WO2023238287A1 - 検査装置、検査素子および検査方法 - Google Patents
検査装置、検査素子および検査方法 Download PDFInfo
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- WO2023238287A1 WO2023238287A1 PCT/JP2022/023154 JP2022023154W WO2023238287A1 WO 2023238287 A1 WO2023238287 A1 WO 2023238287A1 JP 2022023154 W JP2022023154 W JP 2022023154W WO 2023238287 A1 WO2023238287 A1 WO 2023238287A1
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/02—Details
- H01J37/244—Detectors; Associated components or circuits therefor
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/02—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material
- G01N23/06—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material and measuring the absorption
- G01N23/18—Investigating the presence of flaws defects or foreign matter
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/02—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material
- G01N23/04—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material and forming images of the material
- G01N23/046—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material and forming images of the material using tomography, e.g. computed tomography [CT]
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01T—MEASUREMENT OF NUCLEAR OR X-RADIATION
- G01T1/00—Measuring X-radiation, gamma radiation, corpuscular radiation, or cosmic radiation
- G01T1/16—Measuring radiation intensity
- G01T1/1603—Measuring radiation intensity with a combination of at least two different types of detector
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/02—Details
- H01J37/22—Optical, image processing or photographic arrangements associated with the tube
- H01J37/222—Image processing arrangements associated with the tube
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/26—Electron or ion microscopes; Electron or ion diffraction tubes
- H01J37/28—Electron or ion microscopes; Electron or ion diffraction tubes with scanning beams
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/045—Investigating materials by wave or particle radiation combination of at least 2 measurements (transmission and scatter)
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/07—Investigating materials by wave or particle radiation secondary emission
- G01N2223/079—Investigating materials by wave or particle radiation secondary emission incident electron beam and measuring excited X-rays
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/10—Different kinds of radiation or particles
- G01N2223/102—Different kinds of radiation or particles beta or electrons
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/50—Detectors
- G01N2223/505—Detectors scintillation
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/50—Detectors
- G01N2223/507—Detectors secondary-emission detector
Definitions
- the present invention relates to an inspection apparatus, an inspection element, and an inspection technique, and relates to a technique that is effective when applied to an inspection apparatus, an inspection element, and an inspection method used for inspection of semiconductor devices, for example.
- Patent Document 1 describes a technology related to a detector and an electron detection device that can detect X-rays and electrons.
- etching defects in deep holes for example, contact holes and via holes
- an inspection device inspects for etching defects in deep holes by irradiating the deep holes with primary electrons generated by an electron source and detecting secondary electrons and reflected electrons emitted from the deep holes. (scanning electron microscope) is used.
- secondary electrons and reflected electrons will be simply referred to as electrons when there is no need to distinguish them.
- the aspect ratio of deep holes has been increasing as semiconductor devices have become more highly integrated and miniaturized.
- the aspect ratio of the deep hole increases in this way, the probability that electrons generated from the bottom of the deep hole will be absorbed by the side walls of the deep hole increases.
- a situation has arisen in which it is difficult to obtain information about the bottom of a deep hole. This means that it becomes difficult to detect etching defects in deep holes, and improvements are needed.
- the solid angle at which electrons enter the electron detection element from the deep hole and the solid angle at which X-rays enter the X-ray detection element from the deep hole become small. This means that electrons cannot be detected with high efficiency by the electron detection element, and X-rays cannot be detected with high efficiency by the X-ray detection element.
- an inspection device is equipped with an electron detection element that detects electrons and an X-ray detection element that detects X-rays, it is possible to accurately inspect etching defects in deep holes with a high aspect ratio.
- Development of a device is desired. That is, in an inspection apparatus that includes an electron detection element and an X-ray detection element, a device is desired that enables highly accurate inspection of etching defects in deep holes with a high aspect ratio.
- the inspection apparatus in one embodiment includes an electron source that generates primary electrons and makes them incident on a sample, an electron detection element located between the sample stage on which the sample can be placed and the electron source, and an electron detection element. and an X-ray detection element located between the electron source and the electron source.
- the electron detection element includes a scintillator that detects electrons emitted from the sample, and the X-ray detection element detects X-rays emitted from the sample and transmitted through the electron detection element. is configured to do so.
- the inspection element in one embodiment is an inspection element that can be incorporated into an inspection device that detects electrons and X-rays emitted from the sample by injecting primary electrons generated by an electron source into a sample placed on a sample stage.
- the inspection element includes an electron detection element that can be placed between the sample stage and the electron source, and an X-ray detection element that can be placed between the electron detection element and the electron source.
- the electron detection element includes a scintillator that detects electrons emitted from the sample, and the X-ray detection element detects X-rays that are emitted from the sample and have passed through the electron detection element. It is configured as follows.
- the inspection method in one embodiment includes a step of generating primary electrons in an electron source and making them incident on a sample, and an electron detection element including a scintillator, which is located between the sample stage on which the sample is placed and the electron source.
- an electron detection element including a scintillator, which is located between the sample stage on which the sample is placed and the electron source.
- the A step of detecting X-rays is provided.
- the performance of the inspection device can be improved.
- FIG. 1 It is a figure showing a typical composition of an inspection device.
- (a) is a diagram schematically showing the planar shape of the electron detection element when viewed in a plane perpendicular to the incident direction of primary electrons
- (b) is a diagram schematically showing the planar shape of the electron detection element when viewed in a plane perpendicular to the incident direction of primary electrons.
- (a) is a graph showing the calculation result of "SNR" calculated based on the backscattered electron intensity from the bottom of the deep hole
- (b) is a graph showing the calculation result of "SNR" calculated based on the X-ray intensity from the bottom of the deep hole.
- FIG. 3 is a diagram showing a functional block configuration of a control section. It is a flowchart explaining the operation of the inspection device. It is a schematic diagram showing a deep hole sample.
- (a) is a diagram schematically showing an electronic image generated based on the output from the electron detection element
- (b) is a diagram schematically showing an X-ray image generated based on the output from the X-ray detection element. It is a figure which shows an image typically
- (c) is a figure which shows the composite image which combined the characteristic of an electronic image and the characteristic of an X-ray image.
- FIG. 1 is a diagram showing a schematic configuration of an inspection apparatus 100.
- an inspection apparatus 100 includes an electron source 10, a converging lens 11, a deflector 12, an objective lens 13, a sample stage 14, an inspection element 50, and a control section 60.
- the electron source 10 is configured to generate a plurality of primary electrons.
- the converging lens 11 has a function of converging a primary electron beam consisting of a plurality of primary electrons generated by the electron source 10, and the objective lens 13 focuses the primary electron beam on the sample 20 placed on the sample stage 14. It has the function of focusing an electron beam.
- the deflector 12 is configured to be able to change the traveling direction of the primary electron beam, and the deflector 12 allows the irradiation position of the primary electron beam on the sample 20 to be scanned along the inspection range. I can do it.
- the inspection element 50 is configured to be able to detect electrons and X-rays emitted by injecting primary electrons into the sample 20, and includes an electron detection element 30 that detects electrons and an electron detection element 30 that detects X-rays.
- the X-ray detection element 40 is equipped with an X-ray detection element 40 that performs
- the electron detection element 30 is provided between the sample stage 14 on which the sample 20 is placed and the electron source 10. More specifically, the electron detection element 30 is provided between the sample stage 14 and the objective lens 13.
- the X-ray detection element 40 is provided between the electron detection element 30 and the electron source 10. More specifically, the X-ray detection element 40 is provided between the electron detection element 30 and the objective lens 13.
- the electron detection element 30 is configured to include, for example, a scintillator that detects electrons emitted from the sample 20 and a photomultiplier tube that amplifies light generated by the scintillator.
- the X-ray detection element 40 is configured to detect X-rays emitted from the sample 20 and transmitted through the electron detection element 30, and is typified by, for example, a silicon drift detector. It consists of a semiconductor detector, a scintillator, and a photomultiplier tube.
- the electron detection element 30 is composed of a combination of a scintillator and a photomultiplier tube
- the X-ray detection element 40 is also composed of a combination of a scintillator and a photomultiplier tube. It is assumed that there is
- FIG. 2(a) is a diagram schematically showing the planar shape of the electron detection element 30 when viewed in a plane perpendicular to the direction of incidence of primary electrons
- FIG. 2(b) is a diagram showing the shape of the electron detection element 30 in the direction of incidence of primary electrons
- FIG. 4 is a diagram schematically showing the planar shape of the X-ray detection element 40 when viewed from a plane perpendicular to .
- the planar shape of the electron detection element 30 is a concentric circle having a cavity in the center through which primary electrons pass, and the electron detection element 30 has a so-called “annular type". It is composed of "elements”.
- the planar shape of the X-ray detection element 40 is a concentric circle having a cavity in the center through which the primary electrons pass. It is composed of a so-called "annular type element”.
- the inspection element 50 configured in this manner makes the primary electrons (primary electron beam) generated by the electron source 10 incident on the sample 20 placed on the sample stage 14, and collects the electrons and X-rays emitted from the sample 20. Not only can the test element 50 be manufactured and sold integrally with the test device 100 for detection, but also the test element 50 can be manufactured and sold alone.
- control unit 60 is configured to control the operation of the inspection device 100. Specifically, the control unit 60 controls the converging lens 11 and the objective lens 13 to converge the primary electron beam, the deflector 12 to scan the primary electron beam, and controls the output signal from the inspection element 50. It is configured to perform control for signal processing, control of image generation processing and image display processing based on the output signal from the inspection element 50, and the like.
- the inspection apparatus 100 in this embodiment is configured as described above.
- the operation of the inspection apparatus 100 will be explained with reference to FIG.
- the sample 20 is placed on the sample stage 14.
- a plurality of primary electrons are generated in the electron source 10, and a primary electron beam composed of the plurality of primary electrons is emitted from the electron source 10.
- the primary electron beam emitted from the electron source 10 is converged by a converging lens 11 and then passes through a deflector 12 to adjust its traveling direction. Thereafter, the primary electron beam whose traveling direction has been adjusted by the deflector 12 is irradiated onto a first region of the sample 20 by the objective lens 13 .
- the primary electrons collide with electrons bound to atoms (molecules) constituting the sample 20, and as a result, the primary electrons are bound to the atoms (molecules) constituting the sample 20.
- the electrons are scattered and fly out of the atom. This ejected electron is a secondary electron.
- the primary electrons may be scattered and backscattered from atoms constituting the sample 20, and the electrons emitted from the sample 20 by being backscattered from the primary electrons are backscattered electrons.
- the "electrons” emitted from the sample 20 enter the electron detection element 30 arranged between the objective lens 13 and the sample stage 14. Then, the "electrons" incident on the electron detection element 30 are converted into light by a scintillator that is a component of the electron detection element 30, and then the light converted by the scintillator is It is photoelectrically converted and amplified by a photomultiplier tube, and is output as an output signal from the electron detection element 30.
- the X-rays emitted from the sample 20 pass through the electron detection element 30 and then enter the X-ray detection element 40 disposed between the objective lens 13 and the electron detection element 30. Then, the X-rays incident on the X-ray detection element 40 are converted into light by a scintillator, which is a component of the X-ray detection element 40, and then the light converted by the scintillator is transferred to the X-ray detection element 40. It is photoelectrically converted and amplified by a photomultiplier tube, which is a component, and is output as an output signal from the X-ray detection element 40.
- the output signal output from the electron detection element 30 is converted into, for example, an image signal, and then an electronic image is acquired based on this image signal, and the electronic image is displayed.
- the output signal output from the X-ray detection element 40 is converted into an image signal, for example, and then an X-ray image is acquired based on this image signal, and the X-ray image is displayed.
- the traveling direction of the primary electron beam is changed by the deflector 12, and the primary electron beam is scanned from the first region to the second region of the sample 20. Then, in the second region of the sample 20, the same operation as in the first region is repeated. In this way, the inspection device 100 operates.
- the first feature of this embodiment is, for example, as shown in FIG. 1, in an inspection apparatus 100 that includes an electron detection element 30 and an X-ray detection element 40, the electron detection element 30
- the X-ray detection element 40 is disposed between the arrangable sample stage 14 and the electron source 10
- the X-ray detection element 40 is disposed between the electron detection element 30 and the electron source 10.
- the point is that the X-ray detection element 30 and the X-ray detection element 40 are arranged so as to overlap.
- the "electrons" emitted from the sample 20 are absorbed by the electron detection element 30 disposed in front of the X-ray detection element 40.
- "electrons” are prevented from being incident on the X-ray detection element 40, thereby improving the accuracy of X-ray detection in the X-ray detection element 40. That is, since an output signal is also generated when “electrons” enter the X-ray detection element 40, the output signal caused by the "electrons” becomes noise. Therefore, in order to improve X-ray detection accuracy, it is desirable to prevent "electrons" from entering the X-ray detection element 40 as much as possible.
- this electron detection element 30 since the electron detection element 30 is arranged on the side closer to the sample 20, this electron detection element 30 causes "electrons" to enter the X-ray detection element 40. It functions as a shielding member that suppresses this. Therefore, according to the first feature point, the accuracy of X-ray detection by the X-ray detection element 40 can be improved.
- the film thickness of the electron detection element 30 must be sufficient to absorb “electrons”, and must have a sufficient film thickness to absorb “electrons”. It is desirable to have sufficient density to absorb. In this case, since more "electrons" are absorbed by the electron detection element 30, according to the first characteristic point, the efficiency of detecting "electrons" by the electron detection element 30 can also be improved.
- the X-rays emitted from the sample 20 have high transmittance, they pass through the electron detection element 30 in the front and enter the X-ray detection element 40. Therefore, even if the configuration of the first feature point is adopted, there is no problem in X-ray detection.
- the electron detection element 30 can be used to transfer "electrons" to the X-ray detection element 40 without sacrificing the incidence of X-rays into the X-ray detection element 40. It can function as a shielding member that suppresses incidence. As a result, according to the inspection apparatus 100 in this embodiment, the accuracy of X-ray detection can be improved.
- the second characteristic point of this embodiment is that the electron detection element 30 is an "annular element” and the X-ray detection
- the element 40 is also an “annular type element.”
- the second characteristic point is that the planar shape of the electron detection element 30 is a concentric circle having a cavity in the center through which the primary electrons pass, and similarly, the planar shape of the X-ray detection element 40 is It can also be said that they have a concentric circular shape with a cavity in the center through which primary electrons pass.
- the solid angle at which "electrons” enter the electron detection element 30 from the sample 20 and the solid angle at which X-rays enter the X-ray detection element 40 from the sample 20 are increased. I can do it.
- the electron detection element 30 can convert “electrons” into light with high efficiency
- the X-ray detection element 40 can convert X-rays into light with high efficiency. Therefore, according to the second characteristic point, it is possible to improve the "electron" detection efficiency and the X-ray detection efficiency in the inspection apparatus 100.
- the performance of the inspection apparatus 100 can be improved due to the synergistic effect of the first feature point and the second feature point described above.
- Figure 3(a) is a graph showing the calculation result of "SNR" calculated based on the intensity of backscattered electrons from the bottom of the deep hole
- Figure 3(b) is a graph showing the result of calculating the "SNR” based on the intensity of reflected electrons from the bottom of the deep hole. It is a graph showing the calculation result of "SNR" calculated based on.
- the "SNR" based on the intensity of backscattered electrons is about 2 (points surrounded by circles), whereas the "SNR” based on the X-ray intensity is approximately 2. It can be seen that the value is about 8 (point surrounded by a circle). This means that "SNR" based on X-ray intensity has a contrast about four times higher than "SNR" based on backscattered electron intensity. In other words, according to the above-mentioned verification results, the sensitivity to information from the bottom of a deep hole is more sensitive to the detection of X-rays by the X-ray detection element 40 than by the detection of reflected electrons by the electron detection element 30.
- the inspection apparatus 100 can accurately detect information from the bottom of a deep hole by using the output from the X-ray detection element 40. I know that there is. In other words, by using the inspection apparatus 100 in this embodiment, it is possible to inspect, for example, etching defects in deep holes with a high aspect ratio with high precision.
- FIG. 4 is a diagram illustrating the configuration of a modified example.
- light generated from the scintillator included in the electron detection element 30 and light generated from the scintillator included in the X-ray detection element 40 are separated between the electron detection element 30 and the X-ray detection element 40.
- a crosstalk suppressor 70 is provided to suppress crosstalk with light generated from the scintillator.
- the light generated by the electron detection element 30 enters the X-ray detection element 40 and is detected by the photomultiplier tube of the X-ray detection element 40, and It is possible to prevent light generated by the X-ray detection element 40 from entering the electron detection element 30 and being detected by the photomultiplier tube of the electron detection element 30. That is, according to this modification, superimposition of noise signals can be reduced in each of the electron detection element 30 and the X-ray detection element 40. As a result, according to this modification, the accuracy of detecting "electrons" by the electron detection element 30 and the detection accuracy of X-rays by the X-ray detection element 40 can be improved.
- the crosstalk suppressor 70 can be configured from a shielding film that blocks light generated from the scintillator included in the electron detection element 30 and light generated from the scintillator included in the X-ray detection element 40. .
- the crosstalk suppressing section 70 is not only composed of the above-mentioned shielding film, but also includes, for example, the refractive index of the material constituting the electron detection element 30 and the refractive index of the material constituting the X-ray detection element 40. may be composed of a film having a different refractive index, or a spatial region having a refractive index different from the refractive index of the material constituting the electron detection element 30 and the refractive index of the material constituting the X-ray detection element 40. can.
- the crosstalk suppressing section 70 is a film having a refractive index smaller than the refractive index of the material constituting the electron detection element 30 and the refractive index of the material constituting the X-ray detection element 40, or It can be constructed from a spatial region having a refractive index smaller than the refractive index of the material constituting the X-ray detecting element 30 and the refractive index of the material constituting the X-ray detecting element 40.
- the light generated from the scintillator included in the electron detection element 30 is totally reflected due to the refractive index difference at the boundary between the electron detection element 30 and the crosstalk suppressing section 70.
- the light generated from the scintillator included in the electron detection element 30 is confined inside the electron detection element 30.
- light generated from the scintillator included in the X-ray detection element 40 is totally reflected due to the refractive index difference at the boundary between the X-ray detection element 40 and the crosstalk suppressing section 70.
- the light generated from the scintillator included in the X-ray detection element 40 is confined inside the X-ray detection element 40.
- the light generated by the electron detection element 30 is suppressed from entering the X-ray detection element 40 and the light generated by the X-ray detection element 40 is suppressed from entering the electron detection element 30.
- the detection accuracy of "electrons" by the detection element 30 and the detection accuracy of X-rays by the X-ray detection element 40 can be improved.
- the inspection apparatus 100 in this embodiment includes the electron detection element 30 that detects "electrons" emitted from the sample 20 and the X-ray detection element 30 that detects the X-rays emitted from the sample 20. It is equipped with 40.
- the X-ray detection element 40 has the advantage of being able to accurately detect information from the bottom of a deep hole, for example.
- the electron detection element 30 has the advantage of being able to accurately detect the surface shape (information from the surface) of a deep hole.
- the inspection apparatus 100 in this embodiment includes the electron detection element 30 and the X-ray detection element 40, which have different advantages, the inspection apparatus 100 can be improved by combining the respective advantages. It is believed that further performance improvement can be achieved. This point will be explained below.
- FIG. 5 is a diagram showing a functional block configuration of the control section 60.
- the control unit 60 includes an input unit 201, a first image signal conversion unit 202, a second image signal conversion unit 203, an electronic image acquisition unit 204, an X-ray image acquisition unit 205, and a first characteristic It has an image acquisition section 206, a second characteristic image acquisition section 207, a composite image acquisition section 208, an output section 209, and a data storage section 210.
- the input section 201 is configured to input the first output signal output from the electron detection element 30 and the second output signal output from the X-ray detection element 40.
- the electron detection element 30 includes a first scintillator and the X-ray detection element 40 includes a second scintillator
- the The first output signal is a signal based on light obtained by converting "electrons" by the first scintillator.
- the second output signal output from the X-ray detection element 40 is a signal based on light obtained by converting X-rays by the second scintillator.
- the first output amount output from the electron detection element 30 is a signal amount based on the light amount obtained by converting "electrons" by the first scintillator.
- the second output amount output from the X-ray detection element 40 is a signal amount based on the light amount obtained by converting the X-rays by the second scintillator.
- the first image signal conversion unit 202 has a function of converting the first output signal input to the input unit 201 into a first image signal.
- the second image signal conversion section 203 has a function of converting the second output signal input to the input section 201 into a second image signal.
- the electronic image acquisition unit 204 is configured to generate an electronic image based on the first image signal converted by the first image signal conversion unit 202. Then, the electronic image acquired by the electronic image acquisition unit 204 is stored in the data storage unit 210, for example.
- the X-ray image acquisition unit 205 is configured to generate an X-ray image based on the second image signal converted by the second image signal conversion unit 203.
- the X-ray image acquired by the X-ray image acquisition unit 205 is stored in the data storage unit 210, for example.
- the gradation of pixels in an X-ray image is based on the amount of light obtained by converting X-rays with a scintillator. It may be the sum of the units, with the amount of light (less than or equal to the amount of light) being taken as one unit.
- the first characteristic image acquisition section 206 is configured to read out the electronic image generated by the electronic image acquisition section 204 from the data storage section 210 and then acquire a first characteristic image in which features are extracted from this electronic image. There is. The first characteristic image is then stored in the data storage unit 210.
- the second characteristic image acquisition unit 207 reads out the X-ray image generated by the X-ray image acquisition unit 205 from the data storage unit 210, and then acquires a second characteristic image in which features are extracted from this X-ray image. It is configured. The second feature image is then stored in the data storage unit 210.
- the composite image acquisition unit 208 generates a first characteristic image based on the first characteristic image acquired by the first characteristic image acquisition unit 206 and the second characteristic image acquired by the second characteristic image acquisition unit 207.
- the second feature image is configured to obtain a composite image that combines features included in the second feature image and features included in the second feature image. This composite image is stored in the data storage unit 210, for example.
- the output unit 209 is configured to output the composite image acquired by the composite image acquisition unit 208 to the display unit 80, for example. As a result, the composite image is displayed on the display unit 80.
- the control section 60 is configured as described above.
- FIG. 6 is a flowchart illustrating the operation of the inspection apparatus 100.
- the first region of the sample 20 is irradiated with primary electrons (primary electron beam) emitted from the electron source 10 (S102).
- S102 primary electron beam
- S103A the electron detection element 30
- the emitted X-rays pass through the electron detection element 30 and are detected by the X-ray detection element 40 (S103B).
- the detection of "electrons" emitted from the first region of the sample 20 by the electron detection element 30 and the detection of X-rays emitted from the first region of the sample 20 by the X-ray detection element 40 are as follows. done at the same time.
- a first output signal corresponding to the detection of the "electron” is output from the electron detection element 30.
- the first output signal output from the electron detection element 30 is input to the input section 201, and then converted into a first image signal by the first image signal conversion section 202 (S104A).
- a second output signal corresponding to the detection of the X-rays is output from the X-ray detection element 40. Then, the second output signal output from the X-ray detection element 40 is input to the input section 201, and then converted into a second image signal by the second image signal conversion section 203 (S104B).
- the electronic image acquisition unit 204 acquires an electronic image based on the first image signal converted by the first image signal conversion unit 202 (S105A).
- the X-ray image acquisition unit 205 acquires an X-ray image based on the second image signal converted by the second image signal conversion unit 203 (S105B).
- the acquired electronic images and X-ray images are stored in data storage section 210.
- the first feature image acquisition unit 206 extracts features from the electronic image acquired by the electronic image acquisition unit 204, and acquires a first feature image (S106A).
- the second characteristic image acquisition unit 207 extracts features from the X-ray image acquired by the X-ray image acquisition unit 205, and acquires a second characteristic image (S106B).
- the acquired first feature image and second feature image are stored in the data storage unit 210.
- the composite image acquisition unit 208 converts the first characteristic image into a first characteristic image based on the first characteristic image acquired by the first characteristic image acquisition unit 206 and the second characteristic image acquired by the second characteristic image acquisition unit 207.
- a composite image is obtained by combining the included features and the features included in the second feature image (S107). At this time, the obtained composite image is stored in the data storage section 210.
- the output unit 209 outputs the composite image acquired by the composite image acquisition unit 208, for example, to the display unit 80 (S108). As a result, the composite image is displayed on the display unit 80.
- the inspection device 100 operates as described above.
- a further feature of the invention is to create a composite image that combines the features included in the electronic image based on the output from the electron detection element 30 and the features included in the X-ray image based on the output from the X-ray detection element 40. It is at the point of generation. Then, by inspecting the sample 20 based on the generated composite image, highly accurate inspection can be performed. That is, according to a further improvement, the advantages of the electron detection element 30 and the X-ray detection element 40 can be effectively utilized in combination, so that the inspection performance of the inspection apparatus 100 can be improved.
- FIG. 7 is a schematic diagram showing a deep hole sample.
- deep hole CNT1 and deep hole CNT2 are illustrated.
- the deep hole CNT2 is etched to reach the wiring WL, indicating a normal deep hole.
- the deep hole CNT1 does not reach the wiring WL, indicating a deep hole with a defective etching.
- the deep hole sample shown in FIG. 7 is inspected by the inspection apparatus 100 according to this embodiment.
- FIG. 8(a) is a diagram schematically showing an electronic image generated based on the output from the electron detection element 30, and FIG. 8(b) is a diagram schematically showing an electronic image generated based on the output from the X-ray detection element 40.
- FIG. 2 is a diagram schematically showing an X-ray image generated by Further
- FIG. 8(c) is a diagram showing a composite image that combines the characteristics of the electronic image and the characteristics of the X-ray image.
- the advantage of the electronic image based on the output of the electron detection element 30 is that it accurately reflects the surface shape of the sample. Therefore, the opening diameter of deep hole CNT1 and the opening diameter of deep hole CNT2 in FIG. 8(a) are accurate. That is, the feature (advantage) of the electronic image shown in FIG. 8(a) is that the opening diameter of the deep hole CNT1 and the opening diameter of the deep hole CNT2 are accurate.
- the X-ray detection element 40 can obtain information from the bottom of the deep hole with a high aspect ratio, the deep hole CNT1 included in the X-ray image and the deep It can be seen that there is a difference in contrast with the hole CNT2. That is, in the X-ray image shown in FIG. 8(b), it is possible to distinguish between the poorly etched deep hole CNT1 and the normal deep hole CNT2 shown in FIG. 7 based on the contrast difference. As described above, the feature (advantage) of the X-ray image shown in FIG. 8(b) is that there is a contrast difference between the poorly etched deep hole CNT1 and the normal deep hole CNT2.
- the X-ray image based on the output of the X-ray detection element 40 is more difficult to accurately reflect the surface shape of the sample than the electronic image based on the output of the electron detection element 30.
- the aperture diameter of deep hole CNT1 and the aperture diameter of deep hole CNT2 are inaccurate, and are larger than in the electronic image shown in FIG. 8(a).
- the opening diameter of the deep hole CNT1 and the opening diameter of the deep hole CNT2 are inaccurate, and the image is blurred than the electronic image shown in FIG. 8(a).
- the advantage of the electronic image shown in FIG. 8(a) is that the aperture diameter of deep hole CNT1 and the aperture diameter of deep hole CNT2 are accurate, and the X-ray image shown in FIG. 8(b) is The advantage is that the etched defective deep hole CNT1 and the normal deep hole CNT2 can be distinguished based on the contrast difference. Therefore, the inspection apparatus 100 generates a composite image by combining the advantages of the electronic image shown in FIG. 8(a) and the advantages of the X-ray image shown in FIG. 8(b).
- the composite image includes the advantages of the electronic image shown in FIG. 8(a) (outlines of deep-hole CNT1 and deep-hole CNT2) and the X-ray image shown in FIG. 8(b). It can be seen that the advantages (difference in contrast between deep hole CNT1 and deep hole CNT2) are taken into account.
- Electron source 11 Convergent lens 12 Deflector 13 Objective lens 14 Sample stage 20
- Sample 30 Electron detection element 40
- X-ray detection element 50 Inspection element 60
- Control section 70 Crosstalk suppression section 80
- Display section 100 Inspection device 201
- Input section 202 1 image signal conversion section 203 second image signal conversion section 204 electronic image acquisition section 205
- X-ray image acquisition section 206 first characteristic image acquisition section 207
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Abstract
Description
図1は、検査装置100の模式的な構成を示す図である。
図1において、検査装置100は、電子源10と、収束レンズ11と、偏向器12と、対物レンズ13と、試料台14と、検査素子50と、制御部60を有している。
以上のようにして、本実施の形態における検査装置100が構成されている。
続いて、検査装置100の動作について、図1を参照しながら説明する。
まず、試料台14上に試料20を配置する。そして、電子源10において、複数の一次電子を発生させて、複数の一次電子からなる一次電子ビームを電子源10から射出する。電子源10から射出された一次電子ビームは、収束レンズ11で収束された後、偏向器12を通過することにより、進行方向が調整される。その後、偏向器12で進行方向が調整された一次電子ビームは、対物レンズ13によって、試料20の第1領域に照射される。
このようにして、検査装置100が動作することになる。
続いて、本実施の形態における特徴点について説明する。
本実施の形態における第1特徴点は、例えば、図1に示すように、電子検出用素子30とX線検出用素子40とを備える検査装置100において、電子検出用素子30が、試料20を配置可能な試料台14と電子源10との間に配置されているとともに、X線検出用素子40が、電子検出用素子30と電子源10との間に配置され、平面視において、電子検出用素子30とX線検出用素子40とが重なるように配置されている点にある。
上述した特徴点によれば、検査装置100におけるX線の検出精度を向上できることの検証結果について説明する。検証は、深孔試料に対する反射電子強度(BSE(Back Scattered Electron)強度)とX線強度を計算することで行った。具体的に、検証は、深孔の底部からの信号強度に基づいてSNR(Signal Noise Ratio:コントラスト)を計算することで行った。
次に、変形例について説明する。
図4は、変形例の構成を説明する図である。図4において、本変形例では、電子検出用素子30とX線検出用素子40との間に、電子検出用素子30に含まれるシンチレータから発生する光と、X線検出用素子40に含まれるシンチレータから発生する光とのクロストークを抑制するクロストーク抑制部70が設けられている。
上述したように、本実施の形態における検査装置100は、試料20から射出された「電子」を検出する電子検出用素子30と、試料20から射出されたX線を検出するX線検出用素子40を備えている。ここで、X線検出用素子40は、例えば、深孔の底部からの情報を精度良く検出することができる利点を有している。一方、電子検出用素子30は、深孔の表面形状(表面からの情報)を精度良く検出することができる利点を有している。
図5は、制御部60の機能ブロック構成を示す図である。
図5において、制御部60は、入力部201と、第1画像信号変換部202と、第2画像信号変換部203と、電子画像取得部204と、X線画像取得部205と、第1特徴画像取得部206と、第2特徴画像取得部207と、合成画像取得部208と、出力部209と、データ記憶部210を有している。
次に、さらなる工夫点に対応した検査装置100の動作を説明する。
図6は、検査装置100の動作を説明するフローチャートである。
図6において、まず、試料20の第N領域を表す変数Nを「N=1」に設定する(S101)。そして、電子源10から射出された一次電子(一次電子ビーム)を試料20の第1領域に照射する(S102)。これにより、試料20の第1領域からは、「電子」およびX線が射出される。射出された「電子」は、電子検出用素子30において検出される(S103A)。一方、射出されたX線は、電子検出用素子30を透過して、X線検出用素子40において検出される(S103B)。例えば、試料20の第1領域から射出された「電子」の電子検出用素子30での検出と、試料20の第1領域から射出されたX線のX線検出用素子40での検出は、同時に行われる。
以上のようして、検査装置100が動作する。
さらなる工夫点の特徴は、電子検出用素子30からの出力に基づく電子画像に含まれる特徴と、X線検出用素子40からの出力に基づくX線画像に含まれる特徴とを組み合わせた合成画像を生成する点にある。そして、生成された合成画像に基づいて、試料20の検査を実施することにより、高精度の検査を実施することができる。すなわち、さらなる工夫点によれば、電子検出用素子30の長所とX線検出用素子40の長所とを組み合わせて有効活用することができるので、検査装置100における検査性能を向上できる。
以下では、具体例を使用して説明する。
図7は、深孔試料を示す模式図である。図7においては、深孔CNT1と深孔CNT2が図示されている。深孔CNT2は、配線WLまで達するようにエッチングされており、正常な深孔を示している。一方、深孔CNT1は、配線WLまで達しておらず、エッチング不良の深孔を示している。以下では、図7に示す深孔試料を本実施の形態における検査装置100で検査することを考える。
11 収束レンズ
12 偏向器
13 対物レンズ
14 試料台
20 試料
30 電子検出用素子
40 X線検出用素子
50 検査素子
60 制御部
70 クロストーク抑制部
80 表示部
100 検査装置
201 入力部
202 第1画像信号変換部
203 第2画像信号変換部
204 電子画像取得部
205 X線画像取得部
206 第1特徴画像取得部
207 第2特徴画像取得部
208 合成画像取得部
209 出力部
210 データ記憶部
CNT1 深孔
CNT2 深孔
WL 配線
Claims (24)
- 一次電子を発生させて試料に入射させる電子源と、
前記試料を配置可能な試料台と前記電子源との間に位置する電子検出用素子と、
前記電子検出用素子と前記電子源との間に位置するX線検出用素子と、
を備える、検査装置であって、
前記電子検出用素子は、前記試料から射出された電子を検出する第1シンチレータを含み、
前記X線検出用素子は、前記試料から射出されたX線であって前記電子検出用素子を透過した前記X線を検出するように構成されている、検査装置。 - 請求項1に記載の検査装置において、
前記X線検出用素子は、第2シンチレータを含む、検査装置。 - 請求項1に記載の検査装置において、
前記電子検出用素子は、アニュラー型素子であり、
前記X線検出用素子は、アニュラー型素子である、検査装置。 - 請求項1に記載の検査装置において、
前記一次電子の入射方向に垂直な平面で見た場合、
前記電子検出用素子の平面形状は、同心円形状であり、
前記X線検出用素子の平面形状は、同心円形状である、検査装置。 - 請求項1に記載の検査装置において、
前記電子検出用素子における前記電子の検出と、前記X線検出用素子における前記X線の検出とは、同時に行われる、検査装置。 - 請求項1に記載の検査装置において、
前記検査装置は、
前記電子検出用素子からの出力を第1画像信号に変換する第1画像信号変換部と、
前記第1画像信号に基づいて電子画像を取得する電子画像取得部と、
前記X線検出用素子からの出力を第2画像信号に変換する第2画像信号変換部と、
前記第2画像信号に基づいてX線画像を取得するX線画像取得部と、
を有する、検査装置。 - 請求項6に記載の検査装置において、
前記X線検出用素子は、第2シンチレータを含み、
前記X線検出用素子からの出力量は、前記X線を前記第2シンチレータで変換した光量に基づく信号量である、検査装置。 - 請求項7に記載の検査装置において、
前記X線画像における画素の諧調は、一定の時間内における、前記X線検出用素子の前記第2シンチレータで変換した光量の総和に基づく量である、検査装置。 - 請求項6に記載の検査装置において、
前記一次電子を前記試料の第1領域に照射する場合、
前記電子検出用素子は、前記第1領域から射出された電子を検出し、
前記X線検出用素子は、前記第1領域から射出されたX線を検出し、
前記電子画像取得部は、前記第1領域に対応する第1電子画像を取得し、
前記X線画像取得部は、前記第1領域に対応する第1X線画像を取得する、検査装置。 - 請求項9に記載の検査装置において、
前記検査装置は、
前記第1電子画像の特徴を抽出した第1特徴画像を取得する第1特徴画像取得部と、
前記第1X線画像の特徴を抽出した第2特徴画像を取得する第2特徴画像取得部と、
前記第1特徴画像と前記第2特徴画像から合成画像を取得する合成画像取得部と、
を有する、検査装置。 - 請求項1に記載の検査装置において、
前記試料から射出された電子の前記X線検出用素子への入射が、前記試料台と前記X線検出素子の間に設けられている前記電子検出用素子によって抑制される、検査装置。 - 請求項2に記載の検査装置において、
前記電子検出用素子と前記X線検出用素子との間に、前記電子検出用素子に含まれる前記第1シンチレータから発生する光と、前記X線検出用素子に含まれる前記第2シンチレータから発生する光とのクロストークを抑制するクロストーク抑制部が設けられている、検査装置。 - 請求項12に記載の検査装置において、
前記クロストーク抑制部は、前記電子検出用素子に含まれる前記第1シンチレータから発生する光と、前記X線検出用素子に含まれる前記第2シンチレータから発生する光とを遮蔽する遮蔽膜から構成されている、検査装置。 - 請求項12に記載の検査装置において、
前記クロストーク抑制部は、前記電子検出用素子を構成する材料の屈折率および前記X線検出用素子を構成する材料の屈折率とは異なる屈折率を有する膜、あるいは、前記電子検出用素子を構成する材料の屈折率および前記X線検出用素子を構成する材料の屈折率とは異なる屈折率を有する空間領域から構成されている、検査装置。 - 試料台に配置された試料に電子源で発生した一次電子を入射させて前記試料から射出される電子およびX線を検出する検査装置に組み込み可能な検査素子であって、
前記検査素子は、
前記試料台と前記電子源との間に配置可能な電子検出用素子と、
前記電子検出用素子と前記電子源との間に配置可能なX線検出用素子と、
を備え、
前記電子検出用素子は、前記試料から射出された電子を検出する第1シンチレータを含み、
前記X線検出用素子は、前記試料から射出されたX線であって前記電子検出用素子を透過した前記X線を検出するように構成されている、検査素子。 - 請求項15に記載の検査素子において、
前記X線検出用素子は、第2シンチレータを含む、検査素子。 - 請求項15に記載の検査素子において、
前記電子検出用素子は、アニュラー型素子であり、
前記X線検出用素子は、アニュラー型素子である、検査素子。 - 請求項15に記載の検査素子において、
前記一次電子の入射方向に垂直な平面で見た場合、
前記電子検出用素子の平面形状は、同心円形状であり、
前記X線検出用素子の平面形状は、同心円形状である、検査素子。 - 請求項15に記載の検査素子において、
前記電子検出用素子における前記電子の検出と、前記X線検出用素子における前記X線の検出とは、同時に行われる、検査素子。 - 請求項16に記載の検査素子において、
前記X線検出用素子からの出力量は、前記X線を前記第2シンチレータで変換した光量に基づく信号量である、検査素子。 - 請求項15に記載の検査素子において、
前記試料から射出された電子の前記X線検出用素子への入射が、前記試料台と前記X線検出素子の間に設けられている前記電子検出用素子によって抑制される、検査素子。 - 請求項16に記載の検査素子において、
前記電子検出用素子と前記X線検出用素子との間に、前記電子検出用素子に含まれる前記第1シンチレータから発生する光と、前記X線検出用素子に含まれる前記第2シンチレータから発生する光とのクロストークを抑制するクロストーク抑制部が設けられている、検査素子。 - 一次電子を電子源で発生させて試料に入射させる工程、
前記試料が配置される試料台と前記電子源との間に位置し、かつ、シンチレータを含む電子検出用素子によって、前記試料から射出された電子を検出するとともに、前記電子検出用素子と前記電子源との間に位置するX線検出用素子によって、前記試料から射出されたX線であって前記電子検出用素子を透過した前記X線を検出する工程、
を備える、検査方法。 - 請求項23に記載の検査方法において、
前記電子検出用素子は、アニュラー型素子であり、
前記X線検出用素子は、アニュラー型素子である、検査方法。
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JPS5448481A (en) * | 1977-09-26 | 1979-04-17 | Jeol Ltd | Electron ray unit |
JP2001074437A (ja) * | 1999-09-01 | 2001-03-23 | Hitachi Ltd | 回路パターン検査装置及び回路パターン検査方法 |
JP2013026152A (ja) * | 2011-07-25 | 2013-02-04 | Hitachi High-Technologies Corp | 電子顕微鏡 |
JP2015146283A (ja) * | 2014-02-04 | 2015-08-13 | 株式会社日立ハイテクノロジーズ | 荷電粒子線装置及び画像生成方法 |
JP2017067746A (ja) * | 2015-10-01 | 2017-04-06 | 学校法人 中村産業学園 | 相関顕微鏡 |
JP2019186112A (ja) * | 2018-04-13 | 2019-10-24 | 株式会社ホロン | 超高速電子検出器および該検出器を組み込んだ走査型電子ビーム検査装置 |
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US5866904A (en) * | 1990-10-12 | 1999-02-02 | Hitachi, Ltd. | Scanning electron microscope and method for dimension measuring by using the same |
JP5963453B2 (ja) * | 2011-03-15 | 2016-08-03 | 株式会社荏原製作所 | 検査装置 |
WO2018025849A1 (ja) * | 2016-08-02 | 2018-02-08 | 松定プレシジョン株式会社 | 荷電粒子線装置及び走査電子顕微鏡 |
WO2022023304A1 (en) * | 2020-07-31 | 2022-02-03 | Asml Netherlands B.V. | Systems and methods for pulsed voltage contrast detection and capture of charging dynamics |
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JPS5448481A (en) * | 1977-09-26 | 1979-04-17 | Jeol Ltd | Electron ray unit |
JP2001074437A (ja) * | 1999-09-01 | 2001-03-23 | Hitachi Ltd | 回路パターン検査装置及び回路パターン検査方法 |
JP2013026152A (ja) * | 2011-07-25 | 2013-02-04 | Hitachi High-Technologies Corp | 電子顕微鏡 |
JP2015146283A (ja) * | 2014-02-04 | 2015-08-13 | 株式会社日立ハイテクノロジーズ | 荷電粒子線装置及び画像生成方法 |
JP2017067746A (ja) * | 2015-10-01 | 2017-04-06 | 学校法人 中村産業学園 | 相関顕微鏡 |
JP2019186112A (ja) * | 2018-04-13 | 2019-10-24 | 株式会社ホロン | 超高速電子検出器および該検出器を組み込んだ走査型電子ビーム検査装置 |
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KR20240151836A (ko) | 2024-10-18 |
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