The method for filling the flavor generation segment 110 with tobacco sheets is not particularly limited. For example, the tobacco sheets may be wrapped in cigarette paper 112, or the tobacco sheets may be filled into a cylindrical cigarette paper 112. When the flavor generation segment 110 is shaped like a rectangular parallelepiped with a longitudinal direction, the flavor generation segments 110 may be filled so that their longitudinal directions are in an unspecified direction within the cigarette paper 112, or they may be filled aligned along the axial direction of the flavor generation segment 110 or perpendicular to the axial direction. Furthermore, for example, tobacco sheets cut into widths of 0.5 mm to 2.0 mm (lengths, for example, 5 mm to 40 mm) may be filled in a random orientation, or tobacco sheets cut into widths of 1.0 mm to 3.0 mm (lengths, for example, 5 mm to 40 mm) may be filled aligned parallel to the air passage direction, or the tobacco sheets may be crimped (processed to create vertical grain) and then gathered. When the flavor generation segment 110 is heated, the tobacco components contained in the flavor generation segment 110 vaporize, and these are transferred to the cooling section 120 and filter section 130 by suction.

 特に、たばこシートはクリンプ加工した後にギャザー充填(縦方向に空気が流通する複数のチャネルを設ける態様)させることが好ましい。このような態様とすることで、後述する顆粒をたばこシート間に配置させやすくなる。また、通気方向の空気流路が確保されることで、香味成分を使用者に効率的にデリバリーすることができる。
 また、たばこシートは渦巻き状に充填させてもよい。
In particular, it is preferable to perform gather filling (a mode in which multiple channels for vertical air flow are provided) on the tobacco sheet after crimping. This mode makes it easier to arrange the granules described below between the tobacco sheets. Furthermore, by ensuring air flow paths in the ventilation direction, flavor components can be efficiently delivered to the user.
The tobacco sheet may also be packed in a spiral shape.

 香味生成セグメント110に中に充填されるたばこシートの充填量は、香味生成セグメント110のサイズや形状にもよるが、一例として、香味生成セグメント110が長軸長さ12mm×直径7mmのロッド形状の場合、通常150mg~350mg、好ましくは200mg~250mgである。
 香味生成セグメント110中のたばこシートの充填密度は、好ましくは0.33g/cm~0.76g/cm、より好ましくは0.43g/cm~0.54g/cmである。たばこシートの充填密度が上記範囲内であると、たばこ成分の総充填量を抑えつつ十分なデリバリーを確保することができ、デリバリー効率に優れる。
The amount of tobacco sheet filled into the flavor generation segment 110 depends on the size and shape of the flavor generation segment 110, but as an example, if the flavor generation segment 110 is rod-shaped with a major axis length of 12 mm and a diameter of 7 mm, it is typically 150 mg to 350 mg, preferably 200 mg to 250 mg.
The packing density of the tobacco sheet in the flavor generation segment 110 is preferably 0.33 g/cm 3 to 0.76 g/cm 3 , and more preferably 0.43 g/cm 3 to 0.54 g/cm 3. When the packing density of the tobacco sheet is within the above range, sufficient delivery can be ensured while suppressing the total packing amount of tobacco components, resulting in excellent delivery efficiency.

<顆粒>
 本実施形態に係る顆粒は、たばこシートのシート間に配置され、たばこシートと共に香味生成セグメント110に充填されている。特に、クリンプ加工した後にギャザー充填されたたばこシート間に顆粒が挟持される態様であることが好ましい。このような態様とすることで、顆粒がシート間から脱落しづらくなり好ましい。また、たばこ充填物の表面積や通気方向の空気流路を確保しやすくなる。
 顆粒は均一にシート間に挟持されて存在してもよく、不均一にシート間に挟持されてもよいが、デリバリーの観点から可能な限り均一に配置されることが好ましい。言い換えると、顆粒とたばこシートとの接触点が可能な限り多くなるように顆粒を分布させることが好ましい。また、たばこシートを香味生成セグメント110に充填した後に、たばこシートのシート間に顆粒を充填してもよい。
 顆粒は、シートに接着されていてもよい。また、香味生成セグメント110をロッド状に成型する際に顆粒が零れ落ちない程度に保持されていてもよい。シートと顆粒とを接着する接着剤としては、酢酸ビニル系糊剤や、一般的にたばこシートで用いられる成分、例えば、バインダーグアーガム、キサンタンガム、CMC(カルボキシメチルセルロース)、CMC-Na(カルボキシメチルセルロースのナトリウム塩)からなる群から選ばれる少なくとも一種の接着剤であってよい。保持剤としては、エアロゾル源が挙げられ、例えば、グリセリン、プロピレングリコール、トリアセチン、1,3-ブタンジオール、及びこれらの混合物からなる群から選ばれる少なくとも一種の保持剤であってよい。
<Granules>
The granules according to this embodiment are disposed between the tobacco sheets and filled into the flavor generating segment 110 together with the tobacco sheets. In particular, it is preferable that the granules are sandwiched between the tobacco sheets that have been gathered and filled after crimping. This is preferable because it makes it difficult for the granules to fall out from between the sheets. It also makes it easier to ensure the surface area of the tobacco filler and the air flow path in the ventilation direction.
The granules may be evenly or unevenly sandwiched between the sheets, but from the viewpoint of delivery, it is preferable that they be disposed as evenly as possible. In other words, it is preferable that the granules be distributed so that there are as many contact points between the granules and the tobacco sheet as possible. Alternatively, the granules may be filled between the tobacco sheets after the tobacco sheets have been filled into the flavor generation segment 110.
The granules may be adhered to the sheet. Alternatively, the granules may be held in place to prevent spillage when the flavor generating segment 110 is molded into a rod shape. The adhesive for adhering the sheet and the granules may be at least one adhesive selected from the group consisting of a vinyl acetate glue or components commonly used in tobacco sheets, such as binders guar gum, xanthan gum, CMC (carboxymethylcellulose), and CMC-Na (sodium salt of carboxymethylcellulose). The retention agent may be an aerosol source, such as at least one retention agent selected from the group consisting of glycerin, propylene glycol, triacetin, 1,3-butanediol, and mixtures thereof.

 デリバリーの持続性を高めるためには、たばこシート等の、たばこ成分を含む充填物の充填量を増やすことが通常である。一方、充填物を増やしすぎると、デリバリー効率の低下や、吸い始めのデリバリー量(初期パフ)が低下する懸念がある。本実施形態のように、顆粒がたばこシートのシート間に配置されると、たばこ充填物の表面積が大きくなることで、十分な持続性を確保しつつ、デリバリー効率や初期パフを向上させることができる。また、顆粒を通じてシート間の熱伝導性を向上させることができる。さらに、シート同士が密着しづらくなることで、シート間に十分な空気を流すことが可能となり、デリバリー効率を向上させることができる。 In order to improve the durability of delivery, it is common to increase the amount of filler containing tobacco components, such as tobacco sheets. However, if the filler is increased too much, there is a concern that delivery efficiency will decrease and the amount of delivery at the beginning of smoking (initial puff) will decrease. When granules are placed between the sheets of tobacco sheets, as in this embodiment, the surface area of the tobacco filler increases, thereby improving delivery efficiency and initial puffs while ensuring sufficient durability. In addition, the granules can improve thermal conductivity between the sheets. Furthermore, by making it less likely for the sheets to adhere to each other, it becomes possible for sufficient air to flow between the sheets, improving delivery efficiency.

 図6は、本発明の一実施形態に係る香味生成セグメントの長手方向に垂直な断面模式図である。
 図6において、巻紙61で巻装された香味生成セグメント内には、たばこシート62が折り畳まれた形で充填されており、たばこシート62の間に顆粒63が充填されている。なお顆粒63は、たばこシート62に挟持される形で充填されていてもよい。
FIG. 6 is a schematic cross-sectional view perpendicular to the longitudinal direction of a flavor generating segment according to one embodiment of the present invention.
In Fig. 6, a flavor generating segment wrapped in cigarette paper 61 is filled with a folded tobacco sheet 62, and granules 63 are filled between the tobacco sheets 62. The granules 63 may also be filled in a manner that they are sandwiched between the tobacco sheets 62.

 顆粒のベース基材は特に限定されないが、炭酸カルシウム、活性炭、及び結晶セルロースからなる群から選択される少なくとも一種を含むことが熱伝導率の観点から好ましい。これらのベース基材を公知の方法で顆粒形状に成型することができる。 The base material of the granules is not particularly limited, but from the perspective of thermal conductivity, it is preferable that it contains at least one selected from the group consisting of calcium carbonate, activated carbon, and crystalline cellulose. These base materials can be molded into a granular shape using known methods.

 顆粒の熱伝導率は、好ましくは0.10W/mK~250W/mK、より好ましくは1.0W/mK~5.0W/mKである。顆粒の熱伝導率が上記範囲内であると、香味生成セグメント110全体を効率的に加熱することができ好ましい。 The thermal conductivity of the granules is preferably 0.10 W/mK to 250 W/mK, and more preferably 1.0 W/mK to 5.0 W/mK. It is preferable for the thermal conductivity of the granules to be within the above range, as this allows for efficient heating of the entire flavor generation segment 110.

 顆粒は、上記ベース基材と共に他の成分を含有させることで、種々の機能を付与することができる。
 他の成分の例としては、香料、たばこ香味成分、及びニコチンからなる群から選択される少なくとも一種が挙げられる。
 これらの成分が顆粒に担持された状態で香味生成セグメント110に充填することが、成分保持性の観点から好ましい。
 他の成分を顆粒に含有させる方法としては、ベース基材と他の成分とを混合した後顆粒形状に成型する方法が挙げられる。
The granules can be given various functions by containing other components in addition to the base material.
Examples of the other components include at least one selected from the group consisting of flavorings, tobacco flavoring components, and nicotine.
It is preferable to fill the flavor generating segment 110 with these ingredients supported on granules from the viewpoint of ingredient retention.
As a method for incorporating other components into the granules, a method in which the base material and other components are mixed and then molded into a granular shape can be mentioned.

 当該香料の種類は、特に限定されず、良好な香味の付与の観点から、アセトアニソール、アセトフェノン、アセチルピラジン、2-アセチルチアゾール、アルファルファエキストラクト、アミルアルコール、酪酸アミル、トランス-アネトール、スターアニス油、リンゴ果汁、ペルーバルサム油、ミツロウアブソリュート、ベンズアルデヒド、ベンゾインレジノイド、ベンジルアルコール、安息香酸ベンジル、フェニル酢酸ベンジル、プロピオン酸ベンジル、2,3-ブタンジオン、2-ブタノール、酪酸ブチル、酪酸、カラメル、カルダモン油、キャロブアブソリュート、β-カロテン、ニンジンジュース、L-カルボン、β-カリオフィレン、カシア樹皮油、シダーウッド油、セロリーシード油、カモミル油、シンナムアルデヒド、ケイ皮酸、シンナミルアルコール、ケイ皮酸シンナミル、シトロネラ油、DL-シトロネロール、クラリセージエキストラクト、ココア、コーヒー、コニャック油、コリアンダー油、クミンアルデヒド、ダバナ油、δ-デカラクトン、γ-デカラクトン、デカン酸、ディルハーブ油、3,4-ジメチル-1,2-シクロペンタンジオン、4,5-ジメチル-3-ヒドロキシ-2,5-ジヒドロフラン-2-オン、3,7-ジメチル-6-オクテン酸、2,3-ジメチルピラジン、2,5-ジメチルピラジン、2,6-ジメチルピラジン、2-メチル酪酸エチル、酢酸エチル、酪酸エチル、ヘキサン酸エチル、イソ吉草酸エチル、乳酸エチル、ラウリン酸エチル、レブリン酸エチル、エチルマルトール、オクタン酸エチル、オレイン酸エチル、パルミチン酸エチル、フェニル酢酸エチル、プロピオン酸エチル、ステアリン酸エチル、吉草酸エチル、エチルバニリン、エチルバニリングルコシド、2-エチル-3,(5又は6)-ジメチルピラジン、5-エチル-3-ヒドロキシ-4-メチル-2(5H)-フラノン、2-エチル-3-メチルピラジン、ユーカリプトール、フェネグリークアブソリュート、ジェネアブソリュート、リンドウ根インフュージョン、ゲラニオール、酢酸ゲラニル、ブドウ果汁、グアヤコール、グァバエキストラクト、γ-ヘプタラクトン、γ-ヘキサラクトン、ヘキサン酸、シス-3-ヘキセン-1-オール、酢酸ヘキシル、ヘキシルアルコール、フェニル酢酸ヘキシル、ハチミツ、4-ヒドロキシ-3-ペンテン酸ラクトン、4-ヒドロキシ-4-(3-ヒドロキシ-1-ブテニル)-3,5,5-トリメチル-2-シクロヘキセン-1-オン、4-(パラ-ヒドロキシフェニル)-2-ブタノン、4-ヒドロキシウンデカン酸ナトリウム、インモルテルアブソリュート、β-イオノン、酢酸イソアミル、酪酸イソアミル、フェニル酢酸イソアミル、酢酸イソブチル、フェニル酢酸イソブチル、ジャスミンアブソリュート、コーラナッツティンクチャー、ラブダナム油、レモンテルペンレス油、カンゾウエキストラクト、リナロール、酢酸リナリル、ロベージ根油、マルトール、メープルシロップ、メンソール、メントン、酢酸L-メンチル、パラメトキシベンズアルデヒド、メチル-2-ピロリルケトン、アントラニル酸メチル、フェニル酢酸メチル、サリチル酸メチル、4’-メチルアセトフェノン、メチルシクロペンテノロン、3-メチル吉草酸、ミモザアブソリュート、トウミツ、ミリスチン酸、ネロール、ネロリドール、γ-ノナラクトン、ナツメグ油、δ-オクタラクトン、オクタナール、オクタン酸、オレンジフラワー油、オレンジ油、オリス根油、パルミチン酸、ω-ペンタデカラクトン、ペパーミント油、プチグレインパラグアイ油、フェネチルアルコール、フェニル酢酸フェネチル、フェニル酢酸、ピペロナール、プラムエキストラクト、プロペニルグアエトール、酢酸プロピル、3-プロピリデンフタリド、プルーン果汁、ピルビン酸、レーズンエキストラクト、ローズ油、ラム酒、セージ油、サンダルウッド油、スペアミント油、スチラックスアブソリュート、マリーゴールド油、ティーディスティレート、α-テルピネオール、酢酸テルピニル、5,6,7,8-テトラヒドロキノキサリン、1,5,5,9-テトラメチル-13-オキサシクロ(8.3.0.0(4.9))トリデカン、2,3,5,6-テトラメチルピラジン、タイム油、トマトエキストラクト、2-トリデカノン、クエン酸トリエチル、4-(2,6,6-トリメチル-1-シクロヘキセニル)2-ブテン-4-オン、2,6,6-トリメチル-2-シクロヘキセン-1,4-ジオン、4-(2,6,6-トリメチル-1,3-シクロヘキサジエニル)2-ブテン-4-オン、2,3,5-トリメチルピラジン、γ-ウンデカラクトン、γ-バレロラクトン、バニラエキストラクト、バニリン、ベラトルアルデヒド、バイオレットリーフアブソリュート、N-エチル-p-メンタン-3-カルボアミド(WS-3)、又はエチル-2-(p-メンタン-3-カルボキサミド)アセテート(WS-5)等が挙げられ、特に好ましくはメンソールである。また、これらの香料は1種を単独で用いても、又は2種以上を併用してもよい。
 顆粒が香料を含有することで、香気成分のデリバリーをコントロールすることができる。
The type of the flavoring is not particularly limited, and from the viewpoint of imparting a good flavor, the following may be used: acetanisole, acetophenone, acetylpyrazine, 2-acetylthiazole, alfalfa extract, amyl alcohol, amyl butyrate, trans-anethole, star anise oil, apple juice, Peru balsam oil, beeswax absolute, benzaldehyde, benzoin resinoid, benzyl alcohol, benzyl benzoate, benzyl phenylacetate, benzyl propionate, 2,3-butanedione, 2-butanol, butyl butyrate, butyric acid, caramel, cardamom oil, carob absolute, β -Carotene, carrot juice, L-carvone, β-caryophyllene, cassia bark oil, cedarwood oil, celery seed oil, chamomile oil, cinnamaldehyde, cinnamic acid, cinnamyl alcohol, cinnamyl cinnamate, citronella oil, DL-citronellol, clary sage extract, cocoa, coffee, konjac oil, coriander oil, cuminaldehyde, davana oil, δ-decalactone, γ-decalactone, decanoic acid, dill herb oil, 3,4-dimethyl-1,2-cyclopentanedione, 4,5-dimethyl-3-hydroxy-2,5-dihydrofuran-2-one, 3,7 -dimethyl-6-octenoic acid, 2,3-dimethylpyrazine, 2,5-dimethylpyrazine, 2,6-dimethylpyrazine, ethyl 2-methylbutyrate, ethyl acetate, ethyl butyrate, ethyl hexanoate, ethyl isovalerate, ethyl lactate, ethyl laurate, ethyl levulinate, ethyl maltol, ethyl octanoate, ethyl oleate, ethyl palmitate, ethyl phenylacetate, ethyl propionate, ethyl stearate, ethyl valerate, ethyl vanillin, ethyl vanillin glucoside, 2-ethyl-3,(5 or 6)-dimethylpyrazine, 5-ethyl-3-hydroxy-4-methyl-2( 5H)-Furanone, 2-ethyl-3-methylpyrazine, eucalyptol, fenugreek absolute, genet absolute, gentian root infusion, geraniol, geranyl acetate, grape juice, guaiacol, guava extract, gamma-heptalactone, gamma-hexalactone, hexanoic acid, cis-3-hexen-1-ol, hexyl acetate, hexyl alcohol, phenylhexyl acetate, honey, 4-hydroxy-3-pentenoic acid lactone, 4-hydroxy-4-(3-hydroxy-1-butenyl)-3,5,5-trimethyl-2-cyclohexen-1-one , 4-(para-hydroxyphenyl)-2-butanone, sodium 4-hydroxyundecanoate, inmortel absolute, β-ionone, isoamyl acetate, isoamyl butyrate, isoamyl phenylacetate, isobutyl acetate, isobutyl phenylacetate, jasmine absolute, cola nut tincture, labdanum oil, lemon terpeneless oil, licorice extract, linalool, linalyl acetate, lovage root oil, maltol, maple syrup, menthol, menthone, L-menthyl acetate, paramethoxybenzaldehyde, methyl-2-pyrrolyl ketone, anthranil Methyl phenylacetate, Methyl salicylate, 4'-methylacetophenone, Methylcyclopentenolone, 3-methylvaleric acid, Mimosa absolute, Honey syrup, Myristic acid, Nerol, Nerolidol, γ-nonalactone, Nutmeg oil, δ-octalactone, Octanal, Octanoic acid, Orange flower oil, Orange oil, Orris root oil, Palmitic acid, ω-pentadecalactone, Peppermint oil, Petitgrain Paraguay oil, Phenethyl alcohol, Phenethyl phenylacetate, Phenylacetic acid, Piperonal, Plum extract, Propenylguaethol, Propylene acetate Pyr, 3-propylidenephthalide, prune juice, pyruvic acid, raisin extract, rose oil, rum, sage oil, sandalwood oil, spearmint oil, styrax absolute, marigold oil, tea distillate, α-terpineol, terpinyl acetate, 5,6,7,8-tetrahydroquinoxaline, 1,5,5,9-tetramethyl-13-oxacyclo(8.3.0.0(4.9))tridecane, 2,3,5,6-tetramethylpyrazine, thyme oil, tomato extract, 2-tridecanone, triethyl citrate, 4-(2,6,6-trimethyl-1 2,6,6-trimethyl-2-cyclohexenyl)2-buten-4-one, 2,6,6-trimethyl-2-cyclohexene-1,4-dione, 4-(2,6,6-trimethyl-1,3-cyclohexadienyl)2-buten-4-one, 2,3,5-trimethylpyrazine, γ-undecalactone, γ-valerolactone, vanilla extract, vanillin, veratraldehyde, violet leaf absolute, N-ethyl-p-menthane-3-carboxamide (WS-3), or ethyl-2-(p-menthane-3-carboxamide)acetate (WS-5), with menthol being particularly preferred. These flavoring agents may be used alone or in combination of two or more.
By including a flavoring in the granules, the delivery of the flavoring component can be controlled.

 たばこ香味成分としては、たばこ刻み等のたばこ葉由来の成分が挙げられる。たばこ刻みの材料は特に限定されず、ラミナや中骨等の公知のものを用いることができる。
 顆粒がたばこ香味成分を含有することで、たばこ香味成分のデリバリーをコントロールすることができる。
Examples of tobacco flavor components include components derived from tobacco leaves such as tobacco shreds, etc. The material of the tobacco shreds is not particularly limited, and known materials such as lamina and ribs can be used.
By including tobacco flavor components in the granules, the delivery of the tobacco flavor components can be controlled.

 たばこ刻み及びたばこシートの作製に用いるたばこ葉について、使用するたばこの種類は、様々なものを用いることができる。例えば、黄色種、バーレー種、オリエント種、在来種、その他のニコチアナ-タバカム系品種、ニコチアナ-ルスチカ系品種、及びこれらの混合物を挙げることができる。混合物については、目的とする味となるように、前記の各品種を適宜ブレンドして用いることができる。前記たばこの品種の詳細は、「たばこの事典、たばこ総合研究センター、2009.3.31」に開示されている。前記均一化シートの製造方法、すなわち、たばこ葉を粉砕して均一化シートに加工する方法は従来の方法が複数存在している。1つ目は抄紙プロセスを用いて抄造シートを作製する方法である。2つ目は水等の適切な溶媒を、粉砕したたばこ葉に混ぜて均一化した後に金属製板もしくは金属製板ベルトの上に均一化物を薄くキャスティングし、乾燥させてキャストシートを作製する方法である。3つ目は水等の適切な溶媒を、粉砕したたばこ葉に混ぜて均一化したものをシート状に押し出し成型して圧延シートを作製する方法である。前記均一化シートの種類については、「たばこの事典、たばこ総合研究センター、2009.3.31」に詳細が開示されている。 Various types of tobacco can be used as the tobacco leaves used to make shredded tobacco and tobacco sheets. Examples include flue-cured tobacco, burley, oriental tobacco, native tobacco, other Nicotiana tabacum varieties, Nicotiana rustica varieties, and mixtures thereof. Mixtures can be made by blending the aforementioned varieties appropriately to achieve the desired flavor. Details of the tobacco varieties are disclosed in the "Encyclopedia of Tobacco," published by the Tobacco Research Center on March 31, 2009. There are several conventional methods for producing the homogenized sheet, i.e., grinding tobacco leaves and processing them into a homogenized sheet. The first is a method of producing a paper-making sheet using a papermaking process. The second is a method in which an appropriate solvent such as water is mixed with ground tobacco leaves to homogenize them, and then a thin layer of the homogenized material is cast onto a metal plate or metal plate belt and dried to produce a cast sheet. The third is a method in which an appropriate solvent such as water is mixed with ground tobacco leaves to homogenize them, and then the homogenized material is extruded into a sheet to produce a rolled sheet. Details of the types of homogenizing sheets are disclosed in "Encyclopedia of Tobacco," Tobacco Research Center, March 31, 2009.

 香味生成セグメント110に中に充填される顆粒の充填量は、香味生成セグメント110のサイズや形状にもよるが、一例として、香味生成セグメント110が長軸長さ12mm×直径7mmのロッド形状の場合、通常20mg~100mg、好ましくは50mg~80mgである。
 香味生成セグメント110中の顆粒の充填密度は、好ましくは0.04g/cm~0.22g/cm、より好ましくは0.11g/cm~0.17g/cmである。顆粒の充填密度が上記範囲内であると、デリバリー効率の観点から好ましい。
The amount of granules filled into the flavor generating segment 110 depends on the size and shape of the flavor generating segment 110, but as an example, if the flavor generating segment 110 is rod-shaped with a major axis length of 12 mm and a diameter of 7 mm, it is typically 20 mg to 100 mg, preferably 50 mg to 80 mg.
The packing density of the granules in the flavor generating segment 110 is preferably 0.04 g/cm 3 to 0.22 g/cm 3 , more preferably 0.11 g/cm 3 to 0.17 g/cm 3. If the packing density of the granules is within the above range, it is preferable from the viewpoint of delivery efficiency.

 また、デリバリー効率の観点から、香味生成セグメント110中に充填されるたばこシートと顆粒との質量比(たばこシートの質量/顆粒の質量)は、60/40~95/5が好ましく、70/30~80/20がより好ましい。 Furthermore, from the viewpoint of delivery efficiency, the mass ratio of the tobacco sheet to the granules filled in the flavor generation segment 110 (mass of tobacco sheet/mass of granules) is preferably 60/40 to 95/5, and more preferably 70/30 to 80/20.

 顆粒の平均粒子径は250μm~1000μmであることが好ましく、500μm~800μmがより好ましい。顆粒の平均粒子径が250μm以上であると、デリバリー効率向上の効果を十分に得ることができる。また、粒の平均粒子径が1000μm以下であると、顆粒の製造が容易である。
 顆粒の平均粒子径は、顆粒に含まれるベース基材等の量を調整することで適宜調整することができる。また、平均粒子径はマスターサイザー(malvern社製)等のレーザ回折型粒度計を用いて測定される。
The average particle size of the granules is preferably 250 μm to 1000 μm, and more preferably 500 μm to 800 μm. When the average particle size of the granules is 250 μm or more, the effect of improving delivery efficiency can be sufficiently obtained. Furthermore, when the average particle size of the granules is 1000 μm or less, the production of the granules is easy.
The average particle size of the granules can be adjusted appropriately by adjusting the amount of the base material, etc. contained in the granules. The average particle size is measured using a laser diffraction particle sizer such as Mastersizer (manufactured by Malvern).

 顆粒の組成及び製造方法は、上述の例に限定されず、例えば、以下の組成及び製造方法であってもよい。 The composition and manufacturing method of the granules are not limited to the above examples, and may be, for example, the following composition and manufacturing method.

顆粒の組成
 顆粒に含まれる成分は、(A)15~50重量%のたばこ抽出物と、(B)非木材繊維と、(C)バインダーと、(D)10~60重量%のエアロゾル基材と、を含み、前記(B)と(C)の合計が23~50重量%であってもよい。特に断りのない限り重量及び重量%は乾物重量及び乾物重量%である。乾物重量とは、水の重量を除いた重量である。
Granule Composition The components contained in the granules include (A) 15-50% by weight of tobacco extract, (B) non-wood fiber, (C) binder, and (D) 10-60% by weight of aerosol base material, and the total of (B) and (C) may be 23-50% by weight. Unless otherwise specified, weights and weight percentages are dry weights and dry weight percentages. Dry weight is the weight excluding the weight of water.

(1)成分(A):たばこ抽出物
 たばこ抽出物とは、たばこから抽出された香味を呈する物質又は混合物である。たばこ抽出物は公知の方法で準備できる。例えば、以下の方法が挙げられる。1)たばこ原料を、抽出媒体を用いた抽出に供して、たばこ抽出物を得る方法、2)たばこ原料に抽出媒体を加えて加熱し、発生した蒸気を捕集する方法、3)加熱によって蒸気とした抽出媒体をたばこ原料に通過させ、当該通過後の蒸気を捕集する方法。抽出媒体とは、水、又はアルコール等の親水性有機溶媒が挙げられる。1)の方法では作業性等の観点から抽出媒体として水を用いることが好ましい。また、2)又は3)の方法では作業効率の観点から抽出媒体としてプロピレングリコール、グリセリン、又はエタノール等のアルコールを用いることが好ましい。抽出には必要に応じて酸又はアルカリを用いることもできる。抽出によって得た、たばこ抽出物と抽出媒体を含む液体をたばこ抽出液という。
(1) Component (A): Tobacco Extract Tobacco extract is a substance or mixture that exhibits a flavor extracted from tobacco. Tobacco extract can be prepared by known methods. Examples include the following: 1) a method in which tobacco raw material is subjected to extraction using an extraction medium to obtain a tobacco extract; 2) a method in which an extraction medium is added to the tobacco raw material and heated, and the generated vapor is collected; and 3) a method in which the extraction medium is vaporized by heating and passed through the tobacco raw material, and the vapor is collected after passing. Examples of extraction media include water or hydrophilic organic solvents such as alcohol. In method 1), water is preferably used as the extraction medium from the perspective of workability. In methods 2) and 3), alcohols such as propylene glycol, glycerin, or ethanol are preferably used as the extraction medium from the perspective of work efficiency. Acids or alkalis can also be used for extraction as needed. The liquid obtained by extraction, containing the tobacco extract and extraction medium, is called a tobacco extract.

 たばこ原料としては、例えば、ニコチアナ・タバカム(Nicotiana.tabacum)やニコチアナ・ルスチカ(Nicotiana.rustica)等のタバコ属の原料を用いることができる。ニコチアナ・タバカムとしては、例えば、バーレー種又は黄色種等の品種を用いることができる。また、これ以外に、オリエント種やたばこ属の在来種バーレー種を用いてもよい。 Tobacco raw materials can be those of the Nicotiana genus, such as Nicotiana tabacum and Nicotiana rustica. Nicotiana tabacum can be of varieties such as burley or flue-cured varieties. Alternatively, varieties such as the Orient or native burley varieties of the Nicotiana genus can also be used.

 たばこ原料は、刻み又は粉粒体のたばこ原料(以下、「原料片」ともいう)であってもよい。このような場合において、原料片の粒径は、0.5~1.18mmであることが好ましい。このような原料片は、例えば、JIS Z 8801に準拠したステンレス篩を用いて、JIS Z 8815に準拠する篩分けによって得られる。例えば、1)1.18mmの目開きを有するステンレス篩を用いて、乾燥式かつ機械式振とう法によって20分間に亘って原料片を篩分けによって、1.18mmの目開きを有するステンレス篩を通過する原料片を得る。2)続いて、0.50mmの目開きを有するステンレス篩を用いて、乾燥式かつ機械式振とう法によって20分間に亘って原料片を篩分けによって、0.50mmの目開きを有するステンレス篩を通過する原料片を取り除く。このようにすることで、上限を規定するステンレス篩(目開き=1.18mm)を通過し、下限を規定するステンレス篩(目開き=0.50mm)を通過しない原料片を調製できる。 The tobacco raw material may be shredded or powdered tobacco material (hereinafter also referred to as "raw material pieces"). In such cases, the particle size of the raw material pieces is preferably 0.5 to 1.18 mm. Such raw material pieces can be obtained, for example, by sieving in accordance with JIS Z 8815 using a stainless steel sieve conforming to JIS Z 8801. For example, 1) using a stainless steel sieve with 1.18 mm openings, the raw material pieces are sieved by a dry mechanical shaking method for 20 minutes to obtain raw material pieces that pass through the stainless steel sieve with 1.18 mm openings. 2) Subsequently, using a stainless steel sieve with 0.50 mm openings, the raw material pieces are sieved by a dry mechanical shaking method for 20 minutes to remove the raw material pieces that pass through the stainless steel sieve with 0.50 mm openings. By doing this, raw material pieces can be prepared that pass through the stainless steel sieve (mesh opening = 1.18 mm) that defines the upper limit, but do not pass through the stainless steel sieve (mesh opening = 0.50 mm) that defines the lower limit.

 一態様において、たばこ原料はアルカリ処理される。当該処理を経て香味成分を発生させ、これを捕集してたばこ抽出物と水を含むたばこ抽出液を調製してもよい。この際、アルカリ処理したたばこ原料から香味成分を気体として取出し、当該気体を、水に導入して香味成分を液体に移行させることが好ましい。 In one embodiment, tobacco raw materials are treated with alkali. Flavor components are generated through this treatment, and these may be collected to prepare a tobacco extract liquid containing tobacco extract and water. In this case, it is preferable to extract the flavor components as a gas from the alkali-treated tobacco raw material, and then introduce the gas into water to convert the flavor components into a liquid.

 アルカリ物質としては、例えば、炭酸カリウム水溶液等のアルカリ性液体が好ましい。この際、アルカリ物質は、たばこ原料のpHが特定の範囲となるまで供給される。当該pHは好ましくは8.0以上、より好ましくは8.9~9.7である。たばこ原料のpHは、たばこ原料を10倍量の水と混合した際の水のpHである。 The alkaline substance is preferably an alkaline liquid such as an aqueous potassium carbonate solution. In this case, the alkaline substance is supplied until the pH of the tobacco raw material falls within a specific range. This pH is preferably 8.0 or higher, more preferably 8.9 to 9.7. The pH of the tobacco raw material is the pH of the water when the tobacco raw material is mixed with 10 times the amount of water.

 たばこ原料中の水分量は限定されないが、効率的に香味成分を抽出する観点から、その水分量は5~30重量%程度であることが好ましい。たばこ原料中の水分量は公知の方法で測定されるが、例えば、試料を1g採取し、105℃で加熱し、重量変化率が1mg/分以下になるまで加熱したときの重量減少量を水分量とする。この測定には、例えばハロゲン加熱水分計(オーハウス社製、MB45等)を用いることができる。 The moisture content of tobacco raw materials is not limited, but from the perspective of efficiently extracting flavor components, it is preferable that the moisture content be approximately 5 to 30% by weight. The moisture content of tobacco raw materials is measured by known methods; for example, a 1g sample is taken, heated at 105°C, and the moisture content is determined by the weight loss when heated until the weight change rate is 1mg/min or less. This measurement can be performed using, for example, a halogen heating moisture meter (such as the MB45 manufactured by Ohaus).

 たばこ香味成分におけるたばこ抽出物の含有量は15~50重量%であることが好ましい。当該量は適宜調整され、例えば20~40重量%とすることができる。 The tobacco extract content in the tobacco flavor component is preferably 15 to 50% by weight. This amount can be adjusted appropriately, for example, to 20 to 40% by weight.

 (2)成分(B):非木材繊維
 非木材繊維とは木材に由来しない繊維であり、たばこ繊維以外の繊維であることが好ましい。非木材繊維としては、食物繊維が好ましい。食物繊維とはヒトの消化酵素で消化されない食物成分であり、水に溶けない不溶性食物繊維であることがより好ましい。食物繊維は多孔質すなわちスポンジ状であってもよい。多孔質繊維は顆粒の表面積を増大させ、熱伝導性を向上させることができる。入手容易性等の観点から、前記繊維は好ましくはシトラスファイバーである。シトラスファイバーとは柑橘類のアルベドを主原料とする繊維である。また、食物繊維はアスペクト比の小さい短繊維又は柱状粒子であってもよい。特にシトラスファイバーは、少ない使用量でシートに強度を付与することができるので好ましい。非木材繊維中の水分量を測定し、後述する水分量の関係を満たすように非木材繊維の配合量は決定される。非木材繊維中の水分量は公知の方法で測定されるが、例えば、たばこ原料中の水分量と同じ方法で測定される。一態様において、顆粒中の成分(B)の含有量は、10~30重量%である。繊維材料としては木材繊維が知られているが、非木材繊維を用いると、木材繊維を用いた場合に比べて液体の担持能力に優れるという利点がある。したがって、非木材繊維は添加量を少なくすることができ、より香喫味に寄与する成分を多くすることが可能となる。
(2) Component (B): Non-wood fiber. Non-wood fiber is a fiber not derived from wood, preferably a fiber other than tobacco fiber. Dietary fiber is preferred as a non-wood fiber. Dietary fiber is a food component that is not digested by human digestive enzymes, and is more preferably insoluble dietary fiber that does not dissolve in water. Dietary fiber may be porous, i.e., spongy. Porous fiber can increase the surface area of granules and improve thermal conductivity. From the standpoint of availability, the fiber is preferably citrus fiber. Citrus fiber is a fiber derived primarily from the albedo of citrus fruits. Dietary fiber may also be short fibers or columnar particles with a small aspect ratio. Citrus fiber is particularly preferred because it can impart strength to the sheet with a small amount. The moisture content of the non-wood fiber is measured, and the amount of non-wood fiber blended is determined to satisfy the moisture content relationship described below. The moisture content of the non-wood fiber is measured by a known method, for example, the same method as the moisture content of tobacco raw materials. In one embodiment, the content of component (B) in the granules is 10 to 30% by weight. Although wood fiber is a well-known fiber material, the use of non-wood fiber has the advantage of being superior in liquid-carrying capacity compared to wood fiber, and therefore the amount of non-wood fiber added can be reduced, allowing for more components that contribute to flavor and taste.

 (3)成分(C):バインダー
 バインダーとしては、カルボキシアルキルセルロース又はグアーガムが挙げられる。バインダー中の水分量は公知の方法で測定されるが、例えばたばこ原料中の水分量と同じ方法で測定される。
(3) Component (C): Binder Examples of the binder include carboxyalkyl cellulose and guar gum. The moisture content of the binder is measured by a known method, for example, the same method as that for the moisture content of the tobacco raw material.

 シートにおける成分(B)と成分(C)の合計量は、23~50重量%であることが好ましい。当該量が下限値以上であると、顆粒の取扱性が良好となり、かつ顆粒の強度も十分となりやすい。また、当該量が上限値を以下であると、香味が十分となる、又は雑味が抑制される。かかる観点から、当該合計量の下限値は、好ましくは24重量%以上であり、上限値は、好ましくは40重量%以下、より好ましくは30重量%以下である。成分(B)と成分(C)のそれぞれの量は、前記合計量を満足するように決定されるが、一態様において成分(B)の量は10~30重量%又は13~25重量%であり、成分(C)の量は13~20重量%又は10~25重量%である。 The total amount of component (B) and component (C) in the sheet is preferably 23 to 50% by weight. When this amount is equal to or greater than the lower limit, the granules are easy to handle and tend to have sufficient strength. Furthermore, when this amount is equal to or less than the upper limit, the flavor is sufficient or unpleasant flavors are suppressed. From this perspective, the lower limit of this total amount is preferably 24% by weight or more, and the upper limit is preferably 40% by weight or less, more preferably 30% by weight or less. The respective amounts of component (B) and component (C) are determined so as to satisfy the above total amount, and in one embodiment, the amount of component (B) is 10 to 30% by weight or 13 to 25% by weight, and the amount of component (C) is 13 to 20% by weight or 10 to 25% by weight.

 (4)成分(D):エアロゾル基材
 エアロゾル基材としては、グリセリン又はポリエチレングリコール等の多価アルコールが挙げられる。エアロゾル基材中の水分量は公知の方法で測定されるが、例えばたばこ原料中の水分量と同じ方法で測定される。顆粒におけるエアロゾル基材の量は10~60重量%である。当該量が下限値以上であると、喫煙時の煙量が十分となる。また当該量が上限値以下であると、顆粒の取扱性が向上する。かかる観点から、当該量は好ましくは15~50重量%であり、より好ましくは20~40重量%である。
(4) Component (D): Aerosol Base Examples of the aerosol base include polyhydric alcohols such as glycerin or polyethylene glycol. The moisture content in the aerosol base is measured by a known method, for example, the same method as that for the moisture content in tobacco raw materials. The amount of aerosol base in the granules is 10 to 60% by weight. When this amount is equal to or greater than the lower limit, the amount of smoke produced during smoking is sufficient. When this amount is equal to or less than the upper limit, the handleability of the granules is improved. From this perspective, the amount is preferably 15 to 50% by weight, more preferably 20 to 40% by weight.

 (5)その他
 顆粒は、木材繊維を含有していてもよい。木材繊維としては針葉樹パルプ、Vitacel FL400、Vitacel L600/30(いずれもJ. Rettenmaier & Sohne GmbH製)が挙げられる。顆粒を製造するための混合物は、好ましくは水を含み、当該混合物における、水:水以外の成分の重量比が好ましくは(0.2~1):1である。木材繊維中の水分量を測定し、当該関係を満たすように木材繊維の配合量は決定されることが好ましい。木材繊維中の水分量は公知の方法で測定されるが、例えばたばこ原料中の水分量と同じ方法で測定される。一態様において顆粒における木材繊維の含有量は1~10重量%である。
(5) Others The granules may contain wood fibers. Examples of wood fibers include softwood pulp, Vitacel FL400, and Vitacel L600/30 (all manufactured by J. Rettenmaier & Söhne GmbH). The mixture for producing the granules preferably contains water, and the weight ratio of water to components other than water in the mixture is preferably (0.2 to 1:1). It is preferable to measure the moisture content of the wood fibers and determine the amount of wood fibers to satisfy this relationship. The moisture content of the wood fibers is measured by a known method, for example, the same method as that for the moisture content of tobacco raw materials. In one embodiment, the wood fiber content in the granules is 1 to 10% by weight.

顆粒の製造方法
 本実施形態の顆粒は、成分(A)を含むたばこ抽出液と、成分(B)と、成分(C)と、成分(D)との混合物を調製する工程1A、ならびに前記混合物を造粒する工程2A、を備える方法で製造されることが好ましい。
Granule Manufacturing Method The granules of this embodiment are preferably manufactured by a method comprising step 1A of preparing a mixture of tobacco extract containing component (A), component (B), component (C), and component (D), and step 2A of granulating the mixture.

(1)工程1A
(1-1)たばこ抽出液の調製
 本工程では、前述のたばこ原料を抽出に供して、有効成分であるたばこ抽出物と抽出媒体を含むたばこ抽出液を調製する。抽出媒体として水を用いることが好ましい。抽出温度は限定されないが、好ましくは60~100℃、喫味の観点からより好ましくは70~90℃である。抽出時間は好ましくは20~40分である。
(1) Process 1A
(1-1) Preparation of Tobacco Extract In this step, the tobacco raw material described above is subjected to extraction to prepare a tobacco extract containing the tobacco extract as an active ingredient and an extraction medium. Water is preferably used as the extraction medium. The extraction temperature is not limited, but is preferably 60 to 100°C, and more preferably 70 to 90°C from the perspective of smoking taste. The extraction time is preferably 20 to 40 minutes.

(1-2)混合
 混合は公知の方法で実施でき、例えば、各成分をミキサー等で混合することで、混合物を調製できる。混合物は水を含むことが好ましく、中の水:水以外の成分の重量比は、好ましくは(0.2~1):1である。水はたばこ抽出液に含まれる水であってもよいし、これ以外に追加された水であってもよい。特に非木材繊維の含有量を増やす場合は、水の含有量も増やすことが好ましい。
(1-2) Mixing Mixing can be carried out by known methods; for example, a mixture can be prepared by mixing the components in a mixer or the like. The mixture preferably contains water, and the weight ratio of water to components other than water is preferably (0.2 to 1:1). The water may be water contained in the tobacco extract, or may be water added separately. In particular, when the content of non-wood fibers is increased, it is preferable to also increase the content of water.

(2)工程2A
 工程2Aでは、上述の工程2と同様の方法を用いることができる。具体的には、工程2Aでは、工程1Aで得られた混合物を湿式押出し造粒機で造粒(長柱状)した後、短柱状あるいは球状に整粒する。押出し造粒に際する押出圧力は、混合物の粘度等に応じて任意に設定することができる。
(2) Process 2A
In step 2A, the same method as in step 2 described above can be used. Specifically, in step 2A, the mixture obtained in step 1A is granulated (into long columns) in a wet extrusion granulator, and then sized into short columns or spheres. The extrusion pressure during extrusion granulation can be set as desired depending on the viscosity of the mixture, etc.

 押出し造粒により得られた顆粒は、水分調整のために、必要に応じてさらに乾燥させてもよい。たとえば、押出し造粒により得られた顆粒の乾燥減量を測定し、それが、所望の乾燥減量(たとえば5重量%以上、17重量%以下)より高い場合、所望の乾燥減量を得るために顆粒をさらに乾燥させてもよい。所望の乾燥減量を得るための乾燥条件(温度及び時間)は、乾燥減量を所定の値だけ減少させるために必要な乾燥条件(温度及び時間)を予め決定し、その条件に基づいて設定することができる。 The granules obtained by extrusion granulation may be further dried, if necessary, to adjust the moisture content. For example, the loss on drying of the granules obtained by extrusion granulation may be measured, and if it is higher than the desired loss on drying (for example, 5% by weight or more and 17% by weight or less), the granules may be further dried to obtain the desired loss on drying. The drying conditions (temperature and time) required to obtain the desired loss on drying can be determined in advance and set based on the drying conditions (temperature and time) required to reduce the loss on drying by a predetermined value.

 たばこ充填物の水分含有量は、たばこ充填物の全量に対して10重量%以上、15重量%以下を挙げることができ、11重量%以上、13重量%以下であることが好ましい。このような水分含有量であると、巻染みの発生を抑制し、香味生成セグメント110の製造時の巻上適性を良好にする。たばこ充填物に含まれるたばこ刻みの大きさやその調製法については特に制限はない。例えば、乾燥したたばこ葉を、幅0.5mm以上、2.0mm以下に刻んだものを用いてもよい。また、均一化シートの粉砕物を用いる場合、乾燥したたばこ葉を平均粒径が20μm~200μm程度になるように粉砕して均一化したものをシート加工し、それを幅0.5mm以上、2.0mm以下に刻んだものを用いてもよい。 The moisture content of the tobacco filler can be 10% by weight or more and 15% by weight or less, and preferably 11% by weight or more and 13% by weight or less, based on the total amount of the tobacco filler. This moisture content suppresses the occurrence of stains on the roll and improves the suitability for rolling during the production of the flavor generating segment 110. There are no particular restrictions on the size of the tobacco shreds contained in the tobacco filler or their preparation method. For example, dried tobacco leaves shredded to a width of 0.5 mm or more and 2.0 mm or less may be used. Furthermore, when using a ground homogenized sheet, dried tobacco leaves may be ground to an average particle size of approximately 20 μm to 200 μm, homogenized, and then processed into a sheet, which may then be shredded to a width of 0.5 mm or more and 2.0 mm or less.

 また、たばこ充填物は、エアロゾル基材を含んでいてもよい。エアロゾル基材は、加熱されることによりエアロゾルを生成する基材であり、グリセリン、プロピレングリコール、トリアセチン、1,3-ブタンジオール、又はこれらの混合物が例示される。
 たばこ充填物中のエアロゾル基材の含有量は、特に限定されず、十分にエアロゾルを生成させると共に、良好な香味の付与の観点から、たばこ充填物の全量に対して通常5重量%以上であり、好ましくは10重量%以上であり、また、通常50重量%以下であり、好ましくは15重量%以上、25重量%以下である。
The tobacco filler may also contain an aerosol base, which is a base that generates an aerosol when heated, and examples of such a base include glycerin, propylene glycol, triacetin, 1,3-butanediol, and mixtures thereof.
The content of the aerosol base material in the tobacco filler is not particularly limited, but from the viewpoint of generating sufficient aerosol and imparting a good flavor, it is usually 5% by weight or more, preferably 10% by weight or more, and usually 50% by weight or less, preferably 15% by weight or more and 25% by weight or less, relative to the total amount of the tobacco filler.

 たばこ充填物は、上記顆粒に含まれるものとは別に、香料を含んでいてもよい。
 たばこ充填物中の香料の含有量は、特に限定されず、良好な香味の付与の観点から、通常10000ppm以上であり、好ましくは20000ppm以上であり、より好ましくは25000ppm以上であり、また、通常70000ppm以下であり、好ましくは50000ppm以下であり、より好ましくは40000ppm以下であり、さらに好ましくは33000ppm以下である。
The tobacco filler may contain a flavoring agent in addition to that contained in the granules.
The content of the flavoring in the tobacco filler is not particularly limited, but from the viewpoint of imparting a good flavor, it is usually 10,000 ppm or more, preferably 20,000 ppm or more, more preferably 25,000 ppm or more, and is usually 70,000 ppm or less, preferably 50,000 ppm or less, more preferably 40,000 ppm or less, and even more preferably 33,000 ppm or less.

<加熱式たばこの製造方法>
 本実施形態に係る加熱式たばこの製造方法は、特段制限されず、公知の方法を組み合わせて適用することができる。一例としては、たばこシートをローラーから押し出しながらクリンプ加工した後、該たばこシート状に顆粒を添加し、巻紙で巻き上げてロッド状の香味生成セグメント110を作製する。この際、必要に応じてグリセリンなどのエアロゾル源を添加してもよい。そして、香味生成セグメント110と、冷却部120と、フィルター部130とをチップペーパー140で巻き上げることで製造することができる。
<Method of manufacturing heated tobacco products>
The method for producing a heated tobacco product according to this embodiment is not particularly limited, and a combination of known methods can be applied. For example, a tobacco sheet is extruded from a roller and crimped, and then granules are added to the tobacco sheet, which is then rolled up in cigarette paper to produce a rod-shaped flavor generation segment 110. At this time, an aerosol source such as glycerin may be added as needed. The flavor generation segment 110, cooling section 120, and filter section 130 are then rolled up in tipping paper 140 to produce the flavor generation segment 110.

<電気加熱型たばこ吸引システム>
 上述した加熱式たばこ100は、加熱式たばこを加熱する電気加熱型デバイスと共に用いることができる。すなわち、本発明の別の実施形態である電気加熱型たばこ吸引システムは、上述した加熱式たばこと、該加熱式たばこを加熱する電気加熱型デバイスと、を備える電気加熱型たばこ吸引システムである。
 電気加熱型たばこ吸引システムの構成は特段制限されず、例えば図3及び図4に示すような構成とすることができる。図3は、電気加熱型たばこ吸引システム200の内部構造を説明する図である。なお、図3中の加熱式たばこ物品100は、図1における加熱式たばこ100を概略して記載したものである。
<Electrically heated tobacco smoking system>
The above-described heated tobacco product 100 can be used together with an electric heating device that heats the heated tobacco product. That is, an electrically heated tobacco suction system according to another embodiment of the present invention is an electrically heated tobacco suction system that includes the above-described heated tobacco product and an electric heating device that heats the heated tobacco product.
The configuration of the electrically heated tobacco suction system is not particularly limited, and may be, for example, as shown in Figures 3 and 4. Figure 3 is a diagram illustrating the internal structure of the electrically heated tobacco suction system 200. Note that the heated tobacco article 100 in Figure 3 is a schematic representation of the heated tobacco article 100 in Figure 1.

 電気加熱型たばこ吸引システム200は、加熱式たばこ100と、加熱式たばこ100の香味生成セグメント110を加熱する電気加熱型デバイス30とを備える。加熱式たばこ100は、電気加熱型デバイス30の挿入口3Aを通じて収容部310の収容キャビティ313に対して挿抜自在に収容される。 The electrically heated tobacco suction system 200 comprises a heated tobacco product 100 and an electrically heated device 30 that heats the flavor generation segment 110 of the heated tobacco product 100. The heated tobacco product 100 is inserted into and removed from the storage cavity 313 of the storage unit 310 through the insertion port 3A of the electrically heated device 30.

 電気加熱型デバイス30は、使用者による使用の際、加熱式たばこ100が収容キャビティ313に挿入され、この状態で、収容部310に設けられたヒーターを発熱させ、加熱式たばこ100内の香味源を加熱することによって、たばこ成分等の成分を含むエアロゾルを発生させて使用者の吸引に供する。
 また、ヒーターは香味生成セグメント110を直接加熱してもよいが、加熱式たばこ100内のエアロゾル発生源を加熱することで、加熱されたエアロゾルを香味生成セグメント110へと供給し、該加熱されたエアロゾルがさらに香味生成セグメント110内のたばこ成分等を加熱することによって使用者の吸引に供する態様であってもよい。
When the electrically heated device 30 is used by a user, the heated tobacco product 100 is inserted into the storage cavity 313, and in this state, the heater provided in the storage section 310 is made to generate heat, which heats the flavor source within the heated tobacco product 100, thereby generating an aerosol containing components such as tobacco components, which the user can inhale.
In addition, the heater may directly heat the flavor generation segment 110, or alternatively, it may heat an aerosol generation source within the heated tobacco product 100, supply the heated aerosol to the flavor generation segment 110, and the heated aerosol may further heat tobacco components, etc. within the flavor generation segment 110, thereby allowing the user to inhale it.

 電気加熱型デバイス30は、各種構成部品を収容するための筐体であるハウジング31を有する。ハウジング31内には、ヒーター32、温度センサ35、吸引センサ36、制御部37、電源38等が収容されている。 The electric heating device 30 has a housing 31, which is a case for accommodating various components. The housing 31 contains a heater 32, a temperature sensor 35, a suction sensor 36, a control unit 37, a power supply 38, etc.

[収容部]
 ハウジング31は、前端から後端側に向かって加熱式たばこ100を挿抜可能に収容する収容部310を有している。収容部310は、加熱式たばこ100の挿抜方向に延在し、加熱式たばこ100が挿入される空間の外周を画す円筒状の周壁312と、当該空間の後端を画すように周壁312の後端を閉塞する円板状の後壁311とを備えている。収容部310の周壁312や後壁311は、ハウジング31と一体に形成されてもよいし、ハウジング31と別体に形成されて、ハウジング31に組み付けられてもよい。
[Storage section]
The housing 31 has a storage section 310 that stores the heated tobacco product 100 in an insertable and removable manner from the front end to the rear end. The storage section 310 extends in the insertion/removal direction of the heated tobacco product 100 and includes a cylindrical peripheral wall 312 that defines the outer periphery of the space into which the heated tobacco product 100 is inserted, and a disk-shaped rear wall 311 that closes the rear end of the peripheral wall 312 so as to define the rear end of the space. The peripheral wall 312 and rear wall 311 of the storage section 310 may be formed integrally with the housing 31, or may be formed separately from the housing 31 and then assembled to the housing 31.

 収容部310における周壁312の開口端は、ハウジング31の外部に向けて開放されており、加熱式たばこ100を挿入するための挿入口3Aとなっている。そして、周壁312の内部空間は、挿入口3Aを介して加熱式たばこ100の先端部分を挿抜可能な円柱形状の収容キャビティ313となっている。図4において、符号CLは、加熱式たばこ100の挿抜方向における収容キャビティ313の中心軸を示している。以下、この中心軸CLに沿う方向を軸方向とも称す。なお、収容キャビティ313の外径、即ち周壁312の内径は、加熱式たばこ100の外径と等しくてもよいし、僅かに大きくても、又は僅かに小さくてもよい。 The open end of the peripheral wall 312 of the storage section 310 is open toward the outside of the housing 31, and serves as an insertion port 3A for inserting the heated tobacco product 100. The internal space of the peripheral wall 312 serves as a cylindrical storage cavity 313 into which the tip portion of the heated tobacco product 100 can be inserted and removed via the insertion port 3A. In Figure 4, the symbol CL indicates the central axis of the storage cavity 313 in the insertion and removal direction of the heated tobacco product 100. Hereinafter, the direction along this central axis CL will also be referred to as the axial direction. The outer diameter of the storage cavity 313, i.e., the inner diameter of the peripheral wall 312, may be equal to, slightly larger than, or slightly smaller than the outer diameter of the heated tobacco product 100.

 収容部310における周壁312の周囲には、ヒーター32が設けられている。収容部310の周壁312及び後壁311は、ヒーター32の熱に耐え、且つ、ヒーター32の熱を加熱式たばこ100へ伝える材料によって形成されている。そのような収容部310に用いる材料としては、例えば、ステンレスなどの金属や熱耐性のある樹脂とすることができる。ヒーター32は周壁312内に配置されていてもよい。 A heater 32 is provided around the peripheral wall 312 of the storage section 310. The peripheral wall 312 and rear wall 311 of the storage section 310 are formed from a material that can withstand the heat of the heater 32 and transfer the heat of the heater 32 to the heated tobacco product 100. Materials used for such a storage section 310 include, for example, metals such as stainless steel and heat-resistant resins. The heater 32 may be located within the peripheral wall 312.

[ヒーター]
 ヒーター32は、制御部37から電力の供給を受けて発熱し、収容部310に収容された加熱式たばこ100を加熱する。即ち、ヒーター32は、加熱式たばこ100を加熱する加熱部の一形態である。
 ヒーター32の種類は特に限定されないが、例えば鋼材に発熱線(例えば、ニクロム、鉄クロム、鉄ニッケル等、電気抵抗の大きい線材)を張り巡らせて配置したもの、或いは、セラミックヒーター、シーズヒーター(Sheathed Heater)等を用いることができる。なお、シーズヒーターとは、発熱線を充填剤と共に金属パイプで覆ったヒーターである。
[Heater]
The heater 32 generates heat upon receiving power from the control unit 37, and heats the heated tobacco product 100 accommodated in the accommodation unit 310. In other words, the heater 32 is one form of a heating unit that heats the heated tobacco product 100.
The type of heater 32 is not particularly limited, but examples include a steel material with a heating wire (e.g., a wire material with high electrical resistance, such as nichrome, iron chromium, or iron nickel) strung throughout, a ceramic heater, a sheathed heater, etc. A sheathed heater is a heater in which a heating wire is covered with a metal pipe together with a filler.

 図4は、加熱式たばこ100が収容キャビティ313に挿入された状態を示している。この状態で、ヒーター32は、後述のように制御部37から電力の供給を受けて香味生成セグメント110を所定温度で加熱する。ここで収容キャビティ313のうち、ヒーター32の熱によって所定温度で加熱される空間を加熱領域A1とし、軸方向(挿抜方向)において加熱領域A1の挿入口側に隣接した空間を非加熱領域A2としている。非加熱領域A2は、収容キャビティ313の挿入口側に形成され、加熱領域A1は収容キャビティ313の奥側に形成されている。ここでヒーター32は、加熱領域A1において周壁312の周囲又は内部に配置されており、加熱領域A1を外側から加熱する。なお、ヒーター32は、接触している箇所だけ加熱するのではなく、放射や伝熱によってヒーター32から離れた箇所も加熱する。例えばヒーター32は、軸方向においてヒーター32の前端より挿入口側の位置317まで所定温度で加熱する。このため、加熱領域A1は、収容部310の軸方向において、位置317から後壁311までの領域となっている。即ち、位置317は、加熱領域A1と非加熱領域A2との境界であり、非加熱領域A2は、軸方向において、この境界317から収容キャビティ313の前端までとなっている。なお、この境界317は、ヒーター32によって実際に加熱された際に所定温度となる領域と所定温度未満となる領域の境界に定められても良いし、ヒーター32を既定の条件で発熱させた場合に所定温度となる領域と所定温度未満となる領域の境界を推定し、この推定した境界に定められてもよい。なお、本実施形態では、周壁312が所定温度となる領域と所定温度未満となる領域の境界位置を推定し、この境界位置を通り中心軸CLと直交する面を図4に二点鎖線で示したように境界317と定めている。加熱式たばこ100を収容キャビティ313に挿入した場合、香味生成セグメント110が加熱領域A1に位置し、冷却部120の少なくとも一部が非加熱領域A2に位置する。なお、加熱式たばこ100を既定の状態、例えば、加熱式たばこ100の先端102が収容部310の後壁311に突き当たるまで収容キャビティ313へ挿入した状態とした場合に、収容キャビティ313のうち、香味生成セグメント110が位置する部分を加熱領域A1とし、冷却部120が位置する部分を非加熱領域A2としてもよい。 Figure 4 shows the heated tobacco product 100 inserted into the storage cavity 313. In this state, the heater 32 receives power from the control unit 37, as described below, and heats the flavor generation segment 110 to a predetermined temperature. The space in the storage cavity 313 that is heated to a predetermined temperature by the heat of the heater 32 is designated as the heated area A1, and the space adjacent to the insertion opening of the heated area A1 in the axial direction (insertion/removal direction) is designated as the non-heated area A2. The non-heated area A2 is formed on the insertion opening side of the storage cavity 313, and the heated area A1 is formed on the rear side of the storage cavity 313. The heater 32 is disposed around or inside the peripheral wall 312 in the heated area A1, and heats the heated area A1 from the outside. The heater 32 not only heats the area in contact with the heater 32, but also heats areas distant from the heater 32 by radiation and heat transfer. For example, the heater 32 heats at a predetermined temperature from the front end of the heater 32 to position 317 on the insertion opening side in the axial direction. Therefore, the heated region A1 is the region from position 317 to the rear wall 311 in the axial direction of the accommodating portion 310. That is, position 317 is the boundary between the heated region A1 and the non-heated region A2, and the non-heated region A2 is the region from this boundary 317 to the front end of the accommodating cavity 313 in the axial direction. Note that this boundary 317 may be determined as the boundary between the region where the temperature reaches a predetermined temperature and the region where the temperature falls below the predetermined temperature when actually heated by the heater 32, or may be determined as the estimated boundary between the region where the temperature reaches a predetermined temperature and the region where the temperature falls below the predetermined temperature when the heater 32 is operated under predetermined conditions. Note that in this embodiment, the boundary position between the region where the temperature reaches a predetermined temperature and the region where the temperature falls below the predetermined temperature of the peripheral wall 312 is estimated, and the plane that passes through this boundary position and is perpendicular to the central axis CL is determined as the boundary 317, as shown by the two-dot chain line in FIG. 4 . When the heated tobacco product 100 is inserted into the storage cavity 313, the flavor generation segment 110 is located in the heated region A1, and at least a portion of the cooling unit 120 is located in the non-heated region A2. Note that when the heated tobacco product 100 is in a predetermined state, for example, inserted into the storage cavity 313 until the tip 102 of the heated tobacco product 100 hits the rear wall 311 of the storage section 310, the portion of the storage cavity 313 where the flavor generation segment 110 is located may be the heated region A1, and the portion where the cooling unit 120 is located may be the non-heated region A2.

[制御部]
 図5は、制御部37の構成を示す図である。制御部37は、ヒーター32による加熱の制御など、電気加熱型デバイス30の動作状態を制御する。制御部37は、例えばCPU(Central Processing Unit)、DSP(Digital Signal Processor)、又はFPGA(Field-Programmable Gate Array)などのプロセッサ71、及びRAM(Random Access Memory)又はROM(Read Only Memory)などのメモリ72、入出力部73を備えるコンピュータである。また、制御部37は、ヒーター32の駆動回路74を備える。
[Control unit]
5 is a diagram showing the configuration of the control unit 37. The control unit 37 controls the operating state of the electric heating device 30, such as controlling heating by the heater 32. The control unit 37 is a computer including a processor 71 such as a CPU (Central Processing Unit), DSP (Digital Signal Processor), or FPGA (Field-Programmable Gate Array), a memory 72 such as RAM (Random Access Memory) or ROM (Read Only Memory), and an input/output unit 73. The control unit 37 also includes a drive circuit 74 for the heater 32.

 メモリ72は、主記憶部721として機能するものと、補助記憶部722として機能するものとをそれぞれ備えてもよい。なお、メモリ72は、プロセッサ71と一体(1チップ)に形成されてもよい。メモリ72としては、例えば、RAM等の揮発性メモリ、ROM等の不揮発性メモリ、EPROM(Erasable Programmable ROM)、SSD、又はリムーバブルメディアなどの記憶媒体が挙げられる。 Memory 72 may include a memory that functions as a main memory unit 721 and a memory that functions as an auxiliary memory unit 722. Memory 72 may be formed integrally with processor 71 (on one chip). Examples of memory 72 include storage media such as volatile memory such as RAM, non-volatile memory such as ROM, EPROM (Erasable Programmable ROM), SSD, or removable media.

 メモリ72には、電気加熱型デバイス30の動作を実行するための、オペレーティングシステム(Operating System:OS)、各種プログラム(ファームウェア)、各種データテーブル、各種データベース、設定データ、ユーザデータなどが記憶可能である。 The memory 72 can store an operating system (OS), various programs (firmware), various data tables, various databases, setting data, user data, and the like, which are used to execute the operations of the electric heating device 30.

 入出力部73は、利用者(喫煙者)による電源のオン/オフなどの情報をプロセッサ71へ入力する、又は利用者への情報の出力を行う手段である。入出力部73は、例えば、温度センサ35、吸引センサ36を所定のタイミングで動作させると共に、各センサ35,36による検出値を取得するインターフェースである。また、入出力部73は、操作ボタン、及びタッチパネル等の入力手段、並びに表示部、バイブレータ及びスピーカ等の出力手段を備えてもよい。また、入出力部73は、通信回線を介して外部装置と通信を行うための通信部を備えてもよい。例えば、通信部は、通信ケーブルを介して他のコンピュータと接続し、電気加熱型デバイス30を制御するためのプログラムやデータを受信して、メモリ72に格納することで、ファームフェアや加熱プロファイなどを更新することができる。表示部は、情報を表示する手段であり、例えば、LED等のインジケータ、液晶表示装置、有機EL表示装置であってもよい。 The input/output unit 73 is a means for inputting information such as power on/off by the user (smoker) to the processor 71, or for outputting information to the user. The input/output unit 73 is, for example, an interface that operates the temperature sensor 35 and suction sensor 36 at predetermined times and acquires the detected values of each sensor 35, 36. The input/output unit 73 may also include input means such as operation buttons and a touch panel, as well as output means such as a display, vibrator, and speaker. The input/output unit 73 may also include a communications unit for communicating with an external device via a communications line. For example, the communications unit may connect to another computer via a communications cable, receive programs and data for controlling the electric heating device 30, and store them in the memory 72, thereby updating the firmware, heating profile, etc. The display is a means for displaying information, and may be, for example, an indicator such as an LED, a liquid crystal display, or an organic EL display.

 駆動回路74は、プロセッサ71の命令に従って電源38からヒーター32へ電力を供給し、ヒーター32を動作させる。駆動回路74は、例えば、ヒーター32へ流す電流量を調整するコンバータである。 The drive circuit 74 supplies power from the power supply 38 to the heater 32 in accordance with instructions from the processor 71, causing the heater 32 to operate. The drive circuit 74 is, for example, a converter that adjusts the amount of current flowing to the heater 32.

 制御部37は、プロセッサ71がメモリ72に記憶されたプログラムを主記憶部の作業領域に読み出して実行し、所定の機能部、例えば、判定部711、加熱制御部712、及び出力制御部713として機能する。なお、これらの機能部は、プログラム(ソフトウェア)に基づいて実現されるものに限らず、その一部又は全部が、プロセッサ、集積回路、及び論理回路等のハードウェア回路により構成されてもよい。 The control unit 37 functions as predetermined functional units, such as a determination unit 711, a heating control unit 712, and an output control unit 713, when the processor 71 reads and executes a program stored in the memory 72 into the working area of the main storage unit. Note that these functional units are not limited to those realized based on programs (software), and some or all of them may be configured using hardware circuits such as processors, integrated circuits, and logic circuits.

 判定部711は、各センサ35,36の検出結果、及び入力手段からの入力情報に基づいて、利用者による操作、加熱式たばこ100の状態、ヒーター32による加熱状況などの情報を判定する。例えば、判定部711は、吸引センサ36による検出値から、吸引回数を測定し、吸引回数が所定回数に達したか否かを判定する。 The determination unit 711 determines information such as the user's operation, the state of the heated tobacco product 100, and the heating status of the heater 32 based on the detection results of the sensors 35, 36 and input information from the input means. For example, the determination unit 711 measures the number of puffs from the detection value of the suction sensor 36 and determines whether the number of puffs has reached a predetermined number.

 加熱制御部712は、判定部711の判定結果に基づいて、駆動回路74を制御することで、電源38から駆動回路74を介してヒーター32へ供給する電力を制御する。例えば、加熱制御部712は、判定部711により吸引回数が所定回数に達したと判定された場合、加熱を終了する。また、加熱制御部712は、香味生成セグメント110における水分量や香味源の量が所定量まで減少したと判定部711が判定した場合に、ヒーター32へ供給する電力を変更させて加熱温度を変更させる。さらに、加熱制御部712は、香味生成セグメント110における水分量や香味源の量が減少し、加熱を終了させる状態となったと判定部711が判定した場合に、ヒーター32への電力供給を停止して加熱を終了させる。 The heating control unit 712 controls the drive circuit 74 based on the determination result of the determination unit 711, thereby controlling the power supplied from the power source 38 to the heater 32 via the drive circuit 74. For example, the heating control unit 712 terminates heating when the determination unit 711 determines that the number of suctions has reached a predetermined number. Furthermore, when the determination unit 711 determines that the amount of moisture or flavor source in the flavor generation segment 110 has decreased to a predetermined amount, the heating control unit 712 changes the power supplied to the heater 32 to change the heating temperature. Furthermore, when the determination unit 711 determines that the amount of moisture or flavor source in the flavor generation segment 110 has decreased to the point where heating should be terminated, the heating control unit 712 stops the power supply to the heater 32 and terminates heating.

 出力制御部713は、判定部711の判定結果に基づいて、利用者に対する通知や警告等を出力する。例えば、出力制御部713は、残り吸引可能回数が所定回数以下に達した場合に、信号を出力する、この利用者への出力として、出力制御部713は、例えば、表示部への表示、スピーカによる音出力、バイブレータによる振動等の出力を行う。 The output control unit 713 outputs notifications, warnings, etc. to the user based on the determination result of the determination unit 711. For example, the output control unit 713 outputs a signal when the remaining number of possible suctions reaches a predetermined number or less. As an output to the user, the output control unit 713 may, for example, display on a display unit, output sound from a speaker, or vibrate using a vibrator.

 ヒーター32の長軸方向の長さは、香味生成セグメント110の長軸方向の長さをLmmとしたときに、L±5.0mmの範囲内とすることができる。ヒーター32の長軸方向の長さは、香味生成セグメント110に十分に熱を伝え、香味源に含まれるエアロゾル基材や香味成分等を十分に揮発させる、すなわちエアロゾルデリバリーの観点から、Lmm以上であることが好ましく、香味等へ不所望な影響を及ぼす成分の発生を抑制する観点からL+0.5mm以下、L+1.0mm以下、L+1.5mm以下、L+2.0mm以下、L+2.5mm以下、L+3.0mm以下、L+3.5mm以下、L+4.0mm以下、L+4.5mm以下又はL+5.0mm以下であることが好ましい。 The length of the heater 32 in the longitudinal direction can be within the range of L ± 5.0 mm, where L mm is the length of the flavor generation segment 110 in the longitudinal direction. From the perspective of aerosol delivery, i.e., to sufficiently transfer heat to the flavor generation segment 110 and sufficiently volatilize the aerosol base material and flavor components contained in the flavor source, the length of the heater 32 in the longitudinal direction is preferably L mm or more. From the perspective of suppressing the generation of components that have an undesirable effect on the flavor, the length is preferably L + 0.5 mm or less, L + 1.0 mm or less, L + 1.5 mm or less, L + 2.0 mm or less, L + 2.5 mm or less, L + 3.0 mm or less, L + 3.5 mm or less, L + 4.0 mm or less, L + 4.5 mm or less, or L + 5.0 mm or less.

 ヒーター32による加熱式たばこ100の加熱時間や加熱温度といった加熱強度は、電気加熱型たばこ吸引システム200ごとにあらかじめ設定することができる。例えば、電気加熱型デバイス30に加熱式たばこ100を挿入した後に、一定時間の予備加熱を行うことで、加熱式たばこ100における、電気加熱型デバイス30に挿入されている部分の外周面の温度がX(℃)になるまで加熱し、その後、該温度がX(℃)以下の一定温度を保つように、あらかじめ設定することができる。
 上記X(℃)は、加熱により生成される成分等のデリバリー量の観点から、80℃以上、400℃以下であることが好ましい。具体的には、80℃、90℃、100℃、110℃、120℃、130℃、140℃、150℃、160℃、170℃、180℃、190℃、200℃、210℃、220℃、230℃、240℃、250℃、260℃、270℃、280℃、290℃、300℃、310℃、320℃、330℃、340℃、350℃、360℃、370℃、380℃、390℃、400℃とすることができる。
The heating intensity, such as the heating time and heating temperature of the heated tobacco product 100 by the heater 32, can be preset for each electrically heated tobacco suction system 200. For example, by preheating the heated tobacco product 100 for a certain period of time after it is inserted into the electrically heated device 30, the heated tobacco product 100 can be heated until the temperature of the outer surface of the portion of the heated tobacco product 100 that is inserted into the electrically heated device 30 reaches X (°C), and the temperature can then be set in advance to maintain a constant temperature of X (°C) or less.
From the viewpoint of the delivery amount of components generated by heating, the above X (°C) is preferably 80°C or higher and 400°C or lower. Specifically, the X (°C) may be 80°C, 90°C, 100°C, 110°C, 120°C, 130°C, 140°C, 150°C, 160°C, 170°C, 180°C, 190°C, 200°C, 210°C, 220°C, 230°C, 240°C, 250°C, 260°C, 270°C, 280°C, 290°C, 300°C, 310°C, 320°C, 330°C, 340°C, 350°C, 360°C, 370°C, 380°C, 390°C, or 400°C.

 冷却部120に設けられ得る開孔103は、外部からの空気の流入の促進及び加熱により生成される成分や空気の冷却部120内での滞留の抑制の観点から、冷却部120における、電気加熱型デバイス30と接触する領域の吸口端側の端部よりも吸口端側に存在することが好ましい。また、電気加熱型デバイス30の加熱式たばこ100の挿入口3Aは、加熱式たばこ100を挿入し易くするため、テーパー状となっていてもよい。 The opening 103 that may be provided in the cooling section 120 is preferably located closer to the mouth end than the mouth end of the area of the cooling section 120 that comes into contact with the electrically heated device 30, from the standpoint of promoting the inflow of air from the outside and preventing components and air generated by heating from accumulating within the cooling section 120. Furthermore, the insertion port 3A of the electrically heated device 30 for the heated tobacco 100 may be tapered to make it easier to insert the heated tobacco 100.

 図4を用いた上述の説明では、加熱式たばこ100を加熱する手段としてヒーターを用いた態様、具体的には、加熱式たばこ100が電気加熱型デバイスに挿入された場合に加熱式たばこ100を外部から加熱する態様を説明した。しかし、加熱式たばこ100を加熱する手段はこれに限定されず、例えば、棒状又は錘状のヒーターを用い、加熱式たばこ100を電気加熱型デバイスに挿入した際に、該ヒーターが加熱式たばこ100中の香味生成セグメント110に挿入されるような構成とし、加熱式たばこ100を内部から加熱する態様を採用することもできる。また、ヒーターとしてインダクタを備え、加熱式たばこ100中の香味生成セグメント110の内部に香味源等を加熱するためのサセプタを導入する態様を採用することもできる。この態様では、出力制御部713によりインダクタに電力を供給し、誘導加熱でサセプタを加熱することにより、香味源等を加熱することができる。また、ヒーターとしてマイクロ波発生装置を備える態様を採用することもできる。この態様では、出力制御部713によりマイクロ波発生装置に電力を供給し、マイクロ波加熱により香味生成セグメント110中の香味源等を加熱することができる。 4, an embodiment using a heater as a means for heating the heated tobacco product 100 has been described; specifically, an embodiment in which the heated tobacco product 100 is heated from the outside when inserted into an electrically heated device. However, the means for heating the heated tobacco product 100 is not limited to this. For example, a rod-shaped or spindle-shaped heater may be used, and when the heated tobacco product 100 is inserted into an electrically heated device, the heater may be inserted into the flavor generation segment 110 of the heated tobacco product 100, thereby heating the heated tobacco product 100 from the inside. It is also possible to adopt an embodiment in which an inductor is provided as the heater, and a susceptor for heating a flavor source, etc. is introduced into the flavor generation segment 110 of the heated tobacco product 100. In this embodiment, the flavor source, etc. can be heated by supplying power to the inductor via the output control unit 713 and heating the susceptor by induction heating. It is also possible to adopt an embodiment in which a microwave generator is provided as the heater. In this embodiment, the output control unit 713 supplies power to the microwave generator, and the flavor source and the like in the flavor generation segment 110 can be heated by microwave heating.

 本発明を実施例によってさらに具体的に説明するが、本発明はその要旨から逸脱しない限り、以下の実施例の記載に限定されるものではない。 The present invention will be explained in more detail using examples, but the present invention is not limited to the description of the following examples as long as it does not deviate from the gist of the invention.

<加熱式たばこの材料>
・たばこシート:たばこ粉砕物にエアロゾル生成基材としてグリセリンを全体の12質量%となるよう添加した組成物を、厚さ248μm、坪量200gm/mの圧延シートに加工したもの
・顆粒:炭酸カルシウムとカルボキシメチルセルロース(バインダー)を重量比95:5で混合したもの 熱伝導率2.70W/mK 平均粒子径500μm
<Ingredients for heated tobacco>
Tobacco sheet: A composition of ground tobacco with glycerin added as an aerosol-generating base material at a ratio of 12% by mass to the total, processed into a rolled sheet with a thickness of 248 μm and a basis weight of 200 gm/ m². Granules: A mixture of calcium carbonate and carboxymethyl cellulose (binder) in a weight ratio of 95:5. Thermal conductivity: 2.70 W/mK. Average particle size: 500 μm.

<評価方法>
 実施例及び比較例で作製した加熱式たばこを、市販の電気加熱型デバイス(PloomX 日本たばこ産業株式会社製)に挿入してからデバイスのスイッチを入れ、喫煙可能になってから喫煙試験を開始した。
 喫煙試験はボルグワルド社製1本がけ自動喫煙機を用いて、30秒毎に55ml/2秒を1パフとして10パフの喫煙試験を実施した。喫煙試験で発生した主流煙はケンブリッジパッドに捕集され、各パフ毎のケンブリッジパッドの重量測定及びガスクロマトグラフィーから、ニコチン及びエアロゾルのデリバリー量を測定した。
<Evaluation method>
The heated tobacco products prepared in the Examples and Comparative Examples were inserted into a commercially available electric heating device (PloomX, manufactured by Japan Tobacco Inc.), and the device was then turned on. Once the device was ready for smoking, the smoking test was started.
The smoking test was performed using a Borgwald single-puff automatic smoking machine, with 10 puffs at 55 ml/2 seconds every 30 seconds. The mainstream smoke generated during the smoking test was collected on a Cambridge pad, and the nicotine and aerosol delivery amounts were measured by weighing the Cambridge pad and analyzing it with gas chromatography after each puff.

[実施例1]
 たばこシートをローラーから押し出しながらクリンプ加工を施した。さらに、該たばこシート上に顆粒を添加した後、たばこシートを顆粒と共に巻紙でギャザー巻装して、円筒形の香味生成セグメントを作製した。
 香味生成セグメントは、円周22mm、長さ12mmであり、たばこシートの幅は85mm、充填量はたばこシート204mg、顆粒80mgとした。
 吸い口端から遠い順に、先端セグメント、香味生成セグメント、冷却部、フィルター部の順となるよう一列に配置して、これらをチップペーパーで巻装することで同軸に連結し、加熱式たばこを得た。先端セグメントとしては長さ8mmのペーパーフィルタ、冷却部としては長さ20mmの中空管、フィルター部としてはPloom X(商品名 日本たばこ産業株式会社製)に用いられる加熱式たばこ(メビウス ディープレギュラー プルームエックス専用)のフィルターを用いた。
 得られた加熱式たばこを用いて上記喫煙試験を行い、デリバリー量の評価を行った。結果を表1に示す。
[Example 1]
The tobacco sheet was crimped while being extruded from the roller, and then granules were added onto the tobacco sheet, followed by gathering and wrapping the tobacco sheet together with the granules in cigarette paper to prepare a cylindrical flavor generating segment.
The flavor generating segment had a circumference of 22 mm and a length of 12 mm, the tobacco sheet had a width of 85 mm, and the filling amounts were 204 mg of tobacco sheet and 80 mg of granules.
The tip segment, flavor generation segment, cooling section, and filter section were arranged in a line in that order from farthest from the mouth end, and these were connected coaxially by wrapping with tipping paper to obtain a heated tobacco product. The tip segment was an 8 mm long paper filter, the cooling section was a 20 mm long hollow tube, and the filter section was a filter from a heated tobacco product (Mevius Deep Regular, exclusive for Ploom X) used in Ploom X (trade name, manufactured by Japan Tobacco Inc.).
The obtained heated tobacco product was subjected to the above-mentioned smoking test, and the delivery amount was evaluated. The results are shown in Table 1.

[比較例1]
 たばこシートを幅95mm充填量228mgとし、香味生成セグメントに顆粒を充填しなかった以外は実施例1と同様に、加熱式たばこを作製し評価した。結果を表1に示す。
[Comparative Example 1]
A heat-not-burn tobacco product was produced and evaluated in the same manner as in Example 1, except that the tobacco sheet had a width of 95 mm and a filling amount of 228 mg, and no granules were filled in the flavor generating segment. The results are shown in Table 1.

 図7及び図8は、表1の結果をグラフに示したものである。表1、図7及び図8の結果から、実施例1の加熱式たばこは、比較例1よりもたばこシートの充填量が少ないにもかかわらず、同程度のデリバリーが得られることがわかる。
 すなわち、本実施形態に係る顆粒を含む加熱式たばこは、デリバリー効率が向上し、吸い応えの向上が得られる。
Figures 7 and 8 are graphs showing the results of Table 1. The results of Table 1, Figures 7 and 8 show that the heated tobacco product of Example 1 has a smaller tobacco sheet filling amount than Comparative Example 1, yet achieves the same level of delivery.
That is, a heated tobacco product containing the granules according to this embodiment has improved delivery efficiency and a more satisfying smoking experience.

100   加熱式たばこ
101   吸い口端
102   先端
103   開孔
110   香味生成セグメント
111   たばこ充填物
112   巻紙
120   冷却部
130   フィルター部
140   チップペーパー
150   濾材
160   フィルターラッパー
170   添加剤放出容器
R1    リップリリース材料配置領域
200   電気加熱型たばこ吸引システム
30    電気加熱型デバイス
31    ハウジング
310   収容部
311   後壁
312   周壁
313   収容キャビティ
32    ヒーター
35    温度センサ
36    吸引センサ
37    制御部
38    電源
71    プロセッサ
711   判定部
712   加熱制御部
713   出力制御部
72    メモリ
721   主記憶部
722   補助記憶部
73    入出力部
74    駆動回路
61    巻紙
62    たばこシート
63    顆粒
100 Heated tobacco 101 Mouth end 102 Tip 103 Opening 110 Flavor generating segment 111 Tobacco filler 112 Cigarette paper 120 Cooling section 130 Filter section 140 Tipping paper 150 Filter material 160 Filter wrapper 170 Additive release container R1 Lip release material placement area 200 Electrically heated tobacco suction system 30 Electrically heated device 31 Housing 310 Storage section 311 Rear wall 312 Peripheral wall 313 Storage cavity 32 Heater 35 Temperature sensor 36 Suction sensor 37 Control section 38 Power source 71 Processor 711 Determination section 712 Heating control section 713 Output control section 72 Memory 721 Main memory section 722 Auxiliary memory section 73 Input/output section 74 Drive circuit 61 Cigarette paper 62 Tobacco sheet 63 Granules

Claims (12)

 香味生成セグメントを備える加熱式たばこであって、
 前記香味生成セグメントが、たばこシート及び顆粒を含み、
 前記顆粒が、前記たばこシートのシート間に配置されている、
 加熱式たばこ。
A heated tobacco product comprising a flavor generating segment,
the flavor-generating segment comprises tobacco sheets and granules;
The granules are disposed between the sheets of the tobacco sheet.
Heated tobacco.
 前記たばこシートが、クリンプ加工した後にギャザー充填させたものであり、前記顆粒がギャザー充填されたたばこシート間に挟持される、請求項1に記載の加熱式たばこ。 The heated tobacco product of claim 1, wherein the tobacco sheets are gathered and filled after being crimped, and the granules are sandwiched between the gathered and filled tobacco sheets.  前記顆粒の熱伝導率が、0.10W/mK~250W/mKである、請求項1又は2に記載の加熱式たばこ。 The heated tobacco product according to claim 1 or 2, wherein the thermal conductivity of the granules is 0.10 W/mK to 250 W/mK.  前記顆粒が、香料を含有する、請求項1~3のいずれか1項に記載の加熱式たばこ。 The heated tobacco product according to any one of claims 1 to 3, wherein the granules contain a flavoring.  前記顆粒が、たばこ香味成分を含有する、請求項1~4のいずれか1項に記載の加熱式たばこ。 The heated tobacco product according to any one of claims 1 to 4, wherein the granules contain a tobacco flavor component.  前記顆粒が、ニコチンを含有する、請求項1~5のいずれか1項に記載の加熱式たばこ。 The heated tobacco product according to any one of claims 1 to 5, wherein the granules contain nicotine.  前記香味生成セグメント中の前記たばこシートの充填密度が、0.33g/cm~0.76g/cmである、請求項1~6のいずれか1項に記載の加熱式たばこ。 The heated tobacco product according to any one of claims 1 to 6, wherein the packing density of the tobacco sheet in the flavor generating segment is 0.33 g/cm 3 to 0.76 g/cm 3 .  前記香味生成セグメント中の前記顆粒の充填密度が、0.04g/cm~0.22g/cmである、請求項1~7のいずれか1項に記載の加熱式たばこ。 The heated tobacco according to any one of claims 1 to 7, wherein the packing density of the granules in the flavor generating segment is 0.04 g/cm 3 to 0.22 g/cm 3 .  前記香味生成セグメント中の前記たばこシートと前記顆粒との質量比が、60/40~95/5である、請求項1~8のいずれか1項に記載の加熱式たばこ。 The heated tobacco product according to any one of claims 1 to 8, wherein the mass ratio of the tobacco sheet to the granules in the flavor generating segment is 60/40 to 95/5.  前記顆粒の平均粒子径が、250μm~1000μmである、請求項1~9のいずれか1項に記載の加熱式たばこ。 The heated tobacco product according to any one of claims 1 to 9, wherein the average particle size of the granules is 250 μm to 1000 μm.  前記加熱式たばこが、非燃焼加熱式たばこである、請求項1~10のいずれか1項に記載の加熱式たばこ。 The heated tobacco product according to any one of claims 1 to 10, wherein the heated tobacco product is a non-combustion heated tobacco product.  請求項1~11のいずれか1項に記載の加熱式たばこと、前記加熱式たばこを加熱する電気加熱型デバイスと、を備える電気加熱型たばこ吸引システム。 An electrically heated tobacco smoking system comprising the heated tobacco product according to any one of claims 1 to 11 and an electrically heated device that heats the heated tobacco product.
PCT/JP2024/008559 2024-03-06 2024-03-06 Heated tobacco and electrically-heated tobacco inhalation system Pending WO2025186949A1 (en)

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