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WO2009063856A1 - セルロースエーテル誘導体の製造方法 - Google Patents

セルロースエーテル誘導体の製造方法 Download PDF

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Publication number
WO2009063856A1
WO2009063856A1 PCT/JP2008/070486 JP2008070486W WO2009063856A1 WO 2009063856 A1 WO2009063856 A1 WO 2009063856A1 JP 2008070486 W JP2008070486 W JP 2008070486W WO 2009063856 A1 WO2009063856 A1 WO 2009063856A1
Authority
WO
WIPO (PCT)
Prior art keywords
ether derivative
cellulose ether
cellulose
producing cellulose
producing
Prior art date
Application number
PCT/JP2008/070486
Other languages
English (en)
French (fr)
Inventor
Munehisa Okutsu
Takeshi Ihara
Original Assignee
Kao Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kao Corporation filed Critical Kao Corporation
Priority to EP08850551.6A priority Critical patent/EP2210905B1/en
Priority to ES08850551.6T priority patent/ES2539656T3/es
Priority to US12/742,175 priority patent/US8916700B2/en
Priority to CN200880115620.2A priority patent/CN101855246B/zh
Publication of WO2009063856A1 publication Critical patent/WO2009063856A1/ja

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B11/00—Preparation of cellulose ethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B11/00—Preparation of cellulose ethers
    • C08B11/02—Alkyl or cycloalkyl ethers
    • C08B11/04—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals
    • C08B11/08—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals with hydroxylated hydrocarbon radicals; Esters, ethers, or acetals thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B1/00—Preparatory treatment of cellulose for making derivatives thereof, e.g. pre-treatment, pre-soaking, activation
    • C08B1/06—Rendering cellulose suitable for etherification
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B1/00—Preparatory treatment of cellulose for making derivatives thereof, e.g. pre-treatment, pre-soaking, activation
    • C08B1/08—Alkali cellulose
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B1/00—Preparatory treatment of cellulose for making derivatives thereof, e.g. pre-treatment, pre-soaking, activation
    • C08B1/08—Alkali cellulose
    • C08B1/10—Apparatus for the preparation of alkali cellulose
    • C08B1/12—Steeping devices
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B11/00—Preparation of cellulose ethers
    • C08B11/02—Alkyl or cycloalkyl ethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B11/00—Preparation of cellulose ethers
    • C08B11/02—Alkyl or cycloalkyl ethers
    • C08B11/04—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals
    • C08B11/10—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals substituted with acid radicals
    • C08B11/12—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals substituted with acid radicals substituted with carboxylic radicals, e.g. carboxymethylcellulose [CMC]
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H8/00—Macromolecular compounds derived from lignocellulosic materials

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Abstract

　有機ハライド化合物の反応効率が極めて高く、選択的にセルロースエーテル誘導体を製造する方法に関する。 　結晶化度が５０％以下の低結晶性の粉末セルロースを、塩基の存在下、エチレンクロロヒドリン、モノハロ酢酸及びその塩等の有機ハライド化合物と反応させる、カルボキシメチルセルロースやヒドロキシエチルセルロース等のセルロースエーテル誘導体の製造方法である。
PCT/JP2008/070486 2007-11-14 2008-11-11 セルロースエーテル誘導体の製造方法 WO2009063856A1 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EP08850551.6A EP2210905B1 (en) 2007-11-14 2008-11-11 Method for producing cellulose ether derivative
ES08850551.6T ES2539656T3 (es) 2007-11-14 2008-11-11 Método para producir derivado de éter de celulosa
US12/742,175 US8916700B2 (en) 2007-11-14 2008-11-11 Method for producing cellulose ether derivative
CN200880115620.2A CN101855246B (zh) 2007-11-14 2008-11-11 纤维素醚衍生物的制造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007295905A JP2009120716A (ja) 2007-11-14 2007-11-14 ヒドロキシエチルセルロースの製造方法
JP2007-295905 2007-11-14

Publications (1)

Publication Number Publication Date
WO2009063856A1 true WO2009063856A1 (ja) 2009-05-22

Family

ID=40638705

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/070486 WO2009063856A1 (ja) 2007-11-14 2008-11-11 セルロースエーテル誘導体の製造方法

Country Status (7)

Country Link
US (1) US8916700B2 (ja)
EP (1) EP2210905B1 (ja)
JP (1) JP2009120716A (ja)
KR (1) KR20100074252A (ja)
CN (1) CN101855246B (ja)
ES (1) ES2539656T3 (ja)
WO (1) WO2009063856A1 (ja)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012150701A1 (ja) * 2011-05-02 2012-11-08 花王株式会社 アルカリセルロースの製造方法
WO2018061890A1 (ja) * 2016-09-29 2018-04-05 住友精化株式会社 水溶性ヒドロキシエチルセルロースの製造方法

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8436165B2 (en) 2007-02-16 2013-05-07 Kao Corporation Process for producing noncrystalline cellulose
WO2011108505A1 (ja) * 2010-03-02 2011-09-09 花王株式会社 カチオン化セルロース及びカチオン化ヒドロキシアルキルセルロースの製造方法
WO2013086111A1 (en) * 2011-12-07 2013-06-13 University Of Florida Research Foundation, Inc. Modified cellulose, methods of manufacture thereof and articles comprising the same
CN103920181A (zh) * 2014-04-03 2014-07-16 石家庄亿生堂医用品有限公司 一种水溶性止血材料及其制备方法
CN109836506B (zh) * 2017-11-29 2021-08-20 上海长光企业发展有限公司 一种食品级纤维素胶及其制备方法
EP3722326A4 (en) * 2017-12-07 2021-11-10 Nippon Paper Industries Co., Ltd. CARBOXYMETHYLATED CELLULOSE
US12123109B2 (en) * 2017-12-07 2024-10-22 Nippon Paper Industries Co., Ltd. Carboxymethylated cellulose nanofibers
CN110156899A (zh) * 2019-05-14 2019-08-23 吉林省荣普达石油技术有限公司 一种两性离子化羟乙基纤维素改性物及其制备方法
TWI798649B (zh) * 2021-02-24 2023-04-11 財團法人紡織產業綜合研究所 醫療敷材
CN114292340B (zh) * 2022-01-18 2023-03-03 万华化学集团股份有限公司 一种制备聚季铵盐-10的方法

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6020901A (ja) * 1983-07-08 1985-02-02 ザ・ダウ・ケミカル・カンパニ− ヒドロキシアルキルアルキルセルロースエーテルを製造するための連続添加方法
JPS61241337A (ja) * 1985-04-19 1986-10-27 Kanebo Ltd 微小セルロ−ズ粒子およびその製造法
JPS62236801A (ja) 1986-04-08 1987-10-16 Asahi Chem Ind Co Ltd 可溶性セルロ−スの製造方法
JPH06199902A (ja) 1992-12-29 1994-07-19 Sumitomo Seika Chem Co Ltd ヒドロキシエチルセルロースの製造方法
JPH08245701A (ja) 1995-03-08 1996-09-24 Daicel Chem Ind Ltd 透明性に優れたヒドロキシアルキルセルロース及びその製造法
JPH09176201A (ja) 1995-12-26 1997-07-08 Daicel Chem Ind Ltd カルボキシメチルセルロースの製造方法
JP2000513042A (ja) * 1997-04-25 2000-10-03 ロディア アセトウ 反応性セルロース及びその製造方法
JP2001086957A (ja) * 1999-09-24 2001-04-03 Asahi Kasei Corp 崩壊性セルロース含有食品組成物
JP2002114801A (ja) 2000-07-31 2002-04-16 Kao Corp 多糖類誘導体の製造法
JP2002512271A (ja) * 1998-04-20 2002-04-23 ヴオルフ・ヴアルスロデ・アクチエンゲゼルシヤフト セルロースの活性化及び誘導体化の方法
JP2003064184A (ja) 2001-08-24 2003-03-05 Toray Ind Inc セルロース溶液及び熱可塑性セルロースエステルの製造方法
JP2004331918A (ja) 2003-05-12 2004-11-25 Asahi Kasei Chemicals Corp 非晶質セルロース微粉体

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US2618632A (en) * 1949-04-05 1952-11-18 Hercules Powder Co Ltd Mixed cellulose ether and preparation thereof
DE2357079C2 (de) * 1973-11-15 1982-07-29 Hoechst Ag, 6000 Frankfurt Verfahren zum Herstellen von Wasser aufnehmenden, aber darin zu mehr als 50% unlöslichen Celluloseethern
JPS5222079A (en) * 1975-08-13 1977-02-19 Toyo Pulp Kk Modification of cellulose
JPS572301A (en) * 1980-06-06 1982-01-07 Toray Ind Inc Preparation of cellulosic derivative
US5417984A (en) * 1992-12-14 1995-05-23 Biocontrol, Inc. Low crystallinity cellulose excipients
JP2002519153A (ja) * 1998-07-01 2002-07-02 アコーディス スペシャリティー ファイバーズ リミティド 傷手当用品及びその製造並びにその使用に適切な材料の製造
JP5377816B2 (ja) * 2005-06-16 2013-12-25 信越化学工業株式会社 セルロースエーテルの製造方法

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6020901A (ja) * 1983-07-08 1985-02-02 ザ・ダウ・ケミカル・カンパニ− ヒドロキシアルキルアルキルセルロースエーテルを製造するための連続添加方法
JPS61241337A (ja) * 1985-04-19 1986-10-27 Kanebo Ltd 微小セルロ−ズ粒子およびその製造法
JPS62236801A (ja) 1986-04-08 1987-10-16 Asahi Chem Ind Co Ltd 可溶性セルロ−スの製造方法
JPH06199902A (ja) 1992-12-29 1994-07-19 Sumitomo Seika Chem Co Ltd ヒドロキシエチルセルロースの製造方法
JPH08245701A (ja) 1995-03-08 1996-09-24 Daicel Chem Ind Ltd 透明性に優れたヒドロキシアルキルセルロース及びその製造法
JPH09176201A (ja) 1995-12-26 1997-07-08 Daicel Chem Ind Ltd カルボキシメチルセルロースの製造方法
JP2000513042A (ja) * 1997-04-25 2000-10-03 ロディア アセトウ 反応性セルロース及びその製造方法
JP2002512271A (ja) * 1998-04-20 2002-04-23 ヴオルフ・ヴアルスロデ・アクチエンゲゼルシヤフト セルロースの活性化及び誘導体化の方法
JP2001086957A (ja) * 1999-09-24 2001-04-03 Asahi Kasei Corp 崩壊性セルロース含有食品組成物
JP2002114801A (ja) 2000-07-31 2002-04-16 Kao Corp 多糖類誘導体の製造法
JP2003064184A (ja) 2001-08-24 2003-03-05 Toray Ind Inc セルロース溶液及び熱可塑性セルロースエステルの製造方法
JP2004331918A (ja) 2003-05-12 2004-11-25 Asahi Kasei Chemicals Corp 非晶質セルロース微粉体

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP2210905A4 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012150701A1 (ja) * 2011-05-02 2012-11-08 花王株式会社 アルカリセルロースの製造方法
JP2012246480A (ja) * 2011-05-02 2012-12-13 Kao Corp アルカリセルロースの製造方法
US9416198B2 (en) 2011-05-02 2016-08-16 Kao Corporation Method for producing alkali cellulose
WO2018061890A1 (ja) * 2016-09-29 2018-04-05 住友精化株式会社 水溶性ヒドロキシエチルセルロースの製造方法
JPWO2018061890A1 (ja) * 2016-09-29 2019-07-11 住友精化株式会社 水溶性ヒドロキシエチルセルロースの製造方法
JP7030705B2 (ja) 2016-09-29 2022-03-07 住友精化株式会社 水溶性ヒドロキシエチルセルロースの製造方法

Also Published As

Publication number Publication date
EP2210905A4 (en) 2012-06-27
US8916700B2 (en) 2014-12-23
ES2539656T3 (es) 2015-07-02
CN101855246B (zh) 2013-07-24
EP2210905B1 (en) 2015-04-01
KR20100074252A (ko) 2010-07-01
JP2009120716A (ja) 2009-06-04
EP2210905A1 (en) 2010-07-28
CN101855246A (zh) 2010-10-06
US20100311964A1 (en) 2010-12-09

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