US410295A - Folger - Google Patents
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- Publication number
- US410295A US410295A US410295DA US410295A US 410295 A US410295 A US 410295A US 410295D A US410295D A US 410295DA US 410295 A US410295 A US 410295A
- Authority
- US
- United States
- Prior art keywords
- naphthol
- beta
- celsius
- acid
- folger
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000002253 acid Substances 0.000 description 10
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 8
- CCGUZCYGCSFTGL-UHFFFAOYSA-N [C].C1=C(C=CC2=CC=CC=C12)O Chemical compound [C].C1=C(C=CC2=CC=CC=C12)O CCGUZCYGCSFTGL-UHFFFAOYSA-N 0.000 description 6
- 159000000011 group IA salts Chemical class 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- JWAZRIHNYRIHIV-UHFFFAOYSA-N 2-Naphthol Chemical compound C1=CC=CC2=CC(O)=CC=C21 JWAZRIHNYRIHIV-UHFFFAOYSA-N 0.000 description 4
- 229950011260 betanaphthol Drugs 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/15—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction of organic compounds with carbon dioxide, e.g. Kolbe-Schmitt synthesis
Definitions
- the invention consists in a process for the manufacture of beta-naphthol carbon acid of: re the melting-point of 216" Celsius by meansol the reaction of carbonic acid upon the alkaline salts of the beta-na iihthol under pressure and at a temperature of 200 to 250 ("elsius.
- the beta-naphthol carbon acid the prod'uc 15 tion of which has been specified in United States Patent No. 350,468, granted to myself: and Carl Kolbe jointly, on the 5th day of January, 1880, is produced, if carbonic acid is allowed to react on the alkaline salts of 20 the bcta-naphthol under pressure and at a temperature of 120 to H5 Celsius.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Financial Or Insurance-Related Operations Such As Payment And Settlement (AREA)
- Display Devices Of Pinball Game Machines (AREA)
Description
UNITED STATES PATENT OFFICE.
RUDOLF SCHMITT, OF DRESDEN, ASSIGNOR TO DR. F. VON ITEYDEN NAUTI- FOLGER, OF RADEBEUL, SAXONY, GERMANY.
PROCESS OF MAKING BETA-NAPHTHOL CARBON ACID.
SPECIFICATION forming part of Letters Patent No. 410,295, dated September 3, 1889.
Application filed June 22, 1889. Serial No. 315,232. (No specimens.)
To all whom, it may concern.-
Be it known that I, RUnoLr ScHMrr'r, of Dresden, in the iliinu'doin oi Sa." my, German Empire, have invested a new and Im- 5 proved Process of lilanulacturin l-leta-Naphthol Carbon Acid, of which the following is a specification.
The invention consists in a process for the manufacture of beta-naphthol carbon acid of: re the melting-point of 216" Celsius by meansol the reaction of carbonic acid upon the alkaline salts of the beta-na iihthol under pressure and at a temperature of 200 to 250 ("elsius.
The beta-naphthol carbon acid, the prod'uc 15 tion of which has been specified in United States Patent No. 350,468, granted to myself: and Carl Kolbe jointly, on the 5th day of January, 1880, is produced, if carbonic acid is allowed to react on the alkaline salts of 20 the bcta-naphthol under pressure and at a temperature of 120 to H5 Celsius. The
very inconstant acid thus obtained again decomposes very easily into carbonic acid and beta-naphthol and melts at 157 Celsius.
z 5 I have now found that if in the above op- Celsius, consisting in producing the reaction of carbonic acid upon the alkaline salts of 40 the beta-naphthol under pressure and at a temperature of 200 to 250 Celsius, substantially as herein set forth.
In testimony that 1 claim the foregoing, as my invention I have signed my name in pres- 5 ence of two subscribing witnesses.
RUDOLF SCHMIIT.
Witnesses:
WILHELM WIESENHL TTER, GEoRe RICHTER.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US410295A true US410295A (en) | 1889-09-03 |
Family
ID=2479229
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US410295D Expired - Lifetime US410295A (en) | Folger |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US410295A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2534022A (en) * | 1948-04-05 | 1950-12-12 | Tewin Ind Inc | Manufacture of salts of 2:1-hydroxynaphthoic acid |
| US2682916A (en) * | 1946-07-02 | 1954-07-06 | Ritter Co Inc | Medical practice chair with adjustable seat frame |
| US2808434A (en) * | 1952-09-27 | 1957-10-01 | Hoechst Ag | Process of preparing 2-hydroxynaphthalene-3-carboxylic acid |
| US4819430A (en) * | 1983-01-21 | 1989-04-11 | Hydreco, Inc. | Variably charged hydraulic circuit |
-
0
- US US410295D patent/US410295A/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2682916A (en) * | 1946-07-02 | 1954-07-06 | Ritter Co Inc | Medical practice chair with adjustable seat frame |
| US2534022A (en) * | 1948-04-05 | 1950-12-12 | Tewin Ind Inc | Manufacture of salts of 2:1-hydroxynaphthoic acid |
| US2808434A (en) * | 1952-09-27 | 1957-10-01 | Hoechst Ag | Process of preparing 2-hydroxynaphthalene-3-carboxylic acid |
| US4819430A (en) * | 1983-01-21 | 1989-04-11 | Hydreco, Inc. | Variably charged hydraulic circuit |
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