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US4284393A - Powder manufacturing apparatus - Google Patents

Powder manufacturing apparatus Download PDF

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Publication number
US4284393A
US4284393A US06/150,931 US15093180A US4284393A US 4284393 A US4284393 A US 4284393A US 15093180 A US15093180 A US 15093180A US 4284393 A US4284393 A US 4284393A
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US
United States
Prior art keywords
powder
container
gas
melt
receiving
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US06/150,931
Inventor
Gunnar Brunosson
Hans-Gunnar Larsson
Erik Westman
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ABB Norden Holding AB
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ASEA AB
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Publication date
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid

Definitions

  • This invention relates to apparatus for manufacturing powder by a melt atomization process, said apparatus being of the kind comprising a container, means for forming a stream of the melt in said container, and means for directing a jet of gas transversely into the melt stream in order to atomize the melt stream into droplets which solidify in said container to form powder which falls to the lower part of the container.
  • the apparatus may be used for all kinds of material but is primarily intended for manufacturing metallic powders having high contents of alloying materials, for example high-speed steel. In this case, the fine droplets formed solidify rapidly into a powder so that a fine-grained structure is obtained after solidification.
  • the powder-receiving and transporting means of the apparatus may consist simply of an inclined bottom of the container onto which the powder falls and then slides by gravity to said outlet.
  • the bottom may be shaped as a channel to direct the powder to the outlet, and the bottom may be provided with openings or nozzles for the injection of gas to fluidize the powder, which not only has a cooling effect on the powder but also facilitates its movement towards said outlet.
  • said powder-receiving and transporting means may consist of a shaking table which, by its shaking movements, causes transportation of the powder to said outlet.
  • This table may be channel shaped in order to direct the powder to said outlet.
  • a shaking table of the kind which throws the powder obliquely upwards, thus displacing the powder stepwise towards said outlet, is most suitable. Because the powder is thrown up into the flow of re-introduced gas, a very efficient cooling is achieved.

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  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Glanulating (AREA)

Abstract

Apparatus for manufacturing powder, especially metallic powder, by a melt atomization process, comprises a closed container in which a jet of gas is directed transversely into a stream of the melt and breaks it down into droplets which rapidly solidify and are thrown in a parabolic trajectory to the lower part of the container. In the lower part of the container there is an inclined bottom or a shaking table on which the powder flows to an outlet opening. Means are provided for withdrawing gas from the container, cooling it and re-introducing it into the lower part of the container where it is forced by guide means to flow in contact with the powder flowing to the outlet opening. The flow direction of this re-introduced gas is substantially opposite to the direction of flow of the powder to the outlet opening, so that it has an efficient cooling effect on the powder.

Description

TECHNICAL FIELD
This invention relates to apparatus for manufacturing powder by a melt atomization process, said apparatus being of the kind comprising a container, means for forming a stream of the melt in said container, and means for directing a jet of gas transversely into the melt stream in order to atomize the melt stream into droplets which solidify in said container to form powder which falls to the lower part of the container. The apparatus may be used for all kinds of material but is primarily intended for manufacturing metallic powders having high contents of alloying materials, for example high-speed steel. In this case, the fine droplets formed solidify rapidly into a powder so that a fine-grained structure is obtained after solidification.
BACKGROUND ART
An apparatus of the kind referred to has been proposed, in which gas is withdrawn from the container and cooled and then directly re-circulated in the container for cooling the powder formed. In this known apparatus, the powder collected in the lower part of the container can have such a high temperature that, upon contact with air, it adsorbs such an amount of harmful gases that the quality of the powder may become deteriorated to an unacceptable extent. This involves complications when withdrawing the powder from the container, which either must be performed in an inert atmosphere, or the powder must be allowed to cool before it is withdrawn from the container. However, a compact mass of powder cools slowly and is difficult to cool.
DISCLOSURE OF INVENTION
According to the invention, apparatus for manufacturing powder by a melt atomizing process comprises a container, means for forming a stream of the melt in said container, means for directing a jet of gas transversely into the melt stream in order to atomize the melt stream into droplets which solidify in said container to form powder which falls onto a powder-receiving and transporting means in a lower part of said container for transporting the powder to an outlet for powder from the container, means for withdrawing gas from said container, means for cooling at least a part of the withdrawn gas, means for re-introducing at least part of the cooled gas into said lower part of the container, and guide means for forcing said re-introduced gas to flow in contact with the powder on said powder-receiving and transporting mens in a direction substantially opposite to the direction of flow of the powder as it is transported to said outlet by said powder-receiving and transporting means.
The powder-receiving and transporting means of the apparatus may consist simply of an inclined bottom of the container onto which the powder falls and then slides by gravity to said outlet. The bottom may be shaped as a channel to direct the powder to the outlet, and the bottom may be provided with openings or nozzles for the injection of gas to fluidize the powder, which not only has a cooling effect on the powder but also facilitates its movement towards said outlet.
Alternatively, said powder-receiving and transporting means may consist of a shaking table which, by its shaking movements, causes transportation of the powder to said outlet. This table may be channel shaped in order to direct the powder to said outlet. A shaking table of the kind which throws the powder obliquely upwards, thus displacing the powder stepwise towards said outlet, is most suitable. Because the powder is thrown up into the flow of re-introduced gas, a very efficient cooling is achieved.
The guide means for forcing said re-introduced gas to flow in contact with the powder may be formed by a wall of the container disposed above and substantially parallel to the powder-receiving surface of said powder-receiving and transporting means.
BRIEF DESCRIPTION OF DRAWING
The invention will now be described, by way of example, with reference to the accompanying drawing, in which
FIG. 1 is a schematic sectional view of a first embodiment of apparatus in accordance with the invention, and
FIG. 2 is a schematic sectional view of a modified part of the apparatus of FIG. 1.
DESCRIPTION OF PREFERRED EMBODIMENTS
The apparatus shown in FIG. 1 comprises a container 1 with an atomizing space 2 and a collecting chamber 3 for powder 4 produced by atomization of a melt 6 contained in a casting box 5 arranged above the space 2. The melt 6, which for example may be a high-speed steel melt, runs through an outlet opening 7 in the bottom of the box 5 and falls as a stream 8 into a gas jet 9 issuing in a substantially horizontal direction from a nozzle 10. The gas jet 9 atomizes the melt stream 8 in the space 2, and the droplets of melt that are formed solidify in the collecting chamber 3 to produce the powder 4. The container 1 suitably has a shape similar to the trajectory of the powder in the container.
In the lower part of the collecting chamber 3 there is a shaking table 11 of channel-section which rests on resilient supports 12 and is activated by a drive means 13. The powder 4 which falls onto the shaking table 11 is moved towards an outlet opening 14 at the bottom of the container 1. The outlet opening 14 is in the form of a tube 15 with a clack valve 16 which is pivotally journalled around a substantially horizontal shaft 17 and provided with a counterweight 18. The valve 16 opens when the column 19 of powder in the tube 15 has reached a certain height, such that the weight of the powder column overcomees the closing moment exerted by the counterweight 18. The powder column 19 thus serves as a gas lock preventing gas from flowing out of, and air from flowing into, the chamber 3. The powder falling from the tube 15 is collected in a container 29.
Gas is withdrawn from the collecting chamber 3 through a cleaner 20 and a cooler 21, both mounted on the container 1. Part of the withdrawn gas is compressed in a compressor 22 and is conducted via a conduit 23 to the nozzle 10. The remainder of the cooled gas is returned to the container 1 by means of a fan 24, partly to the atomizing space 2 via a conduit 25 and partly via a conduit 28 to the lower part of the collecting chamber 3 near to the outlet opening 14. The cooled gas issuing from the conduit 28 is forced to pass through a gap 26 between a wall 27 of the container 1 and the shaking table 11 and thus cools the powder 4 flowing in the opposite direction on the table 11. An efficient cooling of the powder 4 is obtained in this way, particularly when using a shaking table of the kind which throws the powder up into the stream of cooling gas. For example, a cooling of the powder down to a temperature of 50° C. may be achieved, at which temperature the powder may be handled in air without any major inconvenience.
FIG. 2 shows part of a modified embodiment of the apparatus of FIG. 1. The difference between the apparatus of FIG. 2 and that of FIG. 1 is that the shaking table 11 of FIG. 1 is omitted, and instead the container 1 has an inclined bottom 30 which receives the powder 4. A plenum chamber 31 is arranged to supply gas under pressure to nozzles or openings 32 in the bottom 30 for the purpose of fluidizing the powder 4 and so encouraging it to flow along the channel formed by the sides of the container 1 and the bottom 30 to the outlet opening 14. The gas supply to the plenum chamber 31 may be taken from the compressor 22 (FIG. 1) via a pipe 33. In all other respects the apparatus of FIG. 2 is the same as that of FIG. 1.

Claims (7)

What is claimed is:
1. Apparatus for manufacturing powder by a melt atomization process, said apparatus comprising
a container,
means for forming a stream of the melt in said container,
means for directing a jet of gas transversely into the melt stream in order to atomize the melt stream into droplets which solidify in said container to form powder which falls onto a powder-receiving and transporting means in a lower part of said container for transporting the powder to an outlet for powder from the container,
means for withdrawing gas from said container,
means for cooling at least a part of the withdrawn gas,
means for re-introducing at least part of the cooled gas into said lower part of the container, and
guide means for forcing said re-introduced gas to flow in contact with the powder on said powder-receiving and transporting means in a direction substantially opposite to the direction of flow of the powder as it is transported to said outlet by said powder-receiving and transporting means.
2. Apparatus according to claim 1, wherein said powder-receiving and transporting means is provided by an inclined bottom of said container.
3. Apparatus according to claim 1, wherein said powder-receiving and transporting means is provided by a table and means for imparting a shaking movement to said table.
4. Apparatus according to claim 3, wherein said table is adapted to throw the powder upwardly therefrom.
5. Apparatus according to claim 2, wherein said bottom is channel-shaped.
6. Apparatus according to clam 5, wherein said bottom is formed with openings or nozzles for injecting gas in order to fluidize the powder on the bottom.
7. Apparatus according to claim 3 or claim 4, wherein said table is chaannel-shaped.
US06/150,931 1979-05-31 1980-05-19 Powder manufacturing apparatus Expired - Lifetime US4284393A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
SE7904750A SE425837B (en) 1979-05-31 1979-05-31 PLANT FOR GASATOMIZING A MELTING, INCLUDING COOLING ORGAN
SE7904750 1979-05-31

Publications (1)

Publication Number Publication Date
US4284393A true US4284393A (en) 1981-08-18

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ID=20338179

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US06/150,931 Expired - Lifetime US4284393A (en) 1979-05-31 1980-05-19 Powder manufacturing apparatus

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US (1) US4284393A (en)
JP (1) JPS565903A (en)
DE (1) DE3019047C2 (en)
FR (1) FR2457731A1 (en)
GB (1) GB2051882B (en)
SE (1) SE425837B (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4995894A (en) * 1989-05-01 1991-02-26 National Slag Limited Enclosures for slag pelletization apparatus and method of operation
US5082483A (en) * 1990-06-08 1992-01-21 National Slag Limited Enclosures for slag pelletization apparatus and method of operation thereof
US5154220A (en) * 1990-12-06 1992-10-13 Crawford Tommy N Method and apparatus for making metal shot
US5490162A (en) * 1991-07-04 1996-02-06 Anton More Process and device for the continuous treatment of silicon
CN108940120A (en) * 2018-07-26 2018-12-07 攀枝花攀钢集团设计研究院有限公司 The method and process units of cooling the quenching granulation of pyrocarbon slugging
CN111558723A (en) * 2020-06-24 2020-08-21 湖南天际智慧材料科技有限公司 Device and method for rapidly producing amorphous powder by water atomization method
US12090554B2 (en) 2019-07-16 2024-09-17 3D Lab Sp. Z O.O. Method and device for producing heavy metal powders by ultrasonic atomization

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4435342A (en) * 1981-11-04 1984-03-06 Wentzell Jospeh M Methods for producing very fine particle size metal powders
DE3211861A1 (en) * 1982-03-31 1983-10-06 Leybold Heraeus Gmbh & Co Kg METHOD AND DEVICE FOR PRODUCING HIGH-PURITY CERAMIC-FREE METAL POWDERS
DE3330836A1 (en) * 1982-08-31 1984-03-08 Aluminium Company of America, 15069 Pittsburgh, Pa. METHOD AND DEVICE FOR PRODUCING SPRAYED METAL
EP0123703A1 (en) * 1983-04-27 1984-11-07 Hackforth, Bernhard Process and apparatus for manufacturing spherical granules by solidification under the control of temperature and grain size
JPS6031813U (en) * 1983-08-11 1985-03-04 林 暁子 ornaments
GB2148330B (en) * 1983-10-24 1987-05-07 British Steel Corp Improvements in or relating to the granulation of slag
JPS60125303A (en) * 1983-12-09 1985-07-04 Sumitomo Electric Ind Ltd Method and device for producing metallic powder
JPS62174303A (en) * 1986-01-25 1987-07-31 Oogawara Kakoki Kk Method and apparatus for solidifying pulverized particle of molten metal
AT407620B (en) 1998-12-09 2001-05-25 Boehler Edelstahl DEVICE AND METHOD FOR PRODUCING METAL POWDER IN CAPSULES
BR9905656A (en) * 1999-11-30 2001-07-24 Viviane Vasconcelos Vilela Ltd Apparatus and process for the extraction of heat and for the solidification of particles of molten materials
WO2023275586A1 (en) * 2021-06-28 2023-01-05 Arcelormittal Gas atomizer

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2630623A (en) * 1948-11-12 1953-03-10 Dow Chemical Co Method of making a die-expressed article of a magnesium-base alloy
US3340566A (en) * 1962-08-16 1967-09-12 Reynolds Metals Co Apparatus for the production of metal particles

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1079363A (en) * 1953-05-18 1954-11-29 Metal powders
DE1207350B (en) * 1963-07-08 1965-12-23 Roman Rummel Dipl Ing Method and device for drawing off melts and for producing granules or fibers
DE1558356A1 (en) * 1966-02-03 1970-07-23 Horn Dr Lutz Powder produced by means of the action of ultrasound on a molten metal by atomizing the metal and process for its production
US3658311A (en) * 1970-02-19 1972-04-25 Kelsey Hayes Co Apparatus for making powder metal
DE2144220C3 (en) * 1971-08-31 1974-04-25 Mannesmann Ag, 4000 Duesseldorf Method and apparatus for producing low-oxygen metal powders
JPS4916185A (en) * 1972-06-12 1974-02-13

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2630623A (en) * 1948-11-12 1953-03-10 Dow Chemical Co Method of making a die-expressed article of a magnesium-base alloy
US3340566A (en) * 1962-08-16 1967-09-12 Reynolds Metals Co Apparatus for the production of metal particles

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4995894A (en) * 1989-05-01 1991-02-26 National Slag Limited Enclosures for slag pelletization apparatus and method of operation
US5082483A (en) * 1990-06-08 1992-01-21 National Slag Limited Enclosures for slag pelletization apparatus and method of operation thereof
US5154220A (en) * 1990-12-06 1992-10-13 Crawford Tommy N Method and apparatus for making metal shot
US5490162A (en) * 1991-07-04 1996-02-06 Anton More Process and device for the continuous treatment of silicon
CN108940120A (en) * 2018-07-26 2018-12-07 攀枝花攀钢集团设计研究院有限公司 The method and process units of cooling the quenching granulation of pyrocarbon slugging
CN108940120B (en) * 2018-07-26 2021-06-29 攀枝花攀钢集团设计研究院有限公司 Method and production device for cooling, quenching and granulating high-temperature carbide slag
US12090554B2 (en) 2019-07-16 2024-09-17 3D Lab Sp. Z O.O. Method and device for producing heavy metal powders by ultrasonic atomization
CN111558723A (en) * 2020-06-24 2020-08-21 湖南天际智慧材料科技有限公司 Device and method for rapidly producing amorphous powder by water atomization method

Also Published As

Publication number Publication date
SE425837B (en) 1982-11-15
FR2457731B1 (en) 1985-02-15
GB2051882A (en) 1981-01-21
DE3019047C2 (en) 1984-05-10
FR2457731A1 (en) 1980-12-26
GB2051882B (en) 1983-02-02
JPS565903A (en) 1981-01-22
DE3019047A1 (en) 1980-12-18
SE7904750L (en) 1980-12-01

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