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US3385570A - Ultrasonic radiation device - Google Patents

Ultrasonic radiation device Download PDF

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Publication number
US3385570A
US3385570A US395481A US39548164A US3385570A US 3385570 A US3385570 A US 3385570A US 395481 A US395481 A US 395481A US 39548164 A US39548164 A US 39548164A US 3385570 A US3385570 A US 3385570A
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United States
Prior art keywords
container
liquid
wall
ultrasonic
vessel
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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US395481A
Inventor
Pijls Hermanus Stepha Josephus
Put Elias
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US Philips Corp
North American Philips Co Inc
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US Philips Corp
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Publication date
Application filed by US Philips Corp filed Critical US Philips Corp
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Publication of US3385570A publication Critical patent/US3385570A/en
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/34Treatment of water, waste water, or sewage with mechanical oscillations
    • C02F1/36Treatment of water, waste water, or sewage with mechanical oscillations ultrasonic vibrations
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
    • A23B11/00Preservation of milk or dairy products
    • A23B11/10Preservation of milk or milk preparations
    • A23B11/16Preservation of milk or milk preparations by irradiation, e.g. by microwaves
    • A23B11/162Preservation of milk or milk preparations by irradiation, e.g. by microwaves by sonic or ultrasonic waves
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/30Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
    • A23L5/32Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using phonon wave energy, e.g. sound or ultrasonic waves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F31/00Mixers with shaking, oscillating, or vibrating mechanisms
    • B01F31/80Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
    • B01F31/86Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations with vibration of the receptacle or part of it
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/10Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/10Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
    • B08B3/12Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00Indexing codes associated with group G01N29/00
    • G01N2291/02Indexing codes associated with the analysed material
    • G01N2291/024Mixtures
    • G01N2291/02491Materials with nonlinear acoustic properties

Definitions

  • the invention relates to an ultrasonic device and more particularly to ultrasonic apparatus for imparting ultrasonic energy to a liquid in a vessel.
  • Devices of this type may be employed, for example, for cleaning purposes, for mixing or emulsifying two different liquids which may be miscible only with difiiculty, and for obtaining biological effects, for example, for killing bacteria in liquids such as milk and so on.
  • the transducer for converting electrical energy into ultrasonic energy is often fastened, either directly or with the interposition of an energy transmitting body for the ultrasonic oscillations, to the bottom or to the side wall of a vessel for the liquid. Then the liquid in the vessel is excited by the ultrasonic oscillations so that the effects described above can be achieved.
  • the invention has for its object to avoid this disadvantage and is characterized in that inside the vessel containing the liquid and near its wall, but beyond the path of the ultrasonic oscillations, from the ultrasonic radiator up into the liquid, acoustic damping material is provided.
  • the invention is based on the following recognition.
  • the single figure shows a beaker-shaped vessel 1, which contains the liquid to be irradiated.
  • the ultrasonic transducer 2 To the bottom wall of this vessel 1 is fastened the ultrasonic transducer 2.
  • the ultrasonic oscillations of the transducer 2 having a frequency of, for example to 50 kc./s., propagate from said bottom wall through the liquid with a wave front extending approximately parallel to the bottom surface of the vessel 1.
  • a bottomless cylinder 3 of acoustic damping material for example, some plastics such as polyethylene,
  • the vessel 1 may, of course, also have a rectangular or other shape.
  • the cylinder 3 preferably has a corresponding shape.
  • said transducer means is positioned against the bottom wall of said container, said acoustic damping means comprising an open ended hollow cylinder composed of acoustic damping material, said cylinder being positioned close to a side wall of said container but not rigidly secured thereto and with its longitudinal axis substantially parallel to the direction of propagation of said Wave energy.
  • said container comprises a first wall bounded by at least one other wall, said transducer means being positioned against a given one of said walls to impart vibrations to said liquid with suificient power to produce cavitation in the liquid, said acoustic damping means comprising an open ended hollow thin-walled member composed of acoustic damping material and arranged so that its longitudinal axis is substantially parallel to the energy propagation path and its walls are arranged close to the walls of said container other than said given wall.
  • said container comprises a first wall bounded by at least one other wall, said transducer means being positioned against said first wall to impart vibrations to said liquid with sufficient power to produce cavitation in the liquid, said acoustic damping means comprising an open ended hollow thin-walled member composed of acoustic damping material arranged within said container so that its wall or walls are positioned close to the bounding wall or walls of said container and substantially parallel to the direction of propagation of said wave energy in the liquid.

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Mechanical Engineering (AREA)
  • Organic Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Environmental & Geological Engineering (AREA)
  • Hydrology & Water Resources (AREA)
  • Zoology (AREA)
  • Nutrition Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Wood Science & Technology (AREA)
  • Cleaning By Liquid Or Steam (AREA)
  • Apparatus For Disinfection Or Sterilisation (AREA)
  • Cleaning Or Drying Semiconductors (AREA)

Description

May 28, 1968 5, J, PIJLS ET AL 3,385,570
ULTRASONIC RADIATION DEVICE Filed Sept. 10, 1964 INVENTORS HERMANUS S.J. PIJLS ELIAS PUT PM $2. 4" AGENT United States Patent 3,385,570 ULTRASONIC RADIATION DEVICE Hermanus Stephanus Josephus Pijls, and Elias Put, Emmasingel, Eindhoven, Netherlands, assignors to North American Philips Company, Inc., New York, N.Y., a corporation of Delaware Filed Sept. 10, 1964, Ser. No. 395,481 Claims priority, application Netherlands, Sept. 12, 1963,
297,855 11 Claims. (Cl. 259-72 The invention relates to an ultrasonic device and more particularly to ultrasonic apparatus for imparting ultrasonic energy to a liquid in a vessel. Devices of this type may be employed, for example, for cleaning purposes, for mixing or emulsifying two different liquids which may be miscible only with difiiculty, and for obtaining biological effects, for example, for killing bacteria in liquids such as milk and so on.
In such devices the transducer for converting electrical energy into ultrasonic energy is often fastened, either directly or with the interposition of an energy transmitting body for the ultrasonic oscillations, to the bottom or to the side wall of a vessel for the liquid. Then the liquid in the vessel is excited by the ultrasonic oscillations so that the effects described above can be achieved.
In practice it has been found that, especially in the case of round, for example, beaker-shaped vessels, a strong, audible tone is often produced which is very troublesome to the user. This phenomenon may occur both with glass vessels and with metal vessels. By means of experiments underlying the invention, it was found that this audible tone corresponded to a resonance frequency of the vessel containing the liquid. By providing damping material on the outer wall of the vessel, the sound level of the audible tone could be reduced, it is true, but at the same time a large amount of useful ultrasonic energy was lost.
The invention has for its object to avoid this disadvantage and is characterized in that inside the vessel containing the liquid and near its wall, but beyond the path of the ultrasonic oscillations, from the ultrasonic radiator up into the liquid, acoustic damping material is provided.
The invention is based on the following recognition.
In order to achieve the aforesaid effects, for example, cleaning or emulsifying, it is necessary to apply enough ultrasonic energy to the liquid such that a strong cavitation occurs therein. This cavitation may be considered to be a non-linear load on the ultrasonic oscillations and subharmonics of these oscillations may be produced in the liquid. If such a subharmonic coincides with a resonance frequency of the vessel containing the liquid-in practice such a vessel may vibrate in many frequencies, so that the probability of coincidence of such a subharmonic with a resonance frequency of the vessel is very great-the vessel will be excited in this frequency. By providing acoustic damping material as described, oscillations of the said audible frequency can be prevented from reaching the wall of the vessel via the liquid. Thus the loss of ultrasonic energy is considerably smaller than in the case of direct damping of the wall of the vessel.
The invention will be described with reference to the embodiment shown in the drawing.
The single figure shows a beaker-shaped vessel 1, which contains the liquid to be irradiated. To the bottom wall of this vessel 1 is fastened the ultrasonic transducer 2. The ultrasonic oscillations of the transducer 2, having a frequency of, for example to 50 kc./s., propagate from said bottom wall through the liquid with a wave front extending approximately parallel to the bottom surface of the vessel 1. A bottomless cylinder 3 of acoustic damping material, for example, some plastics such as polyethylene,
polypropylene, rubber or the like is arranged near the side wall of the vessel 1, but it is not rigidly secured thereto. The useful ultrasonic energy radiating from the bottom of the vessel 1 into the liquid is therefore not damped by the cylinder 3, so that the desired effect on the liquid, for example, cleaning, is substantially not reduced. Since the wall of the vessel 1 is not directly damped acoustically, no additional ultrasonic energy is Withdrawn from the radiator 2 for this reason. The oscillations of audible frequency produced by cavitation phenomena in the liquid, which propagate in many arbitrary directions, will strike the cylinder 3 and will be absorbed to a considerable extent so that they can reach the wall of the vessel 1 only in a materially attenuated state. In this way the said troublesome tone is suppressed. In order to obtain a satisfactory effect, it is found that a wall thickness of only a few millimetres, for example, 2.5 mm., is usually suflicient.
The vessel 1 may, of course, also have a rectangular or other shape. In this case, the cylinder 3 preferably has a corresponding shape.
What is claimed is:
1. Ultrasonic apparatus for treating a liquid in a container comprising, transducer means coupled to one wall of said container so as to vibrate said container to impart ultrasonic wave energy to said liquid along a given path, and acoustic damping means positioned within said container close to another wall thereof, said damping means being positioned wholly outside of said given path whereby ultrasonic wave energy along said given path is substantially unattenuated by said damping means.
2. Apparatus as described in claim 1 wherein said transducer means is positioned against the bottom wall of said container, said acoustic damping means comprising an open ended hollow cylinder composed of acoustic damping material, said cylinder being positioned close to a side wall of said container but not rigidly secured thereto and with its longitudinal axis substantially parallel to the direction of propagation of said Wave energy.
3. Apparatus as described in claim 2 wherein said cylinder is arranged to sit on the bottom wall of said container with its longitudinal axis perpendicular thereto, the diameter of said cylinder being only slightly smaller than the correlative cross-sectional dimension of said container.
4. Apparatus as described in claim 2 wherein said container is a cylinder of a given diameter and wherein said hollow cylinder is arranged to sit on the bottom wall of said container with its longitudinal axis perpendicular thereto, the diameter of said hollow cylinder being only slightly smaller than said given diameter of the container so as to loosely fit therein.
5. Ultrasonic apparatus for treating a liquid in a container comprising, transducer means external to said container and coupled thereto so as to vibrate said container to cause ultrasonic wave energy to propagate through said liquid along a given path substantially parallel to at least one wall of said container, and acoustic damping means positioned within said container close to said wall but out of the propagation path of said ultrasonic wave energy so that any acoustic energy in the liquid reaching said wall is substantially attenuated.
6. Apparatus as described in claim 5 wherein said container comprises a first wall bounded by at least one other wall, said transducer means being positioned against a given one of said walls to impart vibrations to said liquid with suificient power to produce cavitation in the liquid, said acoustic damping means comprising an open ended hollow thin-walled member composed of acoustic damping material and arranged so that its longitudinal axis is substantially parallel to the energy propagation path and its walls are arranged close to the walls of said container other than said given wall.
7. Apparatus as described in claim 5 wherein said container comprises a first wall bounded by at least one other wall, said transducer means being positioned against said first wall to impart vibrations to said liquid with sufficient power to produce cavitation in the liquid, said acoustic damping means comprising an open ended hollow thin-walled member composed of acoustic damping material arranged within said container so that its wall or walls are positioned close to the bounding wall or walls of said container and substantially parallel to the direction of propagation of said wave energy in the liquid.
8. Ultrasonic apparatus for treating a liquid in a container comprising, vibratory transducer means external to said container and coupled to an end wall thereof to cause ultrasonic wave energy to propagate through said liquid in a given direction substantially parallel to the side walls of said container, and an open ended hollow member composed of acoustic damping material arranged within said container close to the side walls thereof and out of the propagation path of said wave energy so as to shield said side walls from the effects of said ultrasonic wave energy.
9. Apparatus as described in claim 8 wherein said end wall is the bottom wall of the container and wherein said transducer means are arranged to cause said wave energy to propagate from said bottom wall through the liquid with a wave front extending approximately parallel to said bottom wall and with sufiicient energy to produce cavitation in the liquid, said hollow member being arranged to sit on said bottom wall of the container so that the wall or walls thereof extend substantially parallel to said given direction of energy propagation.
10. Apparatus as described in claim 8 wherein said container and hollow member have corresponding cylindrical shapes, said container and hollow member being coaxially positioned.
11. Apparatus as described in claim 8 wherein said container and hollow member have different shapes, said container and hollow member being coaxially positioned.
References Cited UNITED STATES PATENTS 2,815,193 12/1957 Brown 25972 2,407,462 9/1946 Whiteley. 3,194,640 7/ 1965 Nesh.
FOREIGN PATENTS 817,583, 8/1959 Great Britain.
ROBERT W. JENKINS, Primary Examiner.

Claims (1)

1. ULTRASONIC APPARATUS FOR TREATING A LIQUID IN A CONTAINER COMPRISING, TRANSDUCER MEANS COUPLED TO ONE WALL OF SAID CONTAINER SO AS TO VIBRATE SAID CONTAINER TO IMPART ULTRASONIC WAVE ENERGY TO SAID LIQUID ALONG A GIVEN PATH, AND ACOUSTIC DAMPING MEANS POSITIONED WITHIN SAID CONTAINER CLOSE TO ANOTHER WALL THEREOF, SAID DAMPING MEANS BEING POSITIONED WHOLLY OUTSIDE OF SAID GIVEN PATH WHEREBY ULTRASONIC WAVE ENERGY ALONG SAID GIVEN PATH IS SUBSTANTIALLY UNATTENUATED BY SAID DAMPING MEANS.
US395481A 1963-09-12 1964-09-10 Ultrasonic radiation device Expired - Lifetime US3385570A (en)

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Application Number Priority Date Filing Date Title
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CH (1) CH429257A (en)
GB (1) GB1012538A (en)
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4424188A (en) 1981-12-31 1984-01-03 International Paper Company Sterilization of packaging material
US6565533B1 (en) 2000-01-21 2003-05-20 Novus International, Inc. Inoculation apparatus and method
US6672317B2 (en) * 1999-08-22 2004-01-06 Beissbarth Gmbh Cleaning device for rotationally symmetrical bodies
US20080049545A1 (en) * 2006-08-22 2008-02-28 United Technologies Corporation Acoustic acceleration of fluid mixing in porous materials
US20120266912A1 (en) * 2011-04-21 2012-10-25 Katholieke Universiteit Leuven, K.U. Leuven R&D Method and Apparatus for Cleaning Semiconductor Substrates
WO2013098673A1 (en) * 2011-12-26 2013-07-04 Koninklijke Philips Electronics N.V. Device and method for generating emulsion

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9005705D0 (en) * 1990-03-14 1990-05-09 Health Lab Service Board Particle manipulation

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2407462A (en) * 1943-05-14 1946-09-10 Whiteley Edward Oldroyd Supersonic treatment of fluid masses
US2815193A (en) * 1954-01-25 1957-12-03 Bendix Aviat Corp Ultrasonic cleaning system
GB817583A (en) * 1956-09-19 1959-08-06 Libbey Owens Ford Glass Co Magnetostrictive device
US3194640A (en) * 1961-02-10 1965-07-13 Nesh Florence Use of ultrasound to induce crystal rearrangements and phase transitions

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2407462A (en) * 1943-05-14 1946-09-10 Whiteley Edward Oldroyd Supersonic treatment of fluid masses
US2815193A (en) * 1954-01-25 1957-12-03 Bendix Aviat Corp Ultrasonic cleaning system
GB817583A (en) * 1956-09-19 1959-08-06 Libbey Owens Ford Glass Co Magnetostrictive device
US3194640A (en) * 1961-02-10 1965-07-13 Nesh Florence Use of ultrasound to induce crystal rearrangements and phase transitions

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4424188A (en) 1981-12-31 1984-01-03 International Paper Company Sterilization of packaging material
US6672317B2 (en) * 1999-08-22 2004-01-06 Beissbarth Gmbh Cleaning device for rotationally symmetrical bodies
US6565533B1 (en) 2000-01-21 2003-05-20 Novus International, Inc. Inoculation apparatus and method
US20030229312A1 (en) * 2000-01-21 2003-12-11 Novus International, Inc. Inoculation apparatus and method
US20080049545A1 (en) * 2006-08-22 2008-02-28 United Technologies Corporation Acoustic acceleration of fluid mixing in porous materials
US20100046319A1 (en) * 2006-08-22 2010-02-25 United Technologies Corporation Acoustic Acceleration of Fluid Mixing in Porous Materials
US8408782B2 (en) 2006-08-22 2013-04-02 United Technologies Corporation Acoustic acceleration of fluid mixing in porous materials
US8789999B2 (en) 2006-08-22 2014-07-29 United Technologies Corporation Acoustic acceleration of fluid mixing in porous materials
US20120266912A1 (en) * 2011-04-21 2012-10-25 Katholieke Universiteit Leuven, K.U. Leuven R&D Method and Apparatus for Cleaning Semiconductor Substrates
US9378989B2 (en) * 2011-04-21 2016-06-28 Imec Method and apparatus for cleaning semiconductor substrates
WO2013098673A1 (en) * 2011-12-26 2013-07-04 Koninklijke Philips Electronics N.V. Device and method for generating emulsion

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CH429257A (en) 1967-01-31
GB1012538A (en) 1965-12-08
NL297855A (en) 1900-01-01

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