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WO2009035110A1 - フルオロアルキルアイオダイドの製造方法 - Google Patents

フルオロアルキルアイオダイドの製造方法 Download PDF

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Publication number
WO2009035110A1
WO2009035110A1 PCT/JP2008/066599 JP2008066599W WO2009035110A1 WO 2009035110 A1 WO2009035110 A1 WO 2009035110A1 JP 2008066599 W JP2008066599 W JP 2008066599W WO 2009035110 A1 WO2009035110 A1 WO 2009035110A1
Authority
WO
WIPO (PCT)
Prior art keywords
formula
compound represented
fluoroalkyl iodide
producing
even number
Prior art date
Application number
PCT/JP2008/066599
Other languages
English (en)
French (fr)
Inventor
Shoji Furuta
Original Assignee
Asahi Glass Company, Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Glass Company, Limited filed Critical Asahi Glass Company, Limited
Priority to JP2009532257A priority Critical patent/JPWO2009035110A1/ja
Publication of WO2009035110A1 publication Critical patent/WO2009035110A1/ja

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/278—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of only halogenated hydrocarbons

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

　所望の重合度のフルオロアルキルアイオダイド（テロマー）の選択率が高く、かつ生産性が高いフルオロアルキルアイオダイドの製造方法を提供する。 　ラジカル開始剤の存在下、下式（１）で表される化合物に下式（２）で表される化合物を付加させて、下式（３）で表される化合物を得る際に、ラジカル開始剤として、下式（４）で表わされる化合物を用いる。 ＲｆＩ・・・（１）、ＣＦ２＝ＣＦ２・・・（２）、ＲｆＣＦ２ＣＦ２Ｉ・・・（３）、｛Ｆ（ＣＦ２）ｘＣＯＯ｝２・・・（４）。 ただし、Ｒｆは、炭素数が２～１６の偶数であるフルオロアルキル基であり、ｘは、２～１４の偶数である。
PCT/JP2008/066599 2007-09-13 2008-09-12 フルオロアルキルアイオダイドの製造方法 WO2009035110A1 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2009532257A JPWO2009035110A1 (ja) 2007-09-13 2008-09-12 フルオロアルキルアイオダイドの製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-237661 2007-09-13
JP2007237661 2007-09-13

Publications (1)

Publication Number Publication Date
WO2009035110A1 true WO2009035110A1 (ja) 2009-03-19

Family

ID=40452116

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/066599 WO2009035110A1 (ja) 2007-09-13 2008-09-12 フルオロアルキルアイオダイドの製造方法

Country Status (3)

Country Link
JP (1) JPWO2009035110A1 (ja)
KR (1) KR20100065142A (ja)
WO (1) WO2009035110A1 (ja)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009073762A (ja) * 2007-09-20 2009-04-09 Asahi Glass Co Ltd フルオロアルキルアイオダイドの製造方法
JP2010018533A (ja) * 2008-07-09 2010-01-28 Asahi Glass Co Ltd フルオロアルキルハライドの製造方法
JP2010018532A (ja) * 2008-07-09 2010-01-28 Asahi Glass Co Ltd フルオロアルキルハライドの製造方法
CN112898117A (zh) * 2021-01-27 2021-06-04 济南齐氟新材料技术有限公司 一种全氟烷基碘的制备方法

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102644317B1 (ko) * 2021-10-06 2024-03-05 ㈜대동켐텍 PFOA Free 불소계 텔로머 화합물의 제조방법

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4868508A (ja) * 1971-12-24 1973-09-18
JP2006298817A (ja) * 2005-04-20 2006-11-02 Asahi Glass Co Ltd フルオロアルキルアイオダイドおよびその製造方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4868508A (ja) * 1971-12-24 1973-09-18
JP2006298817A (ja) * 2005-04-20 2006-11-02 Asahi Glass Co Ltd フルオロアルキルアイオダイドおよびその製造方法

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009073762A (ja) * 2007-09-20 2009-04-09 Asahi Glass Co Ltd フルオロアルキルアイオダイドの製造方法
JP2010018533A (ja) * 2008-07-09 2010-01-28 Asahi Glass Co Ltd フルオロアルキルハライドの製造方法
JP2010018532A (ja) * 2008-07-09 2010-01-28 Asahi Glass Co Ltd フルオロアルキルハライドの製造方法
CN112898117A (zh) * 2021-01-27 2021-06-04 济南齐氟新材料技术有限公司 一种全氟烷基碘的制备方法
CN112898117B (zh) * 2021-01-27 2023-10-10 济南齐氟新材料技术有限公司 一种全氟烷基碘的制备方法

Also Published As

Publication number Publication date
KR20100065142A (ko) 2010-06-15
JPWO2009035110A1 (ja) 2010-12-24

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