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WO2008057620A3 - Method for preparing single walled carbon nanotubes from a metal layer - Google Patents

Method for preparing single walled carbon nanotubes from a metal layer Download PDF

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Publication number
WO2008057620A3
WO2008057620A3 PCT/US2007/065508 US2007065508W WO2008057620A3 WO 2008057620 A3 WO2008057620 A3 WO 2008057620A3 US 2007065508 W US2007065508 W US 2007065508W WO 2008057620 A3 WO2008057620 A3 WO 2008057620A3
Authority
WO
WIPO (PCT)
Prior art keywords
metal layer
single walled
walled carbon
carbon nanotubes
multiplicity
Prior art date
Application number
PCT/US2007/065508
Other languages
French (fr)
Other versions
WO2008057620A2 (en
Inventor
Howard Tennent
Hai-Feng Zhang
Jun Ma
Original Assignee
Hyperion Catalysis Int
Howard Tennent
Hai-Feng Zhang
Jun Ma
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from PCT/US2006/012001 external-priority patent/WO2006110346A1/en
Application filed by Hyperion Catalysis Int, Howard Tennent, Hai-Feng Zhang, Jun Ma filed Critical Hyperion Catalysis Int
Priority to CN2007800194147A priority Critical patent/CN101454242B/en
Priority to AU2007317741A priority patent/AU2007317741A1/en
Priority to CA002647569A priority patent/CA2647569A1/en
Priority to JP2009503276A priority patent/JP2009538809A/en
Priority to EP07868204A priority patent/EP2001794A4/en
Publication of WO2008057620A2 publication Critical patent/WO2008057620A2/en
Publication of WO2008057620A3 publication Critical patent/WO2008057620A3/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B82B3/0009—Forming specific nanostructures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/152—Fullerenes
    • C01B32/156—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/159—Carbon nanotubes single-walled
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/16—Preparation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/16—Preparation
    • C01B32/162—Preparation characterised by catalysts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/02—Single-walled nanotubes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2202/00—Structure or properties of carbon nanotubes
    • C01B2202/20—Nanotubes characterized by their properties
    • C01B2202/36—Diameter

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Composite Materials (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

Methods of preparing single walled carbon nanotubes are provided. An arrangement comprising one or more layers of fullerene in contact with one side of a metal layer and a solid carbon source in contact with the other side of metal layer is prepared. The fullerene/metal layer/solid carbon source arrangement is then heated to a temperature below where the fullerenes sublime. Alternatively, a non-solid carbon source may be used in place of a solid carbon source or the metal layer may simply be saturated with carbon atoms. A multiplicity of single walled carbon nanotubes are grown on the fullerene side of the metal layer, wherein at least 80% of the single walled carbon nanotubes in said multiplicity have a diameter within ± 5% of a single walled carbon nanotube diameter D present in said multiplicity, said diameter D being in the range between 0.6-2.2 nm.
PCT/US2007/065508 2006-03-29 2007-03-29 Method for preparing single walled carbon nanotubes from a metal layer WO2008057620A2 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
CN2007800194147A CN101454242B (en) 2006-03-29 2007-03-29 Method for preparing single-walled carbon nanotubes from metal layer
AU2007317741A AU2007317741A1 (en) 2006-03-29 2007-03-29 Method for preparing single walled carbon nanotubes from a metal layer
CA002647569A CA2647569A1 (en) 2006-03-29 2007-03-29 Method for preparing single walled carbon nanotubes from a metal layer
JP2009503276A JP2009538809A (en) 2006-03-29 2007-03-29 Method for producing single-walled carbon nanotubes from a metal layer
EP07868204A EP2001794A4 (en) 2006-03-29 2007-03-29 Method for preparing single walled carbon nanotubes from a metal layer

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US74392706P 2006-03-29 2006-03-29
US60/743,927 2006-03-29
PCT/US2006/012001 WO2006110346A1 (en) 2005-03-29 2006-03-29 Method for preparing single walled carbon nanotubes from a metal layer
USPCT/US2006/012001 2006-03-29

Publications (2)

Publication Number Publication Date
WO2008057620A2 WO2008057620A2 (en) 2008-05-15
WO2008057620A3 true WO2008057620A3 (en) 2008-06-26

Family

ID=39924877

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2007/065508 WO2008057620A2 (en) 2006-03-29 2007-03-29 Method for preparing single walled carbon nanotubes from a metal layer

Country Status (7)

Country Link
EP (1) EP2001794A4 (en)
JP (1) JP2009538809A (en)
KR (1) KR20090019777A (en)
CN (1) CN101454242B (en)
AU (1) AU2007317741A1 (en)
CA (1) CA2647569A1 (en)
WO (1) WO2008057620A2 (en)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5360643B2 (en) * 2008-05-23 2013-12-04 国立大学法人 名古屋工業大学 Carbon nanotube manufacturing method and manufacturing apparatus
JP5369508B2 (en) * 2008-06-12 2013-12-18 株式会社Ｉｈｉ Hydrogen separation method and hydrogen separation apparatus
EP2459483A2 (en) 2009-07-31 2012-06-06 Massachusetts Institute of Technology Systems and methods related to the formation of carbon-based nanostructures
KR101110578B1 (en) * 2009-10-27 2012-02-15 거림테크 주식회사 Method for preparing oriented graphene-containing coating and method for preparing oriented graphene-containing film
WO2012091789A1 (en) 2010-10-28 2012-07-05 Massachusetts Institute Of Technology Carbon-based nanostructure formation using large scale active growth structures
JP6086387B2 (en) * 2011-03-08 2017-03-01 国立大学法人名古屋大学 Method for producing carbon nanotube
JP5770683B2 (en) * 2012-06-20 2015-08-26 日本電信電話株式会社 Method for forming carbon nanotube
JP6373284B2 (en) 2013-02-28 2018-08-15 エヌ１２ テクノロジーズ， インク．Ｎ１２ Ｔｅｃｈｎｏｌｏｇｉｅｓ， Ｉｎｃ． Nano-structured film cartridge-based dispensing
EP2933228A1 (en) * 2014-04-15 2015-10-21 Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V. Process for preparing single wall carbon nanotubes of pre-defined chirality
CN104532206A (en) * 2014-12-12 2015-04-22 中国科学院重庆绿色智能技术研究院 Preparation method of graphene doped film growing on insulating substrate in in-situ growth mode

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020130610A1 (en) * 2000-11-13 2002-09-19 James Gimzewski Crystals comprising single-walled carbon nanotubes
US20020159943A1 (en) * 1997-03-07 2002-10-31 William Marsh Rice University Method for forming an array of single-wall carbon nanotubes and compositions thereof
US20040179989A1 (en) * 2003-03-14 2004-09-16 Height Murray J. Method and apparatus for synthesizing filamentary structures
WO2004106234A1 (en) * 2003-02-07 2004-12-09 Bussan Nanotech Research Institute Inc. Process for producing monolayer carbon nanotube with uniform diameter
US20050255030A1 (en) * 2002-07-16 2005-11-17 William Marsh Rice University Process for functionalizing carbon nanotubes under solvent-free conditions

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2002214190A1 (en) * 2000-11-13 2002-05-21 International Business Machines Corporation Crystals comprising single-walled carbon nanotubes
US7052668B2 (en) * 2001-01-31 2006-05-30 William Marsh Rice University Process utilizing seeds for making single-wall carbon nanotubes
WO2002080361A1 (en) * 2001-03-30 2002-10-10 California Institute Of Technology Carbon nanotube array rf filter
JP2003292314A (en) * 2002-03-29 2003-10-15 Toray Ind Inc Method for producing carbon nanotube
JP3877302B2 (en) * 2002-06-24 2007-02-07 本田技研工業株式会社 Method for forming carbon nanotube
JP2004083293A (en) * 2002-08-22 2004-03-18 Fujitsu Ltd Method for producing carbon nanotubes using fullerene
JP4963539B2 (en) * 2004-05-10 2012-06-27 株式会社アルバック Method for producing carbon nanotube and plasma CVD apparatus for carrying out the method
US8529862B2 (en) * 2005-03-29 2013-09-10 Hyperion Catalysis International, Inc. Method for preparing single walled carbon nanotubes from a metal layer

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020159943A1 (en) * 1997-03-07 2002-10-31 William Marsh Rice University Method for forming an array of single-wall carbon nanotubes and compositions thereof
US20020130610A1 (en) * 2000-11-13 2002-09-19 James Gimzewski Crystals comprising single-walled carbon nanotubes
US20050255030A1 (en) * 2002-07-16 2005-11-17 William Marsh Rice University Process for functionalizing carbon nanotubes under solvent-free conditions
WO2004106234A1 (en) * 2003-02-07 2004-12-09 Bussan Nanotech Research Institute Inc. Process for producing monolayer carbon nanotube with uniform diameter
US20060093545A1 (en) * 2003-02-07 2006-05-04 Bussan Nanotech Research Institute Inc. Process for producing monolayer carbon nanotube with uniform diameter
US20040179989A1 (en) * 2003-03-14 2004-09-16 Height Murray J. Method and apparatus for synthesizing filamentary structures

Also Published As

Publication number Publication date
CN101454242B (en) 2012-04-11
CA2647569A1 (en) 2008-05-15
AU2007317741A1 (en) 2008-05-15
EP2001794A2 (en) 2008-12-17
JP2009538809A (en) 2009-11-12
WO2008057620A2 (en) 2008-05-15
KR20090019777A (en) 2009-02-25
EP2001794A4 (en) 2012-06-20
CN101454242A (en) 2009-06-10

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